SPECIFICATION FOR PRECIPITATION-HARDENING

NICKEL ALLOY BARS, FORGINGS, AND FORGING

STOCK FOR HIGH-TEMPERATURE SERVICE
SB-637

(Identical with ASTM Specification B 637-93a)

1. Scope 4. Ordering Information

1.1 This specification covers hot- and cold-worked 4.1 Orders for material under this specification shall
precipitation-hardenable nickel alloy rod, bar, forgings, include the following information:
and forging stock for high-temperature service (Table 1).
4.1.1 Alloy (Table 1).
1.2 The values stated in inch-pound units are to be
regarded as the standard. The values given in parentheses 4.1.2 Condition (temper) (Table 4).
are for information only.
4.1.3 Shape — Rod or bar (round, rectangle,
square, hexagon, octagon).
2. Referenced Documents
4.1.3.1 Forging (sketch or drawing).
2.1 ASTM Standards:
E 8 Test Methods of Tension Testing of Metallic Mate- 4.1.4 Dimensions, including length.
rials
E 29 Practice for Using Significant Digits in Test Data 4.1.5 Quantity (mass or number of pieces).
to Determine Conformance With Specifications
E 38 Methods for Chemical Analysis of Nickel-Chro- 4.1.6 Forging Stock — Specify if material is stock
mium and Nickel-Chromium-Iron Alloys for reforging.
E 139 Practice for Conducting Creep Creep-Rupture, and
Stress-Rupture Tests of Metallic Materials 4.1.7 Finish.
E 354 Test Methods for Chemical Analysis of High-
Temperature, Electrical, Magnetic, and Other Similar 4.1.8 Certification — State if certification is re-
Iron, Nickel, and Cobalt Alloys quired (Section 15).

4.1.9 Samples for Product (Check) Analysis —

Whether samples for product (check) analysis shall be
3. Terminology furnished (9.2).
3.1 Descriptions of Terms Specific to This Standard:
3.1.1 bar — material of rectangular (flats), hexago- 4.1.10 Purchaser Inspection — If the purchaser
nal, octagonal, or square solid section in straight lengths. wishes to witness tests or inspection of material at the
place of manufacture, the purchase order must so state
3.1.2 rod — material of round solid section fur- indicating which tests or inspections are to be witnessed
nished in straight lengths. (Section 13).

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SB-637 1998 SECTION II

TABLE 1
CHEMICAL REQUIREMENTS
Product (Check) Analysis Variations, Product (Check) Analysis Variations,
Composition Under min or Over max, of the Composition Under min or Over max, of the
Element Limits, % Specified Limit of Element Limits, % Specified Limit of Element

UNS N07252 (Formerly Grade 689) UNS N07001 (Formerly Grade 685)
Carbon 0.10–0.20 0.01 0.03–0.10 0.01
Manganese 0.50 max 0.03 1.00 max 0.03
Silicon 0.50 max 0.03 0.75 max 0.05
Phosphorus 0.015 max 0.005 0.030 max 0.005
Sulfur 0.015 max 0.003 0.030 max 0.005
Chromium 18.00–20.00 0.25 18.00–21.00 0.25
Cobalt 9.00–11.00 0.10 under min, 0.15 over max 12.00–15.00 0.15
Molybdenum 9.00–10.50 0.15 3.50–5.00 0.10
Titanium 2.25–2.75 0.07 2.75–3.25 0.07
Aluminum 0.75–1.25 0.10 1.20–1.60 0.10
Zirconium ... ... 0.02–0.12 0.01 under min, 0.02 over max
Boron 0.003–0.01 0.002 0.003–0.01 0.002
Iron 5.00 max 0.07 2.00 max 0.05
Copper ... ... 0.50 max 0.03
Nickel RemainderA ... RemainderA ...
UNS N07500 (Formerly Grade 684) UNS N07750 (Formerly Grade 688)
Carbon 0.15 max 0.01 0.08 max 0.01
Manganese 0.75 max 0.03 1.00 max 0.03
Silicon 0.75 max 0.05 0.50 max 0.03
Phosphorus 0.015 max 0.005 ... ...
Sulfur 0.015 max 0.003 0.01 max 0.003
Chromium 15.00–20.00 0.15 under min, 0.25 over max 14.00–17.00 0.15 under min, 0.25 over max
Cobalt 13.00–20.00 0.15 under min, 0.20 over max 1.00 maxB 0.03
Molybdenum 3.00–5.00 0.10 ... ...
Columbium (Nb) + tantalum ... ... 0.70–1.20 0.05
Titanium 2.50–3.25 0.07 2.25–2.75 0.07
Aluminum 2.50–3.25 0.20 0.40–1.00 0.05 under min, 0.10 over max
Boron 0.003–0.01 0.002 ... ...
Iron 4.00 max 0.07 5.00–9.00 0.10
Copper 0.15 max 0.02 0.50 max 0.03
Nickel RemainderA ... 70.00 min 0.45
UNS N07718 (Formerly Grade 718) UNS N07080 (Formerly Grade 80A)
Carbon 0.08 max 0.01 0.10 max 0.01
Manganese 0.35 max 0.03 1.00 max 0.03
Silicon 0.35 max 0.03 1.00 max 0.05
Phosphorus 0.015 max 0.005 ... ...
Sulfur 0.015 max 0.003 0.015 max 0.003
Chromium 17.0–21.0 0.25 18.00–21.00 0.25
CobaltB 1.0 max 0.03 ... ...
Molybdenum 2.80–3.30 0.05 under min, 0.10 over max ... ...
Columbium (Nb) + tantalum 4.75–5.50 0.15 under min, 0.20 over max ... ...
Titanium 0.65–1.15 0.04 under min, 0.05 over max 1.80–2.70 0.05 under min, 0.07 over max
Aluminum 0.20–0.80 0.05 under min, 0.10 over max 0.50–1.80 0.05 under min, 0.10 over max
Boron 0.006 max 0.002 ... ...
Iron RemainderA ... 3.00 max 0.07
Copper 0.30 max 0.03 ... ...
Nickel 50.0–55.0 0.35 RemainderA ...
UNS N07752
Carbon 0.020–0.060 0.01
Manganese 1.00 max 0.03
Silicon 0.50 max 0.03
Phosphorus 0.008 max 0.003
Sulfur 0.003 max 0.001
Chromium 14.50–17.00 0.15 under min, 0.25 over max
Cobalt 0.050 max 0.03
Columbium + tantalum 0.70–1.20 0.05
Titanium 2.25–2.75 0.07
Aluminum 0.40–1.00 0.05 under min, 0.10 over max
Boron 0.007 max 0.002
Iron 5.00–9.00 0.10
Copper 0.50 max 0.03
Zirconium 0.050 max 0.01
Vanadium 0.10 max 0.01
Nickel 70.0 min 0.45
A The element shall be determined arithmetically by difference.
B If determined.

854
 PART B — NONFERROUS MATERIAL SPECIFICATIONS SB-637

5. Chemical Composition 7.1.6 Dimensions and tolerances for forging stock

shall be as agreed upon between the purchaser and the
5.1 The material shall conform to the requirements
manufacturer.
as to chemical composition prescribed in Table 1.
5.2 If a product (check) analysis is performed by
the purchaser, the material shall conform to the product
(check) analysis variations prescribed in Table 1.
8. Workmanship, Finish, and Appearance
8.1 The material shall be uniform in quality and
condition, smooth, commercially straight or flat, and
6. Mechanical Properties
free of injurious imperfections.
6.1 Tensile and Hardness Requirements — The mate-
rial shall conform to the requirements for tensile and
hardness properties prescribed in Table 2.
6.2 Stress-Rupture Requirements — The material 9. Sampling
shall conform to the requirements for stress-rupture
9.1 Lot — Definitions:
properties prescribed in Table 3.
9.1.1 A lot for chemical analysis shall consist of
one heat.
7. Dimensions and Permissible Variations
9.1.2 Mechanical Properties — A lot for tension,
7.2 Diameter, Thickness, or Width — The permissible hardness, and stress-rupture testing shall consist of all
variations from the specified dimensions of cold-worked material from the same heat, nominal diameter or
rod and bar shall be as prescribed in Table 5, and of thickness, or forging size, and condition (temper).
hot-worked rod and bar as prescribed in Table 6.
9.1.2.1 For forging stock, a lot shall consist of
7.1.1 Out of Round — Cold-worked and hot-
one heat.
worked rod, all sizes, in straight lengths, shall not be
out-of-round by more than one half the total permissible
variations in diameter shown in Tables 5 and 6, except 9.1.2.2 Where material cannot be identified by
for hot-worked rod 1⁄2 in. (12.7 mm) and under, which heat, a lot shall consist of not more than 500 lb (227
may be out-of-round by the total permissible variations kg) of material in the same size and condition (temper).
in diameter shown in Table 6.
9.2 Test Material Selection:
7.1.2 Corners — Cold-worked bar shall have practi-
cally exact angles and sharp corners. 9.2.1 Chemical Analysis — Representative samples
shall be taken during pouring or subsequent processing.
7.1.3 Cut Lengths — A specified length to which
all rod and bar will be cut with a permissible variation 9.2.1.1 Product (Check) Analysis shall be wholly
of +1⁄8 in. (3.18 mm), −0 for sizes 8 in. (203 mm) the responsibility of the purchaser.
and less in diameter or the distance between parallel
surfaces. For larger sizes, the permissible variation shall 9.2.2 Mechanical Properties — Samples of the
be + 1⁄4 in. (6.35 mm), −0. material to provide test specimens for mechanical prop-
erties shall be taken from such locations in each lot
7.1.4 Straightness for Cold-Worked and Hot-
as to be representative of that lot.
Worked Rod and Bar — The maximum curvature (depth
of chord) shall not exceed 0.050 in. multiplied by the
length in feet (0.04 mm) multiplied by the length in
centimeters. Material under 1⁄2 in. (12.7 mm) in diameter
or the distance between parallel surfaces shall be reason- 10. Number of Tests
ably straight and free of sharp bends and kinks.
10.1 Chemical Analysis — One test per lot.
7.1.5 For forgings, dimensions and tolerances shall
be as specified on the order, sketch, or drawing. 10.2 Tension — One test per lot.

855
 TABLE 2 SB-637
TENSILE AND HARDNESS REQUIREMENTSA
Yield
Tensile Strength
Strength, (0.2% offset) Elongation in Reduction
min, psi min, psi 2 in. (50 mm) of Area, Brinell
Alloy Heat Treatment (MPa) (MPa) or 4D, min, % min, % Hardness

N07252 solution + precipitation harden 160 000 90 000 20 18 310 min

(1100) (620)
N07001 solution + stabilize + precipitation harden 160 000 110 000 15B 18B 310 min
(1100) (760)
N07500 (rod and bar) anneal + solution + stabilize + precipitation harden 175 000 105 000 15 15 310 min
(1205) (725)
N07500 (forgings) solution + stabilize + precipitation harden 170 000 100 000 20 18 310 min
(1170) (690)
N07750 Type 1 solution at 2100°F (1149°C) + stabilize + precipitation harden 140 000 90 000 8 ... 262 min
(965) (620)
N07750 Type 2C solution at 1800°F (982°C) + precipitation harden 170 000 115 000 18 18 302 to 363
(1170) (790)
N07750 Type 2D solution at 1800°F (982°C) + precipitation harden 170 000 115 000 15 15 302 to 363

856
(1170) (790) (10)E (12)E
N07750 Type 3 solution anneal at 2000°F (1093°C) + precipitation harden 160 000 100 000 20 20 267–363,
(1103), min (689), min Bm
1998 SECTION II

185 000 130 000 27–40, Rc

(1276), max (896), max
N07752 Type 1 solution anneal at 1975°F (1080°C) + precipitation harden 160 000 100 000 20 20 267 to 363,
(1103), min (689), min Ba
185 000 130 000 27 to 40, Rc
(1276), max (896), max
N07752 Type 2 solution anneal at 1975°F (1080°C) + precipitation harden 140 000 85 000 20 20 ...
(965) (585)
N07718 solution + precipitation harden 185 000 150 000 12 15 331 min
(1275) (1034) (6)E (8)E
N07080 solution + stabilization + precipitation harden 135 000 90 000 20 ... ...
(930) (620)
A The supplier shall demonstrate that the material will meet fully heat-treated properties after full heat treatment in accordance with Table 4.
B Forgings.
C Up to 2.50 in. (63.5 mm), exclusive.
D 2.50 to 4.00 in. (63.5 to 101.6 mm), exclusive.
E These values apply for tension specimens machined tangentially from near the center of large disk forgings over 50 in.2 in cross section or radially from rings 3 in. (76.2 mm) or more in

thickness.
 TABLE 3
STRESS-RUPTURE REQUIREMENTSA
Test
Temperature, Stress, psi Minimum Elongation in 2 in. or 50 mm
Alloy Heat Treatment °F (°C) (MPa)B Hours (or 4D), min, %

N07252 solution + precipitation harden 1500 30 000 100 10

(816) (205)
N07001 solution + stabilize + precipitation harden 1500 33 000 100 5
(816) (230)
N07500 (rod and bar) anneal + solution + stabilize + precipitation harden 1500 38 000 100 5

857
(816) (260)
N07500 (forgings) solution + stabilize + precipitation harden 1500 38 000 100 5
(816) (260)
N07750 Type 1 solution at 2100°F (1149°C) + stabilize + precipitation harden 1350 45 000 100 5 (3 if hours exceed 136)
(732) (310)
N07718 solution + precipitation harden 1200 100 000 23 5
(649) (690)
N07080 solution + stabilize + precipitation harden 1400 47 000 23 3.5
(760) (325)
A The supplier shall demonstrate that the material will meet fully heat-treated properties after full heat treatment in accordance with Table 4.
B Test specimens meeting minimum requirements may be overloaded to produce rupture in a reasonable and practical time period.
PART B — NONFERROUS MATERIAL SPECIFICATIONS
SB-637
 SB-637

TABLE 4
HEAT TREATMENTA
Recommended Annealing Recommended Solution Recommended Stabilizing
Alloy Treatment Treatment Treatment Precipitation Hardening Treatment

N07252 ... 1950 6 25°F (1066 6 14°C), ... 1400 6 25°F (760 6 14°C), hold
hold 4 h, air cool 15 h, air cool or furnace cool
N07001 ... 1825 to 1900°F (996 to 1550 6 25°F (843 6 14°C), 1400 6 25°F (760 6 14°C), hold 16
1038°C), hold 4 h, oil or hold 4 h, air cool h, air cool or furnace cool
water quench
N07500 2150 6 25°F (1177 6 14°C), 1975 6 25°F (1080 6 14°C), 1550 6 25°F (843 6 14°C), 1400 6 25°F (760 6 14°C), hold 16
hold 2 h, air cool (bars only) hold 4 h, air cool hold 4 h, air cool h, air cool or furnace cool
N07750 Type 1 (Service ... 2100 6 25°F (1149 6 14°C), 1550 6 25°F (843 6 14°C), 1300 6 25°F (704 6 14°C), hold 20
above 1100°F) (593°C) hold 2 to 4 h, air cool hold 4 h, air cool h, air cool or furnace cool
N07750 Type 2 (Service up ... 1800 6 25°F (982 6 14°C), ... 1350 6 25°F (732 6 14°C), hold 8
to 1100°F) (593°C) hold 1⁄2 h min, cool at rate h, furnace cool to 1150 6 25°F
equivalent to air cool or (621 6 14°C), hold until total
faster precipitation heat treatment has

858
reached 18 h, air cool
N07750 Type 3 ... 1975–2050°F (1079–1121°C), ... 1300 6 25°F (704 6 14°C), hold 20
hold 1 to 2 h, air cool h, + 4 − 0 h, air cool
1998 SECTION II

N07752 Type 1 ... 1975 6 25°F (1080 6 14°C), ... 1320 6 25°F (715 6 14°C), hold 20
hold 1 to 2 h, cool by water h, + 2 − 0 h, air cool
or oil quenching
N07752 Type 2 ... 1975 6 25°F (1080 6 14°C), ... 1400 6 25°F (760 6 14°C), hold
hold 1 to 2 h, cool by water 100 h, + 4 − 0 h, air cool
or oil quenching
N07718 ... 1700 to 1850°F (924 to ... 1325 6 25°F (718 6 14°C), hold at
1010°C), hold 1⁄2 h min, cool temperature for 8 h, furnace cool to
at rate equivalent to air cool 1150 6 25°F (621 6 14°C), hold
or faster until total precipitation heat
treatment time has reached 18 h,
air cool
N07080 ... 1950 6 25°F (1066 6 14°C), 1560 6 25°F (849 6 14°C), 1290 6 25°F (699 6 14°C), hold 16
hold 8 h, air cool hold 24 h, air cool h, air cool
A The purchaser shall designate on the purchase order or inquiry any partial stage of heat treatment required on material to be shipped.
 PART B — NONFERROUS MATERIAL SPECIFICATIONS SB-637

TABLE 5
PERMISSIBLE VARIATIONS IN DIAMETER OR DISTANCE BETWEEN PARALLEL
SURFACES OF COLD-WORKED RODS AND BARS
Permissible Variations from Specified
Dimension, in. (mm)

Specified Dimension, in. (mm)A Plus Minus

Rods:
1⁄ 3
16 to ⁄16 (1.59 to 4.76), excl 0 0.002 (0.051)
3⁄ to 1⁄ (4.76 to 12.70), excl 0 0.003 (0.076)
16 2
1⁄ to 15⁄
2 16 (12.70 to 23.81), incl 0.001 (0.025) 0.002 (0.051)
Over 15⁄16 to 115⁄16 (23.81 to 49.2), incl 0.0015 (0.038) 0.003 (0.076)
Over 115⁄16 to 21⁄2 (49.2 to 63.5), incl 0.002 (0.051) 0.004 (0.102)
Bars:
1⁄ 3
16 to ⁄16 (1.59 to 4.76), excl 0 0.002 (0.051)
3⁄ to 1⁄ (4.76 to 12.7), excl 0 0.003 (0.076)
16 2

A Dimensions apply to the diameter of rods, to the distance between parallel surfaces of hexagonal, octagonal,
and square bar, and separately to width and thickness of rectangular bar.

TABLE 6
PERMISSIBLE VARIATIONS IN DIAMETER OR DISTANCE BETWEEN PARALLEL
SURFACES OF HOT-WORKED RODS AND BARS
Permissible Variations from Specified
Dimension, in. (mm)

Specified Dimension, in. (mm)A + −

Rod and bar, hot-finished:

1 (25.4) and under 0.016 (0.406) 0.016 (0.406)
Over 1 to 2 (25.4 to 50.8), incl 0.031 (0.787) 0.016 (0.406)
Over 2 to 4 (50.8 to 101.6), incl 0.047 (1.19) 0.031 (0.787)
Over 4 (101.6) 0.125 (3.18) 0.063 (1.60)
Rod, hot-finished and rough-turned
or ground:
Under 1 (25) 0.005 (0.13) 0.005 (0.13)
1 (25) and over 0.031 (0.79) 0
A Dimensions apply to the diameter of rods, to the distance between parallel surfaces of hexagonal, octagonal,
and square bar, and separately to width and thickness of rectangular bar.

859
SB-637 1998 SECTION II

10.3 Hardness — One test per lot. Test ASTM Designation

Chemical analysis E 38, E 354A

10.4 Stress-Rupture — One test per lot. Tension E 8
Rounding procedure E 29
Stress-rupture E 139

11. Specimen Preparation A Methods E 38 is to be used only for elements not covered by
11.1 Rod and Bar: Test Methods E 354.

11.1.1 Tension test specimens shall be taken from 12.2 For purposes of determining compliance with
material in the final condition (temper) and tested in the specified limits for requirements of the properties
the direction of fabrication. listed in the following table, an observed value or a
calculated value shall be rounded in accordance with
11.1.2 All rod and bar shall be tested in full cross- the rounding method of Practice E 29.
section size when possible. When a full cross-section
size test cannot be performed, the largest possible round Rounded Unit for Observed
Test or Calculated Value
specimen shown in Test Methods E 8 shall be used.
Longitudinal strip specimens shall be prepared in ac- Chemical composition, toler- Nearest unit in the last right-
cordance with Test Methods E 8 for rectangular bar ances (when expressed in hand place of figures of the
up to 1⁄2 in. (12.7 mm), inclusive, in thickness, which decimals), and hardness specified limit. If two choices
are possible, as when the dig-
are too wide to be pulled full size. its dropped are exactly a 5 or
a 5 followed only by zeros,
11.1.3 Forging stock test specimens shall be taken choose the one ending in an
from a forged-down coupon or a sample taken directly even digit, with zero defined
from stock. as an even digit.
Tensile strength and yield Nearest 1000 psi (6.9 MPa)
strength
11.2 Forgings:
Elongation Nearest 1%
Rupture life 1h
11.2.1 The tension test specimen representing each
lot shall be taken from a forging or from a test
prolongation.
13. Inspection
11.2.2 The axis of the specimen shall be located 13.1 Inspection of the material shall be made as
at any point midway between the center and the surface agreed upon between the manufacturer and the purchaser
of solid forgings and at any point midway between as part of the purchase contract.
the innner and outer surfaces of the wall of hollow
forgings, and shall be parallel to the direction of greatest
metal flow.
14. Rejection and Rehearing
11.2.3 The specimens shall be the largest possible 14.1 Material, tested by the purchaser, that fails to
round-type shown in Test Methods E 8. conform to the requirements of this specification may
be rejected. Rejection should be reported to the producer
11.3 Stress-rupture specimens shall be the same as or supplier promptly and in writing, in case of dissatis-
tension specimens except modified as necessary for faction with the results of the test, the producer or
stress-rupture testing in accordance with Practice E 139. supplier may make claim for a rehearing.

15. Certification
12. Test Methods
15.1 When specified in the purchase order or contract,
12.1 Determine the chemical composition, mechanical a producer’s or supplier’s certification shall be furnished
and other properties of the material as enumerated in to the purchaser that the material was manufactured,
this specification, in case of disagreement, in accordance sampled, tested, and inspected in accordance with this
with the following methods: specification and has been found to meet the require-

860
PART B — NONFERROUS MATERIAL SPECIFICATIONS SB-637

ments. When specified in the purchase order or contract,

a report of the test results shall be furnished.

16. Product Marking

16.1 Each bundle or shipping container shall be
marked with the name of the material; condition (tem-
per); this specification number; the size; gross, tare, and
net weight; consignor and consignee address; contract or
order number; or such other information as may be
defined in the contract or order.

861