1000 PPM Standards For Atomic Absorption
1000 PPM Standards For Atomic Absorption
1000 PPM Standards For Atomic Absorption
Chemistryinfolabreagentsandresources
Thepreparationof1000ppmatomicabsorptionstandards
AAStockSolutions
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1000ppmStandardsforAtomicAbsorption
SeealsoInterferencesaffectinganalysis
Stocksolutions.Storeinstopperedpolythenebottles
Aluminium
Dissolve1.000gofAluminiummetalin25ml.ofhydrochloricacid(S.G.1.18)andafewdropsofnitricacid(S.G.1.42)
Diluteto1litreinavolumetricflaskwithdeionisedwater.
Antimony
Dissolve1.000gantimonyin10ml.conc.hydrochloricacid,afewdropsofconc.nitricacid,and10goftartaricacid.Diluteto
1litre..
Arsenic
Dissolve1.000gofarsenicpowderin50ml.conc.nitricacid.Diluteto1litrewithdeionisedwateror
Dissolve1.3200garsenousoxide(As2O3),driedto110oC,in50ml.ofconc.hydrochloricacid.Diluteto1litrewith
deionisedwater.
Barium
Dissolve1.4380g.ofbariumcarbonate(BaCO3)in20ml.1Mhydrochloricacid.Diluteto1litreinavolumetricflaskwith
deionisedwater.
Beryllium
Dissolve19,639g.ofberylliumsulphate(BeSO4)in250deionisedwater.Diluteto1litreinavolumetricflaskwith
deionisedwater.
Bismuth
Dissolve1.000g.ofbismuthmetalin50ml.conc.nitricacidDiluteto1litreinavolumetricflaskwithdeionisedwater.
Dissolve1.1148g.ofbismuthtrioxide(Bi2O3)intheminimumquantityofcomc.hydrochloricacid.Diluteto1litreina
volumetricflaskwithdeionisedwater.
Boron
Dissolve5.1744g.ofboricacid(H3BO3)in500ml.ofdeionisedwater.Diluteto1litreinavolumetricflaskwithdeionised
water..
Cadmium
Dissolve1.000g.ofcadmiummetalin20ml.of5M.hydrochloricacidand2dropsofconc.nitricacid.Diluteto1litre.
Dissolve2.0360g.ofcadmiumchloridein250mldeionisedwater.Diluteto1litreinavolumetricflask.
Dissolve2.1032g.ofcadmiumnitratein250ml.ofdeionisedwater.Diluteto1litreinavolumetricflask.
Caesium
Dissolve1.2670g.ofcaesiumchloride(CsCl)in100ml.ofdeionisedwater.Diluteto1litreinavolumetricflaskwith
deionisedwater.
Calcium
Dissolve2.4973g.ofcalciumcarbonate(CaCO3)in25ml.of1Mhydrochloricacid.Thisshouldbeaddeddropwisetoavoid
lossesduringthevigorouseffervescence.Diluteto1litreinavolumetricflaskwithdeionisedwater.
Dissolve2.7693g.ofcalciumchloride(CaCl2)in100ml.deionisedwater.Diluteto1litreinavolumetricflaskwithdeionised
water.
Chromium
Dissolve7.6960g.ofchromiumnitrate(Cr(NO3)3.9H2O)in250ml.ofdeionisedwater.Diluteto1litreinavol.Flask.
Cobalt
Dissolve1.000g.ofcobaltmetalin50ml.of5Mhydrochloricacid.Diluteto1litreinavolumetricflaskwithdeionised
water.or
Dissolve4.9379g.ofcobaltnitrate(Co(NO3)2.6H2Oin250ml.deionisedwater.Diluteto1litreinavolumetricflaskwith
deionisedwater.
Dissolve4.0380g.ofcobalt(111)chloride(CoCl2.6H2O)in200ml.deionisedwater.Diluteto1litreinavolumetricflask
withdeionisedwater.
Copper
Dissolve1,000g.ofcoppermetalin50ml.of5Mnitricacid.Diluteto1litreinavolumetricflaskwihdeionisedwater.or
Dissolve3.7980g.of(Cu(NO3)2.3H2Oin250ml.ofdeionisedwater.Diluteto1litreinavolumetricflaskwihdeionised
water.
Gold
Dissolve1.000g.ofgoldmetalin15ml.ofconc.hydrochloricacidand5ml.ofconc.nitricacid.Diluteto1litreina
volumetricflaskwihdeionisedwater.or
Dissolve1.8110g.ofammoniumchloroaurate(NH4AuCl4)in100ml.ofdeionisedwater.Diluteto1litreinavolumetricflask
wihdeionisedwater.
Iron
Dissolve1.000g.ofironwireorgranulesin20ml.of5MhydrochloricacidDiluteto1litreinavolumetricflaskwihdeionised
water.or
Dissolve4.8400g.ofiron(111)chloride(FeCl3.6H2O)in200ml.ofdeionisedwater.Diluteto1litreinavolumetricflaskwih
deionised.water
Lanthanum
Dissolve1.1782g.oflanthanumoxide(La2O3)in20ml.of5Mhydrochloricacid.Diluteto1litreinavolumetricflaskwih
deionisedwater.
Lead
Dissolve1.000g.ofleadmetalin50ml.of2Mnitricacid.Diluteto1litreinavolumetricflaskwithdeionisedwater.
Dissolve1.5980g.ofleadnitrate(Pb(NO3)2)in100ml.ofdeionisedwater.Diluteto1litreinavolumetricflaskwith
deionisedwater.
Magnesium
Dissolve1.000g.ofmagnesiummetalin50ml.of5Mhydrochloricacid.Diluteto1litreinavolumetricflaskwithdeionised
water.or
Dissolve3.9160g.ofmagnesiumchloride(MgCl2.6H2O)in200ml.ofdeionisedwater.Diluteto1litreinavolumetricflask
withdeionisedwater.
Manganese
Dissolve1.000g.ofmanganesemetalin50ml.ofconc.hydrochloricacid.Diluteto1litreinavolumetricflaskwithdeionised
water.
Dissolve3.6077g.ofmanganessechloride(MnCl2.4H20)in50ml.conc.hydrochloricacid.Diluteto1litreinavolumetric
flaskwithdeionisedwater.
Mercury
Dissolve1.000g.ofmercurymetalin20ml.of5Mnitricacid.Diluteto1litreinavolumetricflaskwithdeionisedwater.or
Dissolve1.3520g.ofmercury(11)chloride(HgCl2)in250ml.ofdeionisedwater.Diluteto1litreinavolumetricflaskwith
deionisedwater.or
Dissolve1.0800g.ofmercury(11)oxidein20ml.of5Mhydrochloricacid.Diluteto1litreinavolumetricflaskwith
deionisedwater.
Molybdenum
Dissolve1.000g.ofmolybdenumpowderin10ml.ofconc.hydrochloricacidand10ml.ofdeionisedwater.Add1ml.of
conc.nitricacid.Useamagneticstirrertocompletelydissolvethemolybdenum.Diluteto1litreinavolumetricflaskwith
deionisedwater.or
Dissolve1.8403g.ofammoniummolybdate(NH4)6MO7O22.4H2Oin500ml.ofdeionisedwater.Diluteto1litreina
volumetricflaskwithdeionisedwater.or
Dissolve1.5000g.ofmolybdenumtrioxide(MoO3)in25ml.conc.hydrochloricacid.Diluteto1litreinavolumetricflaskwith
deionisedwater.
Nickel
Dissolve1.000g.ofnickelin20ml.ofconc.nitricacid.Diluteto1litreinavolumetricflaskwithdeionisedwater.or
Dissolve4.9530g.ofnickelnitrate
(Ni(NO3)2.6H2O)in1litre.ofdeionisedwater.
Potassium
Dissolve11.9070g.ofdrypotassiumchloridein250ml.ofdeionisedwater.Diluteto1litreinavolumetricflaskwith
deionisedwater.
Silica
Dissolveabout7.6g.ofsodiummetasilicate(Na2SiO3.5H2Oindeionisedwater.Diluteto1litreinavolumetricflaskwith
deionisedwater.
Silver
Dissolve1.5750ofsilvernitratein200ml.ofdeionisedwater.Diluteto1litreinavolumetricflaskwithdeionisedwater.
Sodium
Dissolve2.5420g.ofsodiumchloride(NaCl)in200ml.ofdeionisedwater.Diluteto1litreinavolumetricflask.
Strontium
Dissolve2.4150g.ofstrontiumnitrate(Sr(NO3)in200ml.ofdeionisedwater.Diluteto1litreinavolumetricflaskwithwater.
Tin
Dissolve1.000g.oftinmetalin200ml.ofconc.hydrochloricacidand5ml.ofconc.nitricacid.Diluteto1litreinavolumetric
flaskwithdeionisedwater.or
Dissolve2.9540oftin(1V)chloridepentachloride(SnCl4.5H2O)in500ml.deionisedwater.Ifprecipitateforms,redissolve
byadding6Mhydrochloricacid.Diluteto1litreinavolumetricflaskwithdeionisedwater
Uranium
Dissolve21.100g.ofuranylnitratein250ml.ofdeionisedwater.Diluteto1litreinavolumetricflaskwithdeionisedwater.or
Dissolve14.329g.ofuranylchloridein250ml.ofdeionisedwater.Diluteto1litreinavolumetricflaskwithdeionisedwater.
Vanadium
Dissolve1.000g.ofvanadiummetalin25ml.conc.nitricacid.Diluteto1litre.
Dissolve2.2960g.ofammoniummetavanadate(NH4VO3)in20ml.of100volumehydrogenperoxide.Diluteto1litreina
volumetricflaskwithdeionisedwater.
Zinc
Dissolve1.000g.ofzincmetalin30ml.of5Mhydrochloricacid.Diluteto1litreinavolumetricflaskwithdeionisedwater.or
Dissolve1.2450g.ofzincoxide(ZnO)in5mlofdeionisedwaterfollowedby25ml.of5Mhydrochloricacid.Diluteto1litrein
avolumetricflaskwithdeionisedwater
Zirconium
Dissolve1.000g.ofzirconiummetalin25ml.ofhydrofluoricacid(40%w/v)inaP.T.F.E.beaker.Diluteto1litreina
polpropylenevolumetricflaskwithdeionisedwater
or
Dissolve3.7174g.ofdryzirconiumnitratein1litredeionisedwater
Signature:DhanlalDeLloyd,Chem.Dept,TheUniversityofTheWestIndies,St.Augustinecampus
TheRepublicofTrinidadandTobago.
Copyright:delloyd2000Allrightsreserved.