Maintenance Guide ICP-MS
Maintenance Guide ICP-MS
Maintenance Guide ICP-MS
Customer Maintenance
Parts List
Notices
Warranty
Edition
Rev.B, December 2006
Printed in Japan
Agilent Technologies, Inc.
9-1 Takakura-cho, Hachioji-shi,
Tokyo 192-8510 Japan
Technology Licenses
The hardware and/or software
described in this document are furnished under a license and may be
used or copied only in accordance
with the terms of such license.
Safety Notices
CAUTION
A CAUTION notice denotes a
hazard. It calls attention to an
operating procedure, practice, or
the like that, if not correctly performed or adhered to, could result
in damage to the product or loss
of important data. Do not proceed
beyond a CAUTION notice until
the indicated conditions are fully
understood and met.
WARNING
A WARNING notice denotes a
hazard. It calls attention to an
operating procedure, practice,
or the like that, if not correctly
performed or adhered to, could
result in personal injury or
death. Do not proceed beyond a
WARNING notice until the
indicated conditions are fully
understood and met.
Contents
Preface
About the Maintenance Parts P-2
Conventions Used in This Book
P-3
P-4
1-2
2-10
C-1
4-2
5-2
7-2
8-2
9 Miscellaneous Components
Miscellaneous Components 9-2
10-7
11-2
C-3
C-4
Preface
Preface
The Agilent 7500 Series ICP-MS Customer Maintenance Parts List explains the
maintenance parts for use with the Agilent 7500, the Integrated Sample Introduction
System (ISIS), Integrated Auto Sampler ( I-AS), GC-ICP-MS Interface and the
ASX-500 Series ICP-MS Autosampler.
P-2
Notes
Notes contain a reminder about the effect of particular actions. They are indicated as
follows:
NOT E
Cautions
Cautions indicate situations that could overwrite data or require immediate attention
to prevent harm to the instrument. Cautions are indicated as follows:
CA UTI ON
This example shows how a caution is displayed.
Warnings
Warnings indicate situations that could cause bodily harm. Warnings are indicated as
follows:
WA RN IN G
This example shows how a warning is displayed.
P-3
Notice of Trademarks
Tygon and PharMed are registered trademarks of Norton Performance Plastics
Corporation.
Teflon is a registered trademark of E. I. DuPont de Nemours and Company.
Viton is a registered trademark of DuPont Dow Elastomers, L.L.C.
P-4
1-2
)
6'(.1067$+0)
27/267$+0)
61+56&
)
6'(.1067$+0)
)
615#/2.'
27/2
610'$7.+<'4
)
6'(.1067$+0)
6'(.1067$+0)
Table 1-1
)
)
Kit Contents
Description
5042-0918
G1833-65571
Tubing Adapter
G3138-60041
G3138-65158
Sample Tubing
G1820-65478
G1820-65478
5042-4749
G3138-65129
Sample Tubing
G1820-65009
G1820-65009
Teflon Nut
5042-4728
5064-8023
5042-4729
5064-8024
Cross Joint
G1833-60299
G1833-65579*
Bushing
Tubing
Connector
Drain Tank
P/N : 5042-4769 (4 liter)
G1820-65016 (1 liter)
G1820-65505 (for Organic Solvent)
5042-4769 : Polyethelene
G1820-65016 : with Polyvinyl Chloride Connector
G1820-65505 : with Polypropylene Connector
Photo : 5042-4769
1-4
Tubing Cutter
P/N : 8710-1930
1-5
1-6
2-2
Nebulizer
Tubing for
Carrier Gas
2-4
O-ring kit
P/N: G1820-65075
Viton o-rings, 2 sizes, 2 ea.
These o-rings are used for the end cap for the concentric
nebulizer. The smaller o-rings seal between the concentric
nebulizer and the center hole of the end cap, and the larger
o-rings seal between the end cap and spray chamber.
Replacement is required when the o-ring is damaged and
the seal is no longer good.
Tubing for
Make-up Gas
Tubing for
Carrier Gas
End Cap
Nebulizer
Teflon Tubing
for Sample
2-5
2-6
2-7
EzyLok Connector
P/N: G3266-80015
2-8
2-9
Torch
Spray Chamber Injector
Connector Tube
Drain Tube
End Cap
Torch (Quartz)
P/N: G3285-80050
2-11
2-12
Nebulizer
2-13
2-14
2-15
2-16
Connector (Quartz)
P/N : G1833-65426
This connector is used to connect the quartz spray chamber to
the torch.
Connector (Polypropylene)
P/N : G1833-65464
This connector is used to connect the polypropylene spray
chamber to the torch and is used for introducing hydrofluoric
acid. O-rings (G1833-65480) are also required to seal the
connection, to the spray chamber and the injector of the inert
torch.
3-2
Clamps (2/pk)
P/N : G1833-65430
The clamps are used to clamp the connector to the spray
chamber and torch.
3-3
3-4
4-2
Work Coil
P/N : G1833-65432
4-3
4-4
Specifications
7500a
7500i
7500s
7500c
7500ce
7500cs
T-mode
Nickel
G1820-65239
G1820-65360
G1820-65480
T-mode
T-mode
T-mode
Sampling cone
G1820-65238
Skimmer cone
G1820-65050
Nickel
G1833-65497
Nickel
G3270-65024
Nickel
G1820-65237
G1833-65092
G1833-65132
G3270-60106
G1820-65481
T-mode
T-mode
T-mode
Skimmer base
G1833-65407
G1833-65498
G1833-65591
G1833-65408
G1833-65505
G1833-65590
NOT E
: Cannot be used
5-2
5-3
Skimmer Cone
P/N : G1820-65050, Ni Skimmer Cone
G1833-65497, Ni Skimmer Cone
G3270-65024, Ni Skimmer Cone
G1820-65237, Copper base Pt Skimmer Cone
G1833-65092, Copper base Pt Skimmer Cone
G1833-65132, Copper base Pt Skimmer Cone
G3270-60106, Nickel base Pt Skimmer Cone
G1820-65481, Ni Skimmer Cone
Photo : G1820-65050
Application must refer to Interface and Skimmer Base
Conformity Chart.
G1820-65050 :
The Nickel skimmer cone is used as the standard interface of
the Agilent 7500a, i. This skimmer cone is relatively robust to
samples containing high concentrations of matrix and salts,
and is suitable for a wide variety of samples. It is usually used
with the Nickel sampling cone. It can be used with the 7500a,
7500i, and 7500s.
G1820-65237 :
The Platinum skimmer cone is usually used for introduction of
hydrofluoric acid and other reagents for the 7500s. It is usually
used with the Platinum sampling cone. It can be used with the
7500a, 7500i, and 7500s.
G1820-65481 :
This skimmer cone is used for the T-mode option only. It is
used with the Nickel sampling cone for T-mode.
G1833-65497 :
This is used for the 7500c. It is used with the Nickel sampling
cone (G1820-65238).
G3270-65024:
This Skimmer Cone is used as the standard interface for the
7500ce. It is used for the 7500ce only and it is used with the
Nickel Sampling Cone (G1820-65238).
G1833-65132 :
This Platinum skimmer cone is used as the standard interface
of the 7500cs. It can be used for the 7500ce and the 7500cs. It
is used with the Platinum sampling cone (G1820-65239 or
G1820-65360).
5-4
CA UT I ON
The Platinum Skimmer cone must be mounted on the Brass skimmer base; otherwise
the copper base of the skimmer cone will deteriorate and shorten the lifetime of the
skimmer cone itself.
Platinum Skimmer Cone
7500a
G1820-65237
G1833-65408
7500ce/cs
G1833-65132
G1833-65590
Citranox
P/N : 5188-5359
5-5
5-6
Specifications
7500a
7500i
7500s
7500c
7500ce
7500cs
T-mode
Nickel
G1820-65239
G1820-65360
G1820-65480
T-mode
T-mode
T-mode
Sampling cone
G1820-65238
Skimmer cone
G1820-65050
Nickel
G1833-65497
Nickel
G3270-65024
Nickel
G1820-65237
G1833-65092
G1833-65132
G3270-60106
G1820-65481
T-mode
T-mode
T-mode
Skimmer base
G1833-65407
G1833-65498
G1833-65591
G1833-65408
G1833-65505
G1833-65590
NOT E
: Cannot be used
6-2
6-3
Extraction Lens 1
P/N : G1833-65417
Extraction Lens 2
P/N : G1833-65413
6-4
Plate Bias
P/N : G1833-65444 (for Slim Ring Type Quadrupole)
P/N : G1833-65494 (for Eagle Type Quadrupole)
Photo: G1833-65444
6-5
Electron Multiplier
P/N : 5184-1983 (S/N ~JP14100586)
G1833-65575 (S/N JP14100587~)
There are two types of electron multiplier: ETP and HPK.
Order P/N G1833-65575 for instruments with the label "HPK
Installed" (S/N JP14100587 and later), and P/N 5184-1983 for
instruments without such a label (S/N JP14100586 and
earlier). The two types of electron multipliers have similar
performance, but as the tuning conditions are different, using
the same type of electron multiplier is recommended.
The electron multiplier detector should be replaced when
either the Analog HV exceeds 3300v or the pulse HV exceeds
1800v.
6-6
Extraction Lens 2
P/N: G3270-65029
Omega Lens-ce
P/N: G3270-65030
Omega Bias-ce
P/N: G3270-65031
7-2
7-3
Plate Bias
P/N : G1833-65513 (S/N JP14100050 ~ JP14100313)
G1833-65562 (S/N JP14100314 ~)
Check equipment S/N when placing an order.
7-4
O-ring (2/pk)
P/N: G1833-66035
7-5
Alumina Powder
P/N : 8660-0791
7-6
Extraction Lens 2
P/N: G1833-65593
Omega Bias-cs
P/N: G1833-65594
Omega Lens-cs
P/N: G1833-65595
8-2
8-3
Plate Bias
P/N : G1833-65513 (S/N JP14100050 ~ JP14100313)
G1833-65562 (S/N JP14100314 ~)
Check equipment S/N when placing an order.
8-4
O-ring (2/pk)
P/N: G1833-66035
8-5
Alumina Powder
P/N : 8660-0791
8-6
Miscellaneous Components
Miscellaneous Components
Plastic Tray
P/N : G1833-65412
Gas Filter
P/N : G1833-65581
9-2
9-3
Tuning Solution
P/N : 8500-6943, Stock Tuning Solution: Li, Y, Ce and
Tl; 100 mL, 10 mg/L; matrix=2% HNO3
5184-3566, Tuning Solution: Li, Y, Ce, Tl and
Co; 2 x 500 mL, 10 g/L; matrix= 2% HNO3
5185-5959, Tuning Solution: Li, Mg, Y, Ce, Tl
and Co; 2 x 500mL, 1 g/L; matrix= 2% HNO3
LC-ICP-MS Connection Kit
P/N : G1833-65200
Description :
Sample Tubing
Ferrule
Connector
Union
APG Remote Cable
Gender Changer
9-4
10
10
Joint Holder
P/N : G3138-65102, for ICP-MS Pump
G3138-65103, for ISIS Pump
Used to hold the joints.
10-2
Mixer
P/N : G3138-65121
Tubing Adapter
P/N : G3138-65126
Between ISTD peripump tubing/teflon tubing.
Tubing Adapter
P/N : G3138-65158
10-3
Sample Tubing
P/N : G1820-65105, PFA, 0.5mm id, 1.6mm od, 5m
G1820-65478, PFA, 0.3mm id, 1.6mm od, 3m
5064-8016, ETFE, 0.8mm id, 1.6mm od, 5m
5064-8020, PTFE, 2.0mm id, 3.0mm od, 5m
Tee Joint
P/N : 5064-8017
Cross Joint
P/N : 5064-8018
10-4
Union Joint
P/N : 5064-8019
10-5
10-6
10-7
10-8
Y Connector (5/pk)
P/N : G3138-65143
10-9
10-10
11
11
Injector
P/N : G3158-65001
11-2
Ferrule Kit
P/N : G3158-65004
Description:
Reducer Ferrule (1/8in to 1/16in, 2/pk)
Graphite Ferrule (320um, 0.5mm id, 2/pk)
Vespel-Graphite Ferrule (1/4in, 2/pk)
Vespel-Graphite Ferrule (1/16in, 2/pk)
Alignment Boss
P/N : G3158-65008
11-3
11-4
12
12
12-2
G3160-65312
Type C Tray-18 position for 50mL Vial
G3160-65313
Type D Tray - 79 position for 2mL (or 1.5mL) vial and 10
position for 18mL vial
G3160-65314
Type E Tray - 79 position for 6mL vial and 10 position for
18mL vial
Vial
P/N : G3160-65303
6mL vial (Polypropylene), 200 pieces
P/N : G3160-65304
18mL vial (Polypropylene), 55 pieces
P/N : G3160-65305
50mL vial (Polypropylene), 20 pieces
P/N : G3160-65315
2mL vial (Polyethylene), 200 pieces
P/N : G3160-65317
1.5mL vial (PFA), 10 pieces
G3160-65303
for type A, E Tray
G3160-65304
for type B, D, E, Tray
G3160-65305
for type C Tray
G3160-65315
for type D Tray
G3160-65317
for type D Tray
12-3
Probe
P/N : G3160-65306 (0.3mm id)
G3160-65324 (0.8mm id)
Tray Cover
P/N : G3160-65321
External Bottle
P/N : G3160-65307
100mL Bottles (with cap (QTY3), with holed cap (QTY3))
12-4
TubeHolder(forI-AS)
P/N: G3160-65325
Use this adapter for connecting the 1.66mm sample tubing
to the probe.
It is possible to use the sample tubes G1833-65572
(0.15mmid), G1833-65573 (0.2mmid), G1820-65478
(0.3mm id).
Needle Holder
P/N : G3160-80041
Arm
P/N : G3160-80044
Carry Holder for tray and tray cover
P/N : G3160-60015
Convenient holder for lifting and carrying the I-AS tray in
combination with the tray cover.
12-5
12-6
13
13
Sample Probe
P/N : G3286-80100 (0.8 mm id)
G3286-80101 (0.3 mm id)
G3286-80102 (0.5 mm id)
13-2
Rinse Station
P/N : G3286-80224
13-3
13-4
INDEX
8710-1930................................ 1-5
9300-2574......................... 7-5, 8-5
G1820-60160........................... 2-4
G1820-60453........................... 2-2
G1820-65009......................... 2-15
G1820-65016........................... 1-4
G1820-65023........................... 9-2
G1820-65025........................... 5-3
G1820-65027........................... 4-3
G1820-65030........................... 2-4
G1820-65050........................... 5-4
G1820-65052........................... 2-4
G1820-65075........................... 2-5
G1820-65105................ 2-15, 10-4
G1820-65119......................... 2-12
G1820-65138........................... 2-4
G1820-65141......................... 2-12
G1820-65198......................... 2-14
G1820-65199........................... 2-3
G1820-65214........................... 2-2
G1820-65237........................... 5-4
G1820-65238........................... 5-3
G1820-65239........................... 5-3
G1820-65276........................... 2-3
G1820-65337........................... 3-2
G1820-65345........................... 2-3
G1820-65360........................... 5-3
G1820-65435........................... 6-3
G1820-65478................ 2-15, 10-4
G1820-65480........................... 5-3
G1820-65481........................... 5-4
G1820-65482........................... 1-4
G1820-65491........................... 2-5
G1820-65503........................... 1-4
G1820-65504........................... 1-4
G1820-65505........................... 1-4
G1820-65515........................... 1-4
G1820-65518......................... 2-14
I-1
G3139-65005........................... 2-7
G3139-65006........................... 2-7
G3139A#011............................ 2-6
G3139A#012............................ 2-6
G3139A#021............................ 2-6
G3139A#022............................ 2-6
G3139A#131............................ 2-6
G3139A#301............................ 2-6
G3154-65001........................... 9-4
G3154-65002........................... 9-4
G3158-65000......................... 11-2
G3158-65001......................... 11-2
G3158-65002......................... 11-2
G3158-65003......................... 11-2
G3158-65004......................... 11-3
G3158-65005......................... 11-3
G3158-65006......................... 11-3
G3158-65007......................... 11-3
G3158-65008......................... 11-3
G3160-60015......................... 12-5
G3160-65300......................... 12-2
G3160-65301......................... 12-2
G3160-65302......................... 12-2
G3160-65303......................... 12-3
G3160-65304......................... 12-3
G3160-65305......................... 12-3
G3160-65306......................... 12-4
G3160-65307......................... 12-4
G3160-65308......................... 12-2
G3160-65309......................... 12-2
G3160-65310......................... 12-2
G3160-65311......................... 12-2
G3160-65312......................... 12-2
G3160-65313......................... 12-2
G3160-65314......................... 12-2
G3160-65315......................... 12-3
G3160-65317......................... 12-3
G3160-65320......................... 12-4
I-3
G3286-80100 ........................
G3286-80101 ........................
G3286-80102 ........................
G3286-80103 ........................
G3286-80104 ........................
G3286-80105 ........................
G3286-80106 ........................
G3286-80107 ........................
G3286-80117 ........................
G3286-80118 ........................
G3286-80200 ........................
G3286-80224 ........................
13-2
13-2
13-2
13-2
13-2
13-2
13-2
13-2
13-2
13-2
13-3
13-3