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6890 Split Animation

The document is a series of slides describing the components and functioning of an Agilent 6850/6890 gas chromatograph split/splitless inlet. It shows diagrams of the inlet with labels for components like the septum, liner, and columns. It also includes animations showing how the inlet works in different modes like split injection and setting the total flow, pressure, and split ratio to prepare for sample injection, vaporization, separation into the column, and detection. The final slides discuss using the gas saver feature to reduce the total flow after injection is complete to save carrier gas.

Uploaded by

Waleed El-azab
Copyright
© © All Rights Reserved
Available Formats
Download as PPT, PDF, TXT or read online on Scribd
121 views

6890 Split Animation

The document is a series of slides describing the components and functioning of an Agilent 6850/6890 gas chromatograph split/splitless inlet. It shows diagrams of the inlet with labels for components like the septum, liner, and columns. It also includes animations showing how the inlet works in different modes like split injection and setting the total flow, pressure, and split ratio to prepare for sample injection, vaporization, separation into the column, and detection. The final slides discuss using the gas saver feature to reduce the total flow after injection is complete to save carrier gas.

Uploaded by

Waleed El-azab
Copyright
© © All Rights Reserved
Available Formats
Download as PPT, PDF, TXT or read online on Scribd
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Slide #1

6850/6890 Split Animation


Split/Splitless Inlet - Component Identification
Septum
Liner
Liner O-Ring
Gold Seal
Capillary Column
5/4/00
Slide #2
6850/90 Split/Splitless Inlet - Component Identification
Septum
SEPTUM PURGE
VENT
Inlet Split
Port
Slide #3
6850/90 Split Animation - Default Conditions
FLOW
SENSOR
PROPORTIONAL
VALVE 1
PRESSURE
SENSOR
SEPTUM PURGE
REGULATOR
PURGE
VALVE
OPEN
TOTAL FLOW
CONTROL LOOP
SPLIT
VENT
GOLD SEAL
INPUT
PRESSURE
PROPORTIONAL
VALVE 2
80 PSI
0

ML/MIN
SPLIT VENT
TRAP
0

PSI
Slide #4
6850/90 Split Animation - Total Flow Setting
FLOW
SENSOR
PROPORTIONAL
VALVE 1
PRESSURE
SENSOR
SEPTUM PURGE
REGULATOR
PURGE
VALVE
OPEN
TOTAL FLOW
CONTROL LOOP
SPLIT
VENT

205 ML/MIN
GOLD SEAL
INPUT
PRESSURE
PROPORTIONAL
VALVE 2
80 PSI
PRIMARY FLOW PATH
REDUCED FLOW PATH
205

ML/MIN
SPLIT VENT
TRAP
0

PSI
Slide #5
6850/90 Split Animation - Inlet Pressure Setting
FLOW
SENSOR
PROPORTIONAL
VALVE 1
PRESSURE
SENSOR
SEPTUM PURGE
REGULATOR
FIXED @ 3ML/MIN
PURGE
VALVE
OPEN
TOTAL FLOW
CONTROL LOOP
GOLD SEAL
INPUT
PRESSURE
PROPORTIONAL
VALVE 2
80 PSI
PRIMARY FLOW PATH
REDUCED FLOW PATH
205

ML/MIN
SPLIT VENT
TRAP
10

PSI
SPLIT
VENT

200 ML/MIN
COLUMN FLOW
2 ML/MIN
PRESSURIZED GAS
BACK PRESSURE CONTROL LOOP
Slide #6
6850/90 Split Ready for Injection
Animation
FLOW
SENSOR
PROPORTIONAL
VALVE 1
PRESSURE
SENSOR
SEPTUM PURGE
REGULATOR
FIXED @ 3ML/MIN
PURGE
VALVE
OPEN
TOTAL FLOW
CONTROL LOOP
INPUT
PRESSURE
PROPORTIONAL
VALVE 2
80 PSI
205

ML/MIN
SPLIT VENT
TRAP
10

PSI
SPLIT
VENT

200 ML/MIN
COLUMN FLOW
2 ML/MIN
BACK PRESSURE CONTROL LOOP
Split Ratio - 100:1
Mode: Split
Temp 250 250
Pressure 10.0 10.0
Split Ratio 100
Split Flow 200
Tot Flow 205.0 205.0
Gas Saver OFF
Slide #7
6850/90 Split Insert Syringe
Animation
FLOW
SENSOR
PROPORTIONAL
VALVE 1
PRESSURE
SENSOR
SEPTUM PURGE
REGULATOR
FIXED @ 3ML/MIN
PURGE
VALVE
OPEN
TOTAL FLOW
CONTROL LOOP
GOLD SEAL
INPUT
PRESSURE
PROPORTIONAL
VALVE 2
80 PSI
205

ML/MIN
SPLIT VENT
TRAP
10

PSI
SPLIT
VENT

200 ML/MIN
COLUMN FLOW
2 ML/MIN
BACK PRESSURE CONTROL LOOP
Split Ratio - 100:1
Slide #8
6850/90 Split Inject Sample
Animation
FLOW
SENSOR
PROPORTIONAL
VALVE 1
PRESSURE
SENSOR
SEPTUM PURGE
REGULATOR
FIXED @ 3ML/MIN
PURGE
VALVE
OPEN
TOTAL FLOW
CONTROL LOOP
GOLD SEAL
INPUT
PRESSURE
PROPORTIONAL
VALVE 2
80 PSI
205

ML/MIN
SPLIT VENT
TRAP
10

PSI
SPLIT
VENT

200 ML/MIN
COLUMN FLOW
2 ML/MIN
BACK PRESSURE CONTROL LOOP
Split Ratio - 100:1
Slide #9
6850/90 Split Sample Vaporizes
Animation
FLOW
SENSOR
PROPORTIONAL
VALVE 1
PRESSURE
SENSOR
SEPTUM PURGE
REGULATOR
FIXED @ 3ML/MIN
PURGE
VALVE
OPEN
TOTAL FLOW
CONTROL LOOP
GOLD SEAL
INPUT
PRESSURE
PROPORTIONAL
VALVE 2
80 PSI
205

ML/MIN
SPLIT VENT
TRAP
10

PSI
SPLIT
VENT

200 ML/MIN
COLUMN FLOW
2 ML/MIN
BACK PRESSURE CONTROL LOOP
Split Ratio - 100:1
Glass Wool
Slide #10
6850/90 Split Sample is Split -
Animation Good Liner Design?
FLOW
SENSOR
PROPORTIONAL
VALVE 1
PRESSURE
SENSOR
SEPTUM PURGE
REGULATOR
FIXED @ 3ML/MIN
PURGE
VALVE
OPEN
TOTAL FLOW
CONTROL LOOP
INPUT
PRESSURE
PROPORTIONAL
VALVE 2
80 PSI
205

ML/MIN
SPLIT VENT
TRAP
10

PSI
SPLIT
VENT

200 ML/MIN
COLUMN FLOW
2 ML/MIN
BACK PRESSURE CONTROL LOOP
Split Ratio - 100:1
Smaller O.D. Liner
Open Split Flow Path
Glass Positioning
Bead
Glass
Wool
Tapered Liner
Agilent Split
Liner - 5183-4647
Slide #11
6850/90 Split Split Continues
Animation
FLOW
SENSOR
PROPORTIONAL
VALVE 1
PRESSURE
SENSOR
SEPTUM PURGE
REGULATOR
FIXED @ 3ML/MIN
PURGE
VALVE
OPEN
TOTAL FLOW
CONTROL LOOP
INPUT
PRESSURE
PROPORTIONAL
VALVE 2
80 PSI
205

ML/MIN
SPLIT VENT
TRAP
10

PSI
SPLIT
VENT

200 ML/MIN
COLUMN FLOW
2 ML/MIN
BACK PRESSURE CONTROL LOOP
Split Ratio - 100:1
Slide #12
6850/90 Split Split is Complete
Animation
FLOW
SENSOR
PROPORTIONAL
VALVE 1
PRESSURE
SENSOR
SEPTUM PURGE
REGULATOR
FIXED @ 3ML/MIN
PURGE
VALVE
OPEN
TOTAL FLOW
CONTROL LOOP
INPUT
PRESSURE
PROPORTIONAL
VALVE 2
80 PSI
205

ML/MIN
SPLIT VENT
TRAP
10

PSI
SPLIT
VENT

200 ML/MIN
COLUMN FLOW
2 ML/MIN
BACK PRESSURE CONTROL LOOP
Split Ratio - 100:1
Slide #13
6850/90 Split Sample is separated
Animation and Detected
FLOW
SENSOR
PROPORTIONAL
VALVE 1
PRESSURE
SENSOR
SEPTUM PURGE
REGULATOR
FIXED @ 3ML/MIN
PURGE
VALVE
OPEN
TOTAL FLOW
CONTROL LOOP
INPUT
PRESSURE
PROPORTIONAL
VALVE 2
80 PSI
205

ML/MIN
SPLIT VENT
TRAP
10

PSI
SPLIT
VENT

200 ML/MIN
COLUMN FLOW
2 ML/MIN
BACK PRESSURE CONTROL LOOP
Split Ratio - 100:1
Slide #14
6850/90 Split Gas Saver - Set to 55 ml/min
Animation After the Injection is complete
FLOW
SENSOR
PROPORTIONAL
VALVE 1
PRESSURE
SENSOR
SEPTUM PURGE
REGULATOR
FIXED @ 3ML/MIN
PURGE
VALVE
OPEN
TOTAL FLOW
CONTROL LOOP
INPUT
PRESSURE
PROPORTIONAL
VALVE 2
80 PSI
55

ML/MIN
SPLIT VENT
TRAP
10

PSI
SPLIT
VENT

50 ML/MIN
COLUMN FLOW
2 ML/MIN
BACK PRESSURE CONTROL LOOP
Split Ratio - 100:1
Mode: Split
Temp 250 250
Pressure 10.0 10.0
Split Ratio 100
Split Flow 200
Tot Flow 205.0 205.0
Gas Saver ON
Saver Flow 50.0
Saver Time 0.5

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