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Xenon nitrate

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Xenon nitrate is a transient compound made by reacting xenon difluoride with anhydrous nitric acid.

Production

Attempted production has used this method:[1]

XeF2 + 2HNO3 → Xe(NO3)2 + 2HF

However this decomposes rapidly: Xe(NO3)2 → Xe + O2NOONO2 (an unstable nitrogen peroxide)

XeF2 + HNO3 → FXeNO3 + HF

However a nixed nitrate definitely exists FXeONO2.[1]

This is formed via the reaction:[1]

[FXeOXeFXeF][AsF6] + 2NO2F → FXeONO2 +NO2AsF6.

Purification of FXeONO2 can take place by dissolving in SO2ClF which leaves the nitronium arsenic hexafluoride behind as a solid.[1]

An alternate low yield method to make FXeONO2 is to dissolve xenon diflouride in liquid dinitrogen tetroxide.[1]

Xe2 + NO+ + NO3- → FXeONO2 + NOF at 0°C

This method is inefficient as not much nitrate ion exists in the liquid and the xenon nitrate decomposes.[1]

Properties

FXeONO2 is a white crystalline material.[1]

FXeONO2 is not particularly stable and slowly breaks down at -78°C yielding XeF2.N2O4. This happens on a timescale of several days.[1] At 0°C FXeONO2 has a half life of seven hours decomposing to XeF2.[1]

References

  1. ^ a b c d e f g h i Moran, Matthew D. (2007). Synthesis and Structural Characterization of new Xenon(II) Compounds and the Use of a Xenon(II) Cation as an Oxidant for the Preparation of Halogenated Hydrocarbons (PDF). McMaster University. pp. 42, 99–145. Retrieved 4 Oct 2014.