Dilo

SF6-Multimeter
Operating Manual (original version)

Type-No.: 3-038
SF6-Multimeter | 3-038
Page
1. General information 4
 1.1 Safety notes and standard symbols 4
 1.2 Initial setting into operation 5
 1.3 Correct use of the SF6 Multimeter 5
 1.4 Obligation to exercise due care 6
 1.5 Instructions for exchanging the measuring gas modules 7
2. Overview - SF6-Multimeter 8
 2.1 Technical data 9 / 10 / 11
 2.2 Accessories 12
3. Functional description 13
 3.1 Operation mode of the SF6-volume percentage sensor 13
 3.2 Operation mode of the moisture sensor 13
 3.3 Operation mode of the SO2-sensor 13
 3.4 Operation mode of the temperature measurement 14
 3.5 Gas flow diagramm 15
4. Description of the menu and the measuring process 16 / 17

 4.1 Navigation with the navigation turning knob 17
 4.2 Overview 18 / 19 / 20
 4.3 Description of the menu 21
 4.3.1 “Start measurement” 21
 4.3.2 “Data transmission” 22
 4.3.3 “Measuring data” 22
 4.3.4 “Settings” 22 / 23
 4.4 Storage of measuring data 24
 4.5 Individual measurement 24 / 25
 4.6 Permanent measurement 26
5. Transmission of the measuring data on a PC or laptop 27

 5.1 Installation of the USB-driver 27
 5.2 Read-out the measuring data from the SF6-Multimeter 28
6. Limit value contacts – Pin allocation Out Vol.-% Moisture 29
7. Back view of the SF6-Multimeter 30

 7.1 Return of the measuring gas modules 31
8. Fault correction 31 / 32
www.dilo-gmbh.com | C 2901-05 | Page 2 / 35

9. Discharge gas collection unit (B151R20, optional) 33
10. Appendix 34 / 35
Please read this operating manual before putting the device into operation. Thus operating faults can be avoided.
In case of nonobservance of the operating manual the manufacturer cannot assume any liability or warranty.
The copyright of this documentation remains with DILO Armaturen und Anlagen GmbH, D-87727 Babenhausen.
Any use not permitted by the author (multiplication, leaving to third persons etc.) is subject to penalty and
indemnification.

1. General information
1.1 Specific safety notes and standard symbols
In the following operating manuals specific safety warnings are given in order to draw your
attention to residual risks which cannot be avoided during the operation of the device.
These residual risks contain dangers for

 Persons
 Product and machine
 The environment
The symbols used in the operating manuals should draw your attention specially to the
safety notes! If the device is not used for the purposes for which it is intended there is the risk of
danger. For this reason observe the safety notes:
This symbol refers to risks for persons (danger to life, danger of injury)
Danger
This symbol refers to risks for machines, material and the environment.
Warning
This symbol refers to electric shock
The most important aim of the safety notes is to prevent personal injuries.
 If the warning sign „Danger“, appears, danger from machines, materials and the environment
are not excluded.
 If the warning sign „Warning“, appears, there is no danger for persons.
The corresponding symbol which is used cannot replace the text of the safety note.
Therefore the complete text must always be read.
This symbol is not for safety notes, but for information to better understand the the
device.

1.2 Initial operation
All personnel involved in the operation and repair of DILO devices should be specially trained and
instructed.
For the initial operation of the SF6-Multimeter no special measures must be taken.
For the measurement follow the instructions of chapter 4.5 “Individual measurement” or chapter 4.6
“Permanent measurement”.
1.3 Correct use of the SF6-Multimeter
The SF6-Multimeter serves for the determination of the SF6-volume percentage of moisture and SO2
(sulphur dioxide) in the SF6-gas. After the measurement the measuring values can be stored in the SF6-
Multimeter and if necessary they can also be transmitted immediately or later to a PC or Laptop.
The measuring gas is released via the open “gas outlet” stub on the back. For environmental protection
a B151R20 discharge gas collection unit is available as option. With this unit the measuring gas can be
collected completely. It is also possible to lead the used gas into the gas collecting bag. As the inlet
valve of the SF6-Multimeter closes in time and thus the measurement is interrupted an overpressure in
the gas collecting bag cannot be generated.
In case of long-time application without using a discharge gas collection unit pay attention that the
corresponding rooms are ventilated sufficiently.
The use of the device for different gas mixtures (SF6-N2/air or SF6-CF4) is only possible as option and
by switching over.
Do not close the “Gas outlet“ during the operation of the device otherwise
the measuring process is interrupted.

1.4 Obligation to exercise due care
The device has been designed and constructed bearing in mind the standards to be
observed as well as additional technical specifications.
Safe use of the machine can only be achieved if all the necessary measures are followed.
The operator has to ensure that
 the SF6-Multimeter is only used for the purposes for which it is intended.
 the SF6-Multimeter is only operated in accordance with the instructions and in good condition
 complete and legible operating manuals are available on site.
 only qualified personnel operates or repairs the SF6-Multimeter.
 this personnel is regularly instructed in safety procedures and environmental protection and
that this personnel is fully aware of the complete operating manuals and particularly in the
safety notes.
 the safety and warning notes mounted on the SF6-Multimeter are legible and not removed.
The parts inside the SF6-Multimeter are under dangerous supply voltage in case
of connected power connecting cable. Prior to opening the housing disconnect
the device from the power supply and switch off the device so that it does not
Danger run with accumulators.
In the power supply of the device there are lithium ions accumulators.
Do not damage the device otherwise short-circuits can be generated.
Danger

1.5 Instructions for exchanging measuring gas modules
There are 3 modules in the SF6-Multimeter of which the measuring gas module SF6-volume percentage
sensor and the module moisture SO2-sensor can be exchanged in case a recalibration is necessary
(point 7.1).
For exchanging a module 4 screws are to be loosened on the back (Ill. 7.1).
Prior to opening the housing switch off and unplug the device so that it is
not battery-operated (exception chapter 8 elimination of fault).
Tilt the front cover by loosening both upper screws and pull off the flat strip line to the graphic display in
the middle.
Opening of the upper coupling:

Press the fitting and the bushing of the coupling as illustrated. Then the fitting is opened. (see illustration
1.1).
Ill. 1.1 Opening of the upper coupling
Opening of the lower coupling:

Press the bushing of the coupling backwards. The fitting is opened.
The measuring gas module and the connecting hoses are marked by
different colours. The connecting hoses and measuring gas modules of the
same colours belong together and must not be mixed. When coupling again
pay attention that coloured markings match with the colours on the
Warning measuring gas modules.
The measuring gas module can only be pulled out from the back of the SF6-
Multimeter if both couplings are disconnected internally and the 4 screws of
the measuring gas module on the back are unscrewed.

2. Overview of SF6-Multimeter
The SF6-Multimeter allows the measurement of the SF6-volume percentage, the gas moisture and the
SO2-concentration with one measuring process. After each measurement the measuring values can be
stored, indicating the user name and a name of the measuring point.
The measuring values of the SF6-volume percentage, the gas moisture and the SO2-concentration are
digitally indicated on the display. In the standard version the SF6-volume percentage sensor is calibrated
for SF6/N2 or SF6/air and measures the SF6-content in volume percent in such a gas mixture. The
SF6- volume percentage sensor works independently of air pressure and installation position.
The moisture sensor measures the dew point temperature of SF6-gas in °C dew point. The measuring
value of the dew point in °C can be automatically indicated or converted into all indicating units in case of
modified setting. A conversion into the dew point under pressure in the compartment is also possible.
Furthermore, the SF6-Multimeter includes a temperature sensor which measures the temperature of the
SF6-gas.
The main components of the SF6-Multimeter are as follows:

 a measuring gas module with an SF6-volume percentage sensor,
 a measuring gas module with moisture and SO2-sensor as well as
 a module with a power supply unit; the module with the power supply unit also includes
accumulators
 a board with the central unit, pressure sensors and tubing with solenoid valve and pressure
reducer,
 all components of the SF6-Multimeter are installed in a portable and modular housing
The modular construction enables to send each single measuring gas module for verification, calibration
or exchange to the manufacturer. In principle, it is also possible to measure with only one measurement
gas module.
The SF6-Multimeter is very easy to operate on the front side where the following can be found:
the “Gas inlet“, a graphic display (128x64 pixel), two LED control lamps, a navigation turning knob with
integrated pressure point for navigation in the operating menu, two buttons (ON/OFF, ) as well as the
“Purge“ bypass valve which allows quick rinsing (with long connecting hoses) and shortening of the
response time.
On the back there is the “Gas outlet“ stub where the measuring gas flows through and can be collected
for reuse. All modules are assembled from the back of the SF6-Multimeter.
The lithium ions accumulator installed in the power supply unit enables net-independent working.
Loading of the accumulator is done automatically if the device is connected to the power supply and
switched on. Overloading or total discharging of the accumulator is impossible, which raises the lifetime
considerably.
We recommend instructing the personnel on careful handling of SF6-gas, moisture and SO2
measurement.

2.1 Technical data
ill. 2.1 SF6-Multimeter with standard accessories
Dimensions: (with handle on the front side)
Length (L): 450 mm

Width (B): 280 mm
Height (H): 185 mm
Weight: 9.6 kg
Dimensions: transport case
Length (L): 540 mm

Width (B): 460 mm
Height (H): 305 mm
Weight: 10.5 kg
ill. 2.2 transport case

General data:
Input pressure: pe 0.5 – 10 bar
Operating temperature: -20°C - +40 °C
Operating voltage: 90 – 264 V /50-60Hz, max. 28 W
Power supply must be protected via a residual
current device (RCD) with a max. operating
current of 30mA.
Interfaces: USB (slave)
Mains fuse: 2 x 1 A/T (inert)
Duration of measurement
(individual measurement): 6 – 15 min. (ajustable)
Limit value (volume percent) (potential-free): 0.0 – 99.9 vol.-% Limit
value (dew point) (potential-free): -60 °C - +10 °C
Accumulator: lithium-ions accumulator
(for about 6-8 h working time)
14.4 V; 4.5 Ah, 4S2P, 64.8 Wh
Flow rate (all sensors): 17.5 – 20.5 lN SF6/h = 106 – 125 g SF6/h
Max. number of measuring values
to be stored: 100
Input pressure sensor: ± 0.5% FS, i. e. max. ± 0.08 bar
Output pressure sensor: ± 0.5% FS, i. e. max. ± 5 mbar
Volume percentage sensor:

Measuring media: SF6/N2 or SF6/air gas mixture (3-
038-
R020/R021/R022) and SF6/CF4 gas
Mixtures (3-038-R030/R031/R032)
Measuring range: 0.0 to 100.0 vol.-% SF6

Measuring accuracy: ± 1 vol.-% for gas mixtures SF6/N2 or SF6/air
± 2 vol.-% for gas mixtures SF6/CF4
Measuring condition: measurement is carried out under atmospheric
pressure
Flow rate: 0.3 – 0.5 lN SF6/h = 1.8 – 3.1 g SF6/h
Operating temperature: -20 °C to +40 °C
Recommended calibration interval: every 2 years

Moisture sensor:
Measuring range: -60 °C to - +20 °C dew point temperature
Measuring accuracy: ± 2 °C at - 40°C to + 10°C dew point temperature
± 3 °C at < - 40°C dew point temperature
Measuring condition: Measurements are carried out at atmospheric pressure.
The device converts dew points under pressure.
Flow rate: 16 – 17 lN SF6/h = 98 – 104 g SF6/h
Operating temperature: -20 °C to +60 °C
SO2-sensor:
Measuring ranges: 0 … 100 ppmV, resolution 1 ppmV
0 … 20 ppmV, resolution 0.1 ppmV
0 … 500 ppmV, resolution 1
ppmV Measuring accuracy: < ± 2 % from the end value
Operating temperature range: - 20 °C to + 45 °C
Response time: T90 (final value 90%) < 20 s
Long time stability: 0,5 … < 2 % signal degradation per month (linear)
Recommended calibration interval: 2 years (see indication on the menu)
Protection against SO2 overcharge: automatically
Flow rate: 1-3 lN SF6/h = 6 – 18 g SF6/h
Modules: Order no.

SF6-volume percentage sensor module 3-038-10, 3-038-11
Moisture SO2 sensor module 3-038-60, 3-038-62, 3-036-63
Power supply module 3-038-01

2.2 Accessories
The SF6-Multimeter includes:

 housing with handle for transportation and placing
 4 m long connecting hose with DILO couplings DN8 and DN20
 Power plug with 2 m long connecting cable
 USB connecting cable
 connecting plug for Out vol.-% moisture
 CD-ROM with software for evaluation and reading of the measured values and saving on the PC
 transport case
1 operating manual (multilingual)

3. Functional description
3.1 Function of the SF6 volume percentage sensor
The measuring principle is based on the evaluation of the different velocities of sound of gases. The
velocity of sound in air is normally about 330 m/s, while in SF6-gas it is only about 130 m/s. The velocity
of sound measured in the measuring cell is temperature compensated and converted into SF6 volume
percent by means of a microprocessor.
3.2 Function of the moisture sensor
The moisture sensor is based on the absorption of water molecules in a special ceramic substrate.
Therefore the electric capacity of the sensor element changes which is registered by the evaluation
electronics and is converted into a standard signal.
3.3 Function of the SO2 sensor
The electrical conductivity of the electro-chemical sensor used changes as soon as SO2-gas molecules
react with the sensor. The cross sensitivity to other gases is very low – dependant on the gas type.
The SF6-gas passed diffuses into the SO2 sensor where it reacts with the electrode to be measured due
to the oxidation process in accordance with the following equation:
Equation 1: measuring process

Sulphur dioxide (SO2): SO2 + 2H2O = H2SO4 + 2H+ + 2e-
The backplate electrode tries to compensate the reaction on the electrode to be measured like a certain
balance by means of oxygen reduction where water is produced.
Equation 2: compensation reaction

Oxygen reduction: ½ O2 + 2H+ + 2e- = H2O
Two reactions reflect the total reaction of the measuring cell as follows:
SO2 + ½ O2 + H2O = H2SO4
If SO2 exists in the SF6-gas to be examined, equation 1 changes its electro-chemical potential so that
electrodes are released. Consequently a voltage change is detected, which is converted into the ppmv-
values.
The SO2-sensor contains a transmitter board which enables temperature compensation and calibration
for the measuring range.

3.4 Function of the temperature measurement
The temperature of the measuring gas recorded by the device is effected by an integrated temperature
sensor (in gas flow direction) near the moisture sensor. As the flow rate is too low, there is practically no
cooling-down of the gas by expansion.
The gas temperature in the gas compartment and the measured gas temperature
can deviate from each other as the gas temperature is measured inside the device
and not directly at the gas compartment. This could have an influence on the
calculated gas density. For the calculation of the gas density a possible N2 or CF4
content is taken into consideration.

3.5 Gas flow diagram
Pos. Designation Order no.

1 Coupling NW 5 1-05-1358-R012
2 Solenoid valve 1-05-1061-R006
3 Pressure sensor 200 psi abs. 1-05-1270-R005
4 Pressure regulator pe 0.5 bar 1-05-1431-R001
5 Coupling piece 1/8“ internal thread 1-05-1358-R014
6 Coupling 1/8“ internal thread 1-05-1358-R013
3-038-60 or
7 Moisture SO2 sensor module 3-038-62 or
3-038-63
8 Coupling piece 1/8“ internal thread 1-05-1358-R014
9 Coupling 1/8“ internal thread 1-05-1358-R013
3-038-10 or
10 SF6 volume percentage sensor module
3-038-11
11 Pressure sensor 15 psi 1-05-1270-R003
12 Precise valve (rinsing valve) 1-05-1370-R001
13 Coupling plug 1-05-1358-R002

4. Description of the menu and measuring process
Operating lamp
Purge
ON/OFF button
Navigation
turning knob
Gas
inlet
Measuring
gas hose
Illustration 4.1: Front view of the SF6-multimeter with its operating elements
Manual switching on and off of the SF6-multimeter is carried out via the „ON/OFF“ button on front side
(see ill. 4.1). The device is switched on if the yellow “Operating“ LED lights up.
The green “AC Power“ LED indicates that the SF6-multimeter is connected to the power supply. For this
purpose the mains switch on the power supply unit on the back of the SF6-multimeter has to be switched
on and the SF6-multimeter must be connected to the power supply via the power cable. The accumulator
is only charged if the device is turned on.
When turning on the device there is a noise. However this noise is normal as it results from the
integrated diaphragm pump that starts running for a short time when switching on the device.
Mains operation
If the device is switched on and in mains operation the yellow “Operating“ LED, the blue display and the
green “AC Power“ LED light up. In the upper line, right on the display a socket symbol (ill. 4.6) as well as
the loading status in percent are indicated. In case the device is mains operated all sensors remain
switched on permanently (measuring values are indicated permanently) and the device never turns off
automatically.

Battery operation
In battery operation only the yellow “Operating“ LED and the blue display light up. On the display right on
the top only the battery symbol and the loading status in percent (ill. 4.7) are indicated.
If the device is in battery operation and not in the measuring mode all sensors are switched off after 30
seconds in order to save accumulator time. This can be recoginzed from the fact that only placeholders
„---.-„ instead of measuring values are indicated on the display instead of the measuring values which
are normally indicated permanently in Run mode as in mains operation.
In case neither the navigation turning knob nor a button is activated for more than 2 minutes (default) the
device switches to the shutdown mode and turns off. During the 20 seconds shutdown phase there is a
warning signal. If the navigation turning knob is activated during this time the device switches to battery
operation again if not the device turns off automatically. In the “Settings“ menu the Switch-off time (for
battery operation) is selectable in the range of 1…15 minutes. (Default 2 minutes).
Manual switching off of the SF6-Multimeter is effected by activating the

“ON/OFF“ button for about 3 seconds until a beep tone can be heard.
In battery operation the device switches off automatically (after running of

the switch-off time if the navigation turning knob is no longer activated).
4.1 Navigation with the navigation turning knob
The navigation turning knob allows quick navigation in the menus and input of text. With the navigation
turning knob different menu items can be selected (as from the base menu) by turning the knob.
The selected menu items are invertedly illustrated at the bottom of the display cell. The selected menu
item is activated by pressing the navigation turning knob shortly. If it is another submenu it is opened,
otherwise the selected command is carried out.
In case the beeper is switched on an acoustic sound is released when another

menu is selected during each turning step on the navigation turning knob. The
acoustic sound is also released if there is a positive feedback after selection or
important messages.
With the button (ESC-key) an instruction is interrupted or it is put one menu level higher if you are in a
submenu at the moment.

4.2 Overview
After switching on the device a start screen appears (ill. 4.2), which is replaced by the component test
after a short initialisation time (ill. 4.3). The component test verifies which components are installed in the
SF6-multimeter and whether they are ready for operation. The test of each component is confirmed (by a
checkmark). If a component is missing or fails during the self-test a question mark”?” is indicated.
The next screen shows the number of days which are within the recommended calibration interval (ill.
4.4). If the recommended calibration interval is exceeded the number of negative days (ill. 4.5) is
indicated. This menu is to be confirmed by pressing the navigation turning knob. In case the calibration
interval is exceeded measurements can still be carried out with the device.
If one of the sensors is not present or failed the self-test a permanent placeholder (“- -.-“) is indicated in
the base menu instead of the measuring value. Such a placeholder is indicated temporarily even if the
SF6-multimeter in battery operation switches to the energy saving mode (ill. 4.8).
The base menu

After switching on the device the base menu remains visible (ill. 4.6). From the base menu all functions
and other submenus can be selected. There is a status bar on the lower side of the screen on the
display, which informs you on the user commands that can be started or on actual running commands.
The values measured presently are indicated as from line 3 (SF6-volume percentage, moisture and SO2).
In the sixth line the input pressure measured presently on the “Gas inlet“ is indicated.
The seventh line can be turned off (blank line) via the “Settings“ menu or the gas density or the gas
temperature can be indicated (ill. 4.7). The gas density is determined with the gas temperature
measured, the input pressure and the SF6-volume percentage.
The units are indicated behind the measuring values and the following further explanations in the last
column:
 SF6-volume percentage; referring to the CF4 carrying gas the „ CF4 “ symbol is indicated
for differentiation (only for option CF4 as carrying gas).
 Gas humidity in °C or °F referring to atmosphere (atm) or under pressure in the compartment
(i IN).
 SO2-value as SO2-concentration in ppmV.
 Input pressure in bar pe or pa
 Selectively blank line or gas temperature in °C or °F or gas density in kg/m3 or lb/ft3

If no measurement is started no gas flows through the sensors. Thus the

sensors only show measuring values which correspond to the present gas
state in the sensors.
ill. 4.2 ill. 4.3
ill. 4.4 ill. 4.5
ill. 4.6 ill. 4.7

ill. 4.8 ill. 4.9
ill. 4.10 ill. 4.11
Ill. 4.12 ill. 4.13
ill. 4.14 ill. 4.15

4.3 Menu description
The menu navigation on the display is self-explanatory. Therefore not every detail is described in the
following explanation.
The following menu items can be selected:
4.3.1 “Start measurement“

This item starts on the basis of the settings adjusted. The measurement is started by pressing the
navigation turning knob. Measurements can be carried out in the “Individual measurement” or
“Permanent measurement” mode.
In the individual measurement mode the solenoid valves open and the preset time for the
individual measurement is running (ill. 4.16). The time meter can be observed in the first line on
the top of the left hand side. The time meter counts backwards. During the measurement the
measuring values are updated permanently. If the time meter reaches zero the solenoid valves
close automatically and the measurement is completed. If necessary, the SO2-sensor is rinsed
with air. The measuring values are recorded and there is a query whether the measuring values
should be saved or not (ill. 4.17).
ill. 4.16 ill. 4.17
In case of “Storing? yes“ selection the measuring values can be stored by indicating the user
name and a name for the measuring point.
The permanent measurement mode is provided for the application in an industrial process or if
measuring values are to be monitored permanently for a longer time. The time meter on the top of
the left hand side starts at zero and counts upwards. The measuring data in the permanent
measurement mode is also permanently updated on the display. The switching contacts for the
measuring value volume percentage and for the measuring value dew point temperature switch
according to the settings. The permanent measurement mode can be left again with the -button
(ESC-key). The recent measuring values are also indicated.

4.3.2 “Data transmission“
The selection of the window “Data transmission – Wait for PC start“ (ill. 4.14) is necessary so
that the measuring values stored in the flash memory can be transmitted to a PC or Laptop by
means of the programme on the enclosed CD. The menu item can be left again with the -button
(ESC-key). See chapter 5.
The “Data transmission – Wait for PC start“ menu item must be selected
before a transmission of the measuring data on PC or Laptop is possible.
4.3.3 “Measuring data“

After calling the “Measuring data” menu item all measuring values stored in the flash memory
can be indicated on the display with indication of the user name, name of measuring point with
date, time and consecutive number (via navigation with the navigation turning knob, see chapter
4.1).
Delete measuring data in the flash memory:

If the measuring data menu item is left again with the -button (ESC-key) a window with the
query Delete all data? appears automatically. This query call is to be replied to with Yes or No
with the -button (ESC-key), which corresponds to “No“.
Only all measuring data can be deleted on the flash memory. It is not
possible to delete individual measuring data.
4.3.4 ”Settings“
All settings which refer to the measurement and the indication of the units are done in the
“Settings“ menu,
choose between:
 Temperature unit: as desired: °C
°F
 Gas density unit: as desired: kg/m3
lb/ft3
 Moisture unit: as desired: °C under atmosphere
g/m3 under atmosphere
ppmV
ppmM

 Pressure unit: as desired: bar
psi
Pa
MPa
 Pressure mode: as desired: pe overpressure
pa absolute pressure
 Carrying gas: as desired: N2
CF4 (only for option)
 Limit value (volume): 0.0 to 99.9 Vol.-%
 Limit value (dew point): -50.0 to +10.0 °C dew point
 Measuring mode: 300 to 900 s (5 to 15 min)
(individual measurement)
 Measuring mode: permanent measurement, individual measurement
 Switch-off time: 1 min to 15 min
(in battery operation)
 Additional indication: as desired switched off
Temperature
gas density
 Contrast (display): 0 to 100 %
 Language: as desired German
English
French
Spanish
Italian
 Beeper: as desired: on
off
 Time: Hour: Minute: Second
 Date: Year: Month: Day:
 System info: The settings window -> system info offers information on the software
versions, the serial numbers and calibration date (ill. 4.15).

4.4 Storage of measuring data
After running down of the individual measurement or after interruption of the permanent
measurement an indication similar to illustration 4.11 appears on the display.
The selection Yes or No and the confirmation is made by turning the navigation turning knob.
In case No is selected the measuring values are rejected and the base menu appears again.
In case Yes is selected the user can input a user name with up to 10 digits in the next window (ill.
4.12) and after OK up to 17 digits (ill. 4.13). After another OK the measuring data and the current
number of the measurement are stored on the flash memory in the device. Then the device
returns to the base menu (ill. 4.6).
Most processes can be interrupted again with the -button ESC-

key) if they have not yet been carried out completely.
4.5 Carrying out a measurement
1. Switch on the SF6-multimeter with the “ON/OFF“ push button.
2. Set or check the Settings -> Measuring mode menu to “Individual measurement” or “Permanent
measurement” via the “Start measurement” base menu (see navigation with the navigation turning
knob chapter 4.1). The measuring mode set last is always kept.
3. Start the Settings -> temperature unit, gas density unit, moisture unit, pressure unit, pressure
mode and carrying gas mode if necessary via the base menu and select the corresponding units
and measuring modes. The units set last and measuring modes are kept as well so that settings
according to item 2 and item 3 could only be necessary occasionally.
4. Close the “Purge“ valve to the stop by turning clockwise.
Before connecting the measuring gas hose to the device ensure that
the “Purge“ valve is closed by turning clockwise. Otherwise
sensitive parts of the measuring systems could be damaged by
Warning coupling the hose to the “Gas compartment“.

5. Connect the measuring gas hose to the coupling (DN8 or DN20) by means of the self-closing
miniature coupling and connect it to the “gas inlet”. Connect the coupling (DN8 or DN20) to the
compartment.
Note: In case moisture (e. g. by condensation) is visible on the couplings it must be wiped with a dry
and lint-free cloth beforehand. Then dry the couplings with a commercial hairdryer for several
minutes, however the temperature of the couplings must not exceed 70°C. If moisture penetrated in
the measuring gas hose disconnect it from the device and rinse it with dry gas for about 5 minutes (e.
g. nitrogen). The connecting coupling on the compartment to be tested must also be dry and clean.
Oil or condensated moisture must not penetrate the SF6-multimeter.
Make sure that the pressure in the gas compartment to be measured does
Warning not exceed pe 10 bar before the SF6-Multimeter is connected.
6. Rinse the measuring gas hose by opening the “Purge“ valve for 2-3 seconds.
Only purge for 2 – 3 seconds. Ensure that the “Gas outlet“ (reverse of
device) is not closed and overpressure is not generated by a connected
measuring gas recovery system.
Attention: The overpressure in the measuring gas system is not monitored
Warning while purging.
7. The measurement is started via the base menu by the “Start measurement“ command line by
pressing the navigation turning knob. The set measuring time is counted downwards by the time
meter left on the top of the display. If the zero value is reached the measuring values on the display
are recorded and the individual measurement is completed.
The solenoid valves in the SF6-multimeter open automatically during the

measurement. If there is back pressure e. g. because the “Gas outlet” is
closed on the outlet or the SF6-gas cannot be transported the input
solenoid valve is closed and the measurement is interrupted by a message.
The back pressure cannot continue to increase. Prior to carrying out a
second measurement the back pressure must be relieved.
8. After the termination of automatic measuring process in the individual measurement mode the query
Storing? Yes No appears.

4.6 Execution of a permanent measurement
1. Switch on the SF6-multimeter with the “ON/OFF“ push-button.
2. Call the Settings -> Measuring mode menu via the “Start measurement“ base menu and set to
permanent measurement. Make further settings according to chapter 4.4 point 2. The measuring
mode set last is always kept.
3. Further procedure as described in chapter 4.4 points 4. and 6.
4. Note: During the permanent measurement the time meter on the top on the left hand side of the
display counts upwards.
5. The permanent measurement mode can only be left again by the -button (ESC-key). The
measuring values measured last also appear in a separate window. (ill. 4.6).
6. After termination of the measuring process in the permanent measurement mode the query
Storage? Yes No appears.

5. Transmission of the measuring data on a PC or Laptop
The stored measuring data of the SF6-multimeter can be transmitted for filing on a PC or Laptop.
Prior to the first data transmission the Setup-programme for loading the USB-driver must be executed
once.
5.1 Installation of the USB-driver
Conditions: Operating system: Windows 2000 or XP

MS - Excel 2000 or 2003
1. Call the programme PreInstaller.exe from the CD of the \CP210x\Win2K_XP directory and indicate a
suitable destination directory e. g. under C:\Programme\...
2. Switch on the SF6-Multimeter.
3. Connect the enclosed USB-cable to the SF6-Multimeter and PC or Laptop.
4. Call the number of the COM interface. This number is needed later.
For this execute the following commands under Windows XP:
Start -> Settings -> System control -> Administration -> Computer administration -> Device -
Manager -> connections (COM and LPT). The driver must indicate the “CP210x USB to UART
Bridge Controller (COM …)“ message. If there is no message from the driver it is not installed
correctly or there is no USB-connection to the SF6-multimeter.

5.2 Readout the measuring data from the SF6-multimeter
Condition:
Installation of the driver must have been executed according to chapter 5.1. For the reading out a data
record the measuring data of at least one measurement must be available in the SF6-multimeter.
Procedure:
1. Connect the PC and SF6-multimeter (front side USB interface) to the USB-cable.
2. Select the Data transmission menu item with the navigation turning knob on the SF6-multimeter and
then press the navigation turning knob. The message ill. 4.14. appears.
Data transmission
Wait for PC start
3. Start the “SF6_measuring record_Rev_xx.xls“ programme.

Allow the macro option if necessary. The programme can be found on the CD of the …\Excel-Macro\
directory.
4. Set the COM-Port to the number, which has been determined according to chapter 5.1, item 4. Store
this data file and use it as ”SF6-measurement report_Rev_xx.xls“ template.
When using such a template the COM-Port on the computer being used need never been adjusted
again.
5. Call the “Template SF6-measuring record_Rev_xx.xls“ file according to point 3.

6. Press the Transmission complete! button. The data of the SF6-Multimeter is transmitted into the
worksheet.
7. Answer the query Storing now? with Yes or No. If it is answered with Yes a window opens in which
a name for the measuring report can be selected individually. In case of No the measuring data
remain in the file. But they can be stored with the storage Excel-command or storage under …
Note: Only delete the measuring data in the worksheet with the Delete button.

6. Limit value contacts – Pin allocation Out Vol.-% Moisture
The Pin allocation for the use of the limit value contacts results from illustration 6.1. The limit value
contacts are only activated by Permanent measurement.
Ill. 6.1 Pin allocation of the limit value contacts for SF6-volume percent and dew point °C

7. Back view of the SF6-multimeter
4 screws for Out Vol.-% Gas outlet

opening the module Moisture
Measuring module SF6- Measuring module Mains switch

volume percentage sensor Power
moisture-SO2- supply
sensor connection
Module with power unit
and
accumulator

7.1 Returning of the measuring gas modules
When returning the modules to the manufacturer use appropriate packing to avoid any damage in transit.
The calibration and final control in accordance with the DILO quality assurance is
indicated with month and year on the test badge.
In case the device is operated longer than the time interval for calibration recommended a warning
message appears when switching on the device (ill. 4.5). The device can still be operated.
The calibration service for the device is listed below.
Calibration of 3-038-10 measuring module, SF6-volume percentage sensor 3-038-20

Calibration of 3-038-11 measuring module, SF6-volume percentage sensor 3-038-21
Calibration of 3-038-60 measuring gas module, moisture SO2-sensor (0-100 ppmv) 3-036-22
8. Fault correction
It is not recommended to carry out repair works of the SF6-Multimeter by yourself. (except for
disassembling the single modules).
Do not carry out any works on the modules. In case of malfunction return them to the
manufacturer of the device.
If there is no indication after switching on the device check whether the yellow “Operating” LED
lights up. If not, the SF6-multimeter should be connected to the power supply in order to load the
accumulator. For this purpose it must be switched on. Furthermore, check whether the correct
power supply is available and the mains plug is fixed tightly.
If this is correct and the yellow “Operating“ LED does not light up check the mains fuse which is near the
mains switch on the back of the device and can be opened by pulling out. In case the mains fuse is all
right the SF6-multimeter can be reset in the base status. For this purpose establish a connection
between the two pins with a screwdriver according to illustration ill. 8.1.

Prior to the removal of the mains fuse unplug the power plug.
If the mains fuse is replaced only use the same type.
Warning See chapter 2.1 “Technical data”.
Ill. 8.1 Reset of the SF6-multimeter in the base status

9. B151R20 Discharge gas collection unit (available as an option)
Legal directives becoming more and more strict and the voluntary self-commitment of the
SF6-users also require the collection of used gas even of smallest amounts of SF6, as being discharged
during measurements. For this purpose, the discharge gas collection unit has been developed.
The SF6-multimeter is equipped with a connection on the back of the device so that it can be connected
to an external discharge gas collection unit.
This connection allows the SF6-Multimeter to be operated with or without the discharge gas collection
unit.
In normal condition the output is open that means the measuring gas can escape into the atmosphere
without any problems.
If the discharge gas collection unit is connected the measuring gas is collected in a depressurized
condition via the connecting hose.
After having reached the internal consumption capacity of the discharge gas collection unit the installed
compressor switches on automatically and the collected measuring gas flows into an internal gas
cylinder, which can take a higher pressure and the gas can be filled in another vessel later.
ill. 9.1 B151R20 Discharge gas collection unit
The B151R20 Discharge gas collection unit is not included in the scope of supply of the SF6-Multimeter.

10. Appendix
Moisture Content Conversion Chart for SF6 at atmospheric pressure
°F °C PPMm PPMv °F °C PPMm PPMv

30 -1 780 6326 -31 -35 27 219
28 -2 700 5677 -33 -36 24 195
27 -3 625 5069 -35 -37 22 178
25 -4 575 4663 -36 -38 19 154
23 -5 500 4055 -38 -39 17 138
21 -6 450 3650 -40 -40 15 122
19 -7 410 3325 -42 -41 13 105
18 -8 390 3163 -44 -42 12 97
16 -9 350 2839 -45 -43 11 89
14 -10 320 2595 -47 -44 9 73
12 -11 290 2352 -49 -45 8.5 69
10 -12 260 2109 -51 -46 7.5 61
9 -13 240 1946 -53 -47 6.8 55
7 -14 220 1784 -54 -48 6 49
5 -15 200 1622 -56 -49 5.5 45
3 -16 185 1500 -58 -50 5 41
1 -17 175 1419 -60 -51 4.2 34
0 -18 150 1217 -62 -52 4 32
-2 -19 145 1176 -63 -53 3.5 28
-4 -20 135 1095 -65 -54 3 24
-6 -21 120 973 -67 -55 2.5 20
-8 -22 110 892 -69 -56 2.3 19
-9 -23 100 811 -71 -57 2 16
-11 -24 90 730 -72 -58 1.7 14
-13 -25 80 649 -74 -59 1.5 12
-15 -26 70 568 -76 -60 1.3 11
-17 -27 64 519
-18 -28 57 462
-20 -29 50 406
-22 -30 44 357
-24 -31 40 324
-26 -32 36 292
-27 -33 32 260
-29 -34 29 235

Best Practice – Correct Dew Point Measurement
Dew point measurement is quite complex. In order to get correct or stable dew point values during
measurement the following basic rules need to be adhered to:
Measurement carried out on SF6 bottle:

1. The SF6 bottle filled with liquid gas must always be placed horizontally prior to measurement,
thus causing gas mixture inside the bottle.
2. The pressure reducer must be made of stainless steel (see Z340R10 adapter kit for measuring
devices) => NO rubber diaphragm!!!
3. No rubber hoses may be used between bottle / gas compartment and measuring device!
4. If possible, only the 6m long measuring gas hose (included in the scope of supply) should be
used. Using longer hoses may cause longer measuring time and dew point falsification.
Conditions having negative effects on dew point values:

1. Use of rubber hoses in measuring line
2. Extreme differences in ambient temperature
3. Alternating measurements with humid and dry gas on the same gas compartment
4. Multiple measurements with automatic pumping back on the same gas compartment
5. Measurements on gas compartments with down piping
6. Rinsing time too short when starting measurements with unknown gas inside hose
Remedial action when dew point values differ:

1. Check the above-mentioned points
2. Set hose length to 12m (=> longer rinsing time)
3. Manual rinsing when gas quality is unknown
4. First measurement without automatic pumping back. Second measurement with automatic
pumping back results in correct dew point.
In general, the operating temperature of measuring device needs to be observed:

3-031: + 5°C to 35°C
3-037 / 3-038 Multimeter: 0°C to +40°C
3-038 Multi Analyser: -10°C to +40°C

Dilo

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SF6-Multimeter

Operating Manual (original version)

4. Description of the menu and the measuring process 16 / 17

5. Transmission of the measuring data on a PC or laptop 27

6. Limit value contacts – Pin allocation Out Vol.-% Moisture 29

7. Back view of the SF6-Multimeter 30

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9. Discharge gas collection unit (B151R20, optional) 33

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1.1 Specific safety notes and standard symbols

These residual risks contain dangers for

This symbol refers to electric shock

 If the warning sign „Warning“, appears, there is no danger for persons.

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1.3 Correct use of the SF6-Multimeter

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The operator has to ensure that

 complete and legible operating manuals are available on site.

 only qualified personnel operates or repairs the SF6-Multimeter.

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Opening of the upper coupling:

Ill. 1.1 Opening of the upper coupling

Opening of the lower coupling:

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The main components of the SF6-Multimeter are as follows:

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ill. 2.1 SF6-Multimeter with standard accessories

Dimensions: (with handle on the front side)

Length (L): 450 mm

Dimensions: transport case

Length (L): 540 mm

ill. 2.2 transport case

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Volume percentage sensor:

Measuring range: 0.0 to 100.0 vol.-% SF6

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Modules: Order no.

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The SF6-Multimeter includes:

 4 m long connecting hose with DILO couplings DN8 and DN20

 Power plug with 2 m long connecting cable

 USB connecting cable

 connecting plug for Out vol.-% moisture

1 operating manual (multilingual)

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3.1 Function of the SF6 volume percentage sensor

3.2 Function of the moisture sensor

3.3 Function of the SO2 sensor

Equation 1: measuring process

Equation 2: compensation reaction

SO2 + ½ O2 + H2O = H2SO4

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Pos. Designation Order no.

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Manual switching off of the SF6-Multimeter is effected by activating the

In battery operation the device switches off automatically (after running of

4.1 Navigation with the navigation turning knob

In case the beeper is switched on an acoustic sound is released when another

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The base menu

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If no measurement is started no gas flows through the sensors. Thus the

ill. 4.2 ill. 4.3

ill. 4.4 ill. 4.5

ill. 4.6 ill. 4.7

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ill. 4.8 ill. 4.9

ill. 4.10 ill. 4.11

Ill. 4.12 ill. 4.13

ill. 4.14 ill. 4.15

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The following menu items can be selected:

4.3.1 “Start measurement“

ill. 4.16 ill. 4.17