Fatigue Design Da For The Titanium Alloy, Ti-6Al 6: Ta .: V-2Sn
Fatigue Design Da For The Titanium Alloy, Ti-6Al 6: Ta .: V-2Sn
- -- . ~
-
KAPL-3158
AEC Researclt and
Development Report
KNOLLS
ATOMIC POWER
LABORATORY
\
Fatigue Design Data
-
. for the
--
Titanium Alloy, Ti-6Al .:6 V-2Sn
D.F. Mowbray
GENERALfJ ELECTRIC -
-
PATENT REVIEW APPROV
GOVERNING PATENT REV~SWRELEASE. PROCF.DURES
FILE IN RECEIVING SECTIQ['(. AND R~l,,I~AS~ A~ QN
DISCLAIMER
KAPL-3158
UC-25, Metals, Ceramics, and
· Materiais ··
(TID-4500, 49~h Edition)
._ .
'··
FATIGUE ·DESIGN DATA FOR THE' TITANIUM A.J.;UJY, Ti-6Al-6V-2Sn
D. F. Mowbray
\ __I_:_E_:_E_:_:_.:_.:_R_F_:R_c_I ~_ :_,
:_:_U_:"":"':_:_:_:_:_:_r_s_\
••
~uthorized Classifier
.1,M o?~ Date
/f le?
General Electric Company
KNOLLS ATOMIC POWER LABORATORY
Schenectady, New York
Operated f.or the
United States Atomic Energy Commission
Contract No. W-31-109 Eng-52
UNCLASSIFIED
UNClASSIFIED ·
t.EGAt NOTICE
UNCLASSIFIED KA.PL-.3158
ii
UNCLASSIFIED
KAPL-.3158
UC-25, Metals, Ceramics, and
Materials .
(TID-4500 1 49th Edition)
(Nonstandard)
DISTRIBUTIO~
No. of popies
AEC 1 SNR
Cramer, CC J
Baldwin, EE 2
Div:J.sion of Ter.hni t>,Al Tnfnrmet.i.nn F.xt.P.md.nn J
· Document Library 4.'
Jekkals 1 I lr
Ferril_, D 1.
G.lasser, TH 1
Kelleman 1 RW 1
Miles, A 1
McCalley, RB 1
Mehringer~ FJ 1
Miller, DR 1
Mowbray 1 DF . . 5
Naval Reactors Library 2
Shriver,. PR. 1
Sokol, GJ '1
Technical ~~blications/JG Shaw 1 ·.-- .
TIG File/CJ Schmidt 5
Total
-·
J5
UNCLASSIFIED
iii
'i
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CONTENTS
~
ABS'rRACT • ix
NOONQLATURE . xi
INTRODUCTION 1
TEST DESCRIPI'ION · • 1
Material • .. 1
Sped.mens • . ~ 2
Test Equipment and ProcedUre 5
· TEST .RESULTS . .. 6
..DISCUSSION OF TEST RESULTS • 10
. Unnotched Fatigue Strength • 10
Effect or Mean Stress on Unnotched Fatigue Strength • 14
Notch-Sensitivity • 17
SUMMARY AND.CONC~USIONS. .. 18
REFERENCES 19
APPENDIX .A. MAXIMUM EFFECT OF MEAN STRESS BASED ON A PARABOLIC
DAMAGE LAW •. 21
v KAPL-.Jl5G
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ILLUSTRATIONS
No.
1·
Title
(0002) Pole Figure for the ~Phase of Rolled 1.0-in.-diam.
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Page
vii KAPL-3158'
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ABSTRACT
ix
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NOMENClATURE
*Fictitious stress.
xii KAPL-.3158
..-
D. F. Mowbray
INTRODUCTION
The application of high-strength titanilDil alloy, ~i-6Al-6V-2Sn, is
being increased in the nuclear industry where fatigue loadings are com-
monly encount~red in the low- and intermediate-cyclic-life regions over
the ;ra:nge of .temperature from 75 to 600F.. T9 assist in the design of
components fabricated from bar stock of this alloy, an investigation was
•Jndertaken to (letermine sam~ of the baai.c fatigue properties' at the
cyclic lives and temperatures of interest. Displacement-controlled tes-ts
were conducted on unnotched specimens to establish fatigue c'urves and
the.so called "maxim\Dil effect of mean stress" over the cyclic life region
of -10 2 to 106 .cycles;, load-controlled tests were conducted on notched
spec~ens to determine fatigue notch factors for several different
geometries at 106 .cycles. An equal number of tests were conducted at
both 75 and 600F.
TEST DESCRIPTION
Material
The material used in this investigation was the titanium base alloy
designated.Ti:-6Al-6V-2Sn.l. This titanium alloy is double-vacuum...melted
by consumable electrode·techniques. The material was obtained as 1.0-in.-
diameter hot-rolled bar stock in the ful~y annealed condition. The anneal-
ing treatment consisted of heating in vacuum at 1300F for 2-1/4 hr,
followed by an air cool.
· ·The chemical composition was as follows:
Element wt %
Aluminum 5.6
Va.nadium 5.5
Tin 2.0
Iron o. 76
Copper 0.71
Oxygen 0.155
Carbon 0.023
Nitrogen 0.018
Hydrogen. 0.0053
Titanium Remainder
1 KAPL-3158
2
BAR AXIS
_I_
I
t----2.900---~
DIMENSIONS IN INCHES
KAPL-3158
4
t-------- 4t ------..-1
0235.
•.0233
~I::=::.=:::ttJ,._-Ju
0-001 in. ROOT
radius
A. Small Diameter.
~
~~------~-------- 6-------------~
~-----~
-------~----fl~tln_l~_. . ,: -~-
-=-=-=-
F"==""=-- - -
I· in-12 UNF-2A
THREADS
NOTCH DETAIL
B. Large Diameter.
KAPir3158
,,,
All specimens were machined from the fulzy annealed bar stock. The
machining was performed carefully to prevent _excessive residual stresses
on the specimen surface. After machining, the test-section surfaces of
the unnotched specimens were polished with 600-grit paper in the longi-
tudinal direction. The grooves in the notched specimens were finish-
machined by a lapping operation which minimized the presence of machining
scratches transverse to the test,direction. Following final.machiniog,
the specimens were given an additional 2-hr vacuum-anneal at.l.)OOF (vacuum
was maintained·at 10-5 mm Hg).
Test Equipment and Procedure
The test work in this investigation was conducted by Lesseils and
Associates~ Inc.~ Waltham, Mass. The description of the ·test equipment
and proced~e to follow is abstracted from their data report.
The displacement-controlled tests were conducted in a test machine
which has a rigid frame containing the specimen grips, the lower grip
being driven by a rotating eccentric which m~ be set for any desired
displacement amplitude. The upper specimen grip consists of a cylindrical
rod threaded at its lower end to accept the specimen. It is free to slide
vertically within a hole in the upper frame, except when clamped by screws
on the split, upper crossbar of the frame. The lower grip slides in the
lower .crossbar of the frame, being guided by a very close fit with a
cylindrical impregnated bearing which is pressed into the cross member.
Attached to the bottom of the lower grip is a flex plate, below which is
a push bar instrumented with strain gages for load measurement. The
machine cycling rate is. variable. from 18 to 600 cpm. A cycling rate
of 120 cpm was used for the tests at the lower strain amplitudes and a
rate of 18 cpm at the higher strain amplitudes.
· Specimen strain was me<:u:~w•ed by one of several methods. . In tests
conducted at room temperature at strains <1.9% range., strain. gages were
attached directly to the specimen test sections. Values of strain re-
ported for these tests were the first-cycle strain-gage readings (i.e.,
no variation of strain range ·was noted during the tests). In four tests
conducted at each of the two test temperatures at strains ?4·0% range,
strain was measured by means of a diameter transducer gage, incorporating
an LVDT. Values of strain reported for these tests are transducer
readings at shakedown (the first cycle at room temperature and approxi-
mately the lOOth cycle at 600F). This diameter-transducer gage was also
·used to measure strain in the remaining 600F tests (<1. 5% range), but
the gage was not considered by the author to yield sufficiently accurate
measures of the strain. Consequently, the 600F strains reported at <1.5%
range were determined by dividing the P/A stress by the elastic modulus.
In all of these tests, the material appeared to remain elastic.
6
Signals from the load transducer, specimen strain gages, and diameter
tr~nsducer were amplified and record.edon a Honeywell Visicorder. Records
w.ere made during the first twenty cycles and periodically thereafter.
A small split-shell resistance furnace with appropriate thermocouples
and an indicating pyromet~r-controller were used for the elevated-
temperature tests. At 600F, the temperature gradient along the specimen
test section was < 5F.
The load-controlled tests were conducted on a Schenk six-ton vertical
fatigue machine. This machine incorporates automatic control of the
alternating load, and the temperature in a three-zone f~nace when test-
ing. at elevated temperatures. At the 600F operating level, temperature
level and test-section _temperature gradient were within ±2F.
The purpose of the notched tests was to evaluate Kf only at 106
cycles. To accomplish this, six to nine specimens pf each not'ch geometry
were tested at each of the two test temperatures. Attempts were made in
testing each group of' specimens to fail some qf the specimens below 106
cycles, some above 106 cycles, and some as near 106 cycles as possible.-
Yalues of Kf were then evaluated by plotting the six data points on an
vs cycles-to-failure coordinates, joining a mean line through the points,
determining the value of on corresponding to the mean line at 10 6 · cycles,
and dividing the unnotched value of Sa at 106 cycles by an at 106 cycles.
Specimen failure was considered to be complete specimen separation.
Use of a dispJ,.acement-controlled unnotched test result and a load.::.
controlled notched test result for determining Kf is justified in this
case.-by virtue of the fact that the fatigue stresses at 106 cycles to·
failure were strictly elastic. This can be observed in Figure 4 where
the cyclic and monotonic (static) stress-strain response at the two test
·temperature are plotted. The values of elastic modUli used for con-
structing the elastic portions of the curves were 15.0 x 106 psi at room
temperature and 1,3.6 x 106 psi at 600F. These values are in ·agreement with
~namic test results obtained for the test material, dynamic values
reported in Reference 1, and static stress and strain measurements made
on the unnotched fatigue specimens at room temperature.
TEST RESULTS
The results of the room temperature .and 600F unnotched fatigue tests
are listed in Table 2, and plotted in A and B of Figure 5 in terms of
fictitious stress amplit"1,lde (E€a/2) and cycles to failure. Part A of
Figure 5 presents the room teJ!iperature data and B of Figure 5 the cor-
responding data at 600F. Best-fit curves have been faired (by eye)
through the data points for the fulJ.i-reversed cycle tests (zero pre-
strain) -to establish S-N curves over· the range of cycles from "'10 2 to 106 •.
. KAPL-.3158
7
-----
MONOTONIC
RESPONSE AT 600f
(J)
(J)
w
a::
f-
(J)
AMPLITUDE , %
Data points for tests in which a 1.0% prestrain was superimposed are
plotted in A and B of Figure 5 as solid points. The effect of the tensile
prestrain is to reduce the cyclic strain"required for failure in a given
number of. cycles at lives >5 x 10 3 • These reductions can be considered
appreci.able, particularly at room temperature. For materials Uke the
present one, which possess high ratios of yield-to-ultimate tensile
strength, this result should be anticipated.
In Table 2, the results discus~ed .above are ~lso reported ·in 'tenns
of strain range, which was the controlled test variable. Va;t.ues of
eias"Lic moduli uiled for converting strain-range to fictitious stress-
amplitude are those quoted in the previous section.
KAPL-.3158
8
o ZERO PRESTRAIN
e 1.0% PRESTRAIN
- INDICATES NO FAILURE
I06 r-~r-TO-rrnTr---r-r-rrrnTr-~r-TO-rrnTr--,--,_,rn~--~~~~~
',.
''<'
---·--·
.
CORRECTION FOR _/"
MEAN STRESS (EQU. A.5) ',_
_________ ,a:__ _
..._..__
A. At Room Temperature.
''....:
CORRECTION FOR )',
MEAN STRESS (EQU. A.5) .. , ee e
,_
---- -----
/
......
.
....----~-
104~--~--~~~~~--~~~~~~~-L~~~--~~~wu~~~~~-L~~
~2 ~ ~
CYCLES TO FAILURE
B. At GOOF.
KAP!r3158
UNCLASSIFIED
QQNPlB'SNl'IAL • 9
600
0.50
0.44
0.42
34,300
30,100
28,800
1
1.0
28.4
36.9
310.0
.UNCLASSIFIED
- KAPI.r-3158
10
The results of the notched specimen tests are listed in Table 3 and
plotted in Parts A and B of Figure 6 in terms of stress amplitude and
cycles to failure. Part A of Figure 6 includes the data at room tempera-
ture and B of Figure 6 the corresponding data at 600F. · Best-fit curves
have been faired (by e,ye) through the data points for each notch geametr,y.
. : The values o~ Kr at 106 cycles derived from the notched and un-
not'ched tests· are listed in. Table 4; Also listed are values of the
notch se~sitivity factor 2 (q) defined as: ·
Kf - 1
q =
K' ~ 1
t
This factor is a commonly used index for.judging the notch sensitivity·of
materials in fatigue. It provides a scale of notch sensitivity that
varies from q = 0 1 or no notch effect, to q = 1 1 or full theoretical
effect. Plots of. q vs R for roam temperature and for 600F are shown in
Figure 7.
Attention is directed again to the stress-strain diagrams plotted in
Figure 4· Note that the cycling did not alter the stress-strain behavior
at roam temperature (i.e., no cyclic hardening or softening), whereas at
600F the cycling caused a slight hardening. All the cyclic s~ress-strain
data points plotted are first-cycle values except for the four at 6dOF
which show a deviation from the monotonic curve. The stress values for
these points correspond to the lOOth cycle, where the peak-load valu,es
generally occurred.
KAPL-3158
UNCLASSIFIED
G@N~IQENTIAis "* 11
I
20,000 1J6.0
17,000 261.0
0.001
1
0.160
17,000
17,00C
17,000
lO,OOO.C
1, 550.(1
282.0
None
l
25,000 J9.6
20,000 1JO.O
18,000 UJ.O
15,000. £60.0
J
0.0015 0.480
10,000
10,000
9J2.0
529.6
0.005 0.480 20,000 75.0
15,000 192.0 :.
15,000 400.Q
15,000 1,510.0
i.4,000 285.0 .-
1
0.005
1
0.480
lJ,OOO
12,000
10,000
·8, 140;0
15,110.0
12,020.0
None
· Nc;me
75
600
1
0.015
0.001
I
0.480
0.160
25,000
22,500
22,500
20,000
,15,000
17,000
149.0
1J,OOO.O
J4J.6
21,960.0
9,.320.0
.340.0
None
None
None.
I
17,000 JlJ.O
17,000 32.8.0,
1
0. (X)l
0.0015
0.160
0.1.80
17,000
20,000
20,000
12,000
7,54().0
1,7.0
104.0
5'iU.'O
None
10,000 .527.0
I
0.0015
U.!JU5
I
0.480
0.480
·10,000
10,000
9,000
.9,000
8,ooo
15,000
551.0
46J.O.
5'n.O
8,000.0
4,490.0
81.0
None
-
I
15,000 186.0
12,000 241.0
12,000 . JJ7.0
1
0.005 0.480
12,000
12,000
12,000
822.0
921.0.
8,220.0 None
o:o15 0.480 22,500 . 85.J
22,,ao 89.5
20,000 149.0
:w,ooo 2,320.0
600
J
0.015
1
0.480
20,000
.20,000.
5;090.0 .
.5,JOO.O
..,
20
0=0.160 in.
10 R=QOOI in.
0
30
20 0=0.480 ....
R = 0-015 in.
10
0
0=0.480 in.
R=0.005 in.
30
·;;;
..... 20
ILl
0
:::>
1- 10 0=0480 in.
:J
. [l.
R =o:ool5 in.
·:IE
•<t
0
•, ~
. (/)
"(/)
A. At Room Temperature.
ILl
a:
1-
(/)
30
C)
z 2
~ 0 =0.160 in.
o-
<t
z R =0.001 in.
,,,a:
1-
...J
<t
30
-G)--
20 0
o~o4eo in.
10
R =0.015 in.
0
B. At .600F.
KAPL-3158
13
Notch -Notch
·Radius,· Diameter, . 5
T~perature, F in. · in. •xt
~ ~
Kr Kr
~-
_q
.. '
1,1
>-
-~ 0.6
--
i=
~ 0,5
---
Vl
J: 0,4
~
-~ 0.3
0.2
0.1
KAPL-Jl58
14
0 Ti-6AI-6V·2Sn, 75°F
0 Tf-6Af-6V-2Sn,600"F
6 Tf-6AI-4V, 80°F (REF. 3)
1()3 104
CYCLES TO FAILURE
KAPL-3158
15
'/YIELD LINE
,.
'
''
z s I -------
C)
~
~
z
a ,., LINE
I '
ffi I '
~ I
I
'
'
~
sm 'sb Su
MEAN STRESS ---...
LINE:
PARABOLIC LINE
I ''
''
''
Sm ' Sb Su
MEAN STRESS --+
B. Gerber Parabolic Diagram.
KAPL-3158
17
Attempts to describe the titanium data with the Goodman law in the
method for estimating the maximum effect of mean stress did not yield
satisfactory results. The correction to the fatigue curve 'fell well
belowthe experimental data. For this reason the Gerber law was employed
with the same method to see if a better description of the data could
be achieved. The results are shown in A and B of Figure 5 by the dotted
lines. One· can observe that the maximum effect of mean stress concept
incorporating the Gerber parabolic dam~e law produces a.fairly good
description of the test. data, although it appears conservative in the
very high cyclic life region. Values of ~ and Su used were 150,000 and
160,000 psi at room temperature and 120,000 and 1.30,000 psi at 600F. An
·equation expressing the maximum effect of mean ·stress in terms of the
Gerber law is derived in Appendix A.
· Notch Se:nsi 1-.5vi.ty
The high values of Kf (a maximum value of 5.9) determined by the
fatigue tests and the steep rise in the q vs R curves of Fi~ure 7, at
the low values of R, indicate that this 9articular titanium:alloy has a
high fatigue-notch sensitiyity. At notch· radii~ 0.005 in., the room-
temperature fatigue-notch sensitivity is comparable to that of heat-
. treated steel having a .tensile strength of 200,000 psi; 9 th~ 600F notch
sensitivity is comparable to that of heat-treated steel having a tensile
strength of 125,000 psi. 9 There is, however, same relaxation in the
high-notch sensitivity at the larger radii, as the values of q are less
at R = 0.015 in. than at R = ~.005 in. For most mat~rials,the q vs R
curve does not achieve a maximum, but continues to rise with increasing
R,.as,ymptotically approaching a q value of 1.0.·
Another method used fo~ expressing the fatigue-notch sensitivity of
metals is the e-concept •. The 8-concept is based on the premise that the
stress at some finite distance, 8 1 below the notch root is the stress
which limits fatigue life.. The concept considers that because metals are
granular structures·and because fatigue cracks initiate on slip planes in
the grains, it should be necessary to increase the elastic stress amplitude
·so that the fatig~e limit below the notch root is. exceeded to some·finite
. depth, which is de[loted 8.. By considering a finite volume of material
below the notch root, the 8-concept takes into consideration stress
gradient effects.• · That is 1 it predicts that Kf increases as the net-
section thi'ckness increases, and that Kr is a maximum· for some value of ,
notch-root radius >0.
The 8-concept is especially ·useful for estimating the fatigue..,r:lotch
factors for crack-like defects. Experimental values of Kf are generally
not available for· crack-like defects for which R -o and Kt- oo. A paper
by 0' Donnell and Purdy-~ 0· ·demonstrated the use of the 8-concept for
KAPL-3158
18
KAPL-3158
19
REFERENCES
1. Titanium. Engineering Bulleti-n No. 10~ "Properties of Ti-6Al-6V-2Sn,"
Titanium Metals Corporation of America.
2. Peterson~ R. E. Stress Concentration Design Factors. New_York:
John Wiley and ~6ns, lnc. 195J.
3· Manson 1 s; S., and M. H. Hirschberg. "Fatigue Behavior in Strain
· Cycling in ·the Low- and Intermediate-Cycle· Range." Fatigue - -!!!,
Interdisciplinary Approach. Syracuse University Press. 1964.
Pp. 133.-173.
4· Richards, c. w. Engineering Materials Science. Wadsworth Publfshing
Company~ .Inc. Pp. 356~360.
5. !anger, B. F. "Design of Pressure Vessels for ).ow-Cycle Fatigue."
J .. of Basic Engr· ~ September 1962. P. 389.
6. 0' Donnell, W. J. ~ and B. F. Langer. , "Fatigue Design Basis for .
Zircaloy Components." Nuc. Sci. and Eng. ~ 1964. Pp._ 1-12.
7. Mowbray, D. F. "Effects of 1.0% Superimposed Mean· Strai~ o~ the
Bending Fatigue Strength of Zircaloy=4·" Nuclear Applications, l·
February 1, 1965. Pp. 39-48. · · ·
8. Mowbray 1 D. F.~ G. J. Sokol, and R. E. Savidge. "Fatigue Character-
istics·of Ni-Cr-Fe Alloys with Emphasis·on Pressure Vessel-Cladding."
KAPL-3108. July·l, 1965. ·
9. Peterson, R. E. "Analytical Approach to· Stress Concentration Effeat
of Aircraft Materials." WADC-TR ... 59-507. August 1959. Pp. 27.3-299.
10. 0' Donnell, W. J ., and c. M. Purdy. "The Fatigue Strength of Members
Containing Cracks·." ASME Trans.·~· May 1964. P. 205.
11. Neuber, H. "Theory of ~etch Stresses~ Principles for Exact Calcula:..
tion of Strength with Reference to Structural Form and Material~"
AEC-TR.:.4547. 1961.
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21
=1 (A.l)
••
To determine an expression for the so-called "maximum effect of mean
stress," the point of ~ntersection of the yield line and parabola defined
by·:·Equ.at:l.on A.l must bed:ocated as shown in Part B of Figure ·9, p. 16.
The equation of the yield line is
·
s"a = s.."-1> ~ sm (A.2)
Upon solving for Sm in Equations A.l and A.2 and equating, the following
;relationship ·results:
(A.J)
s' = (s_ - s~ .) + s
a \.,_b 2Sa. ·u
s~ )
- -
2Sa
+ s u. . · . (s~
-
4S 2
. a
+ 1
·~ - 5t>'
-
· Sa
for Sa < s.. .
-o
:(A. 5)
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23
•'1.•=
TL - K(b I RI lJ I T} = Kf6 .
.
(B.2)
,.-- ~
~
......... IY -R
-
~
T ..._ D jT
I -
. ~
-
.P
The von Mises criterion of failure was used to take into considera-
tion the multiaxial fatigue stresses in the vicinity of the notches.
Considering the radial stress component as negligible, Kf can be ex-
pressed by the von Mises criterion as (considering fatigue rather than
yielding):
1 (B. 3)
J2
KAPL-3158
/
24
= (Ks = l}(Ktn - 1) .
~ ""' 1 + =~=,..,....==-=~~=~ (B.4)
n ~(Ks - 1)2 + (Ktn = 1)2
2. Tangential stress
(B. 5.) .
where
I
Ks = 1 +
cosh u 0
=---~-~...;;,.,.-
uo (.e 21l0. ':" 3~ ( 1 + 2-._ cosh u )
[e 2 .Jcosh2u - i
2(cosh2 u + 1)
KAPL-3158
25
. 1
sinh llo = -;:===- (B.9)
. . .JT/R - 1
. 1
{c+ 21!( -1 + v) }
Ktn = vl- [(1- 21J~ sin vo]'
--.
(B.l2)
. · C = .B ~ E cos 2 v0 (13.14)
1 [ 1 + cos '170 ]
=- ~
(B.l5)
E 1 +. 2v cos v + cos 2
0
v
0
1
cos v 0 = .. .., (B.l7)
. · ~D/2R -t ·1
· KAPL-3158.