Study On Thermal Treatment of Hybrid Technical Yarns: Fibers and Polymers February 2004
Study On Thermal Treatment of Hybrid Technical Yarns: Fibers and Polymers February 2004
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S. M. Ishtiaque
Indian Institute of Technology Delhi
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Introduction
Experimental
Preparation of Hybrid Yarns
In the hybrid yarn glass and polyester multifilaments were
chosen as core and the cotton and polyester staple fibers
were used in sheath. The specifications of these multifilaments and staple fibers are given in Table 1. Four series
of hybrid yarns with different combinations of multifilament
core and staple sheath fibers were spun on DREF-III system.
These are PC (polyester multifilament in core and cotton in
sheath), PP (polyester multifilament in core and staple
polyester fiber in sheath), GC (glass multifilament in core
and cotton in sheath), and GP (glass multifilament in core and
staple polyester in sheath). Keeping the same multifilament
in the core the proportion of staple fibers in the sheath was
adjusted to have the desired core-sheath ratio and thus the
26
Length
(mm)
24.6
44
Fineness
(dtex)/(g/in)*
67.30
620
4.20
1.66
Yarn linear
Spinning
Core-sheath
Delivery rate
density
drum speed
ratio
(m/min)
(tex)
(rpm)
67.30
44.87
33.65
10:90
15:85
20:80
3500
3500
3500
160
160
160
67.30
33.65
22.43
10:90
20:80
30:70
3500
3500
3500
160
160
160
206.67
155.00
124.00
30:70
40:60
50:50
3500
3500
3500
160
160
160
206.67
155.00
124.00
30:70
40:60
50:50
3500
3500
3500
160
160
160
Breaking extension
(%)
10.95
1.30
5.0
22.70
(1)
Sheath-slipping Resistance
The sheath-slipping resistance is the peak resistance force
generated during pulling out of multifilament core from 50
mm of hybrid yarn. Universal tensile testing machine
manufactured by SDL was employed for measuring the
sheath-slipping resistance. The sheath portion was removed
carefully from about 40 to 50 mm from one end of the
hybrid yarn keeping the opened out core filament intact. The
core filament was then passed through the hole of a normal
sewing needle. The other side of the needle (without hole)
was then gripped vertically in the bottom jaw of the
Universal tensile testing machine. The core filament, which
was passed through the needle, was then gripped in the
movable top jaw in such a way that only the entire openedout core filament portion passed through the needle hole.
The initial distance between the jaws was kept at 50 mm and
the crosshead speed was 50 mm/min. The length of the intact
hybrid yarn, on the other side of the needle hole, was kept
exactly 50 mm. The hole of the needle was selected
sufficiently large to allow smooth and uninterrupted passage
of core-filament but did not allow the sheath portion to pass
through. As the top jaw started moving, the load cell
attached with the top jaw measured the pulling out force of
core filament and the peak of the pulling out force was
27
PC1
PC2
PC3
PP1
12.4
12.6
13.1
2.3
12.6
30.1
6.9
15.3
2.8
14.7
29.9
6.6
14.7
14.7
PP2
15.5
15.4
16.0
4.2
15.4
31.3
7.0
PP3
0.07
0.09
0.06
0.06
0.07
0.05
GC1
0.05
0.00
0.00
0.10
0.12
0.04
0.00
0.10
GC2
0.07
0.06
0.04
0.00
0.10
0.06
0.11
GC3
GP1
0.10
0.08
0.04
0.10
0.08
0.08
0.04
0.09
0.00
0.09
0.05
0.04
0.09
0.00
GP2
0.08
0.06
0.05
0.06
0.09
0.05
0.10
GP3
1
Temperature was kept constant at 150 oC, 2Treatment time was fixed at 30 min.
12.2
13.8
15.7
0.05
0.00
0.00
0.00
0.06
0.00
12.9
13.8
15.9
0.00
0.03
0.08
0.08
0.00
0.00
1.8
2.2
3.7
0.05
0.10
0.06
0.08
0.10
0.05
12.2
13.8
15.7
0.05
0.00
0.00
0.00
0.06
0.00
29.6
30.4
32.0
0.08
0.10
0.05
0.00
0.07
0.00
28
36.9
33.1
30.0
5
45.5
18.4
22.1
30
56.7
32.3
26.2
60
43.5
27.3
26.1
100
49.0
27.5
23.3
150
56.7
32.3
26.2
200
101.5
57.1
52.7
5
68.6
45.5
20.6
30
87.3
58.0
35.5
60
98.4
66.5
37.3
100
77.6
42.4
27.1
150
87.3
58.0
35.5
200
151.9
150.0
108.
38.7
33.8
26.2
29.1
23.6
18.5
43.5
27.8
20.2
29.3
22.9
18.8
54.4
34.3
22.6
28.8
23.4
18.6
47.8
28.7
21.2
28.6
23.7
18.0
44.0
26.7
19.6
29.1
23.0
18.2
54.4
34.3
22.6
28.8
23.4
18.6
111.3
62.5
46.7
28.9
23.0
17.9
62.8
40.4
21.0
29.2
23.3
17.9
90.0
56.7
33.8
29.0
23.2
18.4
98.2
69.4
37.0
28.7
22.9
18.0
73.3
43.0
26.2
29.2
22.8
17.9
90.0
56.7
33.8
29.0
23.2
18.4
148.1
140.5
93.9
29.4
23.4
17.3
37.0
33.4
25.2
36.6
33.8
26.3
37.9
33.0
26.6
36.4
34.1
25.6
36.6
33.8
26.3
48.0
42.1
35.7
Sample
code
Sheath-slipping
resistance of
parent yarn (cN)
PC1
PC2
PC3
PP1
PP2
PP3
GC1
GC2
GC3
GP1
32.9
36.3
36.8
35.7
32.2
36.8
45.2
39.6
26.6
32.4
31.9
32.2
28.1
31.9
GP2
21.7
26.1
25.7
25.8
23.6
25.7
30.0
GP3
1
o
2
Temperature was kept constant at 150 C, Treatment time was fixed at 30 min.
29
Temperature2 (oC)
30
60
100
150
200
30
60
100
150
200
600
(10.14)
517
(10.48)
484
(10.78)
589
(11.11)
506
(11.15)
498
(12.06)
607
(11.25)
494
(10.82)
503
(12.65)
596
(10.36)
521
(10.47)
503
(12.35)
574
(10.62)
508
(10.62)
484
(10.93)
607
(11.25)
494
(10.82)
503
(12.65)
603
(13.07)
498
(12.15)
508
(14.44)
600
(10.43)
510
(10.58)
512
(12.02)
603
(10.72)
499
(10.92)
501
(12.11)
564
(10.85)
512
(11.04)
505
(12.52)
619
(9.95)
505
(10.54)
494
(10.85)
603
(10.72)
499
(10.92)
501
(12.11)
596
(11.26)
496
(11.32)
504
(14.33)
748
(10.26)
597
(10.44)
533
(10.79)
773
(11.24)
621
(11.40)
549
(11.97)
780
(11.19)
613
(11.51)
537
(12.05)
801
(11.22)
632
(11.46)
528
(11.89)
788
(10.62)
604
(11.14)
555
(11.68)
780
(11.19)
613
(11.51)
537
(12.05)
776
(13.77)
641
14.13)
530
(15.41)
784
(10.79)
637
(11.01)
521
(11.42)
802
(11.05)
642
(11.13)
549
(11.40)
783
(10.88)
589
(10.96)
551
(11.56)
796
(10.55)
619
(10.62)
559
(11.02)
802
(11.05)
642
(11.13)
549
(11.40)
802
(13.25)
627
(13.86)
538
(14.98)
1802
1796
1859
1848
1906
1881
1892
1866
1920
1806
1789
1852
1848
1906
1881
1814
1827
1871
1855
1827
1868
1790
1878
1827
1844
1829
1880
1826
1822
1869
1790
1878
1827
1849
1840
1871
GC1
1842
1826
1799
1837
1838
1799
1811
GC2
1858
1860
1919
1872
1889
1879
1872
1829
1904
1855
1866
1890
1855
1828
GC3
GP1
1802
1852
1848
1866
1810
1848
1887
GP2
1828
1818
1888
1912
1872
1798
1912
1843
1863
1886
1850
1885
1886
1802
GP3
1
o
2
Temperature was kept constant at 150 C, Treatment time was fixed at 30 min.
The figures in the parenthesis indicate breaking elongation (%).
10.22
9.70
7.95
14.2
12.8
9.6
30
60
10.20
9.71
7.93
14.4
13.4
9.9
10.12
9.66
8.00
13.9
12.6
10.0
10.10
9.64
7.89
14.1
12.8
8.9
100
10.19
9.70
7.96
14.3
11.3
9.2
150
10.12
9.66
8.00
13.9
12.6
10.0
200
10.16
9.68
7.89
14.4
11.9
9.1
30
60
10.24
9.68
7.99
14.0
11.4
8.7
10.18
9.72
7.95
13.9
13.0
9.4
10.06
9.66
7.98
14.5
12.3
9.9
100
10.09
9.64
8.01
14.1
12.8
8.9
150
10.18
9.72
7.95
13.9
13.0
8.9
200
10.11
9.60
7.90
13.8
12.7
9.1
1038
993
940
1126
966
931
1073
956
922
1056
1006
945
1112
991
892
1073
956
922
1082
974
910
1091
1012
929
1103
984
904
1099
1021
890
1091
1004
924
1103
984
904
1055
978
911
1150
1061
971
1168
1032
980
1204
1082
982
1188
1075
1004
1197
1058
1016
1204
1082
982
1169
1045
948
1221
1066
1012
1218
1102
1021
1182
1067
977
1190
1055
972
1218
1102
1021
1182
1106
978
Temperature was kept constant at 150 oC, 2Treatment time was fixed at 30 min.
30
Conclusions
The core-sheath type hybrid yarns are most suitable for
various technical applications. The main problem with these
yarns is poor sheath-slipping resistance, which results in
disintegration of the yarn structure during end use. This
problem can be reduced to a great extent by thermal
treatment of hybrid yarns, particularly when both or any one
of the component fibres is thermoplastic in nature.
The thermal shrinkage of core-sheath type hybrid yarn
with polyester multifilament core increases with the increase
in treatment temperature, but the treatment time shows no
significant effect on thermal shrinkage these yarns. Also the
decrease in proportion of sheath fiber results in increase in
thermal shrinkage of these yarns. No impact of thermal
treatment on shrinkage has been observed in the yarns with
glass multifilament in the core. Increase in proportion of
sheath fiber shows increase in sheath-slipping resistance for
parent yarn as well as for thermally treated yarns. For hybrid
yarns with polyester multifilament in core, as the treatment
temperature increases the sheath-sipping resistance also
increases significantly and it is higher in case of wet treatment
than dry treatment. The increase in proportion of sheath
fibers, in case of hybrid yarns with polyester multifilament
in core, results an increase in breaking strength and this
trend is valid for parent as well as thermally treated yarns.
With the increase in treatment temperature, for the hybrid
yarns with polyester multifilament in core, the breaking
elongation increases but the breaking strength reflects no
specific trend with regard to treatment temperature. There is
no significant effect of core-sheath ratio, time and temperature
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