BS 1881-106 Concrete Air Content
BS 1881-106 Concrete Air Content
BS 1881-106 Concrete Air Content
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Testing concrete —
Part 106: Methods for determination of
air content of fresh concrete
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UDC 666.972.017:691.32:620.1
BS 1881-106:1983
This British Standard was published under the direction of the Cement,
Gypsum, Aggregates and Quarry Products Standards Committee CAB/–. Its
preparation was entrusted to Technical Committee CAB/4 upon which the
following bodies were represented:
The following bodies were also represented in the drafting of the standard,
through subcommittees and panels:
This British Standard,
having been prepared under
the direction of the Cement, British Civil Engineering Test Equipment Manufacturers’ Association
Gypsum, Aggregates and Coopted members
Quarry Products Standards
Committee, was published
under the authority of the
Standards Board and comes
into effect on Amendments issued since publication
31 May 1983
Amd. No. Date of issue Comments
© BSI 12-1998
6068 July 1989
The following BSI references
relate to the work on this 6723 July 1991 Indicated by a sideline in the margin
standard:
Committee reference CAB/4
Draft for comment 81/12319 DC
Contents
Page
Committees responsible Inside front cover
Foreword ii
1 Scope 1
2 Definitions 1
3 Sampling 1
4 Preparing the sample for test 1
5 Method A 1
6 Method B 5
7 Calculation and expression of results 9
8 Report 9
Figure 1 — Method A apparatus 3
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© BSI 12-1998 i
BS 1881-106:1983
Foreword
This Part of this British Standard, prepared under the direction of the Cement,
Gypsum, Aggregates and Quarry Products Standards Committee, is a revision of
clause 6 of BS 1881-2:1970. This revision includes two methods of measuring the
total air content, one of which is a revision of the method included in the 1970
edition.
Testing in accordance with both methods given in this Part of this standard will
comply with ISO 4848. Together with Parts 102, 103, 104 and 107, this Part of
BS 1881 supersedes BS 1881-2:1970, which is withdrawn.
No estimate of repeatability or reproducibility is given in this Part of this British
Standard. Reference should be made to BS 5497-1 for further information on the
determination of repeatability and reproducibility.
A British Standard does not purport to include all the necessary provisions of a
contract. Users of British Standards are responsible for their correct application.
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Summary of pages
This document comprises a front cover, an inside front cover, pages i and ii,
pages 1 to 10, an inside back cover and a back cover.
This standard has been updated (see copyright date) and may have had
amendments incorporated. This will be indicated in the amendment table on
the inside front cover.
ii © BSI 12-1998
BS 1881-106:1983
1 Scope b) Mixing the sample. The coning procedure is not suitable for
very high workability concrete and the following alternative
This Part of this British Standard describes two method of mixing is recommended. Having poured the
methods for determination of air content of concrete on to the sampling tray, use the shovel to turn the
concrete from the outside toward the centre, working
compacted fresh concrete, made with normal weight progressively once round all sides of the sampling tray.
or relatively dense aggregate having a nominal CAUTION. When cement is mixed with water,
maximum size of 40 mm or less. Neither of the alkali is released. Take precautions to avoid dry
methods is applicable to aerated concrete, very stiff cement entering the eyes, mouth and nose when
concrete which cannot be compacted by vibration mixing concrete. Prevent skin contact with wet
alone nor to concrete made with lightweight cement or concrete by wearing suitable protective
aggregates, air cooled blast-furnace slag or clothing. If cement or concrete enters the eye,
aggregates of high porosity. immediately wash it out thoroughly with clean
NOTE The titles of publications referred to in this standard are water and seek medical treatment without delay.
listed on the inside back cover.
Wash wet concrete off the skin immediately.
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2 Definitions 5 Method A
For the purposes of this Part of this British
5.1 General. In this method, the operational
Standard, the definitions given in BS 5328 and
principle consists of introducing water to a
BS 1881-101 apply.
predetermined height above a sample of concrete of
known volume and the application of a
3 Sampling predetermined air pressure over the water. The
Obtain the sample of fresh concrete by the reduction in volume of the air in the concrete sample
procedure given in BS 1881-101 or BS 1881-125. is measured by observing the amount the water
Commence the determination of air content as soon level is lowered under the applied pressure, the
as possible after sampling. latter amount being calibrated in terms of
percentage of air in the concrete sample.
4 Preparing the sample for test 5.2 Apparatus
4.1 Apparatus 5.2.1 General. The apparatus, one form of which is
4.1.1 Sampling tray, minimum shown diagrammatically in Figure 1, consists of the
dimensions 900 mm × 900 mm × 50 mm deep of following.
rigid construction and made from a non-absorbent 5.2.2 Container. A flanged cylindrical vessel of steel
material not readily attacked by cement paste. or other hard metal, not readily attacked by cement
4.1.2 Square mouthed shovel, size 2 in accordance paste, having a nominal capacity of at least 5 L and
with BS 3388. a ratio of diameter to height of not less than 0.75 nor
4.2 Procedure. Empty the sample from the more than 1.25. The outer rim and upper surface of
container(s) on to the sampling tray. Ensure that no the flange and the interior surfaces of the vessel
more than a light covering of slurry is left adhering shall be machined to a smooth finish. The container
to the container(s). shall be watertight and in addition it and the cover
assembly shall be suitable for an operating pressure
Thoroughly mix the sample by shovelling it to form of approximately 100 kN/m2 and be sufficiently rigid
a cone on the sampling tray and turning this over to limit the pressure expansion constant, D,
with the shovel to form a new cone, the operation (see 5.3.4) to not more than 0.1 % air content.
being carried out three times. When forming the
cones deposit each shovelful of the material on the 5.2.3 Cover assembly. A flanged rigid conical cover
apex of the cone so that the portions which slide fitted with a standpipe. The cover shall be of steel or
down the sides are distributed as evenly as possible other hard metal not readily attacked by cement
and so that the centre of the cone is not displaced. paste and shall have interior surfaces inclined at not
Flatten the third cone by repeated vertical insertion less than 10° from the surface of the flange. The
of the shovel across the apex of the cone, lifting the outer rim and lower surface of the flange and the
shovel clear of the concrete after each insertion. sloping interior face shall be machined to a smooth
finish. The cover shall have provision for being
NOTE The following modifications to the mixing procedures
may be necessary when preparing samples of very high clamped to the container to make a pressure seal
workability concrete (e.g. superplasticized concrete) for test. without entrapping air at the joint between the
a) Sampling tray. The vertical lips on the edges of the tray flanges of the cover and the container.
may have to be larger to contain the sample without spillage
during mixing.
© BSI 12-1998 1
BS 1881-106:1983
The standpipe shall consist of a graduated glass 5.2.11 Compacting bar or vibrator. Compacting bar
tube of uniform bore, or a metal tube of uniform bore made from iron or steel, weighing 1.8 ± 0.1 kg,
with a glass gauge attached. The graduated scale at least 380 mm long and having a ramming
shall indicate air content from 0 % to at least 8 % face 25.0 ± 0.5 mm square, or a vibrating hammer
and preferable 10 %. The scale shall be graduated or table suitable for compacting the concrete in
with divisions every 0.1 % air content, the divisions accordance with 5.5.2 or 5.5.3.
being not less than 2 mm apart. A scale in 5.2.12 Container with spout. A container fitted with
which 25 mm represents 1 % of air content is a spout having a capacity of 2 L to 5 L to fill the
convenient. apparatus with water.
The cover shall be fitted with a suitable device for 5.2.13 Mallet. A soft-faced mallet with a mass of
venting of the air chamber, a non-return air inlet approximately 250 g.
valve and a small valve for bleeding off water. The
applied pressure shall be indicated by a pressure 5.2.14 Balances. A balance capable of weighing up
to 1 kg to an accuracy of ± 0.5 g over the range used
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2 © BSI 12-1998
BS 1881-106:1983
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© BSI 12-1998 3
BS 1881-106:1983
5.3.6 Required operating pressure. Place the 5.4.2 Aggregate sample size. Determine the
calibration cylinder support centrally on the bottom aggregate correction factor by applying the
of the clean container and place the cylinder on the operating pressure on a combined sample of the
support with its open end downward. Place the coil coarse and fine aggregates in the approximate
spring on the cylinder and clamp the cover assembly proportions and moisture conditions that exist in
carefully in place. the concrete sample. Obtain the sample of
Fill the apparatus with water at ambient aggregates either by washing the cement from the
temperature to a level above the zero mark on the concrete sample tested for air content, through
air content scale. Close the air vent and pump air a 150 µm BS 410 sieve, or by using a combined
into the apparatus approximately to the operating sample of fine and coarse aggregate similar to that
pressure (about 100 kPa). Lightly tap the sides and used in the concrete. In the latter case calculate the
cover with the mallet to remove as much entrapped masses of fine and coarse aggregates to be used, mf
air as possible adhering to the interior surfaces of and mc, respectively as follows:
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4 © BSI 12-1998
BS 1881-106:1983
Record the reading of the gauge tube as h1, release 5.5.3 Compacting with the vibrator. When
the pressure and take a further reading, h2. Repeat compacting each layer by means of the vibrating
the entire procedure once, obtaining a second pair of hammer or table use applied vibration of the
readings, h1 and h2. Take the average value minimum duration necessary to achieve full
of h1– h2 as the aggregate correction factor, G, compaction of the concrete. Over-vibration may
unless the two values of h1 – h2 differ by more cause excessive segregation and laitance or loss of
than 0.1 % air content in which case carry out entrained air, if present. The required duration of
further determinations until consistent results are vibration will depend upon the consistency of the
obtained. concrete and the effectiveness of the vibrator and
5.5 Compaction of the concrete vibration shall cease as soon as the surface of the
concrete becomes relatively smooth and has a glazed
5.5.1 General. Place the sample of concrete to be appearance. Record the duration of vibration.
tested in the container in such a way as to remove as
much entrapped air as possible (without 5.6 Procedure. Wipe the flanges of the container
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significantly reducing the amount of entrained air, and of the cover assembly thoroughly clean and in
if present) and to produce full compaction of the the absence of the spray tube, place the deflecting
concrete with neither excessive segregation nor plate, if used, centrally on the concrete and pressed
laitance. For this purpose, by means of the scoop, into contact with it. Clamp the cover assembly in
place the concrete in the container in three layers place, care being taken to ensure that there is a good
approximately equal in depth and compact each pressure seal between the cover and the container.
layer by using either the compacting bar or the Fill the apparatus with water and tap lightly with
vibrator in the manner described below in 5.5.2 the mallet to remove air adhering to the interior
or 5.5.3. If the concrete has a slump greater than surfaces of the cover. Bring the level of water in the
approximately 75 mm, do not use vibration. standpipe to zero by bleeding through the small
valve with the air vent open. Close the air vent and
The quantity of material used in the final layer shall apply the operating pressure, P, by means of the air
be, as nearly as possible, just sufficient to fill the pump.
container without having to remove excess material.
A small quantity of additional concrete may be Record the reading on the gauge tube, h1, and
added if necessary and further compacted in order release the pressure. Read the gauge tube again and
to just fill the container, but the removal of excess if the reading, h2 is 0.2 % air content or less record
material should be avoided. the value h1 – h2 as the apparent air content, A1, to
the nearest 0.1 % air content. If h2 is greater
5.5.2 Compacting with compacting bar. When than 0.2 % air content apply the operating pressure,
compacting each layer with the compacting bar, P, again, giving a gauge tube reading h3 and a final
distribute the strokes of the compacting bar in a reading h4 after release of the pressure. If h4 – h2
uniform manner over the cross section of the is 0.1 % air content or less record the value h3 – h4
container, and ensure that the compacting bar does as the apparent air content. If h4 – h2 is greater
not penetrate significantly any previous layer nor than 0.1 % air content it is probable that leakage is
forcibly strike the bottom of the container when occurring and the test shall be disregarded.
compacting the first layer. The number of strokes
per layer required to produce full compaction will 6 Method B
depend upon the consistence of the concrete but in
no case shall the concrete be subjected to fewer 6.1 General. In this method the operational
than 25 strokes per layer. In order to remove principle consists of merging a known volume of air
pockets of entrapped air but not the entrained air, at a known pressure in a sealed air chamber with
after compaction of each layer tap the sides of the the unknown volume of air in the concrete sample,
container smartly with the mallet until large the dial on the pressure gauge being calibrated in
bubbles of air cease to appear on the surface and terms of percentage of air for the resultant pressure.
depressions left by the compacting bar are removed.
Record the number of strokes.
© BSI 12-1998 5
BS 1881-106:1983
approximately 200 kN/m2. stating the accuracy shall be obtained from the
6.2.3 Cover assembly. A flanged rigid cover of steel organization carrying out the check.
or other hard metal not readily attacked by cement Fill the container with water at ambient
paste. The outer rim and lower surface of the flange temperature and place the transparent plate over it
as well as the interior surfaces shall be machined to to eliminate any convex meniscus. Smear a thin film
a smooth finish. The cover shall have provision for of grease on the flange of the container to effect a
being clamped to the container to make a pressure water tight joint between the transparent plate and
seal without entrapping air at the joint between the top of the container. Wipe away surplus water
flanges of the cover and the container. and determine the mass of the container filled with
The cover assembly shall be fitted with a pressure water by weighing on the balance. Screw the
gauge calibrated to indicate air content from 0 % to extension tubing (see Figure 2) into the threaded
at least 8 % and preferably 10 %. Up to an air hole beneath valve A on the underside of the cover
content of 6 % the scale of the gauge shall be assembly and clamp the cover assembly into place,
graduated with divisions every 0.1 % air content. care being taken to ensure that there is a good
6.2.4 Calibration cylinder. A hollow cylindrical pressure seal between cover and container. Close
measure of brass or other non-corrodible metal the main air valve and open valves A and B. Add
water through valve A until all trapped air has been
having a capacity of approximately 0.3 L, which may
expelled through valve B. Pump air into the air
be integral with the cover assembly.
chamber until the pressure reaches the indicated
6.2.5 Transparent plate. A rigid transparent plate, initial pressure line. After allowing a few seconds for
suitable for use as a closure for the container. the compressed air to cool to ambient temperature,
6.2.6 Air pump. A hand pressure pump such as a stabilize the hand on the pressure gauge at the
bicycle tyre pump with a lead facilitating connection initial pressure line by further pumping in or
to the non-return air inlet valve on the cover bleeding off air as necessary. During this process
assembly. lightly tap the gauge and close valve B.
6.2.7 Scoop, as described in 3.1 of Remove water from the apparatus to the calibration
BS 1881-101:1983. cylinder in just sufficient quantity to fill it full or up
to a predetermined line marked on it, then
6.2.8 Compacting bar or vibrator. Compacting bar
determine the mass of water displaced, m3, by
made out of straight steel bar weighing on the balance.
weighing 1.8 kg, 380 mm long and having a
ramming face 25 mm square, or a vibrating hammer
or table suitable for compacting the concrete in
accordance with 6.5.
6 © BSI 12-1998
BS 1881-106:1983
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© BSI 12-1998 7
BS 1881-106:1983
8 © BSI 12-1998
BS 1881-106:1983
allowing a few seconds for the compressed air to cool 7.3 Precision. Precision data are given in Table 1.
to ambient temperature stabilize the hand on the These apply to air content measurements made by
pressure gauge at the initial pressure line by method A on concrete taken from the same sample
further pumping in or bleeding off air as necessary. when each test result is obtained from a single air
During this process lightly tap the gauge. Close both content determination
valve A and valve B and then open the main air Table 1 — Precision data for air content
valve. Tap the sides of the container sharply.
measurements
Lightly tap the pressure gauge to stabilize it and
then the reading of the pressure gauge is equal to Repeatability Reproducibility
Level
conditions conditions
the apparent percentage of air, A. Open valves A
and B in order to release the pressure before the sr r sR R
cover assembly is removed. % % % % %
7 Calculation and expression of results 5.6 0.16 0.4 0.45 1.3
NOTE 1 The precision data were determined as part of an
7.1 Air content of the sample tested. Calculate experiment carried out in 1987 in which precision data were
the air content of the concrete in the container, Ac, obtained for several of the tests described in BS 1881. The
from the formula: experiment involved 16 operators. The concretes were made
using an ordinary Portland cement, Thames Valley sand, and
Ac = A1 – G Thames Valley 10 mm and 20 mm coarse aggregates.
where NOTE 2 The difference between two tests results from the
same sample by one operator using the same apparatus within
the shortest feasible time interval will exceed the repeatability
A1 is the apparent air content of the sample value r on average not more than once in 20 cases in the normal
and correct operation of the method.
tested, to the nearest 0.1 % (see 5.6 and 6.6); NOTE 3 Test results on the same sample obtained within the
G is the aggregate correction factor to the shortest feasible time interval by two operators each using
their own apparatus will differ by the reproducibility value R
nearest 0.1 % (see 5.4.4 and 6.4.4). on average not more than once in 20 cases in the normal and
correct operation of the method.
Express the air content as a percentage to the NOTE 4 For further information on precision, and for
nearest 0.1 %. definitions of the statistical terms used in connection with
precision, see BS 5497-1.
7.2 Air content of the mortar fraction. If
required, calculate the air content of the mortar
8 Report
fraction of the concrete, Am, from the formula:
8.1 General. The report shall affirm that the air
100Ac Vc
Am = ---------------------------------------------------------- content was determined in accordance with this
100V m + A c ( Vc – V m ) Part of this British Standard. The report shall state
whether or not a certificate of sampling is available.
If available, a copy of the certificate shall be
provided.
8.2 Information to be included in the test
report
8.2.1 Mandatory information. The following
information shall be included in the test report:
© BSI 12-1998 9
BS 1881-106:1983
10 © BSI 12-1998
BS 1881-106:1983
Publications referred to
BS 5497-1, Guide for the determination of repeatability and reproducibility for a standard test method.
ISO 4848, Concrete – Determination of air content of freshly mixed concrete – Pressure method1).
© BSI 12-1998
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