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    CoA SB8930.50MG

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    CoA SB8930.50MG

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    cnsx.psc1
    4 views3 pages

    Original Title

    CoA_SB8930.50MG

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    4 views3 pages

    CoA SB8930.50MG

    Uploaded by

    cnsx.psc1

    Copyright:

    © All Rights Reserved
    Download as PDF, TXT or read online from Scribd
    Download as pdf or txt
    of 3

    page 1 of 2

    Version1

    CERTIFIED REFERENCE MATERIAL


    Organic substance

    Ref No: SB8930.50MG Lot No: XXXXXX Certification Date:XXXXXX

    Barcode: XXXXXXXX

    Description of the Reference Material (CRM): Thiobencarb

    CAS No: 28249-77-6 Emperical formula: C12H16ClNOS MW: 257.779

    Certified Purity/ Uncertainty: 98.5 +/- 0.1 %

    Storage Conditions: Store in a freezer at -18°C or below

    Expiry date: XXXXXXXXXX

    Method of certification: CRM's calibration procedure (WQP 5.15.1/22)

    The following methods of analysis are used to determine purity: HPLC

    Analytical Data:
    Column: Chromolith® Performance RP-18e Gradient elution A% B%
    4.6x100 mm, 2µm particle size (time):
    Mobile phase: A: Water B: Acetonitrile 0 80 20
    Flow rate: 2.0 ml/min 7 0 100
    Column temperature: 20 °C 8 0 100
    Injection volume: 10µl 9 80 20
    Detector DAD 11 80 20

    Concept of Certification and traceability statement:


    The reported expanded uncertainty of measurement is stated as the standard uncertainty of measurement
    multiplied by the coverage factor k = 2, which for a normal distribution corresponds to a coverage probability
    of approximately 95%. The standard uncertainty of measurement has been determined in accordance with
    EA 4/02.
    Metrological traceability is established through in-house validated method.
    The measurement results are traceable to SI.

    Intended use:
    For Laboratory Use Only
    This CRM is intended for:
    page 2 of 2

    Calibration of TLC, GC/FID, GC/TCD, GC/ECD, GC/MS, GC/MS/MS, LC/UV, LC/MS and LC/MS/MS
    Validation of analytical methods
    Preparation of "working reference samples"
    Detection limit and linearity studies
    This statement is not intended to restrict the use for other purposes.

    Instructions for the correct use of this reference material:


    This CRM can be used directly or can be diluted in an appropriate solvent. Only a clean glassware should be
    used.

    Stability and storage:


    This CRM is with a guaranteed purity +/- 2% deviation prior to the expiration date. Stability is guaranteed,
    provided that the material is kept in its original packaging, tightly closed stored, as written in the section:
    Storage Conditions.

    Hazardous situation:
    The normal laboratory safety precautions should be observed when working with this CRM.
    Further details for the handling of this chemical are available as safety data sheet.

    Level of homogeneity
    The material was tested for homogeneity by analyzing randomly selected samples according to an in-house
    procedure. The level of homogeneity proved satisfactory for a sample volume of min. 2 mg. The uncertainty
    incorporates the sample standard deviation combined with the uncertainty calculated from homogeneity and
    stability studies.

    This certificate relates solely to the lot number given above.


    All processes (including generating of this certificate) are completely controlled by the specialized Computer-
    Aided-Manufacturing (CAM) software.

    This Certified Reference Material was produced under a quality management system that is:
    - Registered to ISO 9001 Quality Management System (Lloyd's Register Quality Assurance Ltd Cert No
    0039638)
    - Accredited according to ISO/IEC 17025
    - Accredited according to ISO 17034

    This document is designed and the certified value and uncertainty are determined in accordance with ISO
    Guide 31, ISO Guide 35,and Eurachem / CITAC Guides

    Names of certifying officers:

    Laboratory: Margarita Dimitrova

    Manager: Krassimira Taralova

    End
    Peak Integration Report

    Sample Name: Thiobencarb_41484586 Inj. Vol.: 10.00


    Instrument Method: Chromolith short
    Inj. Date / Time: 26-Oct-2022 / 23:50 Run Time: 11.00

    No. Time Peak Name Peak Type Area Height Rel.Area


    min mAU*min mAU %
    4 5.46 Thiobencarb bMB* 85.567 1290.416 98.52
    TOTAL: 85.57 1290.42 98.52

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