Load Testing Refractory Brick at High Temperatures: Standard Test Method For
Load Testing Refractory Brick at High Temperatures: Standard Test Method For
Load Testing Refractory Brick at High Temperatures: Standard Test Method For
3.2 This test method is not applicable for refractory materials that are unstable in an oxidizing atmosphere unless means
are provided to protect the specimens.
1. Scope
1.1 This test method covers the determination of the resistance to deformation or shear of refractory brick when subjected to a specified compressive load at a specified temperature for a specified time.
1.2 The values stated in inch-pound units are to be regarded
as the standard. The values given in parentheses are for
information only.
1.3 This standard does not purport to address the safety
concerns, if any, associated with its use. It is the responsibility
of the user of this standard to establish appropriate safety and
health practices and determine the applicability of regulatory
limitations prior to use.
4. Apparatus
4.1 The apparatus shall consist essentially of a furnace and
a loading device. It may be constructed in accordance with Fig.
1 or Fig. 2 or their equivalent.3
4.1.1 The furnace shall be so constructed that the temperature is substantially uniform in all parts of the furnace. The
temperature as measured at any point on the surface of the test
specimens shall not differ by more than 10F (5.5C) during
the holding period of the test or, on test to failure, above
2370F (1300C). To accomplish this, it may be necessary to
install and adjust baffles within the furnace. A minimum of two
burners shall be used. If difficulty is encountered in following
the low-temperature portion of the schedule (particularly for
silica brick), a dual-burner system is recommended, one to
supply heat for low temperatures and another for the higher
temperatures.
4.2 The temperature shall be measured either with calibrated4,5,6 platinum - platinum - rhodium thermocouples, each
encased in a protection tube with the junction not more than 1
in. (25 mm) from the center of the side or edge of each
specimen or with a calibrated4,5,6 pyrometer. A recording form
of temperature indicator is recommended. If the optical pyrometer is used, observations shall be made by sighting on the face
of the specimens and in the same relative positions as those
specified for the thermocouples.
2. Referenced Documents
2.1 ASTM Standards:
E 220 Method for Calibration of Thermocouples by Comparison Techniques2
3. Significance and Use
3.1 The ability of a refractory brick to withstand prescribed
loads at elevated temperatures is a measure of the hightemperature service potential of the material. By definition,
refractory brick must resist change due to high temperature;
and the ability to withstand deformation or shape change when
subjected to significant loading at elevated temperatures is
clearly demonstrated when refractory brick are subjected to
this test method. The test method is normally run at sufficiently
high temperature to allow some liquids to form within the test
brick or to cause weakening of the bonding system. The result
is usually a decrease in sample dimension parallel to the
applied load and increase in sample dimensions perpendicular
to the loading direction. Occasionally, shear fracture can occur.
Since the test provides easily measurable changes in dimensions, prescribed limits can be established, and the test method
has been long used to determine refractory quality. The test
method has often been used in the establishment of written
specifications between producers and consumers.
5. Test Specimen
5.1 The test specimen shall consist of a minimum of two 9
by 412 by 212 or 3-in. (228 by 114 by 64 or 76-mm) straight
refractory brick, or specimens of this size cut from larger
shapes, utilizing as far as possible existing plane surfaces.
3
Blueprints of detailed drawings of the furnaces shown in Figs. 1 and 2 are
available from ASTM. Request Adjunct No. 12-300160-00.
4
Method E 220 specifies calibration procedures for thermocouples.
5
The National Institutes of Standards and Technology, Gaithersburg, MD 20899,
will, for a fee, furnish calibrations for radiation-type pyrometers and for thermocouples.
6
All temperatures specified in this test conform to the International Practical
Temperature Scale of 1968 (IPTS 1968) as described in Metrologia, Vol 5, No. 2,
1969, pp. 3544.
1
This test method is under the jurisdiction of ASTM Committee C-8 on
Refractories and is the direct responsibility of Subcommiteee C08.01 on Strength.
Current edition approved Dec. 28, 1981. Published March 1982. Originally
published as C16 17 T. Last previous edition C16 77.
2
Annual Book of ASTM Standards, Vol 14.03.
Copyright ASTM, 100 Barr Harbor Drive, West Conshohocken, PA 19428-2959, United States.
C 16
in.
18
24
SI Equivalents
mm
460
610
NOTE 1Recommended designs for the furnace and loading device are
shown in Fig. 1 and Fig. 2. Inside dimensions may vary between those
shown on these drawings. The dimensions of the framework will be
determined by the selection made on inside dimensions, thickness of
refractory wall etc. The framework for either the direct loading or lever
type are shown in sufficient detail so detailed drawings for furnace
construction can easily be made. The use of a flue system with either
design is optional.
NOTE 2Gross errors which may more than double the deformation
will result if the specimen is not set perpendicular to the base of the
support or if the load is applied eccentrically.
7. Procedure
7.1 LoadingCalculate the gross load to be applied
throughout the test from the average cross section of the
2
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NOTE 3It is recommended that a photograph be made of the specimens before and after testing to provide useful information.
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TABLE 1 Time-Temperature Schedules for Heating the Test Furnace All temperatures shall be maintained within 620F (11C) during
the heat-up schedule and 610F (5.5C) during the holding period.
Elapsed Time from
Start of Heating
Schedule 1,
2370F Hold
Schedule 2,
2460F Hold
Schedule 3,
2640F Hold
Schedule 4,
Silica Brick,
Test to Failure
Schedule 5, Test
to Failure
Schedule 6,
2900F Hold
Schedule 7,
3000F Hold
min
0
15
30
45
930
1105
1265
1420
500
595
685
770
930
1150
1330
1500
500
620
720
815
1040
1255
1470
1650
560
680
800
900
245
310
380
450
120
155
195
230
1330
1490
1650
1780
720
810
900
970
1330
1490
1650
1780
720
810
900
970
1330
1490
1650
1780
720
810
900
970
0
15
30
45
1560
1690
1815
1920
850
920
990
1050
1650
1795
1915
2010
900
980
1045
1100
1815
1960
2085
2190
990
1070
1140
1200
535
630
775
1025
280
330
415
550
1910
2005
2100
2180
1045
1095
1150
1195
1910
2005
2100
2180
1045
1095
1150
1195
1910
2005
2100
2180
1045
1095
1150
1195
0
15
30
45
2010
2095
2165
2230
1100
1145
1185
1220
2100
2185
2255
2320
1150
1195
1235
1270
2280
2355
2425
2500
1250
1290
1330
1370
1275
1525
1750
1990
690
830
955
1090
2260
2315
2370
2415
1240
1270
1300
1325
2260
2315
2370
2415
1240
1270
1300
1325
2260
2315
2370
2415
1240
1270
1300
1325
0
15
30
45
2280
1250
2325
1275
2370
1300
Hold for 90 min
2370
1300
2425
1330
2460
1350
Hold for 90 min
2550
1400
2605
1430
2640
1450
Hold for 90 min
2200
2400
2550
2660
1205
1315
1400
1460
2460
2505
2550
2595
1350
1375
1400
1425
2460
2505
2550
2595
1350
1375
1400
1425
0
15
30
45
...
...
...
2640
2685
2730
2775
1450
1475
1500
1525
2640
2685
2730
2775
1450
1475
1500
1525
0
15
30
45
...
...
...
...
...
2820
1550
2865
1575
2900
1595
Hold for 90 min
2820
2865
2910
2955
1550
1575
1600
1625
0
15
30
45
...
...
...
...
...
3000
1650
6h
6h
6h
8 h to 3000F
(1650C)
8 h to 3180F
(1750C)
Total time
2460
1350
Continue at 180F
(100C)/h
to failure
2700
1480 . . .
Continue at 100F
(55C)/h
to failure
8h
Between
Laboratories
79.6
56.3
39.8
32.5
28.1
25.2
8.0
96.5
78.4
67.6
63.6
61.5
60.2
55.2
1
2
4
6
8
10
100
9. Keywords
9.1 compressive load; deformation resistance; high tem-
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