Is 11169-2 (1989) - Steels Forcold Heading - Cold Extrusion, Part 2 - Stainless Steel

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IS 11169-2 (1989): Steels forcold heading/cold extrusion,


Part 2: Stainless steel [MTD 16: Alloy Steels and Forgings]

“!ान $ एक न' भारत का +नम-ण”


Satyanarayan Gangaram Pitroda
“Invent a New India Using Knowledge”

“!ान एक ऐसा खजाना > जो कभी च0राया नहB जा सकता ह”


है”

Bhartṛhari—Nītiśatakam
“Knowledge is such a treasure which cannot be stolen”
IS-11169( Part 2 ) : 1999
(Reaffirmed 2004)

Indian Standard
STEELS FOR COLD HEADING/COLD
EXTRUSION APPLICATIONS-
SPECIFICATION
PART 2 STAINLESS STEELS

UDC 669’14’018’8

Q BIS 1990
BUREAU OF INDIAN STANDARDS
MANAK BHAVAN, 9 BAHADUR SHAH ZAFAR MARG
NEW DELHI 110002
..-C
\
January 1.&O Price Groap 2
.
Alloy Steels and Special Steels Sectional Committee, SMDC 19

FOREWORD.

This Indian Standard ( Part 2 ) was adopted by the Bureau of Indian Standards on 25 May 1989, after
the draft finalized by the Alloy Steels and Special Steels Sectional Committee had been approved by
the Structural and Metals Division Council.
IS 11169 ( Part I ) Steels for cold heading/cold extrusion applications : Part 1 Wrought carbon and
low alloy steels was issued in 1984. This standard covers:
a) Carbon steels,
b) Alloy steels,
c) Carbon steels with boron, and
d) Alloy steels with boron.
In view of the special requirements of stainless steels for cold heading/cold extrusion application, it
was recommended by the committee to treat this topic as a separate part of the standard,
This standard is exclusively covering the application of stainless steels for cold heading processes.
This standard ( Part 2 1 has been prepared keeping in view that the particulars to be specified while
ordering the steel are as per ( Part 1 ) of this standard.
In & preparation of this standard ( Part 2 ), manufacturing and trade practices followed in the
country in this field have been kept in view. Also due weightage has been given to the! need for
international coordination in standardization. The following Indian and international standards have
been referred:
IS 1570 ( Part 5 ) : 1985 Schedules for wrought steels : Part 5 Stainless and heat-resisting
steels (first revision )
IS 6527 : 1972 Stainless steel wire rod
IS0 4954 : 1979 Steels for cold heading and cold extruding
DIN 1654 ( Part 5 ) : 1980 Steels for cold heading and cold extruding, technical conditions of
delivery for stainless steels. Deutsches Institut fiir Normung
( DIN).
For the purpose of deciding whether a particular requirement of this standard is complied with, the
final value, observed or calculated, expressing the result of a test or analysis, shall be rounded off in
accordance with IS 2 : 1960 ‘Rules for rounding off numerical values ( revised )‘. The number of
significant places retained in the rounded offvalue should be the same as that of the specified value m
this standard.
Is 11169 ( Part 2 ) : 1989

Indian Standard
STEELS FOR COLD HEADING/COLD
EXTRUSION APPLICATIONS-
SPECIFICATION
PART 2 STAINLESS STEELS

1 SCOPE Table 1 Summary of Quality Requirement


Classes
1.1 This standard ( Part 2 ) covers the require-
ments for wrought stainless steels intended for SI QaalityTyRpceplllrement Rcqat,;;+ent
cold heading and are delivered as wires, wire rods No.
or bars. It applies to ferritic, martensitic and 6 6
austenitic stainless steels. 1 2 3
i) Chemical composition:
2 REFERENCES
a) Ladle analysis X x X

2.1 The Indian Standards listed below are necessary b) Check analysis x - -
adjuncts to this standard: ii) Mechanical properties:
IS No. Title a) Supply condition* X X X
b) At room temperature? - x X
IS 228 ( in parts ) Methods of chemical analysis
of steels ( second revision ) c) At temperature from - - -
50 to 300°ct
IS 2049 : 1978 Colour code for the identi- *As per delivery conditions covered under 10.
fication of wrought steels for tin the heat treatment conditions specified in
general engineering purposes Tables 5 and 6.
(Jirst revision )
IS 3711 : 1966 Method for selection and pre-
paration of samples and test 5 MANUFACTURE
pieces for mechanical tests for
wrought steels 5.1 Unless otherwise agreed to in the order, the
IS 8910 : 1978 General technical delivery processes used in making the steel are left to the
discretion of the manufacturer. When so desired,
requirements for steel and steel
products the purchaser shall be informed of the steel
making process.
3 SUPPLY OF MATERIAL
6 CHEMICAL COMPOSITION
3.1 General requirements relating to the supply of
material shall conform to IS 8910 : 1978. Steel
covered by the standard shall be ordered and 6.1 The ladle analysis of different grades of steel
delivered on any one of the following basis: when carried out either in accordance with relevant
parts of 1s 228 or any other established instru-
a) Chemical composition, or mental/chemical method should conform to the
values given in Table 2. In case of dispute, the
b) Chemical composition and mechanical procedure given in various parts of IS 228 ( in
properties. parts ) shall be the referee method.
4 REQUIREMENT CLASSES
6.1.1 For cases where the methods of chemical
4.1 When steel is ordered in accordance with this analysis are not covered in any part of IS 228,
standard, one of the three classes ( see Table 1 ) mutually agreed methods may be adopted by the
shall be agreed at the time of enquiry. manufacturer and the customer.

1
IS 11169 ( Pnrt 2 ) : 1989

Table 2 Chemical Compositiolt ( Applicable to LadIe AnaIysis )

CClauses 6.1, 6.2 and 12.1 )

Sl Steel Grade Elements, Percent


IUQ. c
Carbon Silicon Manga- N;;y C%h&one Molybde- Su:Spwr Phos- Others’
(C) (SC) nese num phorus,
(P)
Max
(1)’ (2) (3) (4) (8) (% ,
(11)
i) Ferritic steei 0.12 1-o - O-030 -
x 07Cr17 -Max: *
ii) Martensitic steel 068-0’15 1-o 0 - O-030 -
x 12Cr12
iii) Austenitic steel 0’030 1-O 2-O 8Q-12’0 17.5-20.0 - 0’030 -
x02Cr19NilO Max
x04Cr19NilO O-OS 1’0 2’0 10’5-12’0 17-o-20.0 - O-030
Max
xWCr17Ni12Mo2 0’08 E-0 2-o 10-O.14-O 160-18.0 2-0-3.0 0’030 -
MUX
xO4Crl8NilOTi 0.08 2-o 9’0-12Q 17-O-19+ - 0.030
Max

xO4Cr17Ni12Mo2Ti O-08 f-0 2-O 10’0-14-0 16’0-18.0 20-3-O o-030


Max
x 02Cr17Nil2MoZ 0’030 14 2-O 10%14’0 16%18.0 2’0-3’0 O-030 -
Ma-X

6.2 The permissible variation in the case of 8 MECHANICAL PROPLRTIES


product analysis from the limits specified in
Table 2 shall be according to Table 3. 8.1 For all steels, which are ordered, shall be of
the treatment conditions indicated in 10, the
Table 3 Permissibb Deviation in Check AnaIysis maximum values for tensile and yield strength
( Clauses 6.2 and 12.1 ) (TS) and the minimum value for reduction of
area (RA) as specified in Table 4 shall apply.
Constituent Permissible Content in Permissible
Cast Analysis, Percent Deviation 8.2 For all steels which are ordered in accordance
(Percent) with the requirements of Class 2, the mechanical
properties specified in Table 5 shall apply for
Over
Including reference test pieces which are heat treated io
accordance with the recommendations of Table 6.
Carbon
9 CORROSION RESISTANCE
Silicon
Manganese
9.1 The performance of stainless steeIs under
Chromium 11.5 20 f 020
various conditions of chemical attack cannot be
Molybdenum 2-O 3.0 f 0.10 characterized by test values as general norms. If
Nickel 8.0 14’0 & 0.15 desired, a corrosion test shall be agreed to at the
Sulphur - 0.03 f 0’005
time of enquiry and order.
Phosphorus - OU5 f @005
Titanium 0’40 0.80 f 0’05 10 TREATME&T CONDITION OF
DELIVERY
7 FREEDOM FROM DEFECTS
10.0 The steels shall be usually delivered in one of
7.1 The material shall be free from harmful inter- the foltowing treatment conditions unless speci-
nal and surface defects. fically agreed to. at the time of enquiry/order.

2
IS 11169 ( Part 2 > : 1989

Table 4 Treatment

( CIause 8.1 )

Steel Grade Treatment for Fe&tic and Martensitic Grades

ACorAC+P:C+-AC:C+AC+LC
Treatment for Austenitic Grades
--- -- L ” -
Q or Q+P C+Q E+Q-tLC
r L \
m Reduction Teosile Reduction 5ze--- Re$rrc;an
Strength in Area in Area
MPa Percent “‘%?” Percent str%:th Percent
Max Min Max Mitt Max Min
x07017 570 63 570 60 620 65
x 12cr12 600 60 600 62 640 62
x02Cr19NilO 630 55 630 55 680 55
xO4Cr19NilO 680 5.5 680 55 730 55
x04Cr17NilZMo2 680 55 680 55 730 55
xOlCrlSNilOTi2 680 5.5 680 55 730 55
xO4Cr17Ni12Mo2Ti 680 5s 680 55 730 55
x02017Nil2Mo2 680 5s 680 55 730 55

Table 5 Mechanical Properties of Steels as per Heat Treatment Condition in Table 6


( Clause 8.2 ) 0

k.
Steel Grade Heat Yield Point or Tensile Elongation Impact U
Treatment 0.2% Proof St;;gth Percent N;tc$$ mm
Condition Stress, MPa
Min tiP;l G.L(.%& /s;; *
Ferritic xOlCr17 Annealed 270 450-600 20 -
Martensitic x 12012 Quenched & 450 600-750 18 50
Tempered
Austenitic xOXrI9NilO Quenched 175 450- 700 50 60
x04Cr19NilO 185 500-700 50 60
x04Cr17Ni12MoZ 205 500-700 45 60
xO4CrlSNilOTi 205 500-750 40 60
x04Cr17Nil2Mo2Ti 225 500-750 40 60
x02Cr17Ni12Mo2 225 500-750 40 60

Table 6 Heat Treatment Condition


( Clause 8.2 )

Steel Grade Annealing Quenching Tempering


c-_&-7 r-- ~-h------, Temp “C
Temp “C Cooling Temp “C Cooling
Medium Medium
Ferritic x07Crl7 750-850 Air/water - - -
Martensitic x 12CrI2 700.780 Furnace 950-l 000 Oil or Air 750-850
or Air
Austcnitic x02Cr19NilO - 1 000-I 050
x 04Cr19NilO - - 1 000-l 050
x 04Cr17Ni12Mo2 - - 1050-I ioo
x04Crl8NilOTi - 1 020-l 070
x04Cr17Ni12Mo2Ti - - 1050-I 100
x02Cr17Ni12Mo2 - - 1050-I 100

I 3
i

1s 11169 ( Part 2 ) : 1989

10.1 Ferrltic and Martensitlc St&s 12 RETESTS

AnneaIed ( spheroidization of AC 12.1 Retest for Product Analysis


carbides ) If the results of product analysis do not meet the
Annealed ( spheroidized ) and AC+P composition requirements given in Tables 2 and 3,
peeled unless otherwise agreed to between the purchaser
and the manufacturer, two new samples shall be
Cold drawn and annealed C+AC taken on different pieces from the same cast.
( spheroidized ) Should the two analysis satisfy the requirements.
Cold drawn, annealed ( spheroi- C+AC+LC the lot represented shall be accepted. Should
dized ) and lightly cold reduced either of the tests fail, the material shall be taken
( for example, with reduction of as not complying with this standard.
5 percent )
12.2 Retest for Mechanical Tests in the Heat
10.2 Austenltic Steels Treated Condition

Quenched If the samples selected fail to meet the require-


Q
ments stipulated, two further samples shall be
Quenched and peeled Q+P selected from the same heat treatment batch or
lot. The consignment shall be considered to
Cold drawn and quenched C+Q conform to the requirements if both the additional
Cold dr;,a quenched and C+Q+LC tests are satisfactory. If either of the samples fails,
lightly reduced ( for the manufacturer shall have the right, if he so
example, with reduction of desires in case of heat-treated material, to reheat-
5 percent ) treat the product in any suitable manner before
two fresh samples are taken for testing. If the two
11 SAMPUNG tests satisfy the requirements of this standard, the
lot represented shall be accepted and if either of
11.1 Sampling for Chemical Analysis the samples fails, the material shall be taken as not
complying with this standard.
The ladle analysis shall be supplied by the producer.
If a product analysis is required by the purchaser, 13 PACKING OF MATERIALS AND MARKING
at least one sample product shall be taken from
13.1 Steel bars shall be suitably bundled. A
each cast.
metal tag giving the following information shall
be attached to each bundle:
11.2 Sampling for Mechanical Properties
a) Name or trade-mark of the manufacturer,
If required by the purchaser, one sample product
shall be taken from each size grouping of each b) Steel grade, and
heat-treated batch for testing. If the product is c) The cast number or any other identification
continuously heat-treated, the sampling for mark by which the steel can be traced to
mechanical tests shall be as agreed to between the the cast and heat treatment batch from
purchaser and the manufacturer. which it was made.
General conditions for selection and preparation 13.2 The colour scheme specified in IS 2049 : 1978
of samples and test pieces shall be in accordance or as required
_ by th: purchaser may be adopted
with IS 3711 : 1966. to mark the grade of the material.
-
Standard Mark
The use of the Standard Mark LSgoverned by the provisions of the Bureau of Indian
Standards Act, 1980 and the Rules and Regulations made thereunder. The Standard Mark on
products covered by an Indian Standard conveys the assurance that they have been produced
to comply with the requirements of that standard under a well defined system of inspection,
testing and quality control which IS devised and supervised by BIS and operated by the
producer. Standard marked products are also contmuously checked by BIS for conformity
to that srandard as a further safeguard. Details of conditions under which a hcence for the
use of the Standard Mark may be granted to manufacturers or producers may be obtained
from the Bureau of Indian Standards.
BIS is a statutory institution established under the BurMu o/ Indian Smmfiw~ Act, 1986 to promote
harmonious development of the activities & standardization, marking and quality certification of goods
and attending to connected matters in the country.

. ’ Copyright

BIS has the copyright of all its publications. No part of these publications may be reproduced in
any form without the prior permission in writing of BIS. This does not preclude the free use, in the
course of implementing the standard, of necessary details, such as symbols and sizes, type or grade
designations. Enquiries relating to copyright be addressed to the Director ( Publications j. BIS.

Revision of Indian Standards

Indian Standards are reviewed periodically and revised, when necessary and amendments, u any, arc
issued from time to time. Users of Indian Standards should ascertain that they are in possession of
the latest amendments or edition. Comments on this Indian Standard may be sent to BIS giving the
following reference:
Dot : No. MTD 16 ( 3338 )

Amendments Issued Since Publlcrtlom

Amend No. Date of Issue Text Affected

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