N-6-Trifluoroacetyl-L-lysine is a chemical with a specific purpose. Lookchem provides you with multiple data and supplier information of this chemical.

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N-6-Trifluoroacetyl-L-Lysine
Cas No: 10009-20-8
No Data
1 Kilogram
500 Kilogram/Month
SICHUAN TONGSHENG AMINOACID CO.LTD
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top N-6-Trifluoroacetyl-L-lysine
Cas No: 10009-20-8
USD $ 1.0-1.0 / Kilogram
1 Kilogram
10 Kilogram/Day
HENAN NEW BLUE CHEMICAL CO.,LTD
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N-6-Trifluoroacetyl-L-lysine
Cas No: 10009-20-8
No Data
1 Kilogram
1-1000 Metric Ton/Month
Hangzhou ZeErRui Chemical Co., Ltd.
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High purity Various Specifications N(epsilon)-trifluoroacetyl-L-lysine CAS:10009-20-8
Cas No: 10009-20-8
USD $ 100.0-500.0 / Gram
1 Gram
99999 Gram/Year
Hangzhou Dingyan Chem Co., Ltd
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High quality N-Acetyl-L-Lysine supplier in China
Cas No: 10009-20-8
No Data
1 Kilogram
30 Metric Ton/Month
Simagchem Corporation
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N-6-Trifluoroacetyl-L-lysine
Cas No: 10009-20-8
USD $ 45.0-45.0 / Gram
1 Gram
200 Metric Ton/Year
Jinan Finer Chemical Co., Ltd
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Good quantity N-6-Trifluoroacetyl-L-lysine
Cas No: 10009-20-8
No Data
1 Kilogram
1 Metric Ton/Month
Hangzhou Think Chemical Co. Ltd
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N-6-Trifluoroacetyl-L-lysine
Cas No: 10009-20-8
No Data
1 Kilogram
20 Metric Ton/Month
Henan Allgreen Chemical Co.,Ltd
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Factory Supply L-Lysine, N6-(2,2,2- trifluoroacetyl)-
Cas No: 10009-20-8
No Data
1
1
Ality Chemical Corporation
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H-Lys(Tfa)-OH
Cas No: 10009-20-8
No Data
10 Milligram
Amadis Chemical Co., Ltd.
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Basic information
1. Product Name: N-6-Trifluoroacetyl-L-lysine
2. Synonyms: H-LYS(TFA)-OH;H-LYS(CF3CO)-OH;EPSILON-TFA-LYSINE;LYSINE(TFA)-OH;N-EPSILON-TRIFLUOROACETYL-L-LYSINE;N6-TRIFLUOROACETYL-L-LYSINE;N-ε-Trifluoroacetyl-L-lysine;N1-Trifluoroacetyl-L-Lysine
3. CAS NO:10009-20-8
4. Molecular Formula: C₈H₁₃F₃N₂O₃
5. Molecular Weight: 242.2
6. EINECS: 1308068-626-2
7. Product Categories: Chemical intermediate for LISINOPRIL;API intermediates;Amino Acids & Derivatives;Metabolites & Impurities;amino acid;Amino Acids & Derivatives, Metabolites & Impurities
8. Mol File: 10009-20-8.mol
9. Article Data: 4
Chemical Properties
1. Melting Point: 258
2. Boiling Point: 382.5 °C at 760 mmHg
3. Flash Point: 185.1 °C
4. Appearance: /
5. Density: 1.4
6. Vapor Pressure: 6.55E-07mmHg at 25°C
7. Refractive Index: 1.444
8. Storage Temp.: 2-8°C
9. Solubility: 2 M HCl: 10 mg/mL, clear, colorless
10. PKA: 2.51±0.24(Predicted)
11. BRN: 2122429
12. CAS DataBase Reference: N-6-Trifluoroacetyl-L-lysine(CAS DataBase Reference)
13. NIST Chemistry Reference: N-6-Trifluoroacetyl-L-lysine(10009-20-8)
14. EPA Substance Registry System: N-6-Trifluoroacetyl-L-lysine(10009-20-8)
Safety Data
1. Hazard Codes: N/A
2. Statements: N/A
3. Safety Statements: 22-24/25
4. WGK Germany: 1
5. RTECS:
6. F: 10
7. HazardClass: N/A
8. PackingGroup: N/A
9. Hazardous Substances Data: 10009-20-8(Hazardous Substances Data)

10009-20-8 Usage

Chemical Properties

Off-White Solid

Uses

A cysteine conjugate metabolite adduct formation with specific mitochondrial proteins using antibodies raised against halothane metabolite adducts.

Definition

ChEBI: An N6-acyl-L-lysine where the N6-acyl group is trifluoroacetyl.

Check Digit Verification of cas no

The CAS Registry Mumber 10009-20-8 includes 8 digits separated into 3 groups by hyphens. The first part of the number,starting from the left, has 5 digits, 1,0,0,0 and 9 respectively; the second part has 2 digits, 2 and 0 respectively.
Calculate Digit Verification of CAS Registry Number 10009-20:
(7*1)+(6*0)+(5*0)+(4*0)+(3*9)+(2*2)+(1*0)=38
38 % 10 = 8
So 10009-20-8 is a valid CAS Registry Number.

InChI:InChI=1/C8H13F3N2O3/c9-8(10,11)7(16)13-4-2-1-3-5(12)6(14)15/h5H,1-4,12H2,(H,13,16)(H,14,15)/t5-/m0/s1

10009-20-8 Well-known Company Product Price

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(Code)Product description
CAS number
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TCI America
(T2815) N^ε-Trifluoroacetyl-L-lysine >98.0%(T)
10009-20-8
5g
210.00CNY
Detail

TCI America
(T2815) N^ε-Trifluoroacetyl-L-lysine >98.0%(T)
10009-20-8
25g
680.00CNY
Detail

Sigma
(53604) N_ε-Trifluoroacetyl-L-lysine ≥96.0% (TLC)
10009-20-8
53604-5G-F
499.59CNY
Detail

Sigma
(53604) N_ε-Trifluoroacetyl-L-lysine ≥96.0% (TLC)
10009-20-8
53604-25G-F
1,719.90CNY
Detail

10009-20-8SDS

SAFETY DATA SHEETS

According to Globally Harmonized System of Classification and Labelling of Chemicals (GHS) - Sixth revised edition

Version: 1.0

Creation Date: Aug 17, 2017

Revision Date: Aug 17, 2017

1.Identification

1.1 GHS Product identifier

Product name	N6-trifluoroacetyl-L-lysine

1.2 Other means of identification

Product number	-
Other names	N6-Trifluoroacetyl-L-lysine

1.3 Recommended use of the chemical and restrictions on use

Identified uses	For industry use only.
Uses advised against	no data available

1.4 Supplier's details

1.5 Emergency phone number

Emergency phone number	-
Service hours	Monday to Friday, 9am-5pm (Standard time zone: UTC/GMT +8 hours).

More Details:10009-20-8 SDS

10009-20-8Synthetic route

: 383-63-1
ethyl trifluoroacetate,

: 657-27-2, 10098-89-2
L-Lysine hydrochloride

: 10009-20-8
(S)-6-trifluoroacetylamino-2-aminohexanoic acid

Conditions

Conditions	Yield
With sodium In ethanol at 5 - 20℃;	62%
Stage #1: L-Lysine hydrochloride With ethanol; sodium Stage #2: ethyl trifluoroacetate, In ethanol at 20℃; Cooling with ice; Stage #3: With acetic acid In ethanol	62%
Stage #1: L-Lysine hydrochloride With sodium In ethanol for 1h; Stage #2: ethyl trifluoroacetate, at 5 - 20℃; for 3h; Stage #3: With acetic acid for 0.166667h;	56%

: 383-63-1
ethyl trifluoroacetate,

: 16079-52-0
sodium salt of L-lysine

A: 10009-20-8
(S)-6-trifluoroacetylamino-2-aminohexanoic acid

B: 329-53-3
Nα,Nε-bis(trifluoroacetyl)-L-lysine

Conditions

Conditions	Yield
In ethanol at 5 - 20℃;	A 25% B 56%

: 383-64-2
S-ethyl trifluoroacetate

: 657-27-2, 10098-89-2
L-Lysine hydrochloride

: 10009-20-8
(S)-6-trifluoroacetylamino-2-aminohexanoic acid

Conditions

Conditions	Yield
With sodium hydroxide

: 24424-99-5
di-tert-butyl dicarbonate

: 10009-20-8
(S)-6-trifluoroacetylamino-2-aminohexanoic acid

: 96561-04-5, 16965-06-3
(S)-6-trifluoroacetylamino-2-(tert-butoxycarbonylamino)-hexanoic acid

Conditions

Conditions	Yield
Stage #1: di-tert-butyl dicarbonate; (S)-6-trifluoroacetylamino-2-aminohexanoic acid With triethylamine In N,N-dimethyl-formamide at 20℃; for 3h; Stage #2: With hydrogenchloride In water; N,N-dimethyl-formamide pH=2;	92%
In N,N-dimethyl-formamide at 20℃; for 2h;	92%

: 10009-20-8
(S)-6-trifluoroacetylamino-2-aminohexanoic acid

: 86298-24-0
N-phenyl-1H-benzo[d][1,2,3]triazole-1-carboxamide

: C15H18F3N3O4

Conditions

Conditions	Yield
With triethylamine In water; acetonitrile at 20℃; for 0.5h; chemoselective reaction;	92%

: 75-44-5
phosgene

: 10009-20-8
(S)-6-trifluoroacetylamino-2-aminohexanoic acid

: 42267-27-6
Nε-trifluoroacetyl-L-lysine Nα-carboxanhydride

Conditions

Conditions	Yield
In tetrahydrofuran at 20 - 30℃; for 4.33333h; Inert atmosphere;	86.5%
In 1,4-dioxane at 45℃; for 2h;	70%

: 10009-20-8
(S)-6-trifluoroacetylamino-2-aminohexanoic acid

: 530-62-1
1,1'-carbonyldiimidazole

: N-(4-(2,5-dioxo-4-oxazolidinyl)butyl)-2,2,2-trifluoroacetamide

Conditions

Conditions	Yield
In tetrahydrofuran for 0.4h; Reflux; Large scale;	81.9%

: 32315-10-9
bis(trichloromethyl) carbonate

: 10009-20-8
(S)-6-trifluoroacetylamino-2-aminohexanoic acid

: 42267-27-6
Nε-trifluoroacetyl-L-lysine Nα-carboxanhydride

Conditions

Conditions	Yield
With sodium hydroxide In tetrahydrofuran at 50℃; Inert atmosphere;	75%
With Pinene In ethyl acetate at 105 - 110℃;

: 10009-20-8
(S)-6-trifluoroacetylamino-2-aminohexanoic acid

: 503-38-8
trichloromethyl chloroformate

: 42267-27-6
Nε-trifluoroacetyl-L-lysine Nα-carboxanhydride

Conditions

Conditions	Yield
In tetrahydrofuran for 2h; Inert atmosphere; Reflux;	75%
With sodium hydroxide In tetrahydrofuran for 2h; Inert atmosphere; Reflux;	75%
In ethyl acetate at 70℃; for 4h;	63%

: 10009-20-8
(S)-6-trifluoroacetylamino-2-aminohexanoic acid

: 121-44-8
triethylamine

: 14470-28-1
mono-4-methoxytrityl chloride

: C6H15N*C28H29F3N2O4

Conditions

Conditions	Yield
Stage #1: (S)-6-trifluoroacetylamino-2-aminohexanoic acid With chloro-trimethyl-silane; triethylamine In dichloromethane for 2h; Reflux; Inert atmosphere; Stage #2: mono-4-methoxytrityl chloride In dichloromethane for 2h; Reflux; Inert atmosphere; Stage #3: triethylamine In methanol; dichloromethane for 0.5h; Inert atmosphere;	74%

: 590-28-3
potassium cyanate

: 10009-20-8
(S)-6-trifluoroacetylamino-2-aminohexanoic acid

: Nα-carbamoyl-Nε-trifluoroacetyl-L-lysine

Conditions

Conditions	Yield
In water at 50℃; for 3h; pH=7.5;	73.8%
In water at 50℃; pH=8; Kinetics;

: 10009-20-8
(S)-6-trifluoroacetylamino-2-aminohexanoic acid

: 340701-06-6
docosa-10,12-diynedioic acid mono-(2,5-dioxo-pyrrolidin-1-yl) ester

: 21-[(S)-1-Carboxy-5-(2,2,2-trifluoro-acetylamino)-pentylcarbamoyl]-henicosa-10,12-diynoic acid

Conditions

Conditions	Yield
With potassium hydroxide In tetrahydrofuran at 20℃; for 24h; pH=9;	62%

: 67-56-1
methanol

: 10009-20-8
(S)-6-trifluoroacetylamino-2-aminohexanoic acid

: methyl 2-bromo-6-(2,2,2-trifluoroacetamido)hexanoate

Conditions

Conditions	Yield
Stage #1: (S)-6-trifluoroacetylamino-2-aminohexanoic acid With sulfuric acid; hydrogen bromide; sodium bromide; sodium nitrite In water at 3 - 20℃; Inert atmosphere; Stage #2: methanol With toluene-4-sulfonic acid at 65℃; Inert atmosphere;	62%

: 10009-20-8
(S)-6-trifluoroacetylamino-2-aminohexanoic acid

: 366001-61-8
C16H22F6N4O4

Conditions

Conditions	Yield
phosphorus pentoxide In 1-methyl-pyrrolidin-2-one at 170℃; Product distribution / selectivity;	59%

: 10009-20-8
(S)-6-trifluoroacetylamino-2-aminohexanoic acid

: 501-53-1
benzyl chloroformate

: 14905-30-7
(2S)-2-{[(benzyloxy)carbonyl]amino}-6-[(trifluoroacetyl)amino]hexanoic acid

Conditions

Conditions	Yield
With sodium hydrogencarbonate

: 75-44-5
phosgene

: 10009-20-8
(S)-6-trifluoroacetylamino-2-aminohexanoic acid

A: 42267-27-6
Nε-trifluoroacetyl-L-lysine Nα-carboxanhydride

B: 112139-30-7
C9H11Cl2F3N2O3

Conditions

Conditions	Yield
In tetrahydrofuran; N,N-dimethyl-formamide at 30℃; for 2.5h; Title compound not separated from byproducts;

: 75-44-5
phosgene

: 10009-20-8
(S)-6-trifluoroacetylamino-2-aminohexanoic acid

: 112139-31-8
C9H12ClF3N2O4

Conditions

Conditions	Yield
In tetrahydrofuran at 30℃; for 2.5h;

: 75-77-4
chloro-trimethyl-silane

: 10009-20-8
(S)-6-trifluoroacetylamino-2-aminohexanoic acid

: 110579-79-8
C11H21F3N2O3Si

Conditions

Conditions	Yield
In chloroform; acetonitrile for 2h; Heating;

: 10009-20-8
(S)-6-trifluoroacetylamino-2-aminohexanoic acid

: 10416-59-8, 132255-83-5
N,O-Bis(trimethylsilyl)acetamide

: C14H29F3N2O3Si2

Conditions

Conditions	Yield
In 1,4-dioxane

: 10009-20-8
(S)-6-trifluoroacetylamino-2-aminohexanoic acid

: 7669-54-7
2-nitrobenzenesulfenyl chloride

: 41918-63-2
Nα-(o-nitrophenylsulfenyl)-Nε-(trifluoroacetyl)lysine

Conditions

Conditions	Yield
With sodium hydroxide In acetone

: 10009-20-8
(S)-6-trifluoroacetylamino-2-aminohexanoic acid

: 736142-36-2
21-((S)-5-Amino-1-carboxy-pentylcarbamoyl)-henicosa-10,12-diynoic acid

Conditions

Conditions	Yield
Multi-step reaction with 2 steps 1: 62 percent / aq. KOH / tetrahydrofuran / 24 h / 20 °C / pH 9 2: 46 percent / aq. KOH / tetrahydrofuran; methanol / 12 h / 35 °C / pH 12 - 13 View Scheme

: 10009-20-8
(S)-6-trifluoroacetylamino-2-aminohexanoic acid

: Boc-Ser-Lys(TFA)-Pro-Met-Gly(OBzl)2

Conditions

Conditions	Yield
Multi-step reaction with 3 steps 1: CHCl3; acetonitrile / 2 h / Heating 2: 48 percent / pyridine, triethylamine, pivaloyl chloride / CHCl3; acetonitrile / 1 h / Ambient temperature 3: 53 percent / diphenylphosphorazide, triethylamine / dioxane; dimethylformamide / 7 h, 0 deg C; 40 h, 20 deg C View Scheme

: 10009-20-8
(S)-6-trifluoroacetylamino-2-aminohexanoic acid

: 107994-57-0
Nα-tert-butyloxycarbonyl-L-seryl-Nε-trifluoroacetyl-L-lysine

Conditions

Conditions	Yield
Multi-step reaction with 2 steps 1: CHCl3; acetonitrile / 2 h / Heating 2: 48 percent / pyridine, triethylamine, pivaloyl chloride / CHCl3; acetonitrile / 1 h / Ambient temperature View Scheme

: 10009-20-8
(S)-6-trifluoroacetylamino-2-aminohexanoic acid

: 64851-79-2
Nα-(o-nitrophenylsulfenyl)-Nε-(trifluoroacetyl)-L-lysine N-hydroxysuccinimide ester

Conditions

Conditions	Yield
Multi-step reaction with 2 steps 1: 2N NaOH / acetone 2: dicyclohexylcarbodiimide / dioxane; CH2Cl2 / 7 h / 0 - 20 °C View Scheme

: 10009-20-8
(S)-6-trifluoroacetylamino-2-aminohexanoic acid

: 82175-93-7
N-tert-butoxycarbonyl-L-leucyl-Nε-(trifluoroacetyl)-L-lysyl-L-leucine methyl ester

Conditions

Conditions	Yield
Multi-step reaction with 5 steps 1: 2N NaOH / acetone 2: dicyclohexylcarbodiimide / dioxane; CH2Cl2 / 7 h / 0 - 20 °C 3: 1.) triethylamine / 1.) dioxane, methylene chloride, 15 min, 2.) 0 - 20 deg C, 7 h 4: HCl / ethyl acetate; diethyl ether / 0.33 h / 20 °C 5: 69.5 percent / triethylamine / dioxane; CH2Cl2 / 16 h / 0 - 20 °C View Scheme

: 10009-20-8
(S)-6-trifluoroacetylamino-2-aminohexanoic acid

: 82175-92-6
Nα-(o-nitrophenylsulfenyl)-Nε-(trifluoroacetyl)-L-lysyl-L-leucine methyl ester

Conditions

Conditions	Yield
Multi-step reaction with 3 steps 1: 2N NaOH / acetone 2: dicyclohexylcarbodiimide / dioxane; CH2Cl2 / 7 h / 0 - 20 °C 3: 1.) triethylamine / 1.) dioxane, methylene chloride, 15 min, 2.) 0 - 20 deg C, 7 h View Scheme

: 10009-20-8
(S)-6-trifluoroacetylamino-2-aminohexanoic acid

: Nε-(trifluoroacetyl)-L-lysyl-L-leucine methyl ester hydrochloride

Conditions

Conditions	Yield
Multi-step reaction with 4 steps 1: 2N NaOH / acetone 2: dicyclohexylcarbodiimide / dioxane; CH2Cl2 / 7 h / 0 - 20 °C 3: 1.) triethylamine / 1.) dioxane, methylene chloride, 15 min, 2.) 0 - 20 deg C, 7 h 4: HCl / ethyl acetate; diethyl ether / 0.33 h / 20 °C View Scheme

: 10009-20-8
(S)-6-trifluoroacetylamino-2-aminohexanoic acid

: 82175-94-8
Nα-(o-nitrophenylsulfenyl)-Nε-(trifluoroacetyl)-L-lysyl-L-alanyl-L-alanine methyl ester

Conditions

Conditions	Yield
Multi-step reaction with 3 steps 1: 2N NaOH / acetone 2: dicyclohexylcarbodiimide / dioxane; CH2Cl2 / 7 h / 0 - 20 °C 3: 50.9 percent / triethylamine / dioxane; CH2Cl2 / 16 h / 0 - 20 °C View Scheme

: 10009-20-8
(S)-6-trifluoroacetylamino-2-aminohexanoic acid

: 42267-27-6
Nε-trifluoroacetyl-L-lysine Nα-carboxanhydride

Conditions

Conditions	Yield
Multi-step reaction with 2 steps 1: tetrahydrofuran / 2.5 h / 30 °C 2: 88 percent / tetrahydrofuran / 4 h / 25 °C View Scheme

: 10009-20-8
(S)-6-trifluoroacetylamino-2-aminohexanoic acid

: 103300-89-6
Nε-(trifluoroacetyl)-L-lysyl-L-proline

Conditions

Conditions	Yield
Multi-step reaction with 2 steps 1: tetrahydrofuran; dimethylformamide / 2.5 h / 30 °C 2: 94 percent Chromat. / tetrahydrofuran; H2O / 0.03 h / 0 - 12 °C View Scheme
Multi-step reaction with 3 steps 1: tetrahydrofuran / 2.5 h / 30 °C 2: 88 percent / tetrahydrofuran / 4 h / 25 °C 3: 94 percent Chromat. / tetrahydrofuran; H2O / 0.03 h / 0 - 12 °C View Scheme

10009-20-8Upstream product

10009-20-8Downstream Products

10009-20-8Relevant articles and documents

N-trifluoroacyl lysine derivatives in the synthesis of L-lysyl-L-glutamic acid

Cherevin,Gulevich,Popova,Zubreichuk,Knizhnikov

, p. 1427 - 1431 (2007)

Conditions were developed for simultaneous preparation of N a-trifluoroacetyl-L-lysine and N α,N a-bis(trifluoroacetyl)-L-lysine at overall conversion of initial lysine monohydrochloride up to 82%. By reaction of dimethyl L-glutamate with N α,N a-bis(trifluoroacetyl)-L-lysyl chloride in the presence of triethylamine or with N α- carboxyanhydride of N a-trifluoroacetyl-L-lysine with subsequent removing protecting groups in the formed dipeptides by treating with water-ethanol solution of sodium hydroxide we obtained L-lysyl-L-glutamic acid. Physicochemical characteristics of samples obtained coincided with characteristics of L-lysyl-L-glutamic acid described in the literature thus suggesting that no racemization occurred either at the stage of peptide bond formation or at deprotection.

Control of lysyl oxidase activity through site-specific deuteration of lysine

Pestov, Nikolay B.,Okkelman, Irina A.,Shmanai, Vadim V.,Hurski, Alaksiej L.,Giaccia, Amato J.,Shchepinov, Mikhail S.

, p. 255 - 258 (2011)

Lysyl oxidase (LOX) is implicated in several extracellular matrix related disorders, including fibrosis and cancer. Methods of inhibition of LOX in vivo include antibodies, copper sequestration and toxic small molecules such as β-aminopropionitrile. Here,

THERAPIES FOR CANCER USING ISOTOPICALLY SUBSTITUTED LYSINE

-

Page/Page column 7, (2009/10/22)

Methods of treatment and substances for treatment of cancer may use or cause the creation of isotopically modified lysine at levels that do not occur naturally.

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CAS

10009-20-8

10009-20-8 Suppliers

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Basic information

Chemical Properties

Safety Data

10009-20-8 Usage

Chemical Properties

Uses

Definition

Check Digit Verification of cas no

10009-20-8 Well-known Company Product Price

10009-20-8SDS

SAFETY DATA SHEETS

According to Globally Harmonized System of Classification and Labelling of Chemicals (GHS) - Sixth revised edition

1.Identification

1.1 GHS Product identifier

1.2 Other means of identification

1.3 Recommended use of the chemical and restrictions on use

1.4 Supplier's details

1.5 Emergency phone number

10009-20-8Synthetic route

10009-20-8Upstream product

10009-20-8Downstream Products

10009-20-8Relevant articles and documents

N-trifluoroacyl lysine derivatives in the synthesis of L-lysyl-L-glutamic acid

Cherevin,Gulevich,Popova,Zubreichuk,Knizhnikov

, p. 1427 - 1431 (2007)

Control of lysyl oxidase activity through site-specific deuteration of lysine

Pestov, Nikolay B.,Okkelman, Irina A.,Shmanai, Vadim V.,Hurski, Alaksiej L.,Giaccia, Amato J.,Shchepinov, Mikhail S.

, p. 255 - 258 (2011)

THERAPIES FOR CANCER USING ISOTOPICALLY SUBSTITUTED LYSINE

-

Page/Page column 7, (2009/10/22)