BCF Train (Hydrogen Carrier) : N2 C1 C3+ Vent
BCF Train (Hydrogen Carrier) : N2 C1 C3+ Vent
BCF Train (Hydrogen Carrier) : N2 C1 C3+ Vent
.00
15.00
30.00
60.00
90.00
Seconds
Typical settings (individual analyzers may vary) Cycle time Sort order Sample size Target component Target retention time Inject time 90 seconds 84 40 ul C2 60 seconds 6 seconds Inject time variance Carrier pressure Carrier pressure variance Flow rate Flow rate variance Oven temperature 10% 30 psig 15% 20 ml/min 15% 60 C
%RSD Minimum detectable limit (mol%) Peak detection method Minimum peak area Peak retention time Peak direction Baseline segment start 0 0 0 0 0 0 Baseline segment end 0 0 0 0 0 0 Front height ratio 0.95 0.95 0.75 0.75 0.75 0.75 Slope (rise) 3 3 3 3 3 3 Slope (run) 9 5 5 5 5 5
Minimum
1 2 3 4 5 6
2 2 2 2 2 2
Gate off
Gate on
BCF train
Inject mode 15 (2) seconds The provided illustration shows that during the inject mode, the lighter gasses have already moved through column A and into column B. The heavier gasses are retained on column A.
Backflush mode In column A, C3 and heavier gasses are combined into a group named C3+. The lighter gasses will continue through column B, pass through column A again and cross the detector bead. When the gasses cross the detector bead, they change the amount of energy necessary to maintain the temperature level of the bead. This change in energy is what causes the peak generation for each of the gasses.
Simplified view
Sample & Carrier Column A Column B To Detector & Vent
Simplified view
To Detector & Vent Column A Column B Carrier
GC Valve 1
Col 1A Detector
GC Valve 1
Col 1A Detector
Col 1B Vent
EPC
Carrier In
Carrier In