Construction and Building Materials: Enrique Del Rey Castillo, Nasser Almesfer, Opinder Saggi, Jason M. Ingham
Construction and Building Materials: Enrique Del Rey Castillo, Nasser Almesfer, Opinder Saggi, Jason M. Ingham
Construction and Building Materials: Enrique Del Rey Castillo, Nasser Almesfer, Opinder Saggi, Jason M. Ingham
h i g h l i g h t s
New artificial aggregate made of 100% plastic waste (80% polyolefins and 20% other).
Development of 20 MPa compressive strength concrete mixes using plastic aggregate.
Upcycling of plastic waste to contribute to a circular economy and reduce landfill.
Plastic waste minimization for Improved sustainability through non-structural concrete.
Lightweight concrete for precast elements like sound barriers, facade and ancillary.
a r t i c l e i n f o a b s t r a c t
Article history: The inclusion of an artificial aggregate manufactured using plastic waste to develop a light-weight con-
Received 21 November 2019 crete was studied. Five separate mixes were designed, progressively increasing the amount of artificial
Received in revised form 29 June 2020 aggregate and measuring the fresh and hardened concrete properties, and it was found that the slump
Accepted 8 July 2020
and density of the concrete decreased as the amount of artificial aggregate in the concrete increased.
Both the compressive and the tensile Then the mix that was most suitable to the requirements of the
study in terms of density and compressive strength was chosen for further investigation in stage two.
Keywords:
Fifteen percent of the natural aggregate by weight was replaced in this optimal mix, which equals more
Concrete
Plastic waste
than thirty-seven percent of the volume given the lower density of the manufactured aggregate com-
Manufactured aggregate pared to natural aggregate. A larger number of specimens and more detailed testing was undertaken
Light-weight concrete for stage two when compared to stage one, including establishing the compressive stress–strain relation-
Sustainability ship and the modulus of elasticity of the newly developed concrete mix. The results indicated that plastic
aggregates manufactured following shredding, palletisation and extrusion processes can be used to
obtain a lightweight concrete (1800 kg/m3) while having relatively good compressive strength properties
(20 MPa at 28 days). These results were higher than other results previously reported in the literature on
the replacement of coarse aggregate with plastic, but were marginally lower than results reported in the
literature for studies where fine aggregate was replaced with plastic. It was concluded that the concrete
mix reported herein can be used for a wide spectrum of applications such as non-structural facades and
sound barriers for highways. Further research is required to investigate the durability of concrete with
the artificial aggregate included in the mix, especially if the product is to be subjected to wear and tear
such as in driveways or warehouse slabs.
Ó 2020 Elsevier Ltd. All rights reserved.
https://doi.org/10.1016/j.conbuildmat.2020.120199
0950-0618/Ó 2020 Elsevier Ltd. All rights reserved.
2 E. del Rey Castillo et al. / Construction and Building Materials 265 (2020) 120199
concrete is assumed [4]. Reducing the amount of virgin aggregates plastic is hydrophobic and cannot chemically bind with the cement
being mined is critical if natural ecosystems are to be preserved for paste, and therefore the bond strength between the plastic surface
future generations. and the cement paste is low [14]. This behaviour results in key
Plastics are ubiquitous in society in almost every field and the properties decreasing as the amount of plastic incorporated within
production of plastic products, especially single-use plastic prod- the concrete mix is increased [14].
ucts, has strikingly increased during the 20th century and in the The majority of the reported research existing in the literature
first two decades of the 21st century. In 2017, 64.4 million tons has focused on introducing plastic waste into the concrete mix
of plastic were produced in Europe and 348 million tonnes were by first sorting, cleaning and shredding the plastic waste but with-
produced worldwide, with 60% of that amount being used by only out further altering this plastic waste via processes such as heating
two market sectors, being the packaging industry and the building or chemical treatments. Only one product comparable to that used
and construction industry [5]. Plastic waste can be processed fol- in the current study has been found in the literature, that was
lowing three methods, which are recycling, incineration (often developed using 30% cleaned, sorted and shredded liner low-
combined with an energy recovery process), and landfilling, in density polyethylene (LLDP) as a binding matrix combined with
order of preference [6]. In the same year of 2017, 27.3% of the plas- 70% virgin sand [35–37], whereas the product used in the current
tic waste collected in Europe was disposed of in landfills [5] and in study is made of 100% plastic waste without the addition of any
the USA the situation is far worse, where in 2015 there was 35.4 virgin material. The aggregate product used in this study was made
million tons of plastic produced of which 75.4% finished its useful of 100% plastic waste, with the manufacturing process involving
life in landfills [7], and with the reporting of such data subse- shredding, extrusion and pelletization of the plastic waste. The
quently discontinued with the change of US Government adminis- mechanical and physical properties of the plastic waste were
tration in 2016. On a global scale, only 9.5% of all the plastic ever altered through this manufacturing process to produce the resul-
produced up to 2015 has been recycled and 79% of this plastic is tant aggregate, with the appearance and mechanical properties of
in landfills, although the amount of plastic waste currently going the manufactured aggregate being distinctly different from those
into landfills has reduced to 58%[8]. of typical smooth plastic. All seven grades of plastic as defined
Most types of plastics are non-biodegradable and are chemi- by ASTMD7611 [38] were used during the manufacturing of the
cally unreactive to the environment, so these plastics can remain artificial aggregate, but always using 80% of polyolefins and 20%
in the environment for decades or even centuries. Some types of of the other types, with the mechanical and physical properties
plastic can also release toxic elements into the environment, such of the manufactured aggregate found to be consistent regardless
that dumping plastic waste into landfills is not a viable solution. of the proportions of plastics grades used. The final product has a
While incineration of plastic waste completely eliminates the specific gravity of 0.85 kg/m3 and negligible water absorption.
waste and can be a source of power, this process typically releases The concrete mixes developed with the material used in this study
carbon dioxide and other poisonous chemicals and produces toxic resulted in a compressive strength of 19.7 MPa using an aggregate
fly ash and bottom ash. Recycling is therefore the best solution to made with 100% plastic waste, while the results reported by Alqah-
treat plastic waste, with one of the most commonly used methods tani et al. indicate a maximum compressive strength of 12 MPa
being the reuse of plastic waste into the construction and building using an aggregate made with 30% plastic waste. Therefore, the
industry. Research on the use of plastic waste in cement mortar material used in this study was novel when compared to other
and in concrete is extensive [9–11], with various reviews of the materials reported in the literature.
topic having been compiled recently [12–15]. The inclusion of
other waste materials in concrete for sustainability purposes has
also been intensively investigated, such as fly ash [16,17], geopoly- 2. Research motivation and objective
mer aggregates made with fly ash [18], waste glass [19], or biochar
[20], but the focus of the research reported herein was on plastic The objective of the study reported herein was to obtain a con-
waste. crete mix with a density of 1800 kg/m3, a 28 days compressive
The most common method to introduce plastic waste into con- strength of 20–25 MPa, and a 1-day compressive strength of
crete mixes requires the plastic to be categorised by the different 10 MPa. The reason for targeting a relatively high compressive
types, and to be cleaned before being shredded into particles of dif- strength at an early age was to accelerate the production of precast
ferent shapes and sizes [13,21,22]. The commonly reported result concrete panels and other precast concrete elements, which was
of incorporating plastic into concrete as an aggregate replacement the main market being targeted. The installation of non-
is the reduction of workability, density and mechanical perfor- structural concrete elements such as shade panels, façade panels
mance of the resulting concrete mix, without significantly improv- and highway sound barriers is streamlined when using light
ing the durability of the material [23–25]. An improvement in weight concrete, improving the construction efficiency and reduc-
abrasion resistance was reported in the past when using PET plas- ing the demands on foundation and anchoring elements. The tar-
tic as an aggregate replacement due to the more rough texture of geted concrete mix was not to be used for structural or
the plastic particles compared to the texture of natural aggregates infrastructure applications.
[13,26]. The increment in water absorption of concrete with plastic
waste as an aggregate replacement was widely reported as a result
of the elevated air content that is entrained during mixing, with 3. Materials and methods
the increment in entrained air caused by inadequate blending of
the natural and artificial aggregates due to differences in density, 3.1. Cement
where the plastic waste aggregate typically floated in the cement
paste while the natural aggregates sank [27–30]. Finally, the use Concrete test specimens were made using the same materials
of plastic aggregate increased drying shrinkage due to the lower used in a local ready-mix plant, with a maximum nominal grey-
restraint provided by the plastic aggregate when compared to that wacke aggregate size of 19 mm. Portland cement Type GP as
of the natural aggregate, and increased the resistance to chloride defined by NZS 3122 [39] was used. The physical properties of
ion penetration [31–34]. The main source of the problems associ- the cement are reported in Table 1. Silica fume, with a silica con-
ated with incorporating plastic waste into concrete is the chemical tent of 93% and surface area of 23 m2/g was also added as a supple-
incompatibility between plastic and cement paste, given that mentary cementitious material.
E. del Rey Castillo et al. / Construction and Building Materials 265 (2020) 120199 3
Specific surface area (m2/kg) 339 Standardised off-the-shelf air entraining agent, superplasticizer
Initial setting time (min) 115 and water reducer chemical admixtures were used in the mixes.
Final setting time (hr:min) 2:38
Soundness (mm) 1.3
SO3 (%) 2.5
4. Trial mixes
Specific gravity (g/cm3) 3.15
A total of five mixes were designed and batched according to
the New Zealand Standard on Concrete Production [40], and vari-
ous fresh and hardened properties were investigated following
the New Zealand Standard for testing of concrete [43,44]. The
3.2. Natural aggregate
ingredients used in each mix are reported in this section, together
with the results from the investigated properties of the trial mixes.
Two types of natural coarse aggregates were used, being grey-
wacke Kaipara Brookby (KB) 13 (defined as having 86% of the
aggregates passing between 13.2 mm and 19 mm and in accor- 4.1. Recipes
dance with the New Zealand standard of concrete production
[40], and greywacke KB 07 (also known as Premium All Passing 7 The ingredients used in each trial mix are reported in Table 2,
or PAP7). One fine natural aggregate was used, commonly referred together with the quantity of each ingredient. The water cement
to as McCallum’s Offshore natural sand (MC 01). The sieve analysis ratio and the amount of coarse natural aggregate were kept con-
carried out in compliance with the New Zealand standard for test- stant at 0.405 and 320 kg. The mass amount of PAP7 and sand
ing of water and aggregates [41] for both PAP7 and MC 01 is was progressively reduced while increasing the mass amount of
reported in Fig. 1. Both aggregates comply with the grading artificial aggregate (both coarse and fine aggregate in the ratios
requirements specified in the New Zealand standard [42]. The described in Table 2) until the maximum replacement level of nat-
specific gravity of the KB aggregates is 2680 kg/m3 and the specific ural aggregate by artificial aggregate was 15% by mass (for mix 5).
gravity of the MC 01 sand is 2650 kg/m3, as obtained using the cor- Given that the density of the artificial aggregate was smaller than
responding standards [41]. 0.25 times the density of the artificial aggregate, the volume of
artificial aggregate was 37.1% of the total volume of aggregate for
mix 5. Both the superplasticizer and the water reducer were main-
tained constant at 2 l and 0.9 l respectively.
3.3. Artificial aggregate
Table 2
Mix recipes.
Mix number
Material Density (kg/m3) 1 2 3 4 5
Cement (kg) 3150 400
Water (kg) 1000 162
w/c – 0.405
Fume silica (kg) 2100 20
KB13 mm (kg) 2680 320
PAP7 (kg) 2680 410 410 360 360 320
MC01 Sand (kg) 2650 495 495 445 445 405
Coarse artificial aggregate (kg) 800 30 75 60 100 120
Fine artificial aggregate (kg) 800 30 25 60 60 65
Artificial aggregate (% of total aggregate by weight) – 4.7 7.5 9.6 12.5 15.0
Artificial aggregate (% of total aggregate by volume) – 11.6 18.6 23.7 30.9 37.1
Water reducer (l) 1000 2
Super-plasticiser (l) 1000 0.9
E. del Rey Castillo et al. / Construction and Building Materials 265 (2020) 120199 5
Slump Artificial aggregate content (% of total aggregate by weight) Entrained air (%)
180
15%
160
12.5%
140
100 7.5%
80
60 6.5%
5.8%
40
3.5%
20
0
1 2 3 4 5
Mix number
Fig. 4. Relationship between artificial aggregate content, slump and entrained air.
6 E. del Rey Castillo et al. / Construction and Building Materials 265 (2020) 120199
Table 4
Hardened concrete properties for the trial mixes.
Mix Agg. (%) Density (kg/m3) Compressive strength (MPa) Flexural strength (MPa)
1 day 7 days 28 days 1 day 7 days 28 days
1 4.7 1927 12.0 23.3 27.2 2.4 4.6 4.9
2 7.5 2116 13.2 26.3 36.5 2.5 4.6 5.6
3 9.6 1885 11.6 21.4 22.8 2.4 4.1 4.2
4 12.5 1925 10.6 19.5 22.6 2.0 4.0 4.4
5 15.0 1812 10.0 19.0 22.2 2.2 4.1 4.5
35
Compressi ve strength (MPa)
30
25 1927 Kg/m³
1925 Kg/m³
20
1885 Kg/m³
15.0%
15
12.5%
9.6% 1812 Kg/m³
10
7.5%
4.9%
5
0
1 2 3 4 5
Mix number
Fig. 5. Compressive strength for the five trial mixes.
Fig. 6. Comparison between the current study (crosses) with previous studies on replacement of coarse aggregate (circles) and fine aggregates (triangles).
E. del Rey Castillo et al. / Construction and Building Materials 265 (2020) 120199 7
15.0%
Flexural strength (MPa) 5
12.5%
4
9.6% 1925 Kg/m³
3 1927 Kg/m³
7.5%
1885 Kg/m³
2
1812 Kg/m³
4.9%
1
0
1 2 3 4 5
Mix number
Fig. 7. Flexural strength for the five trial mixes.
40.0 Table 5
Mix 1 d=1927 Kg/m³ Mix 2 d=2116 Kg/m³
Compressive Stregth (MPa)
10.0
5.0
0.0
0 5 10 15 20 25 30
Time (days)
6.0
Flexural Strength (MPa)
5.0
4.0
3.0
Mix 5 d=1925 Kg/m³ Mix 6 d=1812 Kg/m³ Fig. 10. Pictures of the failure observed during testing.
0.0
0 5 10 15 20 25 30
Time (days)
5.2. Statistics
Fig. 9. Evolution of the flexural strength of the trial mixes.
The results of the compressive and tensile strength of the forty
cylinders tested at an age of 28 days are reported in Table 6. The
ture plane from opening beyond a certain width, and the cylinder purpose of testing twenty specimens for each test at an age of
remained cohesive until considerable damage was observed. Even 28 days was to obtain the specified strength value, in addition to
when the typical hourglass shape took form, after large deforma- the average strength value and any other statistical value that
tion was applied into the cylinder, small pieces of concrete were could be useful, as reported in Fig. 11. The specified strength value
still attached to the main body of the cylinder by pieces of aggre- is typically defined as the lower bound characteristic value or 95
gate, as can be seen in Fig. 10a. percentile value, which means that 95% of the strength values (or
8 E. del Rey Castillo et al. / Construction and Building Materials 265 (2020) 120199
Table 6
Details of compression and split tension tests.
Compressive strength (MPa) 19.4 20.9 21.2 21.8 19.8 18.1 16.4 17.1 18.2 18.7
19.8 19.9 21.7 20.4 19.9 18.6 18.4 22.3 19.7 21.8
Split tensile strength (MPa) 2.2 2.1 2.1 2.5 2.3 2.3 2.3 1.9 2.3 2.2
2.3 2.1 2.5 2.2 2.4 2.1 2.5 2.5 2.2 2.1
nineteen out of twenty) should be above that specified value. Hun- displacement better than can natural aggregate, as also observed
dreds or even thousands of data points would be obtained in a typ- before[14].
ical scenario when developing a new concrete mix by a ready mix
plant for commercial use, but that was not a feasible option for this
study and therefore twenty specimens were tested instead. A nor- 6. Conclusions
mal distribution can be assumed, given that normal distribution is
often assumed in testing of concrete strength. The specified value Five mixes were developed and an optimal mix was chosen
would then be calculated as the average value minus 1.645 times based on the mechanical properties and the density, which fulfilled
the standard deviation, which results in a specified compressive the requirements of the target specification (density of 1800 kg/m3,
strength of 17.1 MPa. This result was consistent with the results a 28 days compressive strength of 20–25 MPa, and a 1-day com-
from Table 6 and Fig. 11, as only one value was below 17.1 MPa. pressive strength of 10 MPa). In this optimal mix, 15% of the natu-
ral aggregate was replaced by weight, which equals 37.1% of the
volume given the lower density of the manufactured aggregate
5.3. Stress strain relationships compared to natural aggregate. The mixes were not recommended
for high performance concrete, structural concrete, or for infras-
The stress–strain relationship in compression is reported in tructure projects. A larger concentration of plastic waste in the
Fig. 12. The strain at peak stress was similar to what can be form of coarse aggregate was used in the current study when com-
expected with typical concrete, but the concrete exhibited a less pared to past studies that obtained similar mechanical properties.
brittle failure than for typical concrete with a longer post-peak tail, This improvement is due to the innovative method of extruding
in accordance with observation of the fracture patterns reported and pelletizing the plastic waste, as opposed to the methods
earlier. This observation was in line with previous observations reported in the literature that entail sorting, cleaning and shred-
regarding the contribution of plastic aggregate to the flexural ding the plastic waste or to use plastic as a binder with sand to cre-
strength and potentially to the tensile strength of concrete[14]. ate aggregates. As an example, if mix 5 was used in just 1% of the
The modulus of elasticity E of the artificial aggregate was calcu- concrete produced in New Zealand almost 19 million of tons of vir-
lated according to the pertinent ASTM standard[46]. The value gin aggregate would not be mined, and 9 million tons of plastic
obtained was 20.5 GPa, which is similar to that of normal concrete. would be recycled in an average year. Further research on this
However, the concrete with artificial aggregate experienced more new aggregate needs to be conducted, especially related to durabil-
post-peak deformation capacity than the typical concrete with nat- ity. The main conclusions observed from the study are summarised
ural aggregate, which means that the pieces of artificial aggregate below. While similar observations have been reported in the liter-
that cross the failure plane of the concrete can accommodate the ature, it is noted that the level of plastic replacement achieved in
Fig. 12. Full stress strain response for concrete compressive cylinders of the final mix design tested at 28 days.
the current study was significantly higher than the typical replace- References
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