Cooling System and Temperature Control of an Enclosure
Cooling System and Temperature Control of an Enclosure
Cooling System and Temperature Control of an Enclosure
15-22
https://doi.org/10.46904/eea.24.72.1.1108002 15
Abstract
Reaching of negative temperatures for various applications such as food industry, medicine or experimental physics
implies the use of cryogenic fluids (especially liquid nitrogen) or refrigeration heat pumps. The technological
progress in materials science in the last years allowed the development of other methods to obtain low
temperatures needed for such applications, by means of using the Peltier effect. The Peltier modules were
developed and perfected in last decades, in order to allow temperature differences of 20 ºC to 85 ºC between the
two faces of one module when one side is kept at room temperature, and an electric current is supplied. Thus, the
possibility of developing devices which allow obtaining and controlling temperatures up to -50 ºC were opened,
eliminating all the difficulties related to the use of cryogenic agents, which imply the need of Dewar storage
vessels, cryogenic transfer lines and controlling of cryogenic liquid such as liquid helium or liquid nitrogen (with
boiling temperature of -196 ºC, at atmospheric pressure) or refrigeration systems. In this work are presented the
design, execution and testing results of a thermally controlled enclosure aimed for the calibration of temperature
sensors, in the range of -50 to +20 ºC, using Peltier modules. Despite the high electric power consumption of the
Peltier modules needed to cool down the enclosure due to the low COP (coefficient of performance) compared to
the conventional refrigeration systems, this approach in obtaining negative temperatures presents important
advantages such as the lack of maintenance, low volume, simplicity of temperature control and high temperature
stability (0.1 ºC).
used. The use of this type of technology brings several modules being used to lower the temperature of
advantages over the other methods. Thus, photovoltaic panels in order to increase their
implementing it is much simpler, is more reliable, do efficiency [13], [14].
not involve using of moving parts and does not require
periodic maintenance [2]. In this case, temperature The modern Peltier modules are based on Bi2Te3
control is quite easy to achieve, by controlling the semiconductor, which is the most common used
supply current of the modules [3]. semiconductor used for common applications [3].
Peltier effect was first discovered in 1834 [4] and A thermo-element consisting of an n-type and a p-
is described by a temperature gradient at the type semiconductor is defined by the maximum
junction interface of two metals, when an electric amount of heat that it can extract (the cooling
current is applied [4]. At the middle of 20th century, power), this being described by the following
after the discovery of semiconductors, it was found equation [15]:
that the use of semiconductor is much more effective 1
for achieving the Peltier effect [4]. Today, all the 𝑄𝑄𝑐𝑐 = �𝑆𝑆𝑝𝑝 − 𝑆𝑆𝑛𝑛 �I𝑇𝑇𝑐𝑐 − 𝐼𝐼 2 𝑅𝑅 − 𝑘𝑘(𝑇𝑇ℎ − 𝑇𝑇𝑐𝑐 ). (1)
2
commercial Peltier thermo-elements (Peltier
where Qc being the cooling power [W], Tc and Th are
modules) are made with semiconductors.
the cold and respectively hot side temperatures of
The thermoelectric cooling method (using Peltier
the Peltier thermos-element [K], k is thermal
modules) has a significant advantage, due to the fact
conductivity [Wm-1K-1], R is the total electric
that can cool an object (or an environment) without
resistance of the p and n semiconductors, I is the
using moving parts or other constructive elements
electric current supplied and Sp and Sn are Seebeck
that isolate the system from the environment. These
coefficient of the p and n semiconductors.
devices are called generically Peltier elements or
Thus, the figure of merit Z, which describe the p-
thermo-electric coolers (TECs). Peltier elements can
type and n-type Peltier thermoelement performance
be connected in series or in parallel configuration, to
is [15], [16]:
build more complex Peltier modules with higher
cooling capacity. The temperature difference �𝑆𝑆𝑝𝑝 −𝑆𝑆𝑛𝑛 �
2
An outer cooling unit for the water is required in Another important result of the numerical model
order to maintain to a constant value the water of the enclosure was to evaluate how fast the
temperature. enclosure will reach desired temperature.
The lower the water temperature, the more In order to evaluate the time needed for the
efficient the operation of the Peltier elements will enclosure to reach the desired temperature, the
be. numerical modelling solution of the enclosure
equipped with 18 thermocouples was performed for a
3.3. Numerical modelling
time period of 10 hours.
A geometric model of the thermostatic enclosure Thus, the time required for the enclosure to reach
equipped with 18 Peltier modules (distributed in the imposed minimum temperature of −50 °C was
group of 3 modules on each side) was designed and found to be −3.5 hours.
used in order to numerically evaluate its thermal
profile, and the heat load of each Peltier module was 3.4. System description
set to 3 W. The enclosure body of the cylindrical shape was
The mathematical model used to determine the made of aluminium and on the top of it there was a
temperature gradient along the z-axis of the heat-insulating cover, to assure a proper thermal
enclosures wall is [22]: insulation from the ambient, and a constant and
uniform distribution of temperature along its entire
𝒒𝒒 = −𝑘𝑘∇T (5)
volume.
where q [Wm-2] is the conductive heat flux, T [K] is The geometrical parameters of the enceinte are
the temperature and k [W/(m·K)] is the thermal obtained as a result of the total volume imposed by
conductivity of the material used. the application (Table 1).
In order to achieve uniform temperature inside
the enclosure (low temperature gradient), the Table 1. Characteristics of the enclosure
temperature distribution along the enclosure Z axis De = 200 mm Exterior diameter
need to be kept at low as possible (the heat absorbed Di = 190 mm Interior diameter
by the Peltier modules need to be uniform along the h = 190 mm Height
enclosure walls). For this reason, numerical
evaluation, using FEM technique, was performed. The dimensions of the enceinte were designed
The temperature distribution along the enclosures taking into account the type of sensors subjected to
z-axis was obtained after numerical evaluation calibration, which is in fact, the goal of the project.
(Figure 3). The enclosure assembly is equipped with
18 Peltier modules mounted in groups of 3 modules at
the exterior wall, each group consist of 3 modules.
To ensure a good thermal conductivity and
implicitly to minimize the thermal contact resistance
between the Peltier modules and the body of the
enclosure, a thermal conductive grease was applied,
the thermal conductivity of the paste is 8.5 Wm-1K-1,
and a temperature range from −50 °C to +80 °C.
The temperature controlled the enclosure
assembly (see Figure 4, infra).
The heat of Peltier modules is removed with
6 water heat exchangers made from copper, one for
each group of 3 modules, each heat exchanger is
being equipped with water inlet and outlet
connectors respectively, with a 16 mm diameter, to
Figure 3. Temperature distribution along the enclosure z-axis ensure a good water flow.
The attachment of the heat exchangers to the hot
The goal of the numerical model was to establish
surface of the Peltier modules was also done by
the optimal distribution of the Peltier modules along
thermal conductive grease.
the exterior walls of the enclosure.
Also, these are mechanically attached to the body
As showed (Figure 1, supra), a temperature
of the enclosure with 3 mm diameter screws, and
gradient, along the z-axis (the generator of the
PTFE gaskets was used between the screws and the
enclosure) of 0.9 °C, was found as a result of the
body of the heat exchangers, in order to reduce the
numerical model, the vertical lines at the edges of
conduction heat flux among the body of the enclosure
the graph represent the edges of the enclosure (upper
and the heat exchangers.
and lower end of the enclosure).
The temperature, at the beginning and the end of
the graph (corresponding to 0 mm-360 mm arc
length), is higher due to poor insulation at the top
and bottom of the enclosure.
In order to reach the low temperatures in the The temperature inside the enclosure was
experimental set-up (Figure 6), the air inside the measured for seven temperature values: +10 °C;
enclosure (2) must be replaced with nitrogen gas or +5 °C; 0 °C; -10 °C; -25 °C; -40 °C; -50 °C.
other inert gas, in order to avoid vapour condensation The time required to reach thermal stability inside
or oxidation on the enclosure inside walls. the enclosure for temperature values up to −40 °C
Purging the gas from enclosure is achieved was a maximum of 40 minutes, reaching the
through bulb valves (1), which are connected to the temperature at the −50 °C threshold being achieved
enclosure top cover and a nitrogen gas supply bottle. in 120 minutes.
After this procedure, the Peltier modules (which are The cooling water temperature was 14 ºC at the
parallel electrically connected) attached to the entrance and 16 ºC at the exit.
enclosure exterior walls, are powered by the DC The water flow was 4.8 l/min.
power supply (5), through the high current electric
terminals (4). The inside temperature in the 3. Discussions
enclosure is controlled by a temperature controller There is a continuous need of calibration of
(7) that controls the supply current of the Peltier temperature sensors, and a wide range of solutions in
modules through the SSR electronic relay (6). The the market, but most of the calibration solutions are
heat produced by the Peltier modules and extracted suitable only for the sensors itself.
from enceinte, is removed with cooled water, trough There is a continuous demand for calibrating
rubber pipes (3). The water temperature difference temperature sensors, which are attached to various
between input and output is measured by a portable shape and various size parts, and the temperature
digital multimeter (8). shift induced by these additional cases need to be
Inside the enclosure, two temperature sensors measured.
were installed, the thermos-resistance type sensor For this reason, a cylindrical shape aluminium
(PT100) connected to the OMRON temperature enclosure with a volume of 5.4 dm3 was designed and
controller with which the enclosure temperature is tested for several temperatures in the range
controlled, and a DT470 silicon diode type sensor comprised from room temperature, up to −50 °C.
produced by the LakeShore company, with an Temperature stability obtained inside the
accuracy of ±0.025K [25]. enclosure for each measured value was better than
The DT470 sensor is connected to a LakeShore 218 ±0.1 °C. This high temperature stability was obtained
temperature monitor that has a measuring resolution using a simple temperature control unit and a usual
of ±9 K and an accuracy of ±146 mK [25] which DC SSR, compared to the refrigeration cooling
temperature of the entire system is calibrated. systems which demand a complex temperature
Temperature measurements were performed for control system.
several values of temperature inside the enclosure, Time required to reach a temperature stability
in the range of −50 °C-+20 °C. inside the enclosure for −40 °C was a maximum of
The temperature stability obtained for each 40 min, and 120 minutes for a temperature of −50 °C
temperature value measured value being ± 0.1 °C. for entire volume, but this cool down time can be
According to the results obtained for various improved to at least 20 minutes for −40 °C and
temperature values inside the enclosure (Figure 7), 60 minutes for a temperature of −50 °C, by adding
the automatic PID control system integrated into the additional insulation layers to the enclosure.
temperature controller was able to reach Another way to improve the performances of the
temperature stability, with almost no temperature Peltier elements is to use a lower temperature for the
oscillations. cooling water of the heat exchangers. This
improvement needs additional cooling of the water,
lowering the temperature towards 1-2 ºC, and the
final temperature can be lowered under −50 ºC.
If necessary, the temperature calibration of the
processed sensors can be improved, using higher
calibration accuracy of the measuring temperature
sensor inside the enceinte.
5. Conclusions
This article presents elements of design,
modelling, construction and testing of a temperature-
controlled enclosure intended for the calibration of
temperature sensors (such as platinum resistors,
thermocouples and others) in the temperature range
−50 ºC-+20 ºC.
Figure 7. Temperatures measured inside the enclosure in the The enclosure, made of aluminium, with a
range of −50 °C-+20 °C cylindrical shape, is cooled and the temperature
controlled by Peltier modules is produced by the
European Thermodynamics company.
[24] T. H. Indiketiya, "An Optimum Strategy to Control Peltier Applied Superconductivity Laboratory of ICPE-CA.
Device Cold Side Temperature," 2021 IEEE 11th Annual e-mail: [email protected]
Computing and Communication Workshop and Conference
(CCWC), NV, USA, 2021, pp. 1333-1338, doi: Dan ENACHE was born in 1984 in Fetești,
10.1109/CCWC51732.2021.9376130. Ialomița.
[25] Lakeshore, https://www.lakeshore.com He graduated with a bachelor's degree from
the Faculty of Electrical Engineering in 2012
Funding Sources and with a Master's degree in Electrical
Engineering from the University Politehnica of
The authors wish to acknowledge the financing of Bucharest
this work by Romanian Research, Innovation and (UPB) in 2014.
Digitization Ministry through the contract POC Starting 2021, he is a Doctor of Science in the field of
126/2019/D9. electrical engineering of the University Politehnica of
Bucharest (UPB).
From 2022, he is enrolled in postdoctoral studies in the field
of applied superconductivity within the Doctoral School of the
Authors’ Biographies Faculty of Electrical Engineering within the University
George DUMITRU was born on February 1, Politehnica of Bucharest (UPB).
1983 in Bucharest. Since 2014, he has been working in the Department of Non-
He graduated with a bachelor's degree in Conventional Electrical Engineering of INCDIE ICPE-CA
Physics from the Faculty of Physics of the Bucharest.
University of Bucharest in 2009 and with a Starting 2020, he works as a scientific researcher (CS III) in the
Master's degree in Electrical Engineering from Applied Superconductivity Laboratory in Electrical Engineering
the University Politehnica of Bucharest (UPB) in the Department of Unconventional Electrical Engineering
in 2020. and is the deputy head of the Department of Unconventional
Since 2017, he has been working as a physicist in the Electrical Engineering in INCDIE ICPE-CA Bucharest.
Unconventional Electrical Engineering Department of INCDIE e-mail: [email protected]
ICPE-CA Bucharest.
Starting 2020, he is a PhD student at the Doctoral School of
Electrical Engineering of University Politehnica of Bucharest Mihai GUȚU was born in Bucharest in 1959.
(UPB). He graduated from the Politehnica University
Starting 2020, he worked as a Technological development of Bucharest (UPB), Faculty of Machine
engineer (IDT III) in the Applied Superconductivity Laboratory Construction Technology in 1984, Machine
in Electrical Engineering within the Department of Tools Section.
Unconventional Electrical Engineering and is the deputy head His research concern on CAD designing new
of the Department of Unconventional Electrical Engineering in prototypes and various electromechanical
INCDIE ICPE-CA Bucharest. products.
e-mail: [email protected] He has an experience in research and development of Special
Electric Machines and Command Systems, design and
Ion DOBRIN was born in 1956 in Bucharest. commissioning for deformation processing technology lines,
He graduated from the Faculty of Physics, machine tool design.
University of Bucharest in 1983 and received e-mail: [email protected]
his PhD in Electrotechnical Materials Science
from the University Politehnica of Bucharest Constantin DUMITRU was born in 1994 in
(UPB) in 1999. Tulcea, Romania.
Since 2012 he has been a first-degree He graduated with a bachelor’s degree in
scientific researcher (CS I), and starting 2018 electrical engineering in 2017 and with a
he is head of master’s degree in electrical engineering
the Department of Unconventional Electrical Engineering in from the University Politehnica of
the INCDIE ICPE-CA from Bucharest. Bucharest (UPB) in 2019.
He has more than 35 years of experience in the application of Starting 2019, he is a PhD student at the
superconductivity, cryogenics and materials science in Doctoral School of Electrical Engineering,
electrical engineering, which can be found in: scientific University Politehnica of Bucharest (UPB).
articles published in scientific journals (30), communications Starting 2017, he worked in the Department of Renewable
given at scientific events (25), both in the country and abroad, Sources and Energy Efficiency of Laboratory of Electric
patents (8), books (2), articles in the mass media (4), of which Machines and Drives in INCDIE ICPE-CA Bucharest.
1 interview (audio), medals and prizes awarded at scientific Starting 2021, he works as a scientific researcher (CS) in the
manifestations of invention (12) or special prizes of Electric Machines and Drives Laboratory.
professional associations (Association General of Engineers e-mail: [email protected]
from Romania (2) and 1 international diploma awarded by the
Unified Institute of Nuclear Research from Dubna (USSR)).
Between 2008 and 2019, he held the position of head of the