Lecture Notes Physical Mineral Processes Alle Lectures
Lecture Notes Physical Mineral Processes Alle Lectures
Lecture Notes Physical Mineral Processes Alle Lectures
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SAMPLING
Objectives:
Sampling is the process of securing, a representative fraction/ lot for some purpose
such as assaying. Basic rule for correct sampling: Each particle of ore or concentrate
must have an equal probability of being collected and becoming part of the final sample
for analysis.
Sampling for feasibility: field samples, drill core, bulk sampling (trenching and mined
sample)
Sampling for plant/ operation: Blasthole cutting piles. ROM samples, mill feed,
crusher, mill,. Cons & tailings samples
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Select Sample Size for Desired Precision, Accuracy, and Confidence – Gy’s
Method
W = C x [d3/σ2]
Sampling Error Variance determined by Pierre Gy, 1982
σ2 = C d3 / W
Where:
σ2 - sampling error variance (S2)
C - Sampling constant which is a function of
material characteristics.
d - Nominal top size (95% passing IN cm!!)
W - Sample mass, g
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L – liberation factor
L = (dL/d)0.5
Where in the case of gold mineralization, the value of b is almost always experimentally
found close to 1.5.
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Ore Characterization
Outline
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• These tests can take two forms. The first is the Standard Bond
Crushing Test, which has a requirement of twenty pieces of rock or
core of size +50 – 75 mm (+2” – 3”). Pieces are placed in a twin
pendulum device and impacted to failure to produce an impact
crushing strength, measured in kWh per tonne of ore.
• Twenty specimens are tested to provide a measure of variability of
results, as there is a tendency towards heterogeneity in rocks of
larger sizes. The standard index is used primarily by crusher
manufacturers to assign down rating factors for ore toughness in
crusher selection.
Single Particle Methods (AG and SAG)
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It was noticed that the method can be used unless the Wic and Wir
are significantly higher than the Wib, in which case SABC is indicated
and E (SAG) can be discounted by 10% to arrive at a power efficient
SABC design.
The Barratt Approach and Siddall Approach methods have been found to
predict the single stage grinding power required in a AG/SAG mill. In both
methods, there is a reliance on either pilot plant data or database
correlations in order to establish T 80 (SAG transfer size), and hence the
SAG mill power in a two-stage grinding circuit.
Ore Characterization test requirements for SAG/AG mills.
• Test particles over the entire size range of SAG mill feed for both
impact and abrasion breakage, to determine energy levels expected in
commercial mills
• Determine media competency;
• Slow examination of steady-state mill load characteristics (critical
sized material);
• Generate a breakage vs. energy level map for simulation
• Must be reproducible (need representative samples);
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Unconfined Compressive
Strength Test-1
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The test provides excellent insight into impact breakage and auto
abrasion characteristics of ores, but is currently only performed in a
few laboratories around the world.
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Introduction
In 1951 Mr. Fred C. Bond of the Allis Chalmers Co. proposed his third theory of
comminution. Mr. Bond developed his work index (Wi), which is used extensively to
determine power input. This session describes methods of determining mill power (used
as the basis of mill sizing) and ore testing.
Finding the minimum operating cost to attain the desired final grind
(consumables and power) &
The most efficient circuit is the one that allows the greatest rate of return to a
project.
Mill Power
• Around half the energy used in most mineral processing plant is consumed in
grinding. Usually, it is the single biggest operating cost item, and good energy
utilization is critical to project economics.
• Sizing of grinding mills is mostly carried out by determining the energy required for
the duty and selecting an appropriate unit to deliver that energy.
• Determining the specific energy required can often be done by laboratory testing.
Two forms of testing are common:
‒ Single particle tests e.g. the Impact test or the Drop Weight Test.
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The Bond Grinding Indices are for predicting rod and ball mill power
requirements. They can also be used by operators to assess the power efficiency
of an existing circuit, as explained below. However, the Bond BWI is not a good
predictor of AG/SAG mills unless adapted using empirical factors.
In order to assess AG/SAG behavior, single particle tests have been devised
which look at the energy required to break the particle under impact conditions,
and the relationship between the energy applied and the size distribution of the
“daughter” products.
1 1
W 10 Wi
P80 F80
PRIMARY
CRUSHER FEED PRODUCT
CYCLONE
SCREEN
ROD BALL
MILL MILL
SECONDARY TERTIARY
CRUSHING CRUSHING
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With most materials, for the same range of work, dry grinding requires 1.3 times as
much power as wet grinding. In some special cases, this correction factor can be as low
as 1.1 or great as 2.0
For ball milling, EF2 is a function of the degree of control required on the circuit
product. Open circuit inefficiency factors are as follows:
Using a base diameter of 2.44 m (8’) inside liners the correction for other diameters (in
meters) is given by: 0.2
2.44
EF 3
D
The minimum value applied for EF3 is 0.914 for practical design purposes.
• The influence of Rr should be assessed with caution in the first stage of a two-
stage circuit.
• Do not use EF4 for rod mill prepared feed to a ball mill and do not apply if EF4
< 1.0
F Fo
Rr (Wi 7)
EF 4 o
F
Rr
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EF 5
P80 10.3
1.145 P80
EF 6 1
Rr Ro 2
150
Where:
5L
Ro 8
D
D = inside liner diameter of rod mill (meters)
L = length of rods (meters) = Rod Mill Inside L – 0.15
Rr = Reduction ratio
If the Rr ,or reduction ratio, of the ball feed to product drops below 6, use the EF7
correction factor. The lower the Rr the more power required.
EF 7
2 ( Rr 1.35) 0.26
2 ( Rr 1.35)
Note: Do not apply an EF7 factor greater than 2.0 without conducting continuous test
work.
• When calculating rod mill power for rod milling only, an EF8 value of 1.4 is
used when the feed is prepared by open circuit crushing and 1.2 in closed circuit.
• For Rod/Ball circuits 1.2 is used for the rod milling stage only, if the feed is
prepared in open circuit.
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• With respect to wear resistance, rubber liners are best suited for ball diameters
up to 80 mm.
• Steel liners are best suited to primary ball milling applications requiring larger
than 80 mm balls and rod mills, and ball mills larger than 16.5 ft in diameter.
• EF9 is applied to mills with rubber lifters, as they tend to be somewhat bulkier
than the equivalent steel configuration, reducing the available grinding space.
• Rubber liners also absorb a portion of the impact energy of the steel media,
reducing efficiency.
• It does not predict the behavior of large rocks in grinding circuit where the mode
of breakage is impact dominated versus attrition and abrasion in ball mills
(SAG/AG Mills).
• The Bond Work Index is based on the energy per unit mass required to reduce a
particle from “infinite” size to 80% passing 100 μm. If the P 80 is less than 100
μm, serious discrepancies can occur. The closing screen in the Bond test must
reflect the size to which the particle is to be ground.
• The F80 may be the same, but the amount of fines at say F30 or F20 may be
markedly different.
• A size distribution correction may be necessary to better predict 2nd stage power
requirements for:
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42.31 76.63
N c (rpm) Nc
D D
(D in meters) (D in feet)
• Power drawn is proportional to mill speed, suggesting that mills should be run as
fast as possible.
• However, the useful work done by the grinding charge is related to the mode of
breakage induced, which is in turn influenced by the liner design and charge
level.
Speed guidelines
• Studies such as on the previous slide have produced the following general
guidelines:
• SAG Mills - Typical operating speeds are around 75% N c. Liner damage will
occur if the balls are allowed to impact them directly, and SAG mills usually
have variable speed drives.
• Fine Grinding:
For fine grinding, it is desirable to have the charge cascading rather than
cataracting. This is achieved by selecting a lower mill speed and/or using a wave
liner profile.
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• Impact Breakage
For breakage of larger feed particles, the grinding balls should strike the charge
close to the toe. Higher lifter bars and mill speeds will assist.
• There is also a standard method which uses the size distributions of the streams
to derive a mass balance.
• Use these techniques to check that the mill is grinding the optimum tonnage by
maintaining the target CLR.
Summary
• A key aspect for sizing and selecting grinding mills is to determine the power
required.
• Bond's equation works well for ball mills, but must be modified with efficiency
factors.
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Introduction
The objective is to describe methods of sizing ball and rod mills once the grinding
power requirements for these have been determined. The approach to sizing SAG mills
is fundamentally similar to ball mills with modification for the effect of grates on the
charge, aspect ratio and pebble crushing.
Mill Sizing
Drive Selection
Motor Selection
Mill Discharge and Feed System Selection
Factors that influence Mill sizing: Mill speed. Mill diameter & length, mill discharge
opening size, type of discharge mill head, amount/ size of grinding media, feed size,
feed SG, ore hardness, feed rate, water addition (viscosity).
1. Mill Speed
P s = KTω
Where:
• P s = Power transmitted through shaft from motor
• K = Constant
• T = Torque
• ω = RPM
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2. Mill Dimensions
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Grate discharge draw more power than overflow due to the distance from centroid to
mill center
Critical Speed is the speed at which a ball or rod will be centrifuged in the mill
76.63
Wc Dd
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6. Feed Rate
• The mill work input to grind a tonne of feed of 80 % passing size (F80) to a
product passing size of 80 % (P 80) is calculated by the Bond equation:
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• W = 10 Wi [1/P80 - 1/F80]
where:
W = work input in kWh/t
Wi = Bond Work Index in kWh/t
• WCOR is multiplied by the new mill fresh feed tonnage T to give the mill power
requirement P = T * WCOR
• This is the power that must be applied at the mill drive in order to grind the feed
tonnage T from one size distribution F80 to a finer product size distribution P 80.
• Once the mill power is determined the mill size to draw the required power must
be calculated.
• Power draw theory is based upon a charge load in equilibrium, and relates to its
center of gravity.
Mill Grinding Power and Sizing Calculation: Matching Mill Size to Power
Requirement 2
• W = weight of charge
• D = Diameter
C = distance of center of gravity of charge from
center of mill in feet
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An early theoretical power model of DuPont (1900’s) shows the effect of charge weight,
mill diameter and mill speed on the power draw per unit of mill length (P/L) :
P ∝ D2.5 *L
Therefore the selection of larger diameter (and fewer) mills can significantly reduce the
number of mills required in an application.
‒ manufacturing methods
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There are practical limitations. Currently the largest mills are about:
Summary
• Tumbling mills are sized to deliver the power required to achieve the desired
grind size.
• Several factors influence power draw, including mill speed, dimensions, type,
feed size, type and rate.
• Power draw theory is based upon a charge load in equilibrium, and relates to its
center of gravity
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Exercise: Size a single stage ball mill (overflow) in closed circuit with a cyclone with
the following parameters:
PRIMARY
CRUSHER FEED PRODUCT
CYCLONE
SCREEN
ROD BALL
MILL MILL
SECONDARY TERTIARY
CRUSHING CRUSHING
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• The feed to a standard Bond ball mill grindability test is minus 6 mesh (3360μm)
• However the coarser fraction of a minus ½” single-stage ball mill feed is not
included in the feed to the grindability test mill
• If RWI is different than BWI, then particularly if the former is higher, a two
step calculation should be used to determine the grinding power input, using
2100 μm to divide the calculations.
Step 1:
W = 10 * (13.2 - 13.2) = 1.52 kWh/st
2,100 9,400
Step 2:
W = 10 *(11.7 - 11.7) = 6.29 kWh/st
175 2,100
Step 3:
Total = 1.52 + 6.29 = 7.81 kWh/st
= 7.81 * 1.102* 1.341* 500
= 5766 HP, uncorrected
Where:
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HP = A * B * C * L
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Most overflow discharge ball mills operate with a charge volume that occupies
35% to 45% of the mill volume.
The B Factor must be adjusted to the steel density of the balls (340/315).
To relate critical speed and peripheral speed as mill diameter increases, the average
recommended speed as % of critical speed is shown in the table on the following slide.
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Step 8: -cont-
Through an iterative process, you can find the mill diameter will be >15 ft, therefore use
a speed of 68% of critical.
Being free from the limits imposed on rod mills, ball mills have more variation in length
to diameter ratios, ranging from 1:1 to 2:1. The ratio used varies with
Based on the preceding table, wet milling and a F80 of 9,400 mm and P 80 of 175 microns
(not fine regrind) a L/D ratio of 1.25 is selected.
Step 10:
Calculate Mill Diameter (Inside liners):
Power Equation
Rearranging:
31,075 = D3.5
D = 19.2 feet (inside liners)
L = 1.25 * 19.2
L = 24.0 feet
Step 11:
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Select a 20.0 ft inside shell diameter by 24.0 ft long overflow ball mill @ 40% ball
charge and running at 5,903 hp.
Step 12:
Calculate Maximum Ball Size for Mill Charge:
The equations for selecting the largest diameter (in inches) rod (R) or ball (B) in the
initial mill charge, or make-up charge, for a mill of diameter D is:
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Multiply by the power draw (kw) and divide by feed rate of 500 t/h to give consumption
in kg/t.
Overflow Discharge:
• Suitable for almost all applications
• Simple and trouble-free.
• The discharge trunnion can be furnished with a trommel screen.
Grate Discharge:
• 15-20% higher capacity per unit volume
• Coarser product with high circulating load producing little extreme fines.
• Can have a trommel screen as well.
• Overflow: Common for wet mill rod milling. Diameter of discharge trunnion is
larger than feed to promote flow.
• End Peripheral Discharge: Used when a coarse product is required.
• Center Peripheral Discharge: Suitable for dry grinding at extremely high capacities
and coarse grinding, wet or dry. Also applicable for viscous material and moisture
content 3-15% by mass.
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Summary
Mill sizing led to the selection of:
• A 20.0 ft inside shell diameter by 24.0 ft long overflow ball mill @ 40% ball
charge and running at 5,903 hp.
• Ball size: 2.5 in.
• Ball wear estimate: 0.86 kg/t
• Liner wear estimate: 0.064 kg/t
• Feeder/Discharge Arrangement:
‒ Overflow mill with a spout feeder
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All mining projects pass through a series of stages over the project life that includes:
exploration, discovery, development, production, reclamation/ abandonment.
Steps of mineral development project can be summarized into a few step starting from
geological exploration, mineralogical studies, lab & pilot tests, engineering studies
(mine planning and design).
Transforming an ore into rocks will involve the existence of raw material, technology,
market, economic aspects, and also environmental & social issues.
Rocks, tailing, industrial minerals, recycled materials, and garbage are raw material.
Technology used in one mineral deposit can be adapted or modified to be used in other
similar deposits, but generally not copied.
Definitions:
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Process Development
The flow sheet is critical to establish: design criteria, mass balance, water balance,
energy balance, tailing disposal, plant lay-out, equipment sizing, and costs!
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Key Information for Process flowsheet definition: grades, ore minerals, gangue
minerals. Mineralogical factors, physical properties, chemical properties, liberation,
process recovery.
Definition of Grade
• Very often people make decisions just based on the ore grades…this is wrong
• An ore can have a very high grade but the MINERALS are not concentrable
• Example: Vale Salobo Weathered Copper Ore: Cu adsorbed on FeOOH
• The ore has 2% Cu but cannot be concentrated
We mine ore but we concentrate ore minerals. From ore minerals we extract metals.
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Sometimes it is not possible to concentrate ore mineral. There is no specific ore mineral
to be concentrated, ore mineral is friable then the option is to leach the ore with a
specific reagent usually using “heap leaching”
Grade and recovery are interdependent for a given feed composition. Because liberation
is usually incomplete, even in a well-run separation unit, there is a trade-off between
grade and recovery. If the grade of a product increases, recovery drops. If the grade
decreases, recovery rises.
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Summary
• A geological anomaly does not become an ore body until a process has been
developed that can economically recover the valuable minerals
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Class Objectives:
Course Objectives:
Overall Objective: To produce high quality engineers who are in great demand within
the mining industry.
Definitions
Mineral Processing
The technology of economically converting mineral bearing raw material into individual
mineral constituents; the minerals remaining essentially unaltered in physical and
chemical form throughout. The temperature of the system normally is less than the
boiling point of water. Mineral processing is also known as mineral beneficiation,
milling or concentration.
Unit Operation
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Mineral Processing
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• Equipment Sizing
• Operations/Production Engineer
2. Environmental Review
5. Marketing Study
Operations/Production Engineer
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Sieving Procedure
• Rotap with stack of sieves with largest sieve
at the top.
• Mesh size is the number of openings per
square inch (i.e. larger mesh number corresponds
to smaller size).
• Tyler Sieves, US Mesh Number, Canadian
Mesh Number
• Convention is 2 series (successive meshes
vary by 2)
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100
Cumulative % passing
90
80
70
60
50
40
30
20
10
0
20 100 500
Particle size [microns]
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Gaudin-Schuhmann Function
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Special graph paper available to plot cum. % retained values directly on the Y-axis. A line at cum.%
retained = 36.8 is included for estimation of a
The function was originally developed for coal, but has been found to fit many mineral size
distributions very well, especially finely ground material (e.g. ball mill product)
Stoke’s Law
Stokes’ Law predicts larger particles settle faster than smaller ones and this principle can be
exploited to separate particles by size
v = d2g(ρs - ρf )
18η
where:
v = free falling velocity (cm/sec)
d = particle Stokes’ diameter (cm)
g = acceleration due to gravity (m/s2)
ρs = solid density (g/cm3)
ρf = fluid density (g/cm3)
η = fluid viscosity (cp)
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Summary
• Many online particle size analyzers require regular calibration (sieving used to generate
calibration data)
• Optical methods do not provide reliable estimates of fines
• Fine screening may need to be done wet or using wet pre-screening (eg. removing -38
micron fines)
• Sieves generally cannot be used reliably below 38 microns
• Samples need to be completely dry (oven) prior to sieving