WSS Y10 Experimental Techniques PPT 2

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( Secondary)

• Subject : Chemistry
• Year: 10
• Date: 12/04/2022
• Unit: 12- Experimental techniques and chemical analysis
• Key Learning Area: Separation and purification
(Filtration ,Crystallization & Simple distillation)
Objective of the lesson (LFQ) :
( Key Knowledge and skills students need to develop)
To describe and explain the methods of separation and purification.
Learning Outcomes (WILF)

Able to identify a Able to list the apparatus Able to illustrate the


method to separate for the separation steps required for the
soluble solid and technique process.
insoluble solid from
the liquid

GRADE GRADE
GRADE B A/A*
C/D

WSS 4
Identify Element ,Compound and Mixture
Important terms to remember
(a)solvent - is a substance that dissolves a solute.

(b) Solute - is a substance that is dissolved in a solvent.

(c) Solution as a mixture of one or more solutes dissolved in


a solvent.

(d) Saturated solution - is a solution containing maximum


concentration of a solute dissolved in the solvent at a
specified temperature.
Separation of insoluble solid from its liquid
Filtration
•Used to separate an undissolved solid from a mixture of the solid and a liquid / solution ( e.g.
sand from a mixture of sand and water). 
•Filter paper is placed in a filter funnel above another beaker
•Mixture of insoluble solid and liquid is poured into the filter funnel
•Filter paper will only allow small liquid particles to pass through as the filtrate
•Solid particles are too large to pass through the filter paper so will stay behind as a residue

Residue - as a substance
that remains after
evaporation, distillation,
filtration or any
similar process
Separation of soluble solid from its solution

Crystallization
•Used to separate a dissolved solid from a solution, when the solid is much more soluble in hot solvent than
in cold (e.g. copper sulphate from a solution of copper (II) sulphate in water)
•The solution is heated, allowing the solvent to evaporate to leave a saturated solution behind
•Test if the solution is saturated by dipping a clean, dry, cold glass rod into the solution. If the solution is
saturated, crystals will form on the glass rod
•The saturated solution is allowed to cool slowly and solids will come out of the solution as the solubility
decreases, and crystals will grow
•Crystals are collected by filtering the solution
•They are then washed with cold, distilled water to remove impurities and allowed to dry
Crystallization
To obtain pure copper sulphate from an impure sample
 Copper sulphate solution Let us understand this technique with the
help of experiment

 Obtain saturated solution


 Cool slowly
 Crystal formation

 Separate the copper sulphate crystals from the solution by


the filtration and dry.
Dip a glass rod in hot solution from time to
time. When small crystal form on the glass
rod, the solution is saturated.
Stop heating
To obtain pure copper sulphate from an impure sample
Mini-Plenary
Sand, salt and iron
Mr Rainforest has accidentally mixed up the three pots of
sand, salt and iron filings

Your challenge is to suggest methods to separate the three


substances.
Simple distillation
•Used to separate a liquid and soluble solid from a solution

•The solution is heated and pure water evaporates producing a vapour which rises through
the neck of the round-bottomed flask.

•The vapour passes through the condenser, where it cools and condenses, turning into
pure liquid H2O which is collected in a beaker.

•After all the water is evaporated from the solution, only the solid solute will be left behind.
PLENARY
Label the diagram
1. Bunsen burner
2.Round bottom flask
3.Cork
4.Thermometer.
5.Condenser
6.Water in
7.Water out
8.distillate

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