Ecss Q ST 70 01a

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ECSS-Q-70-01A

11 December 2002

EUROPEAN COOPERATION

ECSS
FOR SPACE STANDARDIZATION

Space product
assurance

Cleanliness and contamination control

ECSS Secretariat
ESA-ESTEC
Requirements & Standards Division
Noordwijk, The Netherlands
ECSS--Q--70--01A
11 December 2002 ECSS

Published by: ESA Publications Division


ESTEC, P.O. Box 299,
2200 AG Noordwijk,
The Netherlands
ISSN: 1028-396X
Price: € 20
Printed in The Netherlands
Copyright 2002 E by the European Space Agency for the members of ECSS

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Foreword

This Standard is one of the series of ECSS Standards intended to be applied


together for the management, engineering and product assurance in space
projects and applications. ECSS is a cooperative effort of the European Space
Agency, national space agencies and European industry associations for the
purpose of developing and maintaining common standards.
Requirements in this Standard are defined in terms of what shall be accomplished,
rather than in terms of how to organize and perform the necessary work. This
allows existing organizational structures and methods to be applied where they
are effective, and for the structures and methods to evolve as necessary without
rewriting the standards.
The formulation of this Standard takes into account the existing ISO 9000 family
of documents.
This Standard has been prepared by the ECSS--Q--70--01 Working Group,
reviewed by the ECSS Technical Panel and approved by the ECSS Steering Board.

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Contents

Foreword . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3

Introduction . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 9

1 Scope . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 11

2 Normative references . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 13

3 Terms, definitions and abbreviated terms. . . . . . . . . . . . . . . . . . . . . . . 15

3.1 Terms and definitions . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 15


3.2 Abbreviated terms . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 19

4 General cleanliness and contamination control aspects. . . . . . . . . 21

4.1 General . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 21
4.2 Contamination attributes . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 21
4.3 Cleanliness levels . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 31
4.4 Cleanliness monitoring . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 36
4.5 Cleaning . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 39
4.6 Modelling . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 41

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5 Cleanliness and contamination control programme. . . . . . . . . . . . . 43

6 Contamination control during the product life cycle . . . . . . . . . . . . 45

6.1 General design provisions . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 45


6.2 Manufacturing, integration and test . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 45
6.3 Budgets, prediction and modelling . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 48
6.4 Cleanliness verification . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 49
6.5 Packing, containerization, transportation and storage . . . . . . . . . . . . . . . . . . . 51
6.6 Launch . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 52
6.7 Mission (external) . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 53
6.8 Mission (internal) . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 55

Annex A (normative) Document requirements list . . . . . . . . . . . . . . . . . . 57

Annex B (informative) Space system cleanliness control flow chart . . . 59

Annex C (informative) Molecular contaminant content of some wipe

materials . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 61

Annex D (informative) Compatibility of various solvents with listed


materials . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 63

Annex E (informative) Non-volatile residue of commercially available

solvents, measured by infrared techniques . . . . 65

Annex F (informative) Cleanroom requirements . . . . . . . . . . . . . . . . . . . . . 67

F.1 Particle levels and cleanroom classification . . . . . . . . . . . . . . . . . . . . . . . . . . . 67


F.2 Interpretation for particles in environments . . . . . . . . . . . . . . . . . . . . . . . . . . . . 69
F.3 Monitoring of cleanroom air . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 69
F.4 Indicative correlation between particles in air and particle fallout . . . . . . . . 70
F.5 Molecular levels . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 70
F.6 Measurement of molecules in environments . . . . . . . . . . . . . . . . . . . . . . . . . . 71
F.7 Design . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 71
F.8 Environmental control . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 72

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F.9 Maintenance and cleaning . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 73


F.10 Access control . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 74
F.11 General requirements for a cleanroom . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 74

Annex G (normative) Cleanliness requirement specification —

Document requirements definition (DRD) . . . . . . 77

G.1 Introduction . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 77
G.2 Scope and applicability . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 77
G.3 Terms, definitions and abbreviated terms . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 77
G.4 Description and purpose . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 78
G.5 Application and interrelationship . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 78
G.6 CRS preliminar y elements . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 78
G.7 CRS contents . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 79

Annex H (normative) Cleanliness and contamination control plan —


Document requirements definition (DRD) . . . . . . 81

H.1 Introduction . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 81
H.2 Scope and applicability . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 81
H.3 Terms, definitions and abbreviated terms . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 81
H.4 Description and purpose . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 82
H.5 Application and interrelationship . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 82
H.6 C&CCP Preliminar y elements . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 82
H.7 C&CCP contents . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 83

Bibliography . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 87

Figures

Figure 1: Product cleanliness levels according to MIL-STD-1246C . . . . . . . . . . . . . . . . . . . . 32


Figure B-1: Space systems cleanliness control flow chart . . . . . . . . . . . . . . . . . . . . . . . . . . . . 60
Figure F-1: Ideal particle-size distribution . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 68

Tables

Table 1: Product cleanliness levels .............................................. 32


Table 2: Correlation between ideal class of MIL-STD-1246 and obscuration factor . . . . . . 34
Table 3: NVR cleanliness levels, according to MIL-STD-1246C ....................... 36
Table 4: Material outgassing criteria values . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 53
Table C-1: . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 61

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Table D-1: ................................................................... 64
Table E-1: . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 65
Table F-1: Airborne particulate cleanliness classes (taken from FED-STD-209E) . . . . . . . . . . 69
Table F-2: Correlation airborne and PFO for cleanrooms . . . . . . . . . . . . . . . . . . . . . . . . . . . . 70
Table F-3: Guide to humidity level selection . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 73

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Introduction

The objective of this Standard is to ensure a successful mission by the definition


of acceptable contamination levels for space system elements, their achievement,
and maintenance, throughout
D performance assessment versus contamination,
D facilities and tools definition for contamination control and monitoring,
D materials and processes selection, and
D planning of activities.

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Scope

This Standard defines the requirements and guidelines for the measurement and
control of particulate and molecular contamination to be met by personnel, items,
facilities and operations of space projects.
It covers mission definition, design, development, production, testing and oper-
ations of space products.
Moreover, it identifies the possible failures and malfunctions due to contamina-
tion, and provides guidelines for maintaining the required levels of cleanliness
during ground activities, launch and mission.
This Standard does not address magnetic, electrical or electrostatic cleanliness.
This Standard applies to all types and combinations of projects, organizations and
products, and during all the project phases.
It also applies to those ground systems that have a hardware interface to space
systems, such as MGSE integration stands.

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Normative references

The following normative documents contain provisions which, through reference


in this text, constitute provisions of this ECSS Standard. For dated references,
subsequent amendments to, or revisions of any of these publications do not apply.
However, parties to agreements based on this ECSS Standard are encouraged to
investigate the possibility of applying the most recent editions of the normative
documents indicated below. For undated references the latest edition of the publi-
cation referred to applies.
ECSS--P--001 Glossary of terms
ECSS--Q--00 Space product assurance — Policy and principles
ECSS--Q--20 Space product assurance — Quality assurance
ECSS--Q--20--07 Space product assurance — Quality assurance for test
centres
ECSS--Q--40 Space product assurance — Safety
ECSS--Q--60 Space product assurance — Electrical, electronic and elec-
tromechanical (EEE) components
ECSS--Q--70 Space product assurance — Materials, mechanical parts
and processes
ECSS--Q--70--02 Space product assurance — Thermal vacuum outgassing
test for the screening of space materials
ECSS--Q--70--05 1) Space product assurance — Detection of organic conta-
mination of surfaces by IR spectroscopy
ECSS--Q--70--50 1) Space product assurance — Particulate contamination
control in cleanrooms by PFO measurement
ECSS--E--10--04 Space engineering — Space environment
FED--STD--209E Airborne particulate cleanliness classes in cleanrooms and
clean zones
NOTE The ISO Technical Committee, ISO/TC 209, is currently
preparing a range of ISO standards (six published as of June
1999) that expand on the requirements, along with new
additions, of FED--STD--209E.

1) To be published.

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Terms, definitions and abbreviated terms

3.1 Terms and definitions


The following terms and definitions are specific to this Standard in the sense that
they are complementary or additional to those contained in ECSS--P--001.

3.1.1
airborne particle
particle suspended in air

3.1.2
airborne particle cleanliness class
level of cleanliness specified by the maximum allowable number of particles per
cubic metre (or cubic foot) of air

3.1.3
bakeout
activity of increasing the temperature of hardware to accelerate its outgassing
rates with the intent of reducing the content of molecular contaminants within
the hardware
NOTE Bakeout is usually performed in a vacuum environment, but
may be done in a controlled atmosphere.

3.1.4
bio-contamination
contamination of materials, devices, individuals, surfaces, liquids, gases or air
with micro-organisms

3.1.5
clean area
general term that includes cleanrooms, controlled areas, good housekeeping
areas, and other areas that have contamination control by physical design and
specified operating procedures

3.1.6
cleaning
actions to reduce the contamination level

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3.1.7
cleanliness (contamination) control
any organized action to control the level of contamination

3.1.8
cleanliness level
quantitative level of contamination

3.1.9
cleanliness verification
activity intended to verify that the actual cleanliness conditions of the space
system, the cleanrooms or the vacuum chambers are in conformance with the
applicable specifications and other cleanliness requirements

3.1.10
cleanroom
area in which the airborne particulate concentrations, temperature, humidity,
molecular species, pressure, activities, and other environmental parameters are
controlled, as specified, to produce acceptable products

3.1.11
clean work station
workbench or similar work area characterized by having its own filtered air or
gas supply

3.1.12
clean zone
defined space in which the contamination is controlled to meet specified cleanli-
ness levels

3.1.13
contaminant
any unwanted molecular or particulate matter (including microbiological matter)
on the surface or in the environment of interest, that can affect or degrade the
relevant performance or life time

3.1.14
contaminate, to
act of introducing any contaminant

3.1.15
contamination budget
permissible contamination levels defined at different stages of the life of the
instrument and satellite

3.1.16
contamination potential
potential amount of contaminant in the source which can produce contamination

3.1.17
controlled area
environmentally controlled area, operated as a cleanroom, with two pre-filter
stages but without the final stage of HEPA (or better) filters used in cleanrooms

3.1.18
fibre
particle with a length to diameter ratio of 10 or more

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3.1.19
FTIR spectrometer
analyser (chemical identification) of organic and inorganic contamination using
infrared wavelengths

3.1.20
HEPA particle filter
throwaway, extended-medium, dry type filter in a rigid frame that has a mini-
mum particle-collection efficiency of 99,97 % (that is a maximum particle penetra-
tion of 0,03 %) for 0,3 µm thermally generated DOP or specified alternative
aerosol

3.1.21
induced contaminant environment
environment created by the presence of contaminating items

3.1.22
molecular contamination
airborne or surface contamination (vapour, gas, liquid, or solid) without observ-
able dimensions (i.e. with dimensions at molecular level)

3.1.23
monitoring
to perform routine, quantitative measurements of environmental parameters in
and around cleanrooms, clean zones, and other clean areas, including contamina-
tion parameters

3.1.24
non-volatile residue (NVR)
quantity of residual soluble, suspended, and particulate matter remaining after
the controlled evaporation of a volatile liquid at a specified temperature

3.1.25
obscuration factor (OF)
ratio of the projected area of all particles to the total surface area on which they
rest

3.1.26
offgassing
evolution of gaseous products from a liquid or solid material into an atmosphere

3.1.27
outgassed quantity
total quantity of outgassed species expressed as a mass (e.g. gram or percent of
the initial specimen) or as pressure × volume (e.g. hPa × m3)

3.1.28
outgassing
evolution of gaseous species from a material, usually in vacuum
NOTE Outgassing also occurs in a higher-pressure environment.

3.1.29
particle
unit of matter with observable length, width and thickness

3.1.30
particle fallout
accumulated deposit of particulate matter on a surface

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3.1.31
particle size
apparent maximum linear dimension of a particle in the plane of observation as
observed with an optical microscope, or the equivalent diameter of a particle
detected by automatic instrumentation
NOTE The equivalent diameter is the diameter of a reference
sphere having known properties and producing the same
response in the sensing instrument as the particle being
measured.

3.1.32
particulate
of or relating to minute separate particles

3.1.33
particulate contamination (PAC)
airborne or surface contamination due to particles

3.1.34
plume
exhaust (molecules or particles) of thrusters and engines

3.1.35
purging
supply of clean gas to protect the critical hardware from contamination

3.1.36
quartz crystal microbalance (QCM)
device for measuring small quantities of mass deposited on a quartz crystal using
the properties of a crystal oscillator

3.1.37
ram direction
in the direction of velocity vector

3.1.38
sensitive item
item whose contamination may affect its performance or life time

3.1.39
ULPA particle filter
throwaway, extended-medium, dry-type filter in a rigid frame that has a mini-
mum particle-collection efficiency of 99,999 % (that is, a maximum particle pen-
etration of 0,001 %) for particles in the size range of 0,1 µm to 0,2 µm

3.1.40
venting
conveying unwanted gaseous products through an aperture

3.1.41
visibly clean
absence of surface contamination when examined with a specific light source,
angle of incidence and viewing distance using normal or magnified vision

3.1.42
wake direction
direction opposite to the velocity vector

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3.1.43
witness sample
sample used to collect contaminants during exposure, usually in an environmen-
tally controlled area, and then analysed or measured

3.2 Abbreviated terms


The following abbreviated terms are defined and used within this Standard:
Abbreviation Meaning
AIT assembly, integration and testing
AIV assembly, integration and verification
AO atomic oxygen
BOL beginning of life
CC contamination control
C&CCP cleanliness and contamination control plan
CRS cleanliness requirement specification
CVCM collected volatile condensable material
DML declared materials list
DOP dioctylphtalate
ECLS environmental control and life support
EGSE electrical ground support equipment
EOL end of life
EVA extra vehicular activity
FTIR Fourier transform infra-red
GSE ground support equipment
HEPA high-efficiency particulate air filter
ICC internal contamination control
IR infra-red
LEO low Earth orbit
LVC leakage/venting control
MBC micro-biological contamination
MGSE mechanical ground support equipment
MLI multi layer insulation
MOC molecular contamination
MRR manufacturing readiness review
NVR non-volatile residual
OF obscuration factor
ORU orbital replaceable unit
PAC particulate contamination
PFO particle fallout
PMP parts, materials and processes
QCM quartz crystal microbalance
RH relative humidity
RML recovered mass loss
TB thermal balance
TML total mass loss

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TRR test readiness review
TV thermal vacuum
UV ultra-violet
ULPA ultra-low-particle airfilter
VBQC vacuum balance quartz crystal
VCM volatile condensable material

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General cleanliness and contamination control


aspects

4.1 General
Contamination control cannot be applied effectively without an understanding of
the contaminant, the contaminant source and the detrimental effect that the
contaminant has.
The known causes of failure and degraded performance of space elements
attributed to contamination, including their sources, are given in this Standard.
When they are not known, tests and analyses can be performed (e.g. outgassing
rates as a function of time, chemical composition of outgassing products, con-
densation rates or degradation as result of radiation).
The results of these tests and analyses can be used to calculate expected conta-
mination levels and their subsequent effects if other relevant parameters are
known.
Preventive cleanliness control is becoming more important as space systems
become more sophisticated and mission durations are extended.
A problem frequently encountered in space technology is the lack of data enabling
a good correlation between contaminant levels and mission performance require-
ments. This kind of information should be available in the mass production areas
of electronics and precision mechanical devices.

4.2 Contamination attributes


4.2.1 Main effects of contamination on space systems
The main effects of contamination are:
D failure of precision mechanisms due to particulate matter,
D light scattering by particle and molecular contaminants,
D electrical discharge or arcing in high voltage equipment due to high outgas-
sing and other contamination,
D noise on slip rings and electrical contacts,
D results of certain experiments obscured by excessive molecular contamina-
tion (e.g. mass spectrometers and ion counters),

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D degradation of optical elements (e.g. lenses, mirrors and windows) due to
molecular contamination, especially X-ray and UV equipment and low tem-
perature IR detectors,
D degradation of thermal control surfaces (absorptivity/emissivity ration, α/ε)
especially in the case of molecular contamination on optical solar reflectors
at low temperatures,
D loss of efficiency in heat pipes,
D effects on conductive and non-conductive surfaces (leak paths in electronics),
D loss of efficiency in solar cell generators,
D corrosion of electrical contacts due to the presence of halogenated solder
fluxes,
D space charge and discharge effects related to contaminants,
D thermal radiation from particles,
D disorientation due to erroneous reaction of star trackers to luminous
particles,
D multipaction in waveguides,
D bad closing of a valve,
D explosion of a cryotechnic motor (Oil + O2),
D HF for a motor,
D disturbance of gas flux and combustion within thrusters, and
D disturbance and propagation within RF wave guides.

4.2.2 Typical contaminants and their sources on ground


4.2.2.1 Particulate contaminants
Many particulate contaminants, such as dirt, sand, industrial fumes, can, to a
large extent, be excluded from cleanrooms by filtering, and the space system can
therefore be protected from them right up to the final preparation at the launch
site.
Nevertheless, a considerable quantity of particulate contaminants are produced
or released during the life cycle of the space system. For example:
D hair cosmetics, dead human skin cells,
D fibres and lint from clothing, dust carried in on hair and clothes,
D chips and burrs from machined surfaces, solder and weld spatters,
D particles produced by wear or shedding, corrosion products, flakes from
coatings and air filters, and
D bacteria, fungi, viruses and secondary products.

4.2.2.2 Molecular contaminants


Molecular contaminants can be produced by the following sources:

4.2.2.2.1 Gases and vapours


These include:
D atmospheric gases, desorbed water, leaks in sealed units (e.g. freon, hydra-
zine, helium, neon and krypton),
D outgassing products from organic materials (e.g. monomers, plasticizers,
additives and solvents),
D vapours from packing materials and test facilities (e.g. vacuum pump oils),
D vapours from substances used in cleanrooms (e.g. plasticizers and cleaning
fluids), and
D secondary products coming from micro-organisms.

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4.2.2.2.2 Liquids
Examples include:
D residues from cleaning agents,
D residues from adhesive masking tapes,
D machine oils,
D coolants,
D lubricants,
D solder fluxes,
D cosmetics,
D grease from human skin, and
D secondary products coming from micro-organisms.

4.2.2.2.3 Other contaminants


These are usually:
D salt,
D acid,
D alkaline,
D corrosion products,
D oxidation products,
D finger prints, and
D stains.

4.2.3 Typical contaminants during operations and their


sources
4.2.3.1 Launch
Launch contaminants can come from the acoustic noise and mechanical vibra-
tions. The contamination source is then the space system itself and the fairing
and structural parts during the first minutes of the launch.
Redistribution of the released particles can occur so that clean surfaces are
covered by particles.
Also the co-passengers can be the source of contamination in the case of multiple
launches.
During the initial lift-off, the pressure inside the fairing drops from atmospheric
pressure to high vacuum within a few minutes, and the turbulence of the air can
also redistribute the particles.
The contamination environment during launch can be severe and there is basi-
cally no control of the contamination during this period.
Next to the particle contamination, the molecular contamination is of importance,
especially the outgassing of the materials, the release of contaminants by
mechanisms, separation mechanisms, such as pyrotechnics and thermal knives,
motors and thrusters.
The mechanism of molecular contamination is based upon outgassing under high
vacuum; however, the period for which the space system is under high vacuum
with other neighbouring hardware is very short.
Predictions of the molecular transfer during this period can be estimated assum-
ing that the Micro-VCM data are known and that the contamination species have
a certain activation energy.
This type of calculation can be made for co-passengers when the outgassing
requirements are less stringent than those for the space system of interest.

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4.2.3.2 Mission (external)

4.2.3.2.1 General
The main problem of contamination in space is that there is limited feedback on
contamination levels, because contamination is seldom measured in orbit.
The observed performance losses are often due to contamination.
Lessons learned from space systems returned to Earth after quite a long exposure
to space e.g. LDEF, Eureca and solar arrays from the Hubble Space Telescope,
indicated visible contamination especially near venting holes and at locations
where photodeposition and photopolymerization occurred due to solar radiation,
or where atomic oxigen has converted the volatile contaminants into non-volatile
contaminants.

4.2.3.2.2 Natural environment


The natural environments described here affect the contaminants in the environ-
ment or on surfaces or affect the deposition of contaminants on surfaces.
Most of the natural environments mentioned in the following subclauses are
described in detail in ECSS--E--10--04.
a. Vacuum and type of gases
The pressure of natural gases around the space system causes reflection of
the outgassing molecules originating from the space system. This reflection
is called “ambient scatter” and can result in a return of the space-system-pro-
duced contaminants to the space system itself.
This type of reflection depends on the level of vacuum and thus upon the
orbital altitude. For low Earth orbits the ambient scatter can result in a
return contamination flux of a few percent.
The gas composition of the Earth environment is such that only in cryogenic
space system applications are contamination problems to be expected.
b. Radiation (solar and other electromagnetic radiation)
Solar radiation and especially the ultra-violet part can have effects such as
polymerization and decomposition of already deposited contaminants.
The generally observed effects are a reduction in reflection and transmission
of light for optical experiments and solar arrays. Another observed effect is
the increase of solar absorptance of thermal control surfaces, which results
in a temperature increase for those surfaces.
Solar radiation can also affect the contamination deposition mechanisms,
and although this combined effect of contamination and electromagnetic
radiation is theoretically difficult to describe, this phenomenon is well
known.
Radiation ionizes the outgassed molecules in space and so can influence the
amount of ionized particles.
Also, the ionized molecules are attracted by a negative charged space system
and thus contaminate it.
c. Thermal aspects (thermal cycling)
Solar radiation, rotating space systems and planetary shieldings cause tem-
perature cyclings and these temperature cyclings have effects on the outgas-
sing of materials and on the condensation and evaporation of contaminants
on surfaces whose temperatures vary.
d. Atomic oxygen (AO) (speed effects)
AO is the main constituent of the residual atmosphere in Earth orbit at
between 200 km and 700 km altitude. The density is a function of altitude
and of other parameters such as solar radiation. In most cases the effect of

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thermal AO on deposited contaminants can be neglected. However, due to the


relative velocity between AO and the space system (approx 8 km/s) the
collisional energy in the ram direction is around 5 eV.
The items and surfaces in the ram direction of the space system can be
attacked by thermal AO, whereas the items and surfaces in the wake direc-
tion are hardly attacked.
The effect of AO can be described as an oxidation and some materials can
become resistant to AO, e.g. non-volatile oxides can be formed on some me-
tals.
Organic materials can be oxidized to volatile products such as CO and H2O.
The presence of silica contaminants on space system surfaces can be
explained by the attack of condensed silicone species by AO and the
formation of SiOx.
e. Charged particles (electrons, ions)
The effect of charged particles on outgassing and on already condensed
contaminants is probably small, but no exact data are known at this moment.
f. Micrometeoroids (debris)
Micrometeoroids have no direct effect on outgassing and on condensed conta-
minants. Micrometeoroids can pierce some materials and can also result in
partly destruction of some materials, which causes release of a large amount
of new particles which escape into space or affect neighbouring items. Im-
pacts can also cause evaporation of the micrometeoroid and of the impacted
surface.
Redistribution of particles, which were already on space system surfaces by
micrometeoroid collisions, have been reported, but the effects are very small.
Based upon this redistribution, the acceptable particle levels for space sys-
tem surfaces at BOL can be specified.
g. Speed effects of space systems w.r.t. molecular speeds
The speed of a space system has no direct effect on the outgassing of materials
or on the deposition mechanisms of contaminants on surfaces.
However, the return contamination flux via the ambient scatter is highly
affected by the local pressure around the space system. This local pressure
depends upon the actual space system speed with respect to the speed of the
natural species. Because of the speed effects, the ram direction pressure can
be orders of magnitude higher than the normal pressure for that orbit and
the ambient scatter is then also orders of magnitude higher than the normal
ambient scatter.
The same can be expected for the wake directions, i.e. orders of magnitude
lower pressures and thus orders of magnitude lower ambient scatter than
expected.

4.2.3.2.3 Induced environment


The space system environment can be seen as being created by the space system
itself or by its operation, by the human space activities and by the docking
vehicles.
a. Gas and fluid leakage from pressurized systems
In space systems one can expect sealed pressurized units, such as batteries
and gyros; for these units leak rates have been specified which do not result
in unacceptable performance losses of those units. However, the level of their
leak rate or their location in the space system can be such that the perform-
ances of sensitive items can be affected. Also the leaks from pressurized units
such as containers holding propulsion gases or fluids (e.g. hydrazine) can
affect contamination sensitive items.

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Within long-term space (station) programmes a number of fluids are used,
which potentially emerge from containments such as tanks, lines and pres-
sure shells to the exterior by leakage, venting or purging.
All fluids contribute to contamination.
b. Cabin leakage of pressurized human habitation systems
Habitation units can have acceptable leak rates, which are related to safety
aspects of the astronauts, the leakage of gases can upset the performance of
contamination-sensitive items, and then the location of these items is import-
ant with respect to the possible cabin leaks.
c. Human waste dumps from habited space systems
Habited space systems generally have overboard dumping of disposals such
as gases, liquids and particles.
As particular matter formed through chemical or physical processes, e.g.
from solid propellant burning at launch, (human) wastes produced inside
and removed by crew, respectively, can be deposited on surfaces or change,
for example, ambient optical conditions. They also can lead, for example, to
malfunctions of mechanical equipment.
d. Contaminants from release mechanisms and moving mechanisms
Release mechanisms such as cable cutters and mechanisms based upon
sealed units with explosives, release particles from adjacent surfaces due to
the mechanical shocks.
Mechanisms that are based upon cutting of cables using thermal knives
release both molecular and particulate contaminants.
e. Contaminants from operating thrusters, engines or other propulsion sys-
tems
Solid booster engines produce particles as well as molecular contaminants,
liquid gas rockets produce mainly gaseous contaminants, and hydrazine
thrusters produce gaseous reaction products and some unburned fuels. Ion
thrusters mainly produce not fully neutralized gaseous products such as
xenon and a small amount of sputtered metal from the neutralizing grid
material.
f. Contaminants from docking activities
Docking contaminants can be the release of particles by mechanical shocks
in the space system as well as the docking system.
g. Environment created by extra vehicular activity (EVA)
The exterior materials of astronaut space suits produce molecular outgassing
contaminants and in the selection of those materials basically the same
outgassing criteria as for the space system materials are applicable.
Particulate contaminants can also be expected and their level depends upon
the astronaut activities.
h. Release of contaminants that were collected during ground activities
During the ground life of the space system, both molecular and particulate
contaminants can be deposited, mainly on the external surfaces. During
launch especially particulate contaminants are released and during the
mission itself their release is mainly caused by shocks. The release of these
particulate contaminants from external surfaces by impingement of
micrometeoroids and debris is small compared to the amount of particles
released from the surface materials by the same impingements.
For molecular contaminants that collected on surfaces during ground
activities, the same outgassing effect can be expected as from material
outgassing.

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i. Secondary products
Secondary products are generated by various intermolecular interactions
and chemical or physical processes due to payload or experiment operations
or interactions of the natural and induced environment constituents and the
space system.

4.2.3.3 Mission (inhabited space cabins)

4.2.3.3.1 General
This subclause deals with the contamination control aspects relevant to the
inhabited areas of space cabins.
Long-term effects of contamination significantly affect the lifetime and
functionality of equipment. An accumulation leads to an impairment in
performance and health status not only with respect to equipment but also
for crew members.
The necessity of service or maintenance and restoration activities are obvi-
ous.

4.2.3.3.2 Sources of contamination - natural environment


The sources of internal and external contamination originate from natural
and induced environments and their interactions.
a. Enriched oxygen
With the internal oxygen content (e.g. up to 40 % O2 in the MIR-station)
oxidation processes (e.g. corrosion) occur. Consequently, the internal
equipment environment is contaminated in shorter time periods by the
corresponding corrosion products (e.g. particles and gases).
b. Reduced pressure (emergency case)
In the case of reduced pressure (e.g. 700 hPa in an emergency), the offgassing
rates of some internal used materials increase. Respective gaseous products
contaminate surfaces or environments especially when the temperature of
material surfaces is below the nominal one.

4.2.3.3.3 Sources of contamination - induced environment (internal)


a. Propellant leakage
Propellants potentially emerge from, for example, tanks, line fittings and
flanges or other equipment by leakage or via internal valves.
Like all fluids, any propellant contributes to contamination.
Each individual application of each propellant is reviewed in the leakage
analysis to ensure an optimum selection of the detection, location and isola-
tion techniques.
b. Fluid leakage
A number of fluids other than propellants are used, which potentially emerge
as contaminants from equipment to the exterior by leakage or via internal
valves.
c. Contamination from experiments (payloads)
Besides fluids, other sources of contamination are caused by material impu-
rities or are of a more particular nature.
Solid materials contain impurities from manufacturing or cleaning processes
which diffuse (outgass) to the exterior already at ambient pressure, especial-
ly at elevated temperatures.
In addition to the already discussed diffusion process from the material,
adsorbed and absorbed contaminants from contaminant environmental
conditions, e.g. during manufacturing, cleaning, interaction, test and launch

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phases, can be desorbed (offgas) from the surfaces. This applies to materials
and equipment brought into the internal volume by extra-vehicular-acti-
vities (EVA suits, repair or servicing of orbital replaceable units) or through
particles formed in chemical or physical processes.
System equipment can also be an important source of contamination, for
instance, via its normal operation and maintenance. Typical payload sources
are bio-contamination from life science experiments and venting from
material science experiments.
d. Human waste
As mentioned before human wastes include:
S fluids released by crew activities (nutrients and waste),
S particles from cloths or tissues (fibres) and from the crew’s biological
processes (e.g. hairs, scales, faeces and urine).
Aside the “contamination standards” with respect to fluids and particles,
some very special problem areas are associated with human waste, such as
contamination by:
S micro-organisms (fungi, yeasts and bacteria) and
S bio-chemical products of human metabolism (urea).
All of these are extremely bio-corrosive with respect to materials surfaces,
especially when (pre-)contamination (water or nutrients) processes are
involved.
In addition, all such human wastes pose risks for the health of crew members
in closed environments.
e. Bio-contamination
The organisms that are responsible for internal bio-contamination are
microbes (fungi, yeasts and bacteria). They can be found in any environment.
On the other hand viruses or prions are per se not alive and depend strongly
on the presence of other host organisms, such as humans, animals or plants
and other bacteria.
Micro-organisms generate contamination substances with their potential
metabolic or biological capabilities. The fluids produced contribute to trace
gas concentration levels and odour.
1. Fungi, spores
Fungi are introduced into internal volumes by sticking to or being present
in living organisms, contaminated equipment, food and airborne
particles. They exist as fungi or can develop from spores. They can be
introduced during the manufacturing, interaction and test, transport
and operational phases.
They grow predominantly in a humid environment, especially in water
films or droplets.
Most living species (except spores) do not survive at elevated tempera-
tures (> 80 ºC) or in dry environments (< 8 % water activity). However,
after settling down and starting to grow in a wet environment, they can
form colonies, draw humidity from the air and continue to live.
Micro-organisms are killed by UV light, elevated temperatures, starva-
tion (lack of water and nutrients) and contact with toxic substances
(disinfectants or detergents and certain metals such as chromium, silver,
copper). Spores are much more resistant to all of these measures.
The characteristic population varies due to changes in the growth envi-
ronment (e.g. crew and sun activity), decontamination activities and
genetic mutations.
Fluid and air loops are favourable areas for microbial growth.

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In the fluid loops, contamination control can be provided by adding bio-


cides.
In the air loop (e.g. cabin air, avionics air and humidity removal), micro-
bial control is very difficult, especially in areas inaccessible to inspection
and maintenance because of limitations on using biocides due to their
impact on crew health.
The areas in the environmental control and life support (ECLS) system
containing condensed water (condensing heat exchanger, condense and
air lines, water separator and condense tank) and cold air are the most
vulnerable due to the existence of saturated air or water.
Outside of the ducting, cold spots with low temperatures and high rela-
tive humidity are prone to condensation, especially in areas with low air
flow velocities (e.g. corners), although condensation is prohibited and
ventilation is required, e.g. in areas accessible to the crew.
The air is filtered by screens, high-performance (HEPA) filters or even
activated charcoal filters (for odour removal). Therefore, microbial conta-
mination in the flow direction can be prevented behind the filter elements
by killing microbes in a dry air stream. However, recontaminations from
the downstream side and during maintenance activities require special
attention.
2. Bacteria
Bacteria are introduced into internal volumes mainly by living organisms
such as crew members, animals or plants (payloads) and associated food
and can be released via body fluids and wastes. They develop in organic
matter (rarely inorganic) and on or within the bodies of living organisms
and lead primarily to the impairment of health and bio/corrosion on
material surfaces.
If suitable living conditions are available (water and nutrients), the
number of microbes can grow exponentially.
Cross-contamination among crew members can be reduced by good
design, by adhering to certain hygiene procedures, and by medication of
infected organisms (antibiotics).
Hygiene methods to prevent infections consist of preventive means (no
direct contact with contaminated matter, periodic cleaning and disinfect-
ing of all surfaces and subsystems prone to microbial contamination, safe
disposal and chemical treatment of biologically active wastes) and
corrective means (immediate cleaning or disinfecting of spoiled areas).
3. Viruses and others
Contrary to fungi and bacteria, viruses and prions need other living
organisms (hosts) to stay alive and reproduce in a suitable environment
(e.g. temperature and humidity).
4. Secondary products
Secondary products generated by microbial growth are fluids (liquids or
gases), odour and (bio)reproduction products (e.g. spores, living cells and
cell debris) originating from the microbes themselves or from bio/cor-
rosion processes and chemical reactions of space system materials
induced through microbial activities.
All of these secondary products are taken into account in the general
internal contamination control concept.

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4.2.4 Effects of contaminants and failure modes due to
contaminants in space
Most of the effects of contamination occur in space, especially when solar radi-
ation is involved. Typical effects of contamination and failure modes are given in
subclause 4.2.1.
For the space environment around the space system, the “column density”, local
gas pressures and gas composition can be limiting factors for some experiments.

4.2.5 Particle transport in space


Only the surfaces in direct view of other surfaces can be contaminated by particles
originating from the other surface and there is no known mechanism during
space missions, that can cause a return of released particles to the space system.
Depending on the mass of particles, return of charged particles to a charged
spacecraft can be expected.

4.2.6 Molecular contaminants transport in space


D Creeping
Liquid contaminants and also lubricants can contaminate adjacent items by
the liquid creeping over surfaces, and silicone fluids especially are known to
have a high creeping effect.
In order to reduce the creeping effect, anti-creep barriers made of special
materials can be applied.
D Direct flux
Contaminants in space move in straight lines from the space system into deep
space and sometimes contamination sensitive items can be located in the
direct flux; however, a design provision is to avoid this location.
D Indirect flux
Contaminants from space systems can impinge on less contamination
sensitive surfaces such as solar arrays and antennas and after reflection
(specular) or re-evaporation (diffusive) these contaminants can affect
contamination sensitive items or areas.
D Collision with natural gases
Contaminants coming from the space system can collide with the natural
gases around the space system and after collision can return to the space
system. This phenomenon is known as ambient atmospheric scattering and
depends upon the density (and thus upon the altitude) of the natural gas.
D Collision with other outgassed molecules
Molecules released from space systems (e.g. outgassing via venting holes)
can collide with other molecules from the same origin or from other origins
(e.g. plumes). After the collisions, some molecules can return to the space
system. This phenomenon is called self-scattering and the return flux strong-
ly depends upon the intensities of the fluxes from the contaminant sources.
D Ionization of gaseous contaminants and the re-attraction by the negative
charged space system
Contaminants emitted from the space system can be ionized in space by solar
radiation (especially ultra-violet radiation, electrons, protons and ions) and
these ions can be re-attracted by a negative charged space system. This
phenomenon is well known, but has not yet been quantified.
One of the simple rules is that instruments that have deployable shutters or
ejectable covers shall be deployed or ejected when the outgassing has dropped
to a certain level or after a pre-determined time after the launch.

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4.3 Cleanliness levels


4.3.1 General
The cleanliness levels concern basically molecular contaminants (MOC) and
particulate contaminants (PAC).
The levels can be defined for surfaces as well as for the relevant environment.
The relevant environment can be a cleanroom, a test facility and the space
environment.

4.3.2 Particulate levels on surfaces


4.3.2.1 General
The way the particulate levels on surfaces are expressed depends very much upon
the size and number of the particles per unit area. Two standard methods of
measurement are given below.
The general concern in space system technology is for particle sizes from 1 µm to
100 µm. Besides the size and number, important parameters for particles inter-
pretation and measurement are:
D shape,
D orientation,
D fluorescence,
D magnetic properties, and
D chemical nature.
The redistribution of particles on surfaces in any environment can occur due to
turbulence (e.g. in vacuum chambers during pump down or during repressuriz-
ation), and during vibration (acoustic, vibration and launch).

4.3.2.2 Expression of levels for particles on surfaces

4.3.2.2.1 Standard method 1 (MIL-STD-1246C)


The MIL--STD--1246C gives the size-number distribution function for particles on
surfaces. Table 1 gives the classification in data terms and Figure 1 gives the
same distribution function in the form of a graph.
Figure 1 gives the cleanliness levels for surfaces for particles from 1 µm to
1 000 µm.
NOTE Levels are measured by counting the number and sizes of
the particles of at least three different sizes on a known
surface area. The data are then plotted in the graph in
Figure 1. A line parallel to those in the graph is then drawn
such that all the measurement points are on the left of this
line. The point in which this line meets the x--axis gives the
actual cleanliness level.

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Figure 1: Product cleanliness levels according to MIL--STD--1246C

Table 1: Product cleanliness levels


Cleanliness level Particle Max. Max. Max.
(according to size (µm) allowable allowable allowable
MIL--STD--1246) particle particle particle
count per count per ft2 count per
0,1 m2 litre
1 1 1,08 1,0 10
5 1 3,02 2,8 28
2 2,48 2,3 23
5 1,08 1,0 10
1 9,07 8,4 84
10 2 7,56 7,0 70
5 3,24 3,0 30
10 1,08 1,0 10
2 57 53 530
25 5 24,8 23 230
15 3,67 3,4 34
25 1,08 1,0 10

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Table 1: Product cleanliness levels (continued)


Cleanliness level Particle Max. Max. Max.
(according to size (µm) allowable allowable allowable
MIL--STD--1246) particle particle particle
count per count per ft2 count per
0,1 m2 litre
5 179 166 1 660
50 15 27,0 25 250
25 7,88 7,3 73
50 1,08 1,0 10
5 1 930 1 785 17 850
100 15 286 265 2 650
25 84,2 78 780
50 11,9 11 110
100 1,08 1,0 10
15 4 520 4 189 41 890
200 25 1 340 1 240 12 400
50 184 170 1 700
100 17,3 16 160
200 1,08 1,0 10
25 8 050 7 455 74 550
300 50 1 100 1 021 10 210
100 103 95 950
250 2,48 2,3 23
300 1,08 1,0 10
50 12 800 11 817 118 170
500 100 1 190 1 100 1 100
250 28,1 26 260
500 1,08 1,0 10
50 105 000 95 807 958 070
750 100 9 630 8 919 89 190
250 231 214 2 140
500 8,75 8,1 81
750 1,08 1,0 10
100 46 100 42 658 426 580
1 000 250 1 100 1 022 10 220
500 42,1 39 390
750 5,18 4,8 48
1 000 1,08 1,0 10

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4.3.2.2.2 Standard method 2 (Obscuration factor)
The obscuration factor (OF) is the ratio of the projected area of all particles to the
total surface area on which they rest.
This OF is in principle independent of the number-size distribution of the
particles and even independent of the shape and colour of the particles. In general
the levels shall be expressed in parts per million (mm2/m2) and the normal
requirements should roughly be between 10 mm2/m2 and 10 000 mm2/m2.
The OF has the advantage that a number of performance loss parameters are
directly related to the particle coverage of the critical item.

4.3.2.3 Correlation for particles on surfaces


The levels expressed in Table 1 and Figure 1 (MIL--STD--1246C) are according to
the following equation:
log n = 0,926 {(logC)2 -- (log d)2} + 0,031 97
where
n is the number of particles per 0,1 m2;
C is the class (e.g. 300);
d is the particle diameter (µm).

The factor 0,926 is a slope factor and is basically only valid for cleaned surfaces;
in practice it is between 0,24 and 0,58.
Moreover, these levels are not linear and the interpretation of the real amounts
becomes difficult, which in turn makes budgeting quite difficult.
The correlation between the ideal levels of MIL--STD--1246C (i.e. the slope factor
of 0,926) and the obscuration factor for particles between 1 µm and 20 µm, is given
in Table 2.
NOTE The definition of the actual slope factor depends basically on
the surface characteristics. For this reason, values reported
in Table 2 are given for reference and the method 2, based
on obscuration factor, is preferred for the expression of par-
ticles on surfaces.

Table 2: Correlation between ideal class of MIL--STD--1246


and obscuration factor
MIL--STD--1246 (class) Obscuration factor (mm2/m2)
50 0,3
100 3,3
200 54
300 329
400 1 274
500 3 814
600 9 619
700 21 469
800 43 707
900 82 799
1 000 148 025

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4.3.3 Particle levels in environments


The environments concerned are cleanrooms (see annex F), test areas or test
volumes and also space itself. The cleanliness levels for gases used for the rel-
evant process or for purging are expressed in the same way.

4.3.4 Molecular levels on surfaces


4.3.4.1 Sources of molecular levels on surfaces
This definition of MOC includes inorganic molecules (e.g. NaCl and residue of
solder fluxes), as well as organic molecules on surfaces.
For organic molecules the space system contaminants are seen as, for example,
hydrocarbon oils, ester types and silicones, mainly molecules coming from test
facilities, and outgassing species from materials.
a. For low temperature applications, the type of molecules can be different as,
for example, water (under 0 ºC) and even gases such as nitrogen can form a
deposit on cold surfaces and as such shall be reflected on the CRS and
C&CCP.
b. The morphology of the deposit (e.g. smooth surface or droplets) can be impor-
tant with regard to the actual performance loss.
Molecules can be deposited on surfaces during several critical phases on the
ground as well as in space. On the ground, the critical periods are during manu-
facturing, activities in cleanrooms, tests (e.g. vacuum tests especially when criti-
cal surfaces are cold) and transport. Molecular contaminants can also be de-
posited during launch and in space and for this type of deposition special
mathematical models have been developed.

4.3.4.2 Acceptance levels for molecular contamination on surfaces


In general, the molecular levels on surfaces are expressed in terms of mass per
unit area (i.e. g/cm 2).
a. The type of species (e.g. silicones) can be specified, as well as the total level.
b. The expression in g/cm 2 generally varies between one monolayer and the
visible level of 3 × 10 --8 g/cm 2 and 1 × 10 --6 g/cm 2 , respectively.
c. The actual requirements depend upon the application and the temperature.
d. Typical for optical instruments, the number of diopters (number of optical
surfaces) is important and it is generally known that for ultra-violet optics
the requirements can be very stringent because of polymerization (mainly
carbon) of the contaminants with incident radiation.
e. Acceptance levels for the MOC are determined by analysis, which takes into
account the above critical parameters and the acceptable performance loss.
f. The specified levels are generally related to the method of measuring the
organic contamination levels.
g. Specifications can be based upon the amount of non-volatile residue (NVR),
which is measured in real mass units per (large) area. Table 3 gives the NVR
cleanliness levels according to MIL--STD--1246C.
h. The acceptance level for NVR of liquid systems (cooling and propulsion
systems) is generally < 1 × 10 --7 g/cm 2.

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Table 3: NVR cleanliness levels, according to
MIL--STD--1246C
NVR limit
NVR level Surface Volume
(mg/0,1 m2) (mg/l)
A/100 0,01 0,1
A/50 0,02 0,2
A/20 0,05 0,5
A/10 0,10 1,0
A/5 0,20 2,0
A/2 0,50 5,0
A 1,00 10,0
B 2,00 20,0
C 3,00 30,0
D 4,00 40,0
E 5,00 50,0
F 7,00 70,0
G 10,00 100,0
H 15,00 150,0
J 25,00 250,0

4.3.5 Molecular levels in environments


The environments that cause most concern for space systems are manufacturing
areas, assembly areas, integration areas, test areas, transport containers, pre-
launch areas, launch areas and space itself.
The contamination levels of natural environments in space (see ECSS--E--10--04)
and the induced environment are be dealt with. The induced environment is
created by the space system itself and the actual processes. The space system
induced environment is caused by, for instance, material outgassing, thrusters,
mechanisms, dumps and the induced environment can be modelled when the
contaminant sources are known and quantified (e.g. outgassing kinetic tests such
as VBQC-tests) and when the distribution methods in space are known. The
natural environment can have some effect upon the actual distribution of the
space system contaminants.
Another effect is the speed of the space system and the speed of the contaminants.
This effect can cause enormous contamination differences in the ram and wake
areas of the space system.
A parameter that can be of importance is the column density of molecules in
space.

4.4 Cleanliness monitoring


4.4.1 Particulate contamination monitoring
D Μonitoring of the cleanroom air
See annex F.
D Visual inspection of surfaces

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Surfaces are examined with the naked eye or with the aid of a microscope.
An ultra-violet lamp (395 nm) increases the visibility of dust particles (“black-
light”).
The “visibly clean” level depends very much on the circumstances in which
the examination is made; it is better to express this level as an obscuration
factor of 300 mm2/m2.
This is independent of: colour of the surface, amount and wavelength of the
inspection light and angle of vision.
D Optical monitoring methods on surfaces
Typical methods are the measurement of transmission or reflection loss and
nephelometry (i.e. scattering of light).
These methods are valid for all types of contaminants, both organic and
inorganic. Photographic determination of dust particles on surfaces is also
possible, as is automatic counting. There are commercially available
instruments (e.g. PFO photometers) that automatically measure the particle
fallout level on sensor plates, exposed during phases of interest.
The method for measuring of the PFO level is described in the
ECSS--Q--70--50.
Other methods for the determination of the particle contamination are:
S the tape lift method, using sticky tapes (according to ASTM--E1216--87);
S microscopic counting;
S method of counting particles removed from a known surface by blowing
and suction of air;
S washing of the surface of interest and counting the particles in the wash-
ing fluid either directly using a commercial instrument, or on a filter after
filtration of the liquid.

4.4.2 Molecular contamination monitoring


a. Visual inspection
Experience with Micro-VCM tests has shown that, generally, levels of
organic contamination above 1 × 10 --6 g/cm 2 can already be visible to the
naked eye.
b. Wipe techniques and visual inspection
Wiping certain areas with a clean tissue concentrates the contaminants. In
practice, a concentration of ten times is possible. This means that, unless the
surface being wiped is abrasive (e.g. aluminium), contamination levels down
to a few times 10 --7 g/cm 2 can be detected in this way.
NOTE If the lens tissue is carefully chosen, perfectly cleaned and
accurately controlled, one can measure up to 0,2 × 10 --7 g/cm 2.
Since with this method “false positives” can always be
measured, indicating contamination where there is none, this
wipe method should not be a “prime” detection method, but a
“support” method, used to confirm a result. Good and reliable
results depend greatly on lens tissue choice and pretreatment.

c. Wipe techniques and physical and chemical analysis


A surface of a known area is wiped with a clean tissue, the tissue is subjected
to extraction with chloroform of spectral grade, and the residue of the chloro-
form is analysed by infrared techniques in accordance with ECSS--Q--70--05.
This method, applied to a wiped area of 100 cm2, permits detection of organic
contamination levels down to 3 × 10 --9 g/cm 2.
The results of this method depend very much on the surface roughness, on
the type of tissue and on the method used to clean (and verify) the tissue.

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The results depend also on the solvent used to wipe: if strong (e.g. chloro-
form), the surface can be damaged and the analyses biased; if soft (e.g.
alcohol), the contaminant is not be fully wiped and thus the pollution is
underestimated. This is a strong limitation of the wipe method, which is,
however, efficient for light molecular deposits (like hydrocarbide).
d. Non-volatile residue
The accuracy and detection limit of this method depend greatly upon the
sensitivity of the balance, the substrate water absorption, the washing effi-
ciency and the solvent background (see NVR-measurement according to
ASTM--E1235M--95).
The levels should be expressed in mass per unit area and the measurements
should be made using infrared spectroscopy (see measurements according to
ECSS--Q--70--05).
Measurements in situ are quite often made using quartz crystal microba-
lances (QCM).
e. Direct analysis of the suspect item
Various analysing techniques can be applied, e.g. infrared analysis, gas chro-
matography, mass spectrometry, ultra-violet degradation, X-ray reflection
loss.
f. Direct analysis of witness samples
Analysis of witness samples, exposed to the hardware concerned:
S Metal witness plates of 15 cm2 area washed and analysed by IR tech-
niques have a detection limit of 6 × 10 --9 g/cm 2.
S IR transparent disks (MgF2, CaF2, ZnSe) analysed directly by IR tech-
nique have a detection limit of 2 × 10 --8 g/cm 2.
NOTE 1 Even if measurements on metal witness samples seem to be
more precise than measurements on IR transparent disks,
they involve a lot of handling (cleaning, verification of back-
ground, exposure, recuperation of contaminants, transfer of
concentrated solvent on a crystal and then analysis) and are
thus less practical than the second method.

NOTE 2 The above detection limits were determined with sophisti-


cated FTIR instruments (purged with dry air, against
disturbance from humidity absorption, and regularly cali-
brated), based upon low signal-to-noise ratios and low NVR
of solvents and wipes. Normally, worse detection limits need
to be considered for routine measurements.

4.4.3 Contamination monitoring in vacuum facility


Monitoring of organic contaminants in vacuum facilities can be achieved using
one of the following methods:
D By means of clean metallic sensors placed on or near suspect places for a
specified time and then subjected to one of the standard analyses. A
combination of a QCM and a mass spectrometer can allow identification of
the different condensed species after a controlled re-evaporation from the
QCM.
D Mass spectrometer measurements can also be used to obtain information on
outgassing products, and their origin if a position-scanning mechanism
(NIPKOV disk) is employed.

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D A QCM which can detect contamination levels down to 1 × 10 --9 g/cm 2, and
can also be used to measure condensation rates. Such QCMs can operate
down to liquid nitrogen temperatures. (QCM can be used under atmospheric
conditions, but humidity shall then be controlled to close tolerances, since
water sorption on the crystal affects the results).
NOTE: In general, the use of witness samples is the simplest and cheapest
method for contamination monitoring in a vacuum chamber.

4.4.4 Contamination monitoring during launch


Contamination measurements during launch are difficult to perform, especially
those of particle levels.
a. For the molecular contamination levels during launch, QCMs can be used,
with the temperature either uncontrolled or kept constant.
b. For the interpretation, the thermal fluxes and the solar fluxes can affect the
QCM readings and corrections can then be required.
The QCMs can be installed on the launcher and the measuring time is limited to
a few minutes; if the QCMs are installed on the space system, the measurements
can continue during mission.
The measurement of particles during launch is extremely difficult and no specific
method has been established for their detection.

4.4.5 Contamination monitoring in space


Measurements of contamination in space are not often made because the policy
of cleanliness control is based upon the basic principle of achieving the lowest
possible contamination levels with existing knowledge and within the allocated
financial budgets.
The manageable factors are then: a good materials and process selection, cleanli-
ness oriented design, good preventive actions and good operations procedures.
a. Particle measurements in space can be made by light scattering measure-
ment, e.g. using the Sun or a laser as the a light source.
b. Particles can also be measured by mass increase measurements using QCMs
with a crystal having a surface to which particles stick.
c. Molecular contaminants in space can be measured using mass spectrome-
ters.
d. Molecular contaminants on surfaces can be measured using a QCM as a
witness sensor, which is located near a sensitive item and maintained at the
same temperature as the item.

4.5 Cleaning
Various methods are employed to clean contaminated items; for example:
D Mechanical cleaning, such as grinding, brushing and blasting.
D Detergent cleaning (or soap cleaning) for, for example, glass, rubbers, plas-
tics, polyamides, PTFE, polypropylene and acrylates and all ferrous metals,
including stainless steel. Such detergents also clean non-ferrous metals,
such as aluminium and brass, but have an oxidizing effect on their surface.
A detergent or soap cleaning is followed up by a final cleaning with solvent
to remove all traces of detergent.
D Chemical cleaning with, for example, acids, alkalines and salts for metals.
D Electrochemical cleaning with, for example, acids, alkalines and salts for
smoothing metal surfaces.

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4.5.1 Removal of particulate contamination
For a number of substances, visibility of particles can be enhanced by the use of
a special ultra-violet lamp (“black light” -- UV--A 365 nm).
D Dust can be removed with the aid of an ordinary vacuum cleaner, combined
with a good brush. Having the exhaust of the vaccum cleaner outside the
cleanroom is preferred to avoid recontamination. Clean air supply to the item
to be cleaned is used, otherwise the contamination of items to be cleaned can
be increased by the relative dirty air which is extracted from the environ-
ment (e.g. when electrostatic attraction can occur). Only vacuum cleaners
equipped with HEPA filters are used in a cleanroom and checked with a UV
lamp while working.
D Wiping is performed with extreme care, otherwise surfaces can be scratched
and “dust” can simply be wiped onto other clean items in the vicinity.
Since, in any case, solvent leads particles to the bottom of cleaned part, those
particles shall be recovered with a vacuum cleaner at the end.
D Another method of removal of particles is the very careful use of a jet of
compressed gas, since contamination of the other clean items in the vicinity
can result. Cleaning agents, such as brushes, wipe tissues or compressed gas,
can themselves contaminate the item to be cleaned and can lead to dust
scratching the surface during cleaning. Ionized air is a good approach in the
removal of particles by air blowing.
D An effective form of wiping can be used of tissues dipped in methanol.
D Larger particles can be removed by means of polyimide adhesive tape, event-
ually rolled around a metal or other appropriate tool (e.g. swabs).
D Cleaning with dry ice (e.g. CO2 jet spray) can be very effective.
D The hardware to be cleaned can be coated with shrinkable polymer film and,
after drying, the film can be removed with the contaminants. Use of this type
of cleaning method needs to be carefully evaluated as it is known to have
detrimental effects on some materials (e.g. gold coatings).

4.5.2 Removal of molecular contamination


Several methods exist for cleaning off molecular contamination, and for which the
final cleanliness levels can be assessed based on experience and on the initial
cleanliness level, as well as on the type of item contaminated.
D Dry wiping: clean lint-free cloth or lens paper is used, however, it has the
disadvantage that it can scratch the surfaces.
D Wet wiping: a clean cloth, brush or paper is used in conjunction with organic
solvents.
D Solvent cleaning: examples are washing, dipping, spraying, vapour cleaning
and ultrasonic cleaning.
D Detergent cleaning or soap cleaning.
D Plasma cleaning (i.e. ionized inert low pressure gas) is very effective for the
removal of polymerized products.
D Volatilizing under vacuum is especially successful for cleaning assembled
units, or when solvent cleaning is too delicate an operation. See also sub-
clause 6.4.3 “Bakeout”.
D Ultra-violet-ozone cleaning: molecules of an organic nature are activated by
ultra-violet light, resulting in dissociation, after which they react with the
ozone produced in the air by ultra-violet light.
D Cleaning with dry ice (CO2 jet spray): this is very effective for the removal
of molecular layers.
D Use of shrinkable polymer film, peeled after drying, can also be very effective
for the removal of molecules (not for optical surfaces).

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4.6 Modelling
Known quantaties of outgassing flux as a function of time and knowing the shape
of the outgassing plume are essential for the modelling of contamination in an
environment around the space system. It is assumed that the temperature of
outgassing sources is known.
Knowledge of the outgassing fluxes as a function of time, the view factors and the
residence times (as a function of surface temperature) of the contaminants on the
surface of interest are are indispensible for the modelling of the contaminants on
surfaces.
For a worst case surface modelling, the Micro-VCM data (ref. ECSS--Q--70--02)
can be taken. It is then assumed that all the contaminants released during the
Micro-VCM test of 24 hours at 125 ºC, are now released during the actual life time
and the second assumption is that the view factor (Vf) is estimated (Vf = part of
the total outgassing amount which impinges on the surface of interest). The third
assumption is that all the TML for surfaces at --100 ºC or lower, all the RML for
surfaces between --100 ºC and +25 ºC or all the CVCM for surfaces at 25 ºC, is
deposited permanently on the surface of interest. Knowledge of the outgassing
rates as a function of time and temperaturefor realistic hardware is indispensible
to achieve more realistic modelling. The same applies to the residence time of the
contaminants on surfaces as a function of surface temperature.
Most modelling methodologies (like e.g. ESABASE outgassing) are based upon
outgassing data obtained during outgassing kinetic tests (ref. ESA--QME--WI--
F--03). The test data obtained from outgassing tests according to ASTM--
E1559--93 can also be used for modelling space system contamination.
Based upon the modelling, contamination budgets are allocated for certain ap-
plications.
Detailed information on plumes and different modelling approaches is given in
ECSS--E--10--04.

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Cleanliness and contamination control


programme

a. The supplier shall establish a cleanliness and contamination control pro-


gramme for each level of configuration item defined in the project, at the
beginning of the project.
The objective of this programme is, starting from the mission performance
requirements, to establish cleanliness and contamination levels to be
achieved at different manufacturing, AIT and mission stages.
b. This shall be documented in the cleanliness requirement specification (CRS).
c. The programme shall implement methods to achieve the specified levels
established and documented in the cleanliness and contamination control
plan (C&CCP).
d. Clear responsibility and authority shall be assigned for the implementation
of the cleanliness and contamination control tasks.
e. Adequate measures shall also be established for the coordination and resol-
ution of cleanliness and contamination control issues among the parties
involved in the project.
NOTE In general, the organization of regular workshops dedicated
to cleanliness and contamination control for a specific pro-
gramme is a good practice for the definition of the CRS.
Surveys should also be made to determine what is really
needed for contamination control, based on mission objec-
tives and scenarios.
For complicated contamination items, the early preparation
of a cleanliness policy document is of great value before the
preparation of the actual CRS and C&CCP, because all rel-
evant data are not available in the early stages of the project
and not all possible steps, such as purging and bakeout, are
defined.

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Contamination control during the product life


cycle

6.1 General design provisions


Contamination control activities during the design phase shall take into account
the following points:
a. selection of materials, mechanical parts and processes,
b. cleaning aptitude of materials and mechanical parts,
c. acquisition of outgassing data of organic materials,
d. volume or quantity of each material used,
e. application and location of materials,
f. vent path or hole of outgassing,
g. measurement of contamination,
h. deployable aperture covers,
i. flash-off heaters on passive radiative coolers, mirrors and detectors,
j. covers over passive radiative coolers,
k. in-bay purging (on-ground and at the launch),
l. verification of the compatibility of the surface treatment with the cleanliness
level,
m. identification of the protection equipment,
n. ground support equipment, and
o. detailed design provisions for specific types of mission are addressed in 6.6,
6.7 and 6.8.

6.2 Manufacturing, integration and test


6.2.1 Manufacturing
a. All elements manufactured in non-clean areas or under non-clean conditions
shall be the object of a cleaning process until the required cleanliness level
is achieved, before they are packaged for delivery.
b. All materials and processes used shall conform to PMP requirements.

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11 December 2002 ECSS
c. Cleaning and packaging operations for all elements shall be processed
according to applicable and validated procedures.
Two cases can be identified:
S Elements that can be cleaned after manufacturing
These elements shall be cleaned so as to guarantee the required
cleanliness level. For a given initial pollution, the cleaning procedure is
validated if it allows to guarantee that both particulate and molecular
contamination are within specified levels.
S Elements that cannot be cleaned after manufacturing
Manufacturing and assembling areas for these different elements shall
meet the required cleanliness level specifications.
In this case the manufacturing process shall be considered in the C&CCP,
in particular for sensitive elements.

6.2.2 Assembly and integration


a. For any contamination critical assembly, a cleanliness control flow chart
should be established, showing, schematically, the stages at which specific
cleanliness controls shall be undertaken.
b. Assembling activities shall be performed only by specifically trained person-
nel.
c. Critical and sensitive elements should only be exposed during essential oper-
ations and returned to their dedicated containers when not in work.
d. A dedicated set of assembly tools and equipment shall be used and main-
tained in clean conditions.
e. Dedicated procedures shall be established for critical item assembly.
NOTE From the particle point of view, the number of 5 µm particles
per given volume of air is much more critical than the
number of smaller particles, since the fallout is mainly de-
termined by particles of 5 µm or larger. The required cleanli-
ness level of a cleanroom can only be selected when the
specified obscuration factors for critical spacecraft surfaces
are known. The particle size 5 µm is often used as a cri-
terion, because for optical surfaces particles larger than
5 µm are critical, whereas for bearings and gears, particles
in the range 10 µm to 40 µm are more harmful.

f. For the selection of the cleanroom, the allocated contamination budget and
the duration of the integration shall be known. Furthermore, the type of
cleanroom shall be selected when the integration takes place. The correlation
between the airborne contamination and the particle fallout for normal
cleanrooms is basically known (see annex F), and so a rough estimate can be
made of the type of cleanroom required. Of course a practical contamination
level for the cleanroom is required with representative activities and a repre-
sentative number of operators. Also, the type of protection required for the
critical hardware (e.g. covers, shields and purging) has an effect on the
expected contamination levels.
g. An audit of the integration and test facilities shall be performed on a regular
basis. The suitability of the facilities shall be verified during MRR or TRR.

6.2.3 Testing
Space system testing generally involves:
D a vibration test,
D an acoustic test,

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D an EMC test,
D a thermal balance test,
D a thermal vacuum test, and
D a solar simulation test;
and these tests can affect the cleanliness of the hardware to be tested, e.g. vibra-
tion and acoustic testing can loosen particles and cause their redistribution; EMC
and acoustic test facilities can be inside cleanrooms, but are basically not clean.
a. The centre where the testing activities take place shall be in conformance
with the relevant requirements of the ECSS--Q--20--07.
b. The test facilities shall be classified with the same cleanliness level as clean-
rooms. The cleanroom requirements are also applicable to the test facilities.
However, for certain conditions, the specified cleanliness level is not guaran-
teed, such as:
S vacuum chambers during operation,
S acoustic facilities during operation,
S EMC chambers, and
S vibration facilities.
c. All the potential sources of contamination from the test facility to the test
item shall be analysed and controlled, for example;
S lubricants,
S gases for purging, and
S coating material on walls.

6.2.4 Vacuum facilities


a. Adequate procedures shall be available for:
S cleaning the test facilities (e.g. solvent and bakeout),
S cleanliness control during pump-down and recovery,
S recovery of storage pumps, and
S cleaning cold trap.
b. For a test in a vacuum facility, it shall be ensured that the material of the test
item does pose any risk of contamination of the facility. If contamination has
occurred, the contaminants are released during the warm phase of the facil-
ity to the test item.
c. The following should be available and verified:
S An approved declared material list (DML).
The DML shall consider the test item in the “test configuration”, i.e.
including the test adapter and all connections (e.g. mechanical, electri-
cal).
S For a flight, hardware may be accepted only having the reference to the
already approved material list.
In such a case the DML shall be provided only for the materials used in
addition to the flight configuration (test configuration).
d. For “clean” vacuum systems, a sensor (or a critical surface) shall not be
contaminated by more than 1 × 10 --7 g/cm 2 during a blank test of 24 hours
duration. The sensor is normally at room temperature, but, more stringent
requirements can be imposed, depending upon the budget allocation for the

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equipment. In fact, for sensitive equipment, 0,3 × 10 --7 g/cm 2, 24 hours (or
0,5 × 10 --7 g/cm 2, week) for a blank test should be specified.
e. The blank test shall be representative of the actual test (inclusive of test
equipment and cabling) and include a pump down and a repressurization.

6.3 Budgets, prediction and modelling

6.3.1 General
a. A contamination budget shall be established in order to determine:
S the on-ground molecular and particulate contamination levels;
S an estimate of the in-orbit molecular contamination, for contamination-
sensitive systems.
b. The contamination budget at different stages in the life of the instrument and
satellite (e.g. end of instrument AIT, end of satellite AIT, beginning of orbital
life, end of orbital life) shall be compared to the cleanliness requirements.
c. If the estimated contamination budget is higher than the specified level, then
precautions to minimize contamination shall be investigated and implem-
ented.

6.3.2 On-ground contamination budget


a. This budget shall be elaborated to evaluate the molecular and particulate
contamination levels generated by the cleanroom and test site environments
on the sensitive surfaces exposed inside.
b. The budget planning for integration of the instrument and satellite shall be
elaborated from the integration and test plan.
c. For each activity, the sensitive surfaces, the duration of the exposure during
each activity, the cleanroom criteria, and the potential means of protection
shall be identified.
d. The consolidation of the budget planning with the results of the witness
samples (molecular contamination levels as a function of time) and the parti-
culate formula shall give the estimated ground contamination budget (in
terms of g/cm 2 and parts per million or in terms of transmittance losses) for
each sensitive exposed surface.
e. The linear dependency of MOC and PAC as a function of time is not always
valid for longer periods.

6.3.3 In-orbit molecular contamination budget


The in-orbit molecular contamination results from the outgassing of organic
materials; molecules outgass from the different materials and can condense on
sensitive surfaces.
a. The temperatures of the surfaces and the view factors between a potential
outgassed surface and a sensitive surface shall be taken into account in the
elaboration of this budget. For sensitive instruments, such as optical instru-
ments, modelling methodologies are used to make an estimate of the superfi-
cial density of contaminants (g/cm 2) condensed on the surfaces as a function
of time.
b. Complementary experimental tests on the outgassed materials should be
proposed to evaluate the transmittance losses induced by the molecular
contaminants in the spectral bands of the instrument. The molecular levels
calculated in the modelling as per a. above are then associated to these
transmittance losses.

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6.3.4 Launch contamination budget


A budget for contamination during the launch phase shall be allocated, based on
the type of launcher, the co-passengers and other relevant aspects.
This budgeting shall be performed at least for contamination sensitive systems.

6.4 Cleanliness verification

6.4.1 General
a. The cleanliness verification shall include all the activities intended to ensure
that the actual cleanliness conditions of the space system, the cleanrooms or
the vacuum chambers conform to the applicable standards or the applicable
CRS (specific to the a certain project).
b. The cleanliness verification shall make use of recognized methods for the
determination or the monitoring of the contamination levels.
c. The cleanliness verification activities shall be specified in the C&CCP.
d. The cleanliness verification of cleanrooms shall also include the verification
of the environmental parameters such as temperature, relative humidity
and the overpressure.
e. The cleanliness verification shall take place under one or more of the follow-
ing conditions:
S at predetermined intervals, independently of the current activity, to con-
firm the efficiency of the established cleanliness control measures;
S after the occurrence of an incident or anomaly that can have influenced
the cleanliness conditions of the space system or cleanroom;
S before the beginning of the ground (e.g. test campaign) or launch acti-
vities, to confirm that the facilities and cleanrooms are conform to the
relevant C&CCP;
S before and after a test in a vacuum chamber.

6.4.2 Cleaning procedures


6.4.2.1 General
a. Once the materials and components are selected and the processes or
manufacturing techniques are known and established, suitable cleaning
procedures shall be chosen in order to ensure that the required cleanliness
levels, expected in the contamination budget, and the final product
cleanliness level are achieved.
b. Cleaning procedures shall be validated by tests on representative samples,
or by experience from previous and similar projects, in which they were
validated.
The choice of the cleaning method obviously depends on the type of contamin-
ants to be removed and the physical or chemical nature of the item to be
cleaned.
For those items that are too delicate to withstand cleaning, preventive conta-
mination control is of the utmost importance.
The cleaning of some parts is particularly important during the course of
manufacture or before processing (e.g. prior to bonding, painting, vacuum
coating, welding and soldering).
c. The procedures concerning cleaning of this type shall be mentioned in the
process specification. In this case, the desirability of cleaning is a matter of
judgement, based on practical experience or on visual inspection, unless a
special surface finish is required.

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6.4.2.2 Cleaning aids
a. Cleaning aids shall not increase the contaminant levels of the items to be
cleaned. Therefore:
S the aids, such as wipe tissues, papers, cloths, brushes and foams shall be
non-fluffing, lint free and dust free;
S damage to surfaces (scratches) shall be minimal;
S organic contaminant content of cleaning wipe materials shall be less than
25 mm2/m2 for wiping extremely clean surfaces.
b. The molecular contaminant content of some wipe materials, measured in
accordance with ECSS--Q--70--05, is reported in Annex C. However, when
wipe materials are selected for cleaning, measurements should be taken to
determine their contaminant content. In principle, all wipe materials should
be precleaned to achieve the required level of cleanliness. Precleaning re-
quires extraction by solvents.

6.4.2.3 Cleaning solvents


The following are the basic rules for the selection of the correct solvent to be used
for molecular contamination removal.
a. Compatibility
The cleaning solvent shall be compatible with the material or item to be
cleaned (see annex D). Moreover, the solvent shall not be corrosive to metals
(see MIL--HDBK--406 and NASA SP--5076), e.g. titanium shall not be cleaned
using methanol, or with chlorocarbon or chlorofluorocarbon, but with
acetone, whereas solid-state detectors, which are liable to be affected by
solvent vapours, shall be cleaned with methanol only.
b. Solvency
When the contaminant is known, the solvent best able to remove the conta-
minant shall be selected.
c. Toxicity and flammability
For most solvents particular precautions shall be taken during the cleaning
process (see MIL--HDBK--406).
d. Residue of organic solvents
For precision cleaning, solvents of high purity shall be used, otherwise conta-
minant levels are raised rather than lowered. Consequently, when a cleaning
liquid is selected, it is only necessary to ensure that it is of a “pro-analyse
quality”, or that NVR is less than 10 mg/l (measured with gravimetric
method). Typical figures for the residue content of cleaning solvents are
listed in annex E, which is based on measurements performed in accordance
with ECSS--Q--70--05. From this list it can be seen that very clean solvents
are commercially available.

6.4.3 Bakeout
The aim of the bakeout process is:
D to improve the outgassing behaviour of a material;
D to reduce the level of surface contamination collected during processing or
testing.
a. Bakeout should be applied for all materials that can be warmed, and more
specifically to:
S harness,
S MLI,
S carbon and glass fibre components, and

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S glued, coated or potted materials.


b. During the bakeout process, the following relevant parameters shall be
monitored:
S vacuum conditions (< 10 --2 Pa),
S temperature (> 60 ºC),
S duration (> 72 h).
The temperature shall be linked to the outgassing material and the cleaning
effect, but the lower the temperature (with given minimum of 60 ºC) the
longer the duration.
c. In addition, the outgassing rate should be monitored.

6.4.4 Purging
The aim of the purging is to avoid external contaminants being deposited on
sensitive equipment, such as optics, by injecting a non-ionized high-purity dry
gas inside a cavity.
a. The purging shall be performed inside a cavity to maintain a constant ex-
change of the gas present in the cavity. This exchange depends on the entry
flow rate of the gas and the total surface leaks.
The purging can be implemented at instrument or satellite level during
functional and performance tests at ambient conditions, during repressuriz-
ation after TB/TV and TV tests, during all the phases without activities and
during storage and transport phases.
b. The purity of the gas and the cleanliness of all the pipes shall be verified
before the first use of the purging system.
c. Filtering systems (both for MOC and PAC) shall be provided before the gas
comes into contact with the hardware.
d. The filtering capabilities shall be compatible with the relevant cleanliness
requirement.
NOTE A good solution, for chamber repressurization, is to add an
HEPA filter to the repressurization piping and to collect the
air for repressurization in a clean area (preferably
class 100).

6.5 Packing, containerization, transportation and storage


a. To maintain the cleanliness levels achieved at any point from initial precision
cleaning to delivery to the launch site, provisions shall be taken for packing,
containerization, transportation and storage.
b. For that, cleanliness protection shall be provided prior to leaving the con-
trolled areas, or whenever a storage period is planned.
c. The container for clean item shall maintain the cleanliness levels specified
for the product.
d. Storage areas shall provide adequate protection to the package and the
product for the intended storage period.
e. When sensitive items are packaged, containers for long-term storage or
transportation, shall include adequate provision for internal flushing with
dry high-purity nitrogen and over-pressurization (100 hPa minimum), ex-
cept if units are put in sealed bags as per bullet h.
f. In the above case, an inlet valve and an outlet valve shall be installed and
clearly identified.
g. The design of the container shall facilitate easy cleaning and inspection of its
surfaces, avoiding any kind of dirt traps.

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h. Small clean parts shall be double bagged in airtight envelopes during storage
or transportation outside controlled clean areas.
i. Bags for contamination-sensitive items shall be flushed with dry nitrogen
and then sealed.
j. Only approved materials that were procured as cleaned films shall be used
(e.g. polyethylene, polypropylene and polyimide).
k. Static sensitive items shall use metallized films.
l. Outer bags shall not enter controlled clean areas.
m. When desiccants are used, they shall be in bags that are clean and do not
produce particulate contamination.
n. Desiccants and humidity indicators shall be placed in the external envelope.
o. Adequate procedures shall be provided for packing, containerization, trans-
portation and storage.
p. PVC (polyvinyl chloride) shall be avoided for optics protection.

6.6 Launch
6.6.1 General
It is assumed that the space system is shipped to the launch base under clean
conditions and that potential contamination during launch preparation is also
controlled.
A final cleaning of external surfaces should take place in order to meet the BOL
requirements.
The moment of a final cleaning is generally just before the entry of the space
system into the fairing, or a final cleaning can even be done just before closing the
fairing.
Purging of the contamination-sensitive instruments should take place until final
closure of the fairing.
Special constructions can be provided, e.g. a purge connection such that purging
can take place until just before launch.
Under normal conditions, purging cannot be re-installed in the case of an aborted
launch.
NOTE There is hardly any contamination control, or even
measurements, during the launch, and contamination of
the hardware is predicted based upon the possible release of
contaminants and the view factors of the sensitive items
with respect to contamination sources.

6.6.2 Specific provisions


6.6.2.1 Launcher level
a. Launcher parts, such as fairings and mechanical systems for double or mul-
tiple launches, shall be clean in order not to contaminate the clean items of
the space system.
b. The materials of the hardware in the vicinity of the space system shall meet
the same outgassing and surface-cleanliness requirements as the space sys-
tem itself.
c. The building environment in which the spacecraft is put inside the fairing
shall be compatible with the spacecraft characteristics.

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6.6.2.2 System (payload) level


a. Specific design provisions can be protection mechanisms to be used to limit
the launch contaminants, especially the “unknown” figure of particle
transfer during launch.
b. A second design aspect is the location of the contamination-sensitive items
with respect to the position of thrusters and of pyrotechnics (or other conta-
mination sources).
c. Also the reflection by atmospheric molecules (i.e. atmospheric scattering) or
by outgassing molecules (i.e. self-scattering) can take place and some form
of modelling is of interest.

6.7 Mission (external)


6.7.1 Molecular outgassing from materials
The materials used for space systems shall be selected based upon low outgassing
criteria. The outgassing criteria are based upon the Micro-VCM test
(ECSS--Q--70--02), and shall take into account the location of the outgassing
source and its mass.
a. The general requirement for materials outgassing is: RML < 1 % and
CVCM < 0,10 % as per ECSS--Q--70.
b. An overall outgassing budget should be allocated per equipment or box. This
should be calculated by adding the outgassing contribution of each constitu-
ent of the equipment.
c. For applications around sensitive items (e.g. optics and detectors) more strin-
gent values should be used, along with performance of bakes on the relevant
hardware. The definition of the outgassing requirements shall take into
account the quantity of material concerned, and the specific environmental
conditions (e.g. available volumes and temperatures).
NOTE Table 4 provides an example of the definition of outgassing
requirements based on good design practice.

d. Some metals such as cadmium and zinc have high vapour pressures and
deposit metallic films on adjacent surfaces. The application of these volatile
metals shall not be used especially when the temperatures are above room
temperatures.
e. Each individual application of any fluid shall be reviewed in the leakage
analysis to ensure optimal selection of detection, location and isolation tech-
niques.
f. The location of the dump lines with respect to the contamination-sensitive
items is critical and during dumping the very critical items should be
shielded.

Table 4: Material outgassing criteria values


Mass of material
concerned CVCM(%) RML(%)
(grams)
> 1 000 < 0,01 < 1
100 – 1 000 < 0,01 < 1
10 – 100 < 0,01 < 1
1 – 10 < 0,03 < 1
< 1 < 0,1 < 1

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6.7.2 Design aspects
a. The sensitivity to contamination shall be one of the drivers in the initial
design of the space system and its instruments.
b. The design shall be cleanliness-oriented and such that the lowest possible
contamination levels can be achieved on-ground as well during the launch
and mission.
In order to achieve the lowest contamination levels, attention shall be paid
to the following:
1. Locate contamination sensitive items far away from the contaminant
sources.
2. Position the sensitive items so that the view factors with respect to conta-
minant sources (e.g. solar arrays, antennas and thrusters) are as low as
possible.
3. Locate the vent holes of the space system and the instruments away from
the sensitive items (= backdoor venting).
4. Manufacture the hardware in such a way that venting (of, for example,
thermal blankets) is directed towards the backdoor.
5. Design baffles or shields for the sensitive items or even for the contamin-
ant sources.
6. Design temporary covers (red-tag covers) or hoods to reduce contamina-
tion during ground life. (Optically transparent covers can be used for
calibration, alignment or functional testing of optical instruments with-
out removing the covers.)
7. Design deployable covers for very sensitive instruments, that are oper-
ated only in space.
8. Design cleaning mechanisms for the removing of contaminants by, for
example, heating the sensitive hardware, manoeuvre the space system in
such a way that in low orbit the AO can perform a cleaning.
9. Selection of materials, processes, mechanisms and components with low
particulate and molecular contamination potential. In this respect low
outgassing materials shall be chosen, and zinc and cadmium (or cadmium
plating) should not be used because of the relatively high vapour pressur-
es of these materials.
10. If the contamination potential of selected materials is still too high, bake-
out of the hardware shall be considered before assembly or even during
tests.
11. The design, manufacturing order and assembly shall be such that
bakeout can still be performed (sometimes baking is carried out before
further assembly is done because of the temperature limitations of
certain hardware or because the products released during the bakeout
can have effects on other items).
12. Where sensitive items are expected, the design of the instruments or
space system shall be such that purging is feasible in the periods of
assembly, integration, tests and launch preparations or even up to
launch.
13. Based upon these effects, the venting holes and other contaminant
sources should be located in the wake side of the space system.
14. On the other hand, the wake side of a space system can be used for special
experiments for which extremely low pressures in relatively low Earth
orbit are required.

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6.7.3 Mission (inhabited space cabins)


A number of fluids other than propellants are present, that can emerge to the
exterior by leakage or intentional use of valves.
a. All fluids shall be considered, whether originating from thermal, environ-
mental or life support systems or subsystems or released due to crew
activities (nutrients, wastes), during maintenance and repair and from
experiments or payloads.
b. Each individual application of each fluid shall be reviewed in a specific
analysis to ensure an optimum level of detection, location and isolation tech-
niques.
c. Design measures shall comprise the usage of easily cleanable surfaces
(shape, materials), safe disposal of wastes in concealed bags or compart-
ments, and removal of airborne microbial contamination by filters.
These aspects shall be considered in the design and operational requirements of
system and equipment hardware.

6.8 Mission (internal)


6.8.1 System level
The flight configuration tasks related to contamination, leakage and venting of
internal fluids, particulates and microbiological matter, comprise the following
activities:
D analyse and specify internal contamination control requirements;
D analyse and specify leakage and venting control requirements;
D define and develop methods and analysis tools;
D define and perform analyses and tests;
D coordinate and supervise the lower level tasks.
a. The ICC and LVC flight configuration level requirements shall be analysed
and completed as a basis for analyses and task planning.
b. If the evolving programme contamination and LVC requirements are
changed due to unresolvable conflicts between design and contamination
and LVC constraints, then the impact of the requirement change shall be
assessed and its acceptability verified at top (system) level.
c. For ICC/LVC, the effort shall be limited as much as possible.
d. ICC shall be achieved by material selection and analytical verification and
optimization of design and operations.
e. If the ICC requirements cannot be met, decontamination equipment shall be
developed.
f. In ICC/LVC, all interfaces to other subsystems and design elements where
contamination and leakage are expected shall be investigated based on
information obtained from the respective subsystem involved.
g. The ICC and LVC shall be achieved by proper material selection (in close
cooperation with PMP), with design optimization and possibly with
operations and maintenance guidelines and constraints based on analytical
predictions and on-ground tests where necessary.
h. The design information and analysis and test results shall be compiled to
ensure transparency and allow analyses with respect to contamination and
the leakage/venting interface, which, in iterative procedure, shall be con-
sidered in the flight configuration level.

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6.8.2 Lower levels
a. Based on overall system knowledge with respect to requirements, design and
operations, support shall be given to the subsystem levels to identify and
evaluate unacceptable contamination loads due to in-orbit operations and
contingency cases and consequent design and operational measures. This
should include the definition of maintenance activities of internal areas and
equipment where restoration or replacement is required prior to EOL of the
flight configuration.
b. Inputs shall also be given to operations to define flight operational ICC tasks.
c. Special attention shall be paid to microbial contamination control.
d. If the baseline design is incompatible with ICC requirements, the design
changes shall be identified and corrective actions shall be taken in close
cooperation with all levels involved.
e. The subsystem level tasks related to internal fluids, particular and microbio-
logical contamination and leakage or venting comprise activities to analyse
and specify requirements, define and perform analyses, integrate and test
ICC and LVC hardware, coordinate and supervise the lower level tasks and
support the higher level.
f. All subsystem parts, materials and processes shall also be in accordance with
the ICC and LVC concept of this C&CCP.
g. The design data and other subsystem information relevant for ICC and LVC
shall be compiled and given to the higher levels to conduct IC and LV analyses
(e.g. performance of decontamination device and filters, mass and volume of
outgassing materials and equipment and related outgassing rates and types
and IC risk information).
h. The component level tasks related to internal fluids, particulate and
microbiological contamination and leakage or venting comprise activities to
analyse requirements, perform analyses, develop and test ICC and LVC
hardware and support the higher level.
i. All components, materials and processes shall be in accordance with the ICC
and LVC concept of the C&CCP (see above).
j. The contamination control and monitoring hardware (e.g. filters and sniffing
lines) shall be designed, developed, tested and verified according to the
requirements of the associated subsystem.

6.8.3 Monitoring
a. In the operational phase, contamination levels shall be monitored. Appropri-
ate sensor elements shall be applied to guarantee the predicted design
life-times at system, subsystem, component or equipment level.
b. Monitoring for particulte and molecular and microbiological contamination
shall be considered only for internal environments.

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Annex A (normative)

Document requirements list

Applicable to Deliver at
DRD DRD title (phase) (frequency
Remarks
number (Grouped by discipline) or
0 A B C D E F
milestone)
Q--70--01A Cleanliness requirement
Annex G specification
Q--70--01A Cleanliness and
Annex H contamination control plan

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Annex B (informative)

Space system cleanliness control flow chart

A--A--
B--B--

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1. Performance requirements
8. Product assurance plan and operational modes

2. Cleanliness oriented design

5. Cleanliness predictions
or modelling
3. Cleanliness requirements
specification

6. Cleaning procedures

4. Cleanliness and contamina-


tion control plan
7. Cleanliness monitoring
procedures
9. Materials, processes and
components selection

10. Procurement 11. Intermediate cleaning 12. Manufacturing process

13. Final cleaning

20. Packing, containerization,


15. Bakeout 14. Assembling
transport

17. Purging 16. Integration 21. Packing, containerization,


transport

18. Tests 22. Packing, containerization,


transport

23. Packing, containerization,


19. Launch preparation transport

24. Launch

25. Mission

Figure B--1: Space systems cleanliness control flow chart

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Annex C (informative)

Molecular contaminant content of some wipe


materials

C--C--

The data in this table are a result of single tests and are simply illustrative.
Table C--1:

Molecular
contaminant
Material
content
(mm2/m2)
Cotton wool 140
Kimt wipes 46
Kleenext 88
Garbyt 23
Greem 105t lens tissue 34
Velin non-fluff tissue 47
Lens tissue (SS--2478t) 14
Filter paper SS--595t 29
Filter paper SS--1575t 21
Filter paper SS--1505t 22

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Annex D (informative)

Compatibility of various solvents with listed


materials

D--D--

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Table D--1:
Solvent
Materials Ethers, Strong Strong
Aliphatic Aromatic Alcohols
cetones acids bases
Polyvinyl chloride (plasticized) ++++ ------ ------ ------ ++++ ++++
Polyvinyl chloride (hard) ++++ + + -- ++++ ++++
Polyethylene ------ ------ ------ -- ++++ ++++
Polystyrene ------ ------ ------ +++ -------- ++++
Polyester ++++ ++++ +++ ? -------- --
Epoxy ++++ ++++ +++ ---- + +++
Polyvinylidene fluoride ++++ ++++ ++ +++ ++++ ++++
Chlorinated polyester ++++ ++++ +++ +++ +++ +++
Fluran ++++ ++++ ++++ ? ++++ ++
Polymethyl methacrylate -------- -------- -------- ------ -------- +
Polycarbonates ++++ -------- ---- + + ----
Polyamides ++++ ++++ ++ ++++ ++ ++
Polyphenylene oxides ++++ -------- ---- ++++ ++ ++
Polysulphides ++++ ---- ---- ++ ++++ ++++
Vinyl esters ++++ -------- -------- ? + ++++
Polyurethane (paints) -------- -------- ++
Phenolics ++++ ++++ ++++ ++++ ++++ ++++
Polytetrafluoroethylene (PTFE) ++++ ++++ ++++ ++++ ++++ ++++
Perchlorotrifluoroethylene (PCTFE) ++++ ++++ ++++ ++ ++++ ------
Diallylphthalate silicone elastomer ------ ------ -- +++ +++ ?
Ethylene propylene ------ ------ ++ +++ +++ ?
Butadiene styrene ---- ------ -- +++ ---- --
Chlorosulphonated polyethylene + ------ -- +++ ++ ?
Polychloroprene polyethylene ++ ------ -- +++ + ?
Fluorocarbon polyethylene ++++ + +++ +++ ?
Acrylate ester polyethylene +++ ------ ------ ------ ?
Butandiene acrylonitrile +++ ------ +++ ? ?
polyethylene
++++ Very good -- Average ? Not known
+++ Good ---- Average
++ Average ------ Bad
+ Average -------- Very bad

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Annex E (informative)

Non-volatile residue of commercially available


solvents, measured by infrared techniques

E--E--

Table E--1:

Non–volatile residue
Product
(NVR) (mm2/m2)
Acetone 0,4
Ethyl alcohol 1,6
Isopropyl alcohol 0,8
Chloroform, spectral grade 0,3
Methanol 0,7
Tetrachlorocarbon 0,2
“from aerosol bottle I” 35
“from aerosol bottle II” 50

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Annex F (informative)

Cleanroom requirements

F--F--

F.1 Particle levels and cleanroom classification


The number of particles per m3 as a function of the diameter from 0,1 µm to 5 µm
as classes is reported in Table F--1 (derived from FED--STD--209E). This classi-
fication depends upon the ideal number-size distribution and is given graphically
in Figure F--1.
NOTE 1 The document FED--STD--209E is fully applicable to the
airborne particulate cleanliness classes in cleanrooms and
clean zones. The information reported below is included for
information and is in conformance with this document.

NOTE 2 Table F--1 gives the particle numbers per m3 and conversion
to the number per cubic foot can be achieved by multiplying
the above numbers by: 0,0283. (The old classes 100, 1 000,
10 000 and 100 000 are now, respectively, Classes M3.5,
M4.5, M5.5 and M6.5).
Concentration limits are calculated by means of the follow-
ing formula:

NOTE 3 particles/m 3 = 10M(0,5/d) 2,2

where

M is the numerical metric class designation (e.g. 3,5);


d is the particle size (in µm).

or, alternatively, by means of the following formula:

particles/ft 3 = Nc(0,5/d) 2,2

where

Nc is the numerical designation of the class, in the old


system (e.g. 100, 10 000).

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Particles per m3
(Particles per ft3)

3 530 000
(100 000)
CLASS M6.5
(CLASS 100 000)
CLASS M5.5
353 000
(CLASS 10 000)
(10 000)

CLASS M4.5
CLASS M3.5 (CLASS 1 000)
35 300
(1 000) (CLASS 100)

3 530
(100)

CLASS M2.5
(CLASS 10)
353
(10)

CLASS M1.5
(CLASS 1)
35,3
(1)

3,53
(0,1)
0,01 0,1 1 10

Particle size (micrometers)

Figure F--1: Ideal particle-size distribution

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Table F--1: Airborne particulate cleanliness classes (taken from FED--


STD--209E)

Class Limits

Class Name 0,1 µm 0,2 µm 0,3 µm 0,5 µm 5 µm


Volume Units Volume Units Volume Units Volume Units Volume Units
Metric Old m3 ft3 m3 ft3 m3 ft3 m3 ft3 m3 ft3
Class Class
M1 350 9,91 75,7 2,14 30,9 0,875 10 0,283 -- --
M1.5 1 1 240 35 265 7,5 106 3 35,3 1 -- --
M2 3 500 99,10 757 21,4 309 8,75 100 2,83 -- --
M2.5 10 12 400 350 2 650 75 1 060 30 353 10 -- --
M3 35 000 991 7 570 214 3 090 87,5 1 000 28,3 -- --
M3.5 100 -- -- 26 500 750 10 600 300 3 530 100 -- --
M4 -- -- 75 700 2 140 30 900 875 10 000 283 -- --
M4.5 1 000 -- -- -- -- -- -- 35 300 1 000 247 7
M5 -- -- -- -- -- -- 100 000 2 830 618 17,5
M5.5 10 000 -- -- -- -- -- -- 353 000 10 000 2 470 70
M6 -- -- -- -- -- -- 1 000 000 28 300 6 180 175
M6.5 100 000 -- -- -- -- -- -- 3 530 000 100 000 24 700 700
M7 -- -- -- -- -- -- 10 000 000 283 000 61 800 1 750

F.2 Interpretation for particles in environments


The disadvantages are that in practice the slope of the actual curves can be
different from the slopes in Figure F--1.
a. The classes can be interpolated to classify a cleanroom or an environment,
other than conventional, when special conditions dictate their use (e.g. M2.2,
M4.3 and M6.4, corresponding to the old classes 5 600 and 70 000).
b. The labelling for an alternative class shall be based on the concentration limit
specified for particles 0,5 µm and larger, in the same manner as the classes
listed in Table F--1 above.
c. Concentration limits for the other particle sizes shall be in the same propor-
tions as those in the next cleaner class in Table F--1; these limits can be
calculated by using the appropriate equation reported under Figure F--1.
d. Similarly, for classes cleaner than class M1, or class 1, the concentration
limits at particle sizes other than 0,5 µm shall be in the same proportion as
those of class M1, or class 1.

F.3 Monitoring of cleanroom air


The cleanroom air is generally monitored with commercially available dust
counters.
a. Particle counts shall be taken continuously or at predetermined intervals
during working periods and at locations that yield the number of particles in
the air as close as possible to the work location.
b. Monitoring techniques and routines shall be established to meet the require-
ments of a specific category of cleanroom or clean work station.
c. The monitoring methods and equipment can be used only if demonstrated to
be of adequate accuracy and repeatability; frequency, sampling air volume
and position shall be established on the basis of the airborne particulate

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cleanliness and the degree to which contamination is controlled for protec-
tion of processes and products.
d. For monitoring purposes only, determining the extent to which particles are
deposited on surfaces can be achieved through the exposure of test surfaces
or samples to the environment and counting the settled particles by appropri-
ate methods.
e. Air monitoring of class M6.5 or better shall be achieved by means of light
scattering equipment.
f. Furthermore, tests shall be performed to determine if leaks exceed the speci-
fied limits:
S in the filter media themselves,
S in the bond between filter media and the interior of the filter frame,
S between filter frame gasket and filter bank supporting frames, and
S between supporting frames and walls or ceilings.
g. The cleanrooms shall be provided with a monitoring function for the
contamination levels and the environmental parameters (i.e. temperature,
relative humidity and differential pressure) as well as an alarm function
which is initiated when certain levels (set well below the “out of specification
limits”) are exceeded.
h. Adequate and planned corrective actions shall be initiated to re-establish the
nominal conditions in the shortest possible time and to prevent recurrence.

F.4 Indicative correlation between particles in air and particle fallout


An exact mathematical correlation between particles in air and PFO cannot be
given (mainly due to operative conditions).
The data contained in Table F--2 are based on several measurements performed
in different cleanrooms and are thus indicative of the expectable PFO.

Table F--2: Correlation airborne and PFO for cleanrooms

Metric class PFO


(mm2/m2/24 h)
3,5 2,0
4,5 10
5,5 52
6,5 275

PFO = 0,069 10(0,72M--1,08)


where M is the metric numerical class (e.g. 3,5)

or:
PFO = 0,069 Nc0,72
where Nc is the old numerical classification (e.g. 100 or 100 000)

F.5 Molecular levels


a. For ground facilities the normal requirements for cleanrooms are that a
critical surface inside that area is not contaminated by more than
0,5 × 10 --7 g/cm 2 during a continuous period of one week.

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b. In case of contamination sensitive equipment, a lower level can be required,


based on the contamination budget (including exposure time).
NOTE 1 In a normal cleanroom (without charcoal filters) levels can
be achieved that are 10 to 100 times better.

NOTE 2 For those hardware items where the cumulation from the
air becomes a major issue (e.g. coated mirrors), the use of
charcoal filters as molecular contamination trap should be
considered.

NOTE 3 Charcoal is an efficient, but dangerous filter. It is important,


on installation, to know exactly (by analysis) the charge in
contaminants. Moreover, in some specific cases, it can
release its charge in contaminants trapped. Hence, it is
essential to know the initial charge, on installation, and to
analyse it regularly in order to be able to monitor the
evolution and when a failure occurs.

F.6 Measurement of molecules in environments


For actual measurements it is advisable to have an overlap, so that accidental
contamination can be measured twice.
a. Sensors shall be exposed during two weeks and one sensor shall be analysed
every week.
b. This measurement shall be performed at two different locations within the
area.
c. These locations shall be selected in order to measure molecules in significant
points of the environment.

F.7 Design
F.7.1 Cleanroom shell, entrances and anterooms
a. Cleanroom shell, floors, walls and ceiling shall be low-shedding and the
finish readily cleanable.
b. The floor covering shall consist preferably of one piece or, if this is not feas-
ible, it shall have the minimum number of joints necessary.
c. It shall have low shedding characteristics and be sufficiently durable to
withstand wear by personnel and operations within the room.
d. The room shall be designed such that only one door or entrance can be opened
at one time, except in case of emergency.
e. Such entrances shall provide an air lock to allow a maintained pressurisation
of the area.
f. Anterooms shall be provided as required for the changing of clothes, and the
storage of clothing, personal belongings and cleaning equipment.

F.7.2 Air supply


a. Air supply and filtration equipment shall have adequate capacity to filter all
new and recirculated air entering the room.
b. Air conditioning equipment for prefiltering (particular and molecular),
cooling, heating, humidification and dehumidification of the cleanroom air
supply shall be supplied as necessary.
c. In laminar flow cleanrooms, the air flow velocity through the cross section
of the room shall be maintained at 27 m/min with a uniformity within ± 20 %
throughout the undisturbed room. Airflow patterns shall be uniform with
minimum turbulence.

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F.7.3 Filters
a. In laminar flow cleanrooms, high-efficiency particle air (HEPA) filters shall
cover either one entire wall or the entire ceiling, except when diffusion
ceiling or wall systems are used or when built-in benches are included in the
incoming air end of the room. In the latter case, the wall filter may cover only
the area extending from the work bench surface to the ceiling. Prefilters shall
be used to prolong the life of the HEPA type final filters.
In cases where a uniform and controlled molecular environment is required
the filtering system should be equipped with additional charcoal filters posi-
tioned after the HEPA filters.
Charcoal filters can be used to filter the make-up air or even to filter all the
air that is circulating in the cleanroom (installation shall be done before
filters).
After filters are changed, airborne contamination (gas and vapour) can be
initiated by the new set of filters.
b. Monitoring shall be effected and any work with highly sensitive equipment
after the installation of new filter sets shall be avoided until contamination
has dropped below the specified acceptance level.
Similar problems recur also when the air flow is stopped and then it is
reactivated; due to the transitory pressure gradients, this operation can
cause the release of contamination previously trapped by HEPA filters,
together with a reduction in the operating life of the filters themselves.
c. As general rule, the air flow inside cleanrooms shall be maintained also
during “at-rest” periods, except for the normal maintenance operations.
d. The same attention shall also be paid to the independent HEPA filtering
systems, such as those equipped for the laminar flow tents and benches,
except if they can work with a reduced air flow rate during stand-by periods.

F.7.4 Cleanroom containers


a. Transport and storage containers shall be made of low particle shedding
materials that do not evolve contaminants.
b. Containers carrying sensitive items (optical units and payloads) shall be
pressurized with gaseous nitrogen.
c. They shall also have as rigorous a cleaning schedule as the parts themselves.
d. Care shall be taken that containers used for transportation of clean parts do
not transfer contamination from surface to surface within the cleanroom
itself.

F.8 Environmental control


F.8.1 Temperature
a. Cleanroom temperature shall be maintained at nominally 22 ºC. Tempera-
ture variations of ± 3 ºC at the control point are acceptable for most
operations, but special conditions can be imposed in case of critical
operations.
b. The temperature distribution inside a cleanroom shall be controlled to
ensure that a nominal temperature is achieved throughout the room.
Automatic devices may be used for temperature monitoring.
c. If items being worked on are extremely sensitive to temperature changes,
automatic devices with a warning system that comes into operation when a
temperature change occurs can be used.

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In practice, it is difficult to maintain a constant temperature to very close


limits in environmentally controlled areas; hence, specified temperatures
should include the widest tolerances permitted by the product requirements.

F.8.2 Pressure
a. A positive pressure differential shall be maintained between the cleanroom
and the outside. Pressure shall decrease successively between the clean-
room, entrance lock, anteroom and the surroundings.
b. The positive minimum pressure delta to be maintained shall be:
S between cleanroom and surrounding area; 1,2 mm H2O (12 Pa);
S between cleanroom and entrance lock; 0,5 mm H2O (5 Pa).
c. Pressure in all areas shall be monitored, in order to take timely corrective
actions in case of a pressure drop.

F.8.3 Humidity
The relative humidity shall be maintained at (55 ± 10)% for general applications
and shall be monitored continuously.
Humidity becomes detrimental due to electrostatic charging or surface corrosion
(see Table F--3).
Table F--3: Guide to humidity level selection

% RH
Effect
Range
0 -- 30 Serious static charge problems
30 -- 50 Safe for highly polished metal surfaces or closed
components
50 -- 65 Marginally safe for humidity sensitive products
Contaminated metal surfaces start to corrode
65 -- 80 Corrosion rate increases largely
Some plastics swell
80 -- 100 Rapid corrosion
Reduced electrical resistivity

F.8.4 Other environmental factors


Other environmental factors, such as light level, electromagnetic radiation, ioniz-
ing radiation and radioactive particles shall be taken into due consideration.

F.9 Maintenance and cleaning


a. All maintenance and cleaning activities shall be listed in a dedicated logbook.
b. A maintenance and cleaning procedure or document shall be available, along
with a planning.
c. Maintenance shall comprise regular inspections of the cleanroom, its control
facilities and its operating equipment, including calibration of all inspection
and monitoring devices (as per ECSS--Q--20).
d. Regular inspections shall be performed of the cleanroom to determine the
quality of the clean facility and to identify any contamination production or
events that are detrimental to the cleanroom cleanliness (e.g. repairs, system
modifications, replacements, filter resistance measurements, leak checks or
air speed measurements).
e. Data shall be recorded in the control documentation.

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f. All other cleanliness inspections shall be performed as required.
g. When the level of contamination becomes higher than allowed (as defined in
the cleanliness requirements specification), corrective actions shall be taken.
The decision as to whether or not to clean depends on the integration flow of
the unit within the cleanroom. Procedures shall cover the cleaning of the
following areas by gross cleaning (dust wiping, or vacuum cleaning):
S cleaning of personnel air lock;
S cleaning of equipment air lock;
S cleaning of cleanroom walls, floors, furniture, crane lifting devices and
GSE.
h. The cleanliness after the cleaning actions shall be verified by inspection (e.g.
with UV or halogen lamp).
i. Any personnel involved in cleaning actions shall be instructed by QA about
the criticality of a cleaning action within a cleanroom.
j. For any further (precision) cleaning activity within the cleanroom, due con-
sideration shall be given to the detrimental effect of the cleaning on the
hardware within the cleanroom.
k. Cleaning tools, solvents and gases that are used for cleaning purposes shall
not have a detrimental effect.
l. The frequency of inspections and cleaning processes for a cleanroom shall be
optimized since the inspections and cleaning can themselves be the source
of contamination.
NOTE Cleanroom air of better than class M6.5 is transported in a
close loop. Since only a limited percentage of fresh air is fed
to the loop, excessive use of solvents outgassing into the air,
even if not flammable or toxic, can cause health problems.

F.10 Access control


a. An access control system shall be available independently for cleanrooms,
storage area and equipment airlock.
b. The access to the areas shall be controlled by a permanently operating access
control or door lock system.
c. Only authorized personnel shall have access to the cleanroom (security lock
at the entrance). Visitors and personnel without a direct work order shall not
be allowed to enter the cleanroom.
d. Visitors, who work in the clean area, shall wear the complete clothing, shall
be identifiable as such and shall be instructed about the behaviour in a
cleanroom.

F.11 General requirements for a cleanroom


F.11.1 Equipment and hardware requirements
a. Racks or cabinets for street clothing shall be separated from those used for
cleanroom clothing.
b. Lint-free clothing shall be available and worn by all personnel within clean-
room area.
c. Head covers or other garments shall be used as required to trap loose
particles of hair or skin flakes.
d. Gloves, finger cots (of approved types), tweezers or clean handling methods
and equipment shall be used while working with or handling sensitive parts
to avoid contamination of those parts by loose skin or natural skin oils.

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e. Exhaust systems for grinding, welding or soldering, machining or related


operations shall be installed.
f. Equipment items with cooling fans are potential contamination sources and
thus appropriate actions shall be undertaken to avoid contamination of
critical hardware.

F.11.2 Procedural and behaviour aspect requirements


a. Written operational guides shall be established to avoid contamination and
degradation of the cleanliness level of an area. These guides shall include,
but not necessarily be limited to, the following requirements:
1. All equipment shall be cleaned by dusting, vacuum suction, washing, or
other means suited to the equipment involved before being brought into
the area.
2. Smoking, eating and drinking shall not be permitted in the cleanroom,
including the entering areas and air locks.
3. Local cleanroom instructions shall specify the amount of protective cloth-
ing to be worn and shall assist in minimum contaminant transfer.
4. If air showers are used, only suitably clothed personnel shall be allowed
to enter.
5. Paper, pencils or erasers shall be kept outside the clean facilities. Only
special non-shedding papers and ball-points shall be used.
6. Cosmetics and medicaments that can produce contamination shall not be
used by any personnel. In particular, eye make-up, rouge, face powder
and hair spray shall be avoided.
7. Fingernail polish shall not be permitted in the area.
8. Hand lotions, creams or soap containing lanolin to tighten skin particles
shall be used as appropriate.
9. Contact of hands with solvents shall be avoided, as many solvents remove
natural oils and cause excessive skin peeling or flaking.
10. Personnel movements to and from the cleanroom shall be kept to a mini-
mum.

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Annex G (normative)

Cleanliness requirement specification —


Document requirements definition (DRD)

G.1 Introduction
As required by ECSS--Q--70--01, this document requirements definition (DRD)
establishes cleanliness and contamination levels to be achieved at different
manufacturing, AIT and mission stages.

G.2 Scope and applicability


G.2.1 Scope
This DRD establishes the data content requirements for the cleanliness
requirement specification. This DRD does not define format, presentation or
delivery requirements for the cleanliness requirement specification (CRS), which
can vary depending on product level (i.e. equipment, subsystem and system), and
specific contractual requirements.

G.2.2 Applicability
This DRD is applicable to all projects using the ECSS standards.

G.3 Terms, definitions and abbreviated terms


G.3.1 Terms and definitions
For the purposes of this DRD, the definitions given in ECSS--P--001 and
ECSS--Q--70--01 apply.

G.3.2 Abbreviated terms


The following abbreviated terms are defined and used within this DRD.
AIT assembly, integration and test
AIV assembly, integration and verification
AO atomic oxygen
BOL beginning-of-life
C&CCP cleanliness and contamination control plan
CRS cleanliness requirement specification

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EOL end-of-life
EVA extra vehicular activity
MOC molecular contamination
PAC particulate contamination

G.4 Description and purpose


Based on system or subsystem contamination budget, a CRS shall be established
and agreed by all parties involved.
The CRS shall define and identify the spacecraft items and the environmental
areas that are sensitive to contamination; a description of the effects of contamin-
ants on performance shall also be given.
The CRS shall give the acceptable contamination levels at BOL and at EOL, and
identify the required contamination level at delivery.

G.5 Application and interrelationship


As it is of fundamental importance for the space system’s performance, the CRS
shall be defined as early as possible in the programme, in order to properly
address the design for cleanliness.
This document should be prepared in collaboration with experimenters and
engineers from the different disciplines.
In case the CRS cannot be produced at an early stage of the design, a cleanliness
control policy document should be used.
This cleanliness control policy document shall give the correlation data between
acceptable performance losses and the contamination levels from library search
or from tests that shall be performed. The cleanliness control policy document
becomes the CRS during the development of the design.

G.6 CRS preliminar y elements


G.6.1 Title
This document shall be titled “Cleanliness requirement specification for [insert
item name]”

G.6.2 Title page


The title page shall identify the project document identification number and the
title of the document.

G.6.3 Approval page


The approval page shall identify the names, titles and affiliations of all parties
who are to approve the CRS. Space shall be provided for the approval parties to
affix and date their signatures.
The title and approval pages may be combined in a single page.

G.6.4 Amendment control table


The amendment control table shall contain the
D change number,
D type of change,
D date of issue, and
D parts of CRS affected.

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G.6.5 Contents list


The contents list shall identify the title of every part, clause and major subclause,
figure, table and annex contained in the document.

G.6.6 Introduction
An introduction shall be included to provide specific information or commentary
about the technical content of the CRS.

G.7 CRS contents


G.7.1 Scope and applicability
This clause shall be numbered 1 and shall describe the scope and applicability of
the CRS. It shall include the identification of the hardware subject of the specifi-
cation and the relevant programme phases involved

G.7.2 References
This clause shall be numbered 2 and shall contain the following subclauses.

G.7.2.1 Normative references


This subclause shall be numbered 2.1 and shall contain the following statement:
“The following normative documents contain provisions which, through refer-
ence in this text, constitute provisions of this cleanliness requirement specifica-
tion:
[insert document identifier] [insert document title]”

G.7.2.2 Informative references


This subclause shall be numbered 2.2 and shall contain the following statement:
“The following documents, although not a part of this cleanliness requirement
specification, amplify or clarify its contents:
[insert document identifier] [insert document title]”

G.7.3 Terms, definitions and abbreviated terms


This clause shall be numbered 3 and shall contain the following subclauses.

G.7.3.1 Terms and definitions


This subclause shall be numbered 3.1, and shall list any applicable project diction-
ary or glossary, and all unusual terms or terms with a meaning specific to this
CRS, with the definition of each term.

G.7.3.2 Abbreviated terms


This subclause shall be numbered 3.2 and shall list all abbreviated terms used in
the CRS, with the fully spelled-out meaning or phrase for each abbreviation.

G.7.4 Description of [insert item name]


This clause shall be numbered with 4 and shall give a general overview of the item
to which the CRS refers.
In particular, this clause shall identify sensitive items and contamination
sources, in consideration of:
D possible impacts of contaminants on their physical or functional characteris-
tics;
D possible effects of contamination on the performance
D their impact as potential sources of contamination.

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This clause shall also state the pressures (or other molecular fluxes) that can be
reached in connection with voltage breakdown, arcing, corona discharges, multi-
paction, opening time of shutters and ejection time of covers.

G.7.5 Environmental factors


This clause shall be numbered 5 and shall be composed of the following sub-
clauses.

G.7.5.1 Ground environmental factors


This subclause shall be numbered 5.1 and shall basically identify major
on-ground activities and their impact on contamination. Usually, the preparation
of a flowchart helps in the description. In this case, it shall be included in an
appendix to the CRS.

G.7.5.2 Flight environmental factors (natural and induced)


This subclause shall be numbered 5.2 and shall describe the environmental
factors that affect the contamination phenomena, such as solar radiation, elec-
tron, proton and AO fluxes, together with the planned mission profile/duration.

G.7.5.3 Temperatures of items sensitive to contamination


This subclause shall be numbered 5.3 and shall provide figures for sensitive-item
temperatures. The expected temperatures of these items can be important for
condensation and the residence times of the contaminants.

G.7.6 Contaminants
This clause shall be numbered 6 and shall include the following subclauses.

G.7.6.1 Contamination sources


This subclause shall be numbered 6.1 and shall identify possible contamination
sources, such as materials outgassing, lubricants escaping from bearings, wear
particles from moving parts, terrestrial contaminants such as dust, plume
contaminants from thrusters and engines, leaks from fuel systems and from
hermetically sealed components, dumps and EVA, co-passengers, fairing and
equipment bay items of the launcher.

G.7.6.2 Chemical nature or type of contaminants


This subclause shall be numbered 6.2 and shall identify the chemical nature of
the contaminants under subclause 6.1 and eventual vapour pressures or con-
densation conditions.

G.7.6.3 Transport mechanisms


This subclause shall be numbered 6.3 and shall identify the transport mechan-
isms of the potential contaminants from the sources under subclause 6.1 to the
contamination sensitive items or areas e.g. direct flux, reflected flux, ambient
scatter, self-scatter and creeping.

G.7.7 Contamination budget


This clause shall be numbered 7 and shall provide the splitting of cleanliness
requirements through the major integration and testing phases.
Acceptable contamination levels of MOC and PAC at delivery, for the items and
areas under clause 4, and the expected contamination levels at BOL and EOL
shall be identified.

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Annex H (normative)

Cleanliness and contamination control plan —


Document requirements definition (DRD)

H.1 Introduction
As required by ECSS--Q--70--01, this document requirements definition (DRD)
defines the methods to achieve the specified cleanliness and contamination levels.

H.2 Scope and applicability


H.2.1 Scope
This DRD establishes the data content requirements for the cleanliness and
contamination control plan. This DRD does not define format, presentation or
delivery requirements for the cleanliness and contamination control plan
(C&CCP), which can vary depending on product level (i.e. equipment, subsystem,
system), and specific contractual requirements.

H.2.2 Applicability
This DRD is applicable to all projects using the ECSS standards.

H.3 Terms, definitions and abbreviated terms


H.3.1 Terms and definitions
For the purposes of this DRD, the definitions given in ECSS--P--001 and
ECSS--Q--70--01 apply.

H.3.2 Abbreviated terms


The following abbreviated terms are defined and used within this DRD.
AIT assembly, integration and test
AIV assembly, integration and verification
BOL beginning-of-life
C&CCP cleanliness and contamination control plan
CRS cleanliness requirement specification
MOC molecular contamination

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PAC particulate contamination
PMP parts, materials and processes

H.4 Description and purpose


A cleanliness and contamination control plan shall be prepared in order to set out
the ways in which the required cleanliness levels are achieved and maintained
during the life of the programme, from design to launch, and which also defines
cleanliness levels throughout the mission up to the end-of-life.

H.5 Application and interrelationship


As it is of fundamental importance for the space system’s performance, the
C&CCP shall be established as early as possible in the programme, in order to
properly address the design.
The C&CCP shall be prepared for all levels of configuration items defined in the
project at the following levels:
D system
D subsystem
D equipment
The C&CCP is based on the requirements defined by the cleanliness require-
ments specification.

H.6 C&CCP Preliminar y elements


H.6.1 Title
This document shall be titled “Cleanliness and contamination control plan for
[insert item name]”

H.6.2 Title Page


The title page shall identify the project document identification number and the
title of the document.

H.6.3 Approval page


The approval page shall identify the names, titles and affiliations of all parties
who are to approve the C&CCP.
Space shall be provided for the approval parties to affix and date their signatures.
Title page and approval page may be combined in a single page.

H.6.4 Amendment control table


The amendment control table shall contain the
D change number,
D type of change,
D date of issue, and
D parts of C&CCP affected.

H.6.5 Contents list


The contents list shall identify the title of every part, clause and major subclause,
figure, table and annex contained in the document.

H.6.6 Introduction
An introduction shall be included to provide specific information or commentary
about the technical content of the C&CCP.

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H.7 C&CCP contents


H.7.1 Scope and applicability
This clause shall be numbered 1 and shall describe the scope and applicability of
the C&CCP. It shall include the identification of the hardware (system, subsys-
tem and equipment) to be monitored and controlled through the C&CCP and the
relevant programme phases involved

H.7.2 References
This clause shall be numbered 2 and shall contain the following subclauses.

H.7.2.1 Normative references


This subclause shall be numbered 2.1 and shall contain the following statement:
“The following normative documents contain provisions which, through refer-
ence in this text, constitute provisions of this cleanliness and contamination
control plan:
[insert document identifier] [insert document title]”

H.7.2.2 Informative references


This subclause shall be numbered 2.2 and shall contain the following statement:
“The following documents, although not a part of this cleanliness and contamina-
tion control plan, amplify or clarify its contents:
[insert document identifier] [insert document title]”

H.7.3 Terms, definitions and abbreviated terms


This clause shall be numbered 3 and shall contain the following subclauses.

H.7.3.1 Terms and definitions


This subclause shall be numbered 3.1, and shall list any applicable project diction-
ary or glossary, and all unusual terms or terms with a meaning specific to this
C&CCP, with the definition of each term.

H.7.3.2 Abbreviated terms


This subclause shall be numbered 3.2 and shall list all abbreviated terms used in
the C&CCP, with the full spelled-out meaning or phrase for each abbreviation.

H.7.4 Description of [insert item name]


This clause shall be numbered with 4 and shall give a general overview of the item
to which the C&CCP is refers.
In particular, this clause shall identify sensitive items and contamination
sources, listing those surfaces/items to be strictly controlled or protected from the
cleanliness point of view due to:
D the possible impacts of contaminants on their physical or functional char-
acteristics;
D their impact as potential sources of contamination.

H.7.5 Cleanliness requirements


This clause shall be numbered 5 and shall contain the following subclauses.

H.7.5.1 Higher level requirements


This subclause shall be numbered 5.1 and shall contain a summary of cleanliness
requirements (e.g. MOC, PAC, level at delivery and at BOL), relevant for the

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system or hardware and eventual sub--assemblies, as derived from CRS or dedi-
cated analysis.

H.7.5.2 Prediction of contamination levels


This subclause shall be numbered 5.2 and shall contain the prediction of conta-
mination levels and eventually a modellization in case the outgassing contribu-
tion is large with respect to other contributions (mainly for sensitive instruments
with tight requirements).

H.7.5.3 Selection of materials and processes


This subclause shall be numbered 5.3 and shall define the requirements that have
design impacts, like: PMP selection criteria (e.g. as per ECSS--Q--70), venting,
purging and thruster locations, in accordance with the mission requirements
(cleanliness/outgassing), and with the outcome of the subclauses 5.1 and 5.2
defined above.

H.7.5.4 Corrective actions


This subclause shall be numbered 5.4 and shall describe the corrective actions in
terms of design, shielding, purging, baking in case the predictions are outside
acceptance limits and in cases where corrective actions are necessary because of
deviation from the original cleanliness policy.

H.7.6 Environment and facilities


This clause shall be numbered 6 and shall contain a brief description of manufac-
turing and AIT areas, their classification, facility location and tools for conta-
mination control.
References for internal procedures dedicated to area or facilities verification,
control and maintenance shall be included.
This clause shall also contain a list (or brief description) of internal procedures
for personnel training and rules to operate under contamination control condi-
tions.

H.7.7 MAIT activities


This clause shall be numbered 7 and shall contain the following subclauses.

H.7.7.1 Contamination allocation


This subclause shall be numbered 7.1 and shall detail the splitting of cleanliness
requirements during manufacturing and AIT (MAIT) phases, according to
planned duration, environment class, type of operation, and dedicated provisions
adopted.
In addition, this subclause shall list all phases where contamination can be
expected and where the levels can exceed the allocated levels.

H.7.7.2 Contamination control definition


This subclause shall be numbered 7.2 and shall describe methods, procedures and
instruments adopted to control contamination levels during manufacturing and
AIT activities on systems or equipment and relevant documentation; in particu-
lar:
D contamination monitoring methods and tools;
D inspection procedures and tools;
D verification of tools or hardware;
D dedicated cautions for critical AIV operations.

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H.7.7.3 Cleaning and decontamination methods and tools


This subclause shall be numbered 7.3 and shall define the cleaning and deconta-
mination methods, procedures and tools, also making reference to their applic-
ability and eventual process parameters (i.e. temperature, pressure and time for
parts bakeout).

H.7.7.4 Packing, storage and transportation


This subclause shall be numbered 7.4 and shall describe the provisions for the
transportation of critical items. Descriptions of containers and packaging tools to
be used during hardware transportation, and the way in which they have to be
stored, handled, monitored and cleaned shall to be included.

H.7.7.5 Contamination control flow


This subclause shall be numbered 7.5 and shall define:
D the sampling plan for PAC and MOC,
D cleaning operations (when planned), and
D inspection points.
The outputs of this definition should be described in the form of a flowchart,
reported in an appendix to the C&CCP.

H.7.7.6 Responsibilities
This subclause shall be numbered 7.6 and shall identify responsibilities for:
D hardware inspections,
D cleanrooms and facilities, and
D contamination monitoring (hardware).

H.7.8 Forms
This clause shall be numbered 8 and shall define the forms that are used to
document the cleanliness and contamination control activities defined by the
C&CCP.
As minimum, the following forms shall be defined:
D PAC and MOC measurement report;
D Cleanliness certificate of conformance.

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Bibliography

ASTM--E1216--87(1992) Standard Practice for Sampling for Surface Particu-


late Contamination by Tape Lift

ASTM--E1235M--95 Standard Test Method for Gravimetric Determina-


tion of Nonvolatile Residue (NVR) in Environmen-
tally Controlled Areas for Spacecraft

ASTM--E1559--93 Standard Test Method for Contamination Outgas-


sing Characteristics of Spacecraft Materials

ECSS--E--10--04 System engineering — Space environment

ESA--QME--WI--F--03 Standard test method for VBQC outgassing kinetics

ISO 15388 Contamination and Cleanliness Control

NASA SP--5076 Contamination control handbook

MIL--STD--1246C Product cleanliness levels and contamination con-


trol progam

MIL--HDBK--406 Contamination control technology cleaning ma-


terials for precision precleaning and use in clean-
rooms and clean work

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ECSS Document Improvement Proposal


1. Document I.D. 2. Document date 3. Document title
ECSS--Q--70--01A 11 December 2002 Cleanliness and
contamination control
4. Recommended improvement (identify clauses, subclauses and include modified text or
graphic, attach pages as necessary)

5. Reason for recommendation

6. Originator of recommendation
Name: Organization:
Address: Phone: 7. Date of submission:
Fax:
e-mail:

8. Send to ECSS Secretariat


Name: Address: Phone: +31--71--565--3952
W. Kriedte ESTEC, P.O. Box 299 Fax: +31--71--565--6839
ESA--TOS/QR 2200 AG Noordwijk e-mail: [email protected]
The Netherlands
Note: The originator of the submission should complete items 4, 5, 6 and 7.

An electronic version of this form is available in the ECSS website at: http://www.ecss.nl/
At the website, select “Standards” -- “ECSS forms” -- “ECSS Document Improvement Proposal”

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