Fluidization PDF

Download as pdf or txt
Download as pdf or txt
You are on page 1of 26

Fluidization

• When a fluid is passed upwards through a bed of particles


the pressure loss in the fluid due to frictional resistance
increases with increasing fluid flow

• A point is reached when the upward drag force exerted by


the fluid on the particles is equal to the apparent weight of
particles in the bed

• At this point the particles are lifted by the fluid, the


separation of the particles increases and the bed becomes
fluidized

28-09-2020 Dr. Sarita Kalla 1


• The force balance across the fluidized bed dictates that
the fluid pressure loss across the bed of particles is
equal to the apparent weight of the particles per unit
area of the bed

28-09-2020 Dr. Sarita Kalla 2


28-09-2020 Dr. Sarita Kalla 3
A plot of fluid pressure loss across the bed versus
superficial fluid velocity through the bed

https://www.youtube.com/watch?v=lFhrpSJZzck
28-09-2020 Dr. Sarita Kalla 4
• OA is the packed bed region

• Solid particles do not move relative to one another and their


separation is constant

• Pressure loss vs fluid velocity relationship is described by the


Carman-Kozeny equation and the Ergun equation

• BC is the fluidized bed region

• At point A, pressure loss rises above the value predicted

• This rise is more marked in small vessels and in powders which


have been compacted to some extent before the test

• Associated with the extra force required to overcome wall


friction and adhesive forces between bed and distributor

28-09-2020 Dr. Sarita Kalla 5


• Superficial fluid velocity at which the packed bed
becomes a fluidized bed is known as the minimum
fluidization velocity, Umf.

• Sometimes referred to as the velocity at incipient


fluidization

• Umf increases with particle size and particle density and


is affected by fluid properties

• To derive expression for Umf, equate expression for


pressure loss in a fluidized bed with pressure loss across
a packed bed
28-09-2020 Dr. Sarita Kalla 6
Applying the Ergun equation-

Multiplying with viscosity, particle mean diameter, and fluid density-n

28-09-2020 Dr. Sarita Kalla 7


or

Where Ar is the dimensionless number known as the


Archimedes number

And Remf is the Reynolds number at incipient fluidization

In order to obtain a value of Umf, we need to know the


voidage of the bed at incipient fluidization,  = mf
28-09-2020 Dr. Sarita Kalla 8
• A typical value of mf is 0.4

• Wen and Yu (1966) produced an empirical correlation for Umf

• This correlation is valid for spheres in the range 0.01 < Remf < 1000
and is often expressed in the form:

• For gas fluidization, the Wen and Yu correlation is often taken as


most suitable for particles larger than 100 mm.
• The correlation of Baeyens and Geldart (1974) is best for particles
less than 100 mm

28-09-2020 Dr. Sarita Kalla 9


Relevant Powder and Particle Properties

• The correct density for use in fluidization equations is the


particle density
• Defined as the mass of a particle divided by its hydrodynamic
volume
• Volume ‘seen’ by the fluid in its fluid dynamic interaction with
the particle
• It Includes the volume of all open and closed pores

28-09-2020 Dr. Sarita Kalla 10


• Bed density is also used in connection with fluidized beds

• For non-porous solids, this is easily measured by a gas


pycnometer or specific gravity bottle, but these devices should
not be used for porous solids since they give the true or
absolute density abs of the material of which the particle is
made and this is not appropriate where interaction with fluid
flow is concerned.

28-09-2020 Dr. Sarita Kalla 11


• For porous particles, the particle density p (also called
apparent or envelope density) is not easy to measure directly.
Bed density is another term used in connection with fluidized
beds; bed density is defined as-

28-09-2020 Dr. Sarita Kalla 12


28-09-2020 Dr. Sarita Kalla 13
Hydrodynamic volume of a particle

28-09-2020 Dr. Sarita Kalla 14


• Another density often used is the bulk density, defined in a
similar way to fluid bed density-

• The most appropriate particle size to use in equations relating


to fluid-particle interactions is a hydrodynamic diameter i.e. an
equivalent sphere diameter derived from a measurement
technique involving hydrodynamic interaction between the
particle and fluid.

28-09-2020 Dr. Sarita Kalla 15


Where xi is the arithmetic mean of adjacent sieves between
which a mass fraction mi is collected.

28-09-2020 Dr. Sarita Kalla 16


Bubbling and Non-bubbling Fluidization

• Beyond the minimum fluidization velocity bubbles or particle-


free voids may appear in the fluidized bed

• At superficial velocities above the minimum fluidization velocity,


fluidization may in general be either bubbling or non-bubbling

• Some combinations of fluid and particles give rise to only


bubbling fluidization and some combinations give only non-
bubbling fluidization

28-09-2020 Dr. Sarita Kalla 17


Bubbles in gas fluidized bad

28-09-2020 Dr. Sarita Kalla 18


• Most liquid fluidized systems, except those involving very dense
particles, do not give rise to bubbling.
• The Figure shows the bed of glass spheres fluidized by water
exhibiting non-bubbling fluidized bed behavior.

Expansion of a liquid fluidized bed: (a) just above Umf (b) liquid
velocity several times Umf
28-09-2020 Dr. Sarita Kalla 19
• Gas fluidized systems give either only bubbling fluidization or
non-bubbling fluidization beginning at Umf, followed by bubbling
fluidization as fluidizing velocity increases

• Non-bubbling fluidization is also known as particulate or


homogeneous fluidization

• Bubbling fluidization is often referred to as aggregative or


heterogeneous fluidization

28-09-2020 Dr. Sarita Kalla 20


Applications of Fluidized Beds

Physical processes

• Physical processes include drying, mixing, granulation, coating,


heating and cooling.
• These processes take advantage of the excellent mixing
capabilities of the fluidized bed.
• Good solids mixing gives rise to good heat transfer,
temperature uniformity and ease of process control
• One of the most important applications is to the drying of
solids.
• Fluidized beds are currently used commercially for drying such
materials as crushed minerals, sand, polymers, pharmaceuticals,
fertilizers and crystalline products.

28-09-2020 Dr. Sarita Kalla 21


• Fluidized beds are often
used to cool particulate
solids following a
reaction

• Cooling may be by
fluidizing air alone or by
use of cooling water
passing through tubes
immersed in the bed

Schematic diagram of a
fluidized bed solid cooler

Schematic diagram of a fluidized bed solid cooler


28-09-2020 Dr. Sarita Kalla 22
Chemical Processes
• Gas fluidized bed is also a good medium to carry out a chemical
reaction involving a gas and a solid.

Advantages of the fluidized bed for chemical reaction include:


• Gas-solid contacting is generally good
• Excellent solids circulation within the bed promotes good heat
transfer between bed particles and fluidizing gas and between
the bed and heat transfer surfaces immersed in the bed
• Gives rise to near isothermal conditions even when reactions
are strongly exothermic or endothermic
• Good heat transfer gives rise to ease of control of the
reaction
• Fluidity of the bed makes for ease of removal of solids from
reactor

28-09-2020 Dr. Sarita Kalla 23


Fluid catalytic cracking
(FCC) unit, a celebrated
example of fluidized bed
technology for breaking
down large molecules in
crude oil to small
molecules suitable for
gasoline, etc.

28-09-2020 Dr. Sarita Kalla 24


Types of gas–solid chemical reactions employing fluidization

28-09-2020 Dr. Sarita Kalla 25


References

Martin Rhodes, "Introduction to Particle Technology", 2nd Edition,


John Wiley & Sons, 2008.

Mechanical Operations. Authors: A.K. Swain, H. Patra and G.K. Roy.


Publisher: Tata McGraw Hill Education Pvt. Ltd., New Delhi

28-09-2020 Dr. Sarita Kalla 26

You might also like