Agitation & Mixing of Fluids

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AGITATION AND MIXING OF

FLUIDS
Purpose of agitation:
intensification of transport processes in agitated batch (heat and mass transfer)
preparation of materials of required properties (suspension, emulsion)
Examples of industrial applications:
blending of two miscible liquids as ethyl alcohol and water
dissolving solids in liquids, such as salt in water
dispersing a gas in a liquid as fine bubbles, such as oxygen from
air in a suspension of microorganisms for fermentation or for the
activated sludge process in waste treatment
liquid-liquid dispersion, such as dispersion of pigment in solvents
suspending of fine solid particles in a liquid, as in catalytic
hydrogenation of a liquid
agitation of the fluid to increase heat tranfer between the fluid and
a coil or jacket in the vessel wall

Method of mixing fluids


mechanical mixing (rotating, vibrating)
hydraulic mixing
pneumatic mixing
pipeline mixing (turbulent flow, static mixer)

A mechanical mixing using


turbines
B mechanical mixing using
blade impellers
C hydraulic mixing
D pneumatic mixing with
stationary inputs
E pneumatic mixing with
automatic regulation
F hydraulic mixing with
antifoaming shower

Pipeline mixing Reynolds experiments

Paul, E. L., Atiemo-Obeng, V. A., Kresta, S. M.:


Handbook of industrial mixing: science and
practice. Canada: Wiley-Interscience, 2003,
1377 p. ISBN 0-471-26919-0

Flow in agitated batch

a axial-flow pattern, baffled vessel, b radial-flow pattern, baffled vessel,


c tangential-flow pattern, unbaffled vessel

Equipment for mechanical mixing


Design layout of mixing equipments

A Centrally placed impeller in bafled vessel, B Side-entring propeller, C Agitator


with draught tube
Mechanical seal

A Equipment with a drive at the top, B Equipment with a drive at the bottom

Design layout of agitators


Close clearance agitator

High-speed impeller

Maine type of close clearance agitators


No.

Layout of agitator

Name

Anchor (paddle)
agitator
CVS 69 1014

Helical-screw agitator
with draught tube
CVS 69 1028

T/d

Geometrical
parameters

1,11

hv / d 0,8
h / d 0,12
H 2 / d 0,055

hv / d 1,5
s/d 1
D/ d 1,1
H / D 1,15

hv / d 1,5

Eccentrically placed
helical-screw agitator

H 2 / d 0,25
s/d 1
c / T 0,02

T/d

Geometrical
parameters

Helical-ribbon
agitator
CVS 69 1029

1,05

hv / d 1
s/d 1
h / d 0,1

Leaf agitator
CVS 69 1016

h/d 1

h / d 0,2
hv / d 1,65
45
45
c / T 0,02
H 2 / d 0,175

No.

Layout of agitator

Name

Multi-stage agitator

Main type of high-speed impellers


T/d

Geometrical
parameters

Six-blade turbine
with disk (Ruschton
turbine)
CVS 69 1021

34

h / d 0,2
1 / d 0,25
d1 / d 0,75
6 blades

Six-blade open
turbine

34

h / d 0,2
6 blades

Pitched six-blade
turbine with pitch
angle 45
CVS 69 1020

34

h / d 0,20
45

No.

Layout of impeller

Name

No.

Layout of impeller

Name

T/d

Geometrical
parameters

Pitched three-blade
turbine with pitch
angle 45
CVS 69 1025.3

34

h / d 0,2
45

34

s/d 1
h / d 0,22
R / d 0,4
R1 / R 0,16

Propeller
CVS 69 1019

High shear stress


impeller
CVS 69 1038.1, .2

24

1st variant
h / d 0,1
d 2 / d 0,8
2nd variant
h / d 0,075
d 2 / d 0,85

Characteristics of mixing system


Power consumption of agitator

P
Po
n3d 5
creeping
flow

Po f Re
transition
zone of flow

Re

nd 2

turbulent
flow

Po B const.
A
Po
Re

baffled
vessel
unbaffled
vessel

Power characteristics of close clearance agitators

1 anchor agitator (CVS 69 1014), 2 helical-screw agitator with draught tube (CVS
69 1028), 3 eccentrically placed helical-screw agitator, 4 helical-ribbon agitator
(CVS 69 1029), 5 leaf agitator (CVS 60 1016), 6 multi-stage agitator

Power characteristics of high-speed impellers operated in baffled vessel

1 six-blade turbine with disk (Ruschton turbine) (CVS 69 1021), 2 six-blade open
turbine, 3 pitched six-blade turbine with pitch angle 45 (CVS 69 1020),
4 Pitched three-blade turbine with pitch angle 45 (CVS 69 1025.3), 5 propeller
(CVS 60 1019), 6a,b high shear stress impeller (CVS 69 1038.1.2)

Blending effect of agitator


During homogenization (or blending) of miscible liquids are compensated temperature and
concentration differences in agitated batch.

Homogenization of miscible liquids: due to recirculation flow (convective diffusion)


due to turbulent flow (turbulent diffusion)
due to molecular diffusion

t n t m f Re

t n t m konst.
t n t m konst.

Homogenization characteristics of agitators

t n t m f Re

1 helical-screw agitator with draught tub (CVS 69 1028), 2 eccentrically placed


helical-screw agitator, 3 helical-ribbon agitator (CVS 69 1029), 4 eccentrically
placed multi-stage agitator, 5 anchor agitator (CVS 69 1014), 6 six-blade turbine
with disk (Ruschton turbine) (CVS 69 1021)

E P tm

1 roubov mchadlo (CVS 69 1028), 2 roubov mchadlo umstn excentricky,


3 psov mchadlo (CVS 69 1029), 4 tynsobn lopatkov mchadlo umstn
excentricky, 5 kotvov mchadlo (CVS 69 1014), 6 turbnov mchadlo (CVS 69
1021), 7 estilopatkov mchadlo (CVS 69 1020), 8 tlopatkov mchadlo (CVS
69 1025.3)

Impellers for dispersing of gas in liquid

Impeller power consumption for gas liquid dispersing

Vg
f 3
nd
P

Pg

Mixing of suspension

Impeller power consumption for mixing of suspension

P
Po
su n3d 5

Po f Re
su cv s 1 cv l

Re

nd 2 su

Just-suspended impeller speed

n2d
Fr
g

Fr C
T

C A exp B cv

c cv

10

cv
0,025
0,05
0,1

Fr'

0,15
1

0,1
0,0001

0,2

0,001

0,01

D/T

0,1

EXAMPLE: Blending efficiency of impellers


Select type of high-speed impeller with minimum energetic requirements
for continual blending (homogenization) of two miscible liquids A + B ( = 5
mPas, = 1100 kgm-3) with flow rate of mixture 10 ls-1. For suitable degree
of homogenization must be residence time of liquids in equipment 5 x longer
than blending time. Mixing equipment has standard geometrical configuration
(baffled cylindrical vessel with diameter T = 1200 mm, T/d = 3.3; H2/d = 1, H/T
= 1 ).

Dimensionless blending time of high-speed impellers in turbulent flow regime


Type of impeller
Six-blade turbine with disk (Ruschton
turbine), CVS 69 1021
Pitched six-blade turbine with pitch
angle 45, CVS 69 1020
Pitched three-blade turbine with pitch
angle 45, CVS 69 1025.3

T/d

H2/d

ntm

3.3

51.8

3.3

53.1

3.3

60.5

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