Is 16353 Product Manual
Is 16353 Product Manual
Is 16353 Product Manual
2. Sampling Guidelines:
-
a) Raw material :
b) Grouping guidelines : -
For Physical test – 8 kg
c) Sample Size :
For Chemical test – 2 kg
Scheme of Inspection
4. : Please refer ANNEX – B
and Testing
ANNEX A
Sl
Tests used in with Clause Reference Test equipment
No.
1 Fineness Clause 6.1 Blaine’s apparatus variable flow type
Stop watch with start-stop mechanism
Mercury for calibration
Balance, Standard weights
Standard Cement
Manometer liquid (di-butyl phthalate or light
mineral oil.)
Mercury of reagent grade or better, Pyknometer
Circular discs of filter paper of medium porosity
(mean pore diameter 7 µ).
Le-Chatelier’s flask
Constant temperature water bath to maintain
temp. within ± 0.1 ° C
2 Soundness by Autoclave Auto clave machine with thermostatic control to
Clause 6.1 Table 2 maintain pressure of 2.1 MPa for 3 hrs, pressure
to be attained within 1-1 ¼ hrs;
L-Shape thermometer LC 1 °C
Pressure gauge 0-42 kg/cm2 LC = 0.4 kg/cm2
Humidity chamber with temperature & RH
control 27 ± 2 °C, RH 90 to 100 %
Standard bar 308 mm, max
Bar moulds 25x25x282 mm
Length comparator with dial gauge
Mineral oil for covering moulds
3 Soundness by Le-chatelier Method Le-Chatelier’s water bath preferably with
Clause 6.1 Table 2 thermostatic control raising temperature from
27 ± 2 0 C to boiling in 27 ± 3 minutes
Le-Chatelier’s moulds with weights and cover
glasses minimum 8 nos.
Humidity chamber with temperature & RH
control 27 ± 2 0 C, RH 90 to 100 %
Steel scale 12" (304.8 mm)
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e) Lab ball mill (motorized) To grind the clinker, slag & gypsum sample in lab
ball mill for testing
f) To weigh the material 1. Platform type balance
2. Electrical balance
3 Weight box with weights (1 mg - 500 g)
9 General test equipments for chemical testing
Clause 5 , Table 1 of IS 16353 : 2015
Muffle Furnace with thermostatic control,
Range 0 – 1200° C
Oven with thermostatic control 0-300° C
Heater and hot plate
Distillation Assembly
Crucible: Platinum or Porcelain / silica
Filter paper (No- 1, 40, 41, 42)
Desiccators with cover & Desiccant
Water bath
pH meter/paper
Glassware - volumetric flask -0-250 ml, beaker 0-
250 ml, measuring cylinder 0-50,100,500, 1000
ml, burette 0-25/50 ml, conical flasks-
0-250 ml, pipette 0-5,10, 25, 50 ml
All chemicals required for complete chemical
analysis of cement
Tongs including platinum tipped tong
Wire gauge with asbestos sheet at the middle
Washing bottle
Mortar mixer- 4.75 l
Glass thermometer
All required chemicals as per IS 4032 for Portland
clinker testing.
The above list is indicative only and may not be treated as exhaustive.
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ANNEX B
1.1 The manufacturer shall prepare a calibration plan for the test equipments. The following
equipments shall be calibrated at a frequency shown against each and records kept.
2. TEST RECORDS – The manufacturer shall maintain test records in various formats,
Form 1 to Form 5 for the tests carried out to establish conformity.
4. CONTROL UNIT –
4.1 For manufacturing units of Portland Cement Clinker: The tests, as indicated in
Table 1 attached and at the levels of control specified therein, shall be carried out on the
whole production of the factory which is covered by this scheme and appropriate records
maintained in accordance with clause 2 above.
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4.2.1 Routine analysis of various raw materials used in the manufacture of Portland
Cement clinker shall be made at intervals of a month or whenever there is a change in the
source/mine area stratification whichever is earlier and appropriate records of the
analysis and of the Physical composition of the mixtures shall be maintained in Form 2.
4.3. DELIVERY – Supplies of Portland cement clinker shall be done in compliance with
clause 10.1 of IS 16353 : 2015.
5. LEVELS OF CONTROL - The tests as indicated in column 1 of Table 1 and the levels of
control in column 3 of Table 1, shall be carried out on the whole production of the factory
which is covered by this plan and appropriate records maintained in accordance with clause 2
above.
5.1. PRODUCTION DATA - The licensee shall send to BIS a statement of quantity
produced, marked and exported by him and the value thereof at the end of each quarter of the
operative period as per the enclosed proforma and shall also submit these details to BIS at
the end of the operative year duly authenticated by a Chartered Accountant.
5.1 All the production which conforms to the Indian Standard and covered by the licence
should be marked with Standard Mark.
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Note -1: Daily composite sample shall be made out of hourly samples for the required period (Pl see IS 3535 Methods of sampling hydraulic cements). Weekly composite sample
shall be made out of daily composite sample. If clinker is dispatched directly from clinkerization unit without storing, weekly composite sample may not be required.
If Clinker is manufactured using same proportion of raw materials from more than one kiln, sample from each kiln shall be tested for requirements as per the above table.
If clinker is manufactured using different proportion of raw materials from more than one kiln, sample from each kiln shall be tested for all requirements as per the above table.
Note-2: The control unit and levels of control as decided by the Bureau are obligatory to which the licensee shall comply with.
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Form No. 1
RAW MATERIAL TESTING
Date of receipt of Date of Name of Material Source of supply and consignment Details of analysis for specified requirements
material testing No.
Form 2
PRODUCTION DATA
(DETAILS OF PRODUCTION ACCEPTED AND REJECTED FOR STANDARD MARK)
Shift Quantity Passed for Standard mark Rejected Remark
Form No. 3
CLINKER CHEMICAL COMPOSITION (DAILY COMPOSITE SAMPLE) – CLINKERIZATION AND LOADING
Date of Total loss on Insoluble Alkali C3S C3 A C3S+ SO3 MgO Chloride Free LSF Alumina Sample Remarks
manufacture ignition residue content C2 S lime factor Pass/Fail
as Na2O
Form No. 4
CLINKER GROUND WITH GYPSUM (DAILY COMPOSITE SAMPLE) – CLINKERIZATION AND LOADING
Date of grinding Fineness SO3 Soundness Setting time Compressive strength Particle Sample Remark
Le-Chatelier Autoclave Initial Final 3 days 7 days 28 days size of Pass/Fail
clinker
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Form No 5
CALIBRATION
Sl. No Date of Result of Calibration (Test records indicating details of standard values and observed values Name of equipment Sl.No.
calibration for each equipment to be kept in proforma for which various columns be devised; as required) Action taken if equipment (If any) &
found defective Remarks
Note: The above records are to be kept separately for each equipment.
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