Chispómetro Isl FP56 5G2
Chispómetro Isl FP56 5G2
Chispómetro Isl FP56 5G2
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(2)
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(4) (6)
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USER MANUAL
Page 2 DOCV208A001-C
Revisions historical
A Creation 11/13/02
Complete revision of the manual
B § 3.4.2.1.4 Adjustment of the pilot light setting 09/12/03
Original issue of the attached file for spare parts
Part I § 4.2.1 Updating of section “Text editing”: Use of the second cursor in the area of
letters
Part I § 7.7 Removal of “trichloroethane” solvent
Part II § 2.2.2 Addition of safety parameter “Probe/cover missing safety” modifiable at
level 2
C 10/11/06
Part II § 3.3 Addition of section 3.3 “Alarm Review”
Part II § 3.5.16 Updating of section ““Check probe positioning” failure”: Duration is
programmable in the safety parameters
Part II § 3.5.18 Updating of section “Heating failure”: addition of a checking parameter
Part III § 3.1.2 Updating of “L” status flag definition
DOCV208A001-C Page 3
FP56/170 5G2
Page 4 DOCV208A001-C
Reserved for public relations department
CUSTOMER N° ................................
REPORT Date .............................
PURPOSE
I wish to Report an error
Submit a suggestion / a comment
Get more information
In the area of Hardware Software Manual
ATTACHED SHEETS
SUBMITTED BY
Name :
Company :
Address :
Phone : Fax : Date:
Send this report to your local Sales office or to Groupe ISL - Service Clients
BP 70285
14653 CARPIQUET CEDEX FRANCE
Tel : (+33) 2.31.26.43.00 – Monday through Friday from 9 :00 a.m. to 5 :00 p.m. French Time
Fax : (+33) 2.31.26.62.93
Mail: mailto:[email protected]
Web: http://www.isl-france.com/
DOCV208A001-C Page 5
FP56/170 5G2
Page 6 DOCV208A001-C
Caution
This ISL analyzer has been carefully designed, manufactured and inspected for
quality. It has been equipped with a number of safety features.
However, the use of this analyzer may involve the handling of solvents,
chemicals, and other potentially dangerous flammable, toxic, etc.) materials.
Please exercise caution when- handling these materials while operating the
analyzer.
Please:
• read the manual
• wear proper protective clothing
• perform all suggested service procedures
• use care to prevent accidents.
Use of Non-ISL Products and Accessories. Defects or damage that result from
the use of Non-ISL branded or certified Products, Accessories, Software or
other peripheral equipment are excluded from warranty.
DOCV208A001-C Page 7
FP56/170 5G2
The values indicated in displays illustrated in this manual are given as examples and must not be
used by the operator for tests. ISL accepts no responsibility for accidents arising from the use of
values indicated in illustrations. This warning is particularly applicable (but not exclusively) to the
creation of a program.
Indications specific to only one of the two methods will be noted in bold italics with indication of
concerned equipment.
Page 8 DOCV208A001-C
CONTENTS
DOCV208A001-C Page 9
FP56/170 5G2
PART II - ADVANCED USE OF FP56 5G2 AND FP170 5G2 ANALYZERS ..........................................II-49
1 - PROGRAMMING: TESTS, PAGES, SAMPLES, OPERATORS, ETC. II-51
1.1 - TEST PRINCIPLE ............................................................................................................................................. II-51
1.2 - TEST PROGRAM PARAMETERS ................................................................................................................... II-51
1.2.1 - Identification and definition parameters ........................................................................................................ II-52
1.2.2 - Initial phase ................................................................................................................................................... II-53
1.2.3 - Standard phase............................................................................................................................................... II-53
1.2.4 - Final phase .................................................................................................................................................... II-54
1.3 - PROGRAM CREATION (access level 1) .......................................................................................................... II-54
1.4 - MODIFICATION OF AN EXISTING TEST (access level 1)............................................................................ II-55
1.5 - SAMPLE EDITING (access level 1) .................................................................................................................. II-56
1.5.1 - Sample display .............................................................................................................................................. II-56
1.6 - EDITING SPECIFICATION PAGES (access level 1) ....................................................................................... II-56
1.6.1 - Page display................................................................................................................................................... II-57
1.7 - OPERATOR NAME EDIT (access level 1) ....................................................................................................... II-57
1.8 - CUSTOMIZE RUN MODE SCREEN (access level 1)...................................................................................... II-57
2 - SETTINGS: THE “ANALYZER SETUP” MENU II-58
2.1 - PRINTER CONFIGURATION .......................................................................................................................... II-58
2.2 - RUN DEFAULT VALUES CONFIGURATION............................................................................................... II-59
2.2.1 - Power on parameters ..................................................................................................................................... II-59
2.2.2 - Safety parameters .......................................................................................................................................... II-59
2.3 - EXTERNAL LINKS SETUP ............................................................................................................................. II-60
2.3.1 - RS 232C link setup........................................................................................................................................ II-60
2.3.2 - External link test............................................................................................................................................ II-64
2.3.3 - RS 485 link – Alan network .......................................................................................................................... II-64
2.4 - TECHNICAL SETUP: INTERNAL PARAMETERS........................................................................................ II-65
2.5 - LABORATORY SETUP .................................................................................................................................... II-65
2.6 - REAL TIME CLOCK......................................................................................................................................... II-65
2.7 - ISL ADJUSTMENT ........................................................................................................................................... II-66
2.8 - CUSTOMIZE RUN MODE SCREEN (access level 1)...................................................................................... II-66
Page 10 DOCV208A001-C
3 - ALARMS II-67
3.1 - ALARM TYPES .................................................................................................................................................II-67
3.1.1 - Failure alarms.................................................................................................................................................II-67
3.1.2 - Report alarms .................................................................................................................................................II-67
3.1.3 - Warning alarms ..............................................................................................................................................II-67
3.2 - ALARM DISPLAY, ALARM STOP ..................................................................................................................II-68
3.3 - ALARM REVIEW ..............................................................................................................................................II-68
3.4 - ALARM HANDLING.........................................................................................................................................II-68
3.5 - FAILURE ALARMS...........................................................................................................................................II-68
3.5.1 - “Fire detection” ..............................................................................................................................................II-68
3.5.2 - Memory failure...............................................................................................................................................II-69
3.5.3 - “Signal conditioning” failure .........................................................................................................................II-69
3.5.4 - “No test flame” failure....................................................................................................................................II-69
3.5.5 - “Glow plug failure” ........................................................................................................................................II-69
3.5.6 - “Sample temperature failure” .........................................................................................................................II-70
3.5.7 - “Abnormal heating rate” ................................................................................................................................II-70
3.5.8 - “Flash detection failure” (thermocouple) .......................................................................................................II-70
3.5.9 - “Heating bath temperature failure”.................................................................................................................II-70
3.5.10 - “Heating bath temperature safety” failure ...................................................................................................II-70
3.5.11 - “Program checksum error”..........................................................................................................................II-71
3.5.12 - “Abnormal flash detection” ........................................................................................................................II-71
3.5.13 - “Abnormal atmospheric pressure” ..............................................................................................................II-71
3.5.14 - “Motor board link failure” ..........................................................................................................................II-71
3.5.15 - “Check test devices positioning” failure .....................................................................................................II-71
3.5.16 - “Check probe positioning” failure ..............................................................................................................II-71
3.5.17 - “Igniter arm unlock” failure ........................................................................................................................II-71
3.5.18 - “Heating failure”.........................................................................................................................................II-71
3.5.19 - “Low battery”..............................................................................................................................................II-72
3.5.20 - “Flame abnormally lit”................................................................................................................................II-72
3.6 - REPORT ALARMS ............................................................................................................................................II-72
3.6.1 - Pre-safety temperature reached ......................................................................................................................II-72
3.6.2 - Flash on first flame test ..................................................................................................................................II-72
3.6.3 - Result out of spec ...........................................................................................................................................II-72
3.6.4 - End of test: flash.............................................................................................................................................II-73
3.6.5 - End of test: no flash........................................................................................................................................II-73
3.6.6 - End of test: safety flash temperature ..............................................................................................................II-73
3.7 - WARNING ALARMS ........................................................................................................................................II-73
4 - RESULTS AND PRINTING II-74
4.1 - RESULTS PAGES ..............................................................................................................................................II-74
4.1.1 - Organization of results in the pages ...............................................................................................................II-74
4.2 - RESULTS............................................................................................................................................................II-75
4.2.1 - Allocation of results pages .............................................................................................................................II-75
4.2.2 - Results display/printing..................................................................................................................................II-75
4.2.3 - Statistics .........................................................................................................................................................II-76
4.2.4 - Pages initialization .........................................................................................................................................II-77
4.3 - LAST RUN RESULTS........................................................................................................................................II-78
4.4 - PRINTOUT .........................................................................................................................................................II-78
4.4.1 - INITIALIZATION .........................................................................................................................................II-79
4.4.2 - ENVIRONMENT PRINTING .......................................................................................................................II-79
4.4.3 - One sample.....................................................................................................................................................II-79
4.4.4 - One specification page ...................................................................................................................................II-79
4.4.5 - One test program ............................................................................................................................................II-79
4.5 - PRINTER INTERFACE TEST ...........................................................................................................................II-79
5 - RS 232C STANDARD INTERFACE II-80
5.1 - RS 232C LINK CHARACTERISTICS ...............................................................................................................II-80
5.2 - OUTLET CONNECTOR BROACHING ............................................................................................................II-80
5.3 - TRANSMITTED DATA .....................................................................................................................................II-81
5.3.1 - Examples of transmitted messages .................................................................................................................II-81
5.3.2 - RESULT MESSAGE FORMAT....................................................................................................................II-81
5.3.3 - Conditions of a test run ..................................................................................................................................II-82
5.3.4 - Test contents ..................................................................................................................................................II-82
5.4 - EXAMPLE OF USING THE RS-232C INTERFACE WITH A PC ...................................................................II-84
5.4.1 - Analyzer setup................................................................................................................................................II-84
5.4.2 - Software setup................................................................................................................................................II-84
DOCV208A001-C Page 11
FP56/170 5G2
PART III - MAINTENANCE OF FP56 5G2 AND FP170 5G2 ANALYZERS.................................... III-87
1 - GENERAL III-89
2 - QUALITY III-89
2.1 - SAMPLE TEMPERATURE MEASUREMENT ADJUSTMENT.................................................................... III-89
2.1.1 - Adjustment periodicity and test start refusal ................................................................................................ III-89
2.1.2 - Adjustment of sample temperature measurement circuit .............................................................................. III-90
2.2 - PROBE CORRECTION.................................................................................................................................... III-92
2.3 - BATH TEMPERATURE MEASUREMENT ADJUSTMENT......................................................................... III-93
2.4 - ATMOSPHERIC PRESSURE MEASUREMENT CALIBRATION................................................................ III-93
3 - DIAGNOSTICS AND MEASURES: THE SERVICE MENU III-94
3.1 - DIAGNOSTICS AND MEASUREMENTS DISPLAY .................................................................................... III-94
3.1.1 - Diagnostics display....................................................................................................................................... III-94
3.1.2 - Measurement display.................................................................................................................................... III-95
3.2 - DIFFERENT DIAGNOSTICS .......................................................................................................................... III-96
3.2.1 - Heating ......................................................................................................................................................... III-96
3.2.2 - Cooling......................................................................................................................................................... III-96
3.2.3 - Printer........................................................................................................................................................... III-96
3.2.4 - RS-232C external link .................................................................................................................................. III-96
3.2.5 - Stirrer (FP170 5G2)...................................................................................................................................... III-97
3.2.6 - Ignition ......................................................................................................................................................... III-97
3.3 - SERVICE PRINTOUT...................................................................................................................................... III-98
3.3.1 - Internal parameters ....................................................................................................................................... III-98
3.3.2 - Measures....................................................................................................................................................... III-98
3.3.3 - Regulation check .......................................................................................................................................... III-98
3.3.4 - Printer reset .................................................................................................................................................. III-98
4 - TECHNICAL SETUP OF THE ANALYZER SETUP MENU III-99
4.1 - PASSWORDS AND MASTER PASSWORDS ................................................................................................ III-99
4.2 - REGULATION PARAMETERS....................................................................................................................... III-99
4.3 - BUZZER PULSE WIDTH .............................................................................................................................. III-100
4.4 - MODIFICATION OF SAMPLE TEMPERATURE CALIBRATION VALUES............................................ III-100
4.5 - UPLOAD / DOWNLOAD............................................................................................................................... III-100
4.5.1 - Principle of Transfer Procedure.................................................................................................................. III-101
4.5.2 - Installation and Starting the Transfer Program........................................................................................... III-101
4.5.3 - Transfer requested by the operator ............................................................................................................. III-101
4.5.4 - Unsuccessful transfer to Analyzer or no display on switching on .............................................................. III-102
5 - STRIPPING DOWN – COMPONENT LOCATION AND REPLACEMENT III-103
5.1 - ANALYZER HOUSING COVER................................................................................................................... III-103
5.1.1 - Dismounting the control unit housing cover .............................................................................................. III-103
5.1.2 - Dismounting the facing cover of the control unit ....................................................................................... III-103
5.1.3 - Dismounting the test unit housing cover .................................................................................................... III-104
5.2 - COMPONENTS LOCATION ......................................................................................................................... III-104
5.3 - COMPONENTS REPLACEMENT ................................................................................................................ III-106
5.3.1 - Sample temperature probe replacement...................................................................................................... III-106
5.3.2 - Flash point detector thermocouple replacement ......................................................................................... III-106
5.3.3 - Igniter replacement..................................................................................................................................... III-106
5.3.4 - Solenoid valve replacement........................................................................................................................ III-106
5.3.5 - Fuses replacement ...................................................................................................................................... III-107
5.3.6 - Battery trouble: replacing the battery ......................................................................................................... III-108
5.4 - EXTERNAL FIRE ALARM DEVICE CONNECTION ................................................................................. III-109
5.4.1 - Characteristics of the series contact provided............................................................................................. III-109
5.4.2 - Series contact connection ........................................................................................................................... III-110
5.4.3 - Fire detection test, thermofuse replacing.................................................................................................... III-110
6 - TROUBLESHOOTING IDEAS III-111
7 - OTHER ACCESSORIES, INSTALLATION/USE III-113
7.1 - DRAUGHT PROTECTION ............................................................................................................................ III-113
Page 12 DOCV208A001-C
PART I - USE OF FP56 5G2 AND FP170 5G2
ANALYZERS
FP56/170 5G2
1 - INTRODUCTION
We would like to take this opportunity to thank you for choosing ISL product. We are confident that you will be
completely satisfied with your new Analyzer and we hope that you continue to call on us for all of your laboratory’s
petroleum testing needs. Before you begin, we ask you to take a few minutes to become acquainted with ISL and its
history.
ISL’s beginnings go back to 1975, when a group of engineers and scientists from the heart of the Northern France’s
petrochemical industry began seeking ways to automate petroleum testing. The neighboring industry served as an
excellent research and development proving ground for their new equipment.
By the end of 70’s, several quality instruments had been developed and were being marketed in Europe under
ATPEM Trademark.
The most famous of these new instruments was the CPP 97, Automatic Cloud and Pour Point Analyzer. Introduced
in the early 1980’s, its successor, the CPP97-6, revolutionized cold flow testing enabling up to six tests automatically
and simultaneously.
Adding new automatic instruments each year, ATPEM soon became a world-wide leader in automatic petroleum test
instrumentation. In 1986, they expanded operations, reorganizing into the company now knows as ISL.
Striving to maintain close contact with customers in over 75 countries, ISL has since grown, founded Sales &
Service branches on each continent. With design, marketing, service and support operating together under the ISL
roof, the company reached “a new dimension” in 1993 by obtaining ISO 9002 certification from the BVQI. Working
hard to extend our quality assurance program, we received ISO 9001 certification in 1995.
Though best known for distillation, viscosity testing, cold behavior instrumentation, flash point, evaporation loss,
oxidation, and asphalt testing equipment, ISL's contributions to automated petroleum testing continue to grow. With
more than 10 patents to date, ISL's constant research into new technologies buttresses our precedent for ultimate
precision, performance and safety. The company now offers over 20 Automatic Analyzers for different applications
giving incontestable benefits to its users in increasing of test precision by elimination of operator subjectivity and
human errors, while increasing productivity and reduce operator time with highest level of safety.
A worldwide distribution network supports our customers with quick, efficient service, and our highly
knowledgeable service staff buttresses this relationship, providing solutions to product or application challenges.
1.2 -GENERALITIES
With the FP56 5G2 / FP170 5G2, ISL has once again developed an ergonomic and convivial petroleum product
Analyzer. Our committed customers will recognize ISL’s experience and reliability as well as the look and design of
the new generation of ISL instruments. The Analyzer you owned is the result of customer feedback and 20 years’
experience in the design and manufacture of petrochemical analysis equipment.
The FP56 5G2 Analyzers comply with ASTM D 56 standard methods and the FP170 5G2 comply with IP 170,
EN/ISO 13736, NF T 66-009 standard methods.
These standards do not define all associated safety procedures. It is therefore the responsibility
of the user to determine those procedures which are applicable.
1.3 -DEFINITIONS*
Flash point, of petroleum product: The lowest temperature at which the application of a test flame results in the
ignition of a part of the vapor, under specific test conditions.
The test sample is deemed to have flashed when an obvious flame appears and instantly
propagates across the sample’s surface.
2 - PRESENTATION
The ISL FP56 5G2 and FP170 5G2 can be used in two modes: Run menu or Main menu.
Run menu has been developed for the rapid start of a test. The operator can start a test simply by entering the
Expected Flash Temperature. He/she may also start a test simply by selecting a pre-programmed sample.
If necessary, a pre-programmed test and a pre-programmed operator can be entered. The laboratory manager may
associate a pre-programmed sample with a results specification page (see in PART II - chapter 1 -
PROGRAMMING: TESTS, PAGES, SAMPLES, OPERATORS, ETC. page II-51). The lab manager can thus
configure the Analyzer for a default test which will be proposed to the operator when selecting Run menu. Run menu
can be used in several different ways (see in PART I - chapter 7 - THE FLASH POINT TEST page I-43).
The main menu allows the operator to use all the Analyzer's functions. In particular, this mode allows the Analyzer
to be used for programs specific to the laboratory, provided that the related passwords are known.
The Analyzer is factory-set for the rapid selection of test programs compliant with all of the standards listed in the
section 1.2 - GENERALITIES of the previous chapter.
Function selection is performed directly from the screen using 2 groups of keys situated to the left and right of the
screen. A "TEST RUNNING" display can be selected. It allows the display of the sample temperature (large digits)
which is readable from a distance of 5 m. The EFP, Analyzer status and glow plug current (when used) are also
displayed.
The other tactile-type keys, essentially used for data entry, are situated just below the screen.
The screen and keypad are resistant to most chemicals encountered in the petrochemical industry.
The customer may choose between testing with a gas flame or an electrical igniter. Both types of ignition systems
can be installed (second as an accessory). Only one type of igniter may be assembled and connected at any given
time. Disassembly and assembly for the replacement of one igniter by the other is easily done.
The flash point detector is a thermocouple mounted on the test arm (swiveling). When the test arm is manually
positioned, the thermocouple is automatically placed on the test cup housing cover.
An intermittent audible alarm is triggered when the test is terminated. A continuous audible alarm is triggered if a
failure prevents a test from being started or from continuing a running test. The origin of these alarms can be
displayed, refer to PART II - section 3.2 - page II-68.
When a test is started, any detected minor anomalies which do not necessitate test termination are signaled as
"warnings" by an audible alarm and a "Warning No. XXX". The list of all possible warning numbers is given in
PART II - chapter 3 - ALARMS page II-67.
All failures are signaled by an audible alarm, the origin of which may be displayed. Certain failures switch the
Analyzer to standby (see the next chapter). All parts of the Analyzer having voltages greater than 24 V are not
accessible to the operator. The cup and cover are equipped with handles (except FP56 5G2 cup).
The Analyzer is equipped with a fire detection system which triggers an audible alarm. In this way, if a fire is
detected, the Analyzer switches power-consuming circuits to standby and disables the gas supply solenoid valve
command of the igniter. The customer may make use of the supplied safety relay to connect an additional fire alarm
and/or extinguisher as an accessory to the system.
The standard versions of the ISL FP56 5G2 and FP170 5G2 Analyzers are equipped with a parallel printer interface,
a RS 232C and a RS 485 interface (refer to section 3.3.3 - FP page I-26).
The term "power-consuming device" is used in this manual to refer to electromechanical and
electrical components having a dedicated power supply. Purely electronic components are not
included in this category (for example, integrated circuits, LEDs, etc...).
• The screen
• The keypad
• The contrast and the brightness adjusting knob
• The test flame and the pilot light adjusting knob of the gas igniter device
SERVICE port
Printer parallel
port
General fuses
Mains switch
Mains socket
Gas supply
nozzle
In standby, the stirrer transmission arm is disengaged (FP170 5G2). The test arm (igniter application / shutter
opening), swiveling on its axis, is placed at the rear of the test unit.
The igniter and its tilting mechanism are mounted on a test arm which serves the double purpose of opening the
shutter (of the cover) and igniter application. A caliber (4 mm) allows flame adjustment.
The test cup and the cover assembly are positioned in the test unit well during a test. Test cover accessories include
the following:
Stirrer (FP170 5G2)
Shutter
Flash point detector connected to the test arm
Pt100 sample temperature probe connected to the connection panel
Tilt
mechanism
Test flame
caliber Flash point
detector
thermocouple
Igniter (electrical
glow plug)
Test arm
Pilot light
Test flame
(gas)
Thermofuse (fire
detector)
Sample probe
Cover cup
Test cover
handle
Shutter
Stirrer
transmission
arm
Stirrer
The following components are situated on the connection panel (in the lateral right side, see Picture 4
below):
The connectors for the sample temperature probe, the flash detector and the ignition system
The gas supply connecting tubes (for the test flame and the pilot light)
The test arm
The stirrer transmission arm (FP170 5G2)
And the fire detection thermofuse (see Picture 2 page I-19)
Thermocouple
connector of the
flash point detector
Left red LED: Heating
Sample control.
temperature probe
connector Right red LED: Flash point
detection.
Igniter
connector Gas igniter nozzle (test
(glow plug) flame)
FP56 5G2 :
ASTM D56 :
TP < 60°C : 1°C/mn
TP > 60°C : 3°C/mn
Rapid: 3°C/mn
FP170 5G2 :
ISO-IP : 1°C/mn
NF : 0,5°C/mn
Rapid: 3°C/mn
A “Diagnostic” mode allows the heater to be controlled (refer to the PART III - section 3 - DIAGNOSTICS AND
MEASURES: THE SERVICE MENU page III-94). The left red indicator light (see Picture 4 page I-20 ) on the test
unit connection panel illuminates to indicate when the heater is on.
The Diagnostics mode can be used to control cooling (refer to the PART III - section 3 - DIAGNOSTICS AND
MEASURES: THE SERVICE MENU page III-94).
The gas test flame device is equipped with a test flame, a pilot light and it is equipped with a flame detector / igniter
(electric glow plug, see Picture 2 page I-19).
The test flame and the pilot light are automatically lit at the start of the test. The flame detection system allows the
flame to be automatically re-lit by the pilot light in the event of extinction, the two flames being in contact in
standby. If the test flame and the pilot light are off, the detection system light the igniter allowing the whole to be lit
again. During the test, if the test flame is absent for more than 2 minutes or if the flame is absent at the moment of
flame application, the test is stopped.
The Analyzer gas inlet is located at the rear of the control unit (see Picture 1 page I-18). Gas supply is controlled by
a solenoid valve which can be manually controlled in Diagnostic mode. Thus, the user can adjust the intensity of the
test flame and the pilot light (rapid reignition of the test flame). Refer to the section 3.4.2.1.3 page I-30).
The gas supply tubes for the test flame and the pilot light and the connector for the igniter are situated on the lateral
connection panel of the test unit (see Picture 4 page I-20).
The electrical igniter is made of an electric glow plug and a holder mechanism. The glow plug comes on for 10
seconds at the beginning of a test, then goes out. It will come on again about 30s before each test. The current may
be read on the "TEST RUN" screen - press <DISPLAY>. During a test, glow plug current is around 10 to 13 A. If
the glow plug current goes outside these limits (see in PART II - chapter 3 - ALARMS page II-67), the test will stop.
The glow plug and its movement may be manually controlled in Diagnostics mode (see in PART III - section 3.2.6 -
Ignition page III-97).
2.2.7 - Shutter
In standby, the test flame (for a gas ignition, igniter for an electrical ignition) / shutter arm is placed next to the cover
and the test unit connection panel. As in the case of the stirrer arm, it is moved into position at the start of the test.
The shutter is automatically opened at the test flame application temperatures. Opening the shutter allows the test
flame to be lowered into the cover opening. The shutter is automatically shut after igniter presentation.
Test flame or igniter (for an electrical ignition) presentation above the shutter can be manually controlled in
Diagnostics mode (refer to the PART III - section 3.2.6 - Ignition page III-97).
2.2.8 - Diagnostics
All diagnostics are presented in the PART III - chapter 3 - DIAGNOSTICS AND MEASURES: THE SERVICE
MENU page III-94.
The standard version of the FP56 5G2 / FP170 5G2 Analyzers is supplied with:
a diskette containing:
Factory-set configuration (internal parameters).
“ISL UDS” PC software for:
• Download of the non-volatile backup memory (NvRam) from a host PC to the Analyzer.
• Upload of the Analyzer non-volatile backup memory to the PC
• Software update (programme code and software texts)
An external connection cable for data transmission (RS 232C serial link)
An external connection cable for connection to the ISL Alan Network (RS 485 serial link)
An RS 232C/RS485 converter
3.1 -SPECIFICATIONS
Dimensions and weight
Height : 370 mm
Width : 360 mm
Depth : 550 mm
Weight: 25 Kg approx.
Standards
Environment
Test temperature range: -30°C to 110°C (-22°F to 230°F)
Operating ambient condition: 15°C to 35°C (60°F to 95°F)
Storage ambient condition: -20°C to 35°C (-4°F to 95°F)
Atmospheric pressure: constant pressure
For safety precautions relating to the LCD screen, refer also to the section 5.3 - page I-41.
Power supply
Voltage: 110/115 VAC or 230/240 VAC (manual switching) 50-60 Hz
Power Consumption: 350W
The Analyzer is delivered with one of the above configurations at the request of the customer.
Before switching on the Analyzer, make sure the mains supply matches the specifications on the
identification plate at the rear of the Analyzer.
Serious damage may result from the using an incorrect voltage supply.
Note: The life duration of the Ram non-volatile memory (NVRam) memory battery (Analyzer switched off) is
approximately 5 to 8 years.
Heating
Heating element: 200 W, low voltage
Cooling
The cooling of the control unit is ensured by a fan located at the rear of the Analyzer. Consequently leave sufficient
space behind the Analyzer for clear ventilation.
Igniter
The standard Analyzer is equipped with a gas ignition device. An additional electrical ignition system is available as
an accessory (see the spare parts list, DOCV208X200).
Gas supply
An optional pressure regulator allows gas pressure reduction for gas supply pressures up to 10 bars.
External link
Fire detection
When fire is detected, an audible alarm is triggered and the Analyzer is switched to standby.
The Analyzer is equipped with a safety relay to which an external fire extinguisher system and/or alarm may be
connected.
Thermofuse: 75°C 250V AC 10A
Temperature measurement
Keyboard
Stand-alone use
Can be used as stand-alone device and delivered as standard with a RS 232C and a RS 485 interface for transfer of
results (refer to the section 3.3.3 - FP page I-26).
Once the Analyzer has been unpacked, it is best to leave it idle in the laboratory for several hours
(especially after storage at low temperatures).
3.3 - CONNECTIONS
NOTE: the connectors are designed for connection of flexible tubes of 10 mm internal diameter.
3.3.3 - FP / PC connection
The FP Analyzers are delivered as standard with a RS 232C and a RS 485 interface.
FP Analyzers allow stand-alone operation or multi-instrument network under ALAN® management software
developed by ISL. The Analyzer connects to the ALAN network via the RS 485 serial interface through two ports
(input/output) located on the back panel (see Picture 1: Rear panel connectors page I-18).
The ISL ALAN software (Automatic Laboratory Analyzer Network) is a true 32-bit multitasking software under
Windows 98, Windows NT4.0 , Windows 2000 Professional or Windows XP Professional . Allowing up to 31
ISL Analyzers to be connected to the same PC computer. It collects and stores the data coming from different ISL
instruments.
Besides multi-Analyzers run control and results database management, the ISL ALAN software can automatically
export results directly to a LIMS system according to specific customized criteria and user defined protocol.
Note: The ALAN Kit is optional hardware and software package. Refer to the ALAN user’s manual.
The ALAN network input and output ports can be connected through a special adapter supplied with the Analyzer to
form a RS 232C serial link for retrieving results on a PC (refer to the PART II - chapter 5 - RS 232C STANDARD
INTERFACE page II-80 for the (EOT-0) message significant) and for a connection to a LIMS. Use the adapter
supplied with the unit. This one has on the same side 2 RS485 series ports to be connected simultaneously to the
inlet and outlet of the ALAN network and a RS 232C series port to be connected to a PC.
When the instrument is connected to ALAN, the direct connection to a LIMS is no longer possible, it has to be done
via the PC.
Note: Alan and RS 232C communication modes must be set. Refer to the PART II - section 2.3 -
page II-60.
The FP Analyzers are delivered as standard with a serial “SERVICE” port and the PC service software “ISLUDS”
which allows FP internal software to be updated by a PC download. It also allows recovery of the contents of the
backup parameter memory (as well as the results) with a view to later reloading (refer to the PART III - section 4.5 -
UPLOAD / DOWNLOAD page III-100).
The probe can be corrected by the user using a temperature table from 0 to 400°C (32-752°F) at intervals of 20°C
(36°F). Refer to the PART III - section 2.2 - PROBE CORRECTION page III-92. This correction is applied only
during test.
• Slide the thermocouple inside tube (rep. 11 Figure 1) located under the arm.
• Then push the thermocouple inside the hole (rep. 12 Figure 1).
• Loosen the screw of the stuffing box (rep. 9 Figure 1)
• Install the thermocouple in its hole and slide it down to the Teflon base (rep. 14), without overshooting, then re-
tighten the screw on the stuffing box (rep. 9).
• Connect the thermocouple to the connection board (lateral right side connection panel, see Picture 4 page I-20).
Flanging screw of
the pilot light
Flanging screw of
the igniter
Screws of the tilter
ring
Test flame
• Insert the igniter (electrical glow plug) and the pilot light in the holder as they are visualized above:
The igniter shoulder come in abutment against the holder.
The fork serving as pilot light indexing is tighten between two plastic washers ensuring insulation of the flame
detection device.
• Tighten the flanging screws of the igniter and the pilot light holder.
• Connect the igniter to the lateral connection panel (see Picture 4 page I-20).
• Connect the flame detector plug (connected to the igniter connector) to the plug located behind the igniter and pilot
light holder, under the pilot light.
• Connect the gas supply silicone tube for the pilot light to the lateral connection panel.
• Refer to the section to adjust the diameter of the pilot light flame.
• Loosen if necessary the test flame flanging screw (hexagon socket screw) located on the right side of the tilter (see
Picture 5 above).
• Insert the test flame tube in the tilter arrangement anticipated with that in mind (lower part).
• Toggle the switch (Diagnostic mode, refer to the PART III - section 3.2.6 - Ignition page III-97 ) and adjust the
depth of the test flame.
• Tighten the test flame flanging screw.
• Press again the shutter maneuvering button (Diagnostic mode) to bring the switch into its initial position.
• Connect the silicon tube from the test flame to the connection panel (see Picture 4 page I-20).
• Refer to the following section to adjust the diameter of the test flame.
Important: Attach the gas supply tube of the test flame under the clip located on the test arm paying attention to
leave enough slack to allow correct movement of the glow plug without hindrance. Use the Diagnostic mode to
control the tilter (refer to the PART III - section 3.2.6 - Ignition page III-97). The gas supply tube of the test flame
must be directed toward the top and do not twist.
3.4.2.1.3. Adjustment of the test flame and the pilot light flame
Two knobs in the front side of the analyzer allows the diameter of the test flame (TEST knob) and the pilot light
flame (PILOT knob) to be adjusted:
Picture 6: Test flame and pilot light flame diameter adjusting knob
• Ignite the test flame. For this, first control the solenoid valve of the gas supply (in diagnostic mode, refer to the
PART III - section 3.2.6 - Ignition page III-97).
• Adjust the diameter of the test flame by comparison with the diameter of the test flame caliber on the igniter holder
(see Picture 5 page I-29).
Flame diameter: 3.2 to 4.2 mm
• Follow the same procedure to adjust the flame diameter of the pilot light.
1.0 mm
• Dismantle the gas test flame tube, the igniter/detector and the pilot light (if they are mounted on the analyzer).
• Activate the tilter (Diagnostic mode, refer to the PART III - section 3.2.6 - Ignition page III-97 ).
• Insert the electrical glow plug in the tilter arrangement anticipated with that in mind (top part) in abutment against
the positioning screw. Then tighten the test flame flanging screw (hexagon socket screw) located on the right side
of the tilter.
• Press again the shutter maneuvering button (Diagnostic mode) to bring the tilter into its rest position.
• Connect the glow plug to the lateral connection panel (see Picture 4 page I-20).
Important: Attach the glow plug wires under the clip located on the test arm paying attention to leave enough slack
to allow correct movement of the glow plug without hindrance.
3.5 - SWITCHING ON
Before connecting the Analyzer to the mains supply, check that the mains voltage corresponds to that
indicated on the rating plate on the rear of the unit.
Before connecting peripherals, both the Analyzer and the peripheral must be switched off.
• Press the main ON/OFF switch (see Picture 1 page I-18) at the rear of the control unit.
• The screen should light up. If not, first check the contrast and backlight settings.
<ENGLISH> <ENGLISH>
Press the key corresponding to the desired language. The screen displayed is the Run Menu mode:
Sample ID:
Sample No.: Next N°
EFP: °C Previous EFP
<Run start>
Test : 1 ISO/ISO °C
Operator: <Display>
<Exit> <Down>
Sample: 23.2 Bath : 23
It is possible to lock the language choice in the power-on parameters, refer to the PART II - section 2.2 - RUN
DEFAULT VALUES CONFIGURATION page II-59.
3.5.2 - Self-test
Selecting <Exit> results in the display of the following screen:
Autotest : OK*
<Main menu> <Run Menu>
The self-test applies to the PROM, RAM and Non-volatile RAM (NVRAM) memories.
• If a memory error is detected during power up, a test can only be started if, at least, the Analyzer is switched off
and on.
4.1 -KEYPAD
(1)
(2)
(3)
(20)
(4)
(19)
(5)
(18) (6)
(7)
(17)
(8)
(16)
(15) (9)
(14)
(13) (10)
(12)
Picture 10: User interface
(11)
The universal type (not specific to any particular language) has been kept simple. It has no alphabetic keys and no
double function keys. It includes:
• Numeric keys,
• Arrow keys (2 vertical and 2 horizontal),
• Full stop and hyphen,
• Backspace: cursor left, delete,
• (ENT): for entry confirmation,
• A reset key,
• Stop keys for: a running test, alarm and printout,
• Function keys on each side of the screen. They relate to the functions displayed at any given time.
• Built-in indicator lights:
- "TEST": green, test running,
- "ALARM": red, failure, error and report alarms - continuous audible alarm.
Text entries (sample ID, operator, etc.) are selected using the screen. When an entry requires text, the alphabet and 6
other characters are displayed. Text is then edited as explained in "Editing text" in section 4.2.1 - Text editing (text
entry) page I-36.
Function keys
(RESET) Abandons all data entry or quits creation/sample display, creation/page display and
creation/display of test program.
(PRINT STOP) Stops printout
(STOP ALARM) Displays the origin of the triggered alarm. The audible alarm can be muted (except in the
case of fire detection) using the screen.
Full stop
Hyphen
(STOP) Abandons the running test - started using "TEST START". For further details, see the
relevant section in chapter 8.
(ENT) Confirmation of entry: a single letter, a block of text, a value, etc.
4.2 -DISPLAY
The LCD graphics screen is incorporated in the keypad so that the functions displayed on the screen can be directly
selected. To do this, the operator uses the function keys situated to the left and right of the screen. The LCD screen
has its own protective film.
In the initial display, the operator should select either "Run Menu" or "Main menu ". For example, select <Run
Menu>. Several entries are available in Run Menu :
Sample ID, type of test and the operator name can be pre-programmed. On selecting these functions, a list is
displayed (maximum 20).
If not entered via a pre-programmed sample, the EFP is entered directly using the EFP key. See "ENTRY OF A
NUMERIC VALUE" below.
• The <Down> key allows the operator to display the page numbers allocated for the results - "in spec" and "out of
spec". The "SAMPLES EDIT" of "RUNS ENVIRONMENT" is used for allocating specification pages (restricted
to use by the laboratory manager - see chapter 6). If there are no page numbers displayed, results will be sent to the
default page 21.
• The <DISPLAY> function displays "TEST RUN" with 4-digit sample temperature (large size). The display can be
read at a distance of 5 meters. The EFP, Analyzer status (e.g., "--> tests"), the date, the time and the glow plug
current (if applicable) are also displayed. The <FLAME TEST> function starts a manual flame test.
• Use the horizontal arrow keys (LEFT/RIGHT) to select digit position and the vertical arrow keys (UP/DOWN) to
increment/decrement the value. The numeric keys on the keypad may also be used.
• Modification of the laboratory manager password is described in PART II - section 2.5 - LABORATORY
SETUP page II-65.
• Modification of the Service password is explained in PART III - section 4.1 - PASSWORDS page III-99.
To check current access level, select <Main menu> then select <Access> from the main menu. The "ACCESS
CONTROL" display appears.
• At power on, the default access level is "0". This parameter can be configured, refer to the PART II - section 2.2.1
- Power on parameters page II-59.
4.4 -FAMILIARISATION
In this manual, the term "select" means "press" the key corresponding to the indicated
function.
Sample ID:
Sample No.: Next No
EFP: °C Previous EFP
<RUN START (E)>
Test:
Operator: <Display>
<Exit> <Down>
Sample: Bath:
Several entries are available via the keys to the left and right of the screen.
If the unit has been prepared correctly, and after having selected the required entries from those listed above, the test
may be started. To do this, select the "RUN START" function key. The type of igniter device connected is
indicated; (G) for gas and (E) for electrical. If no igniter is connected, ( ) is displayed. For the full test start
procedure, see chapter 7 - THE FLASH POINT TEST page I-43. Several Run Menu procedures are available.
• Select <Display> from the "Main menu" or from "Run Menu" to activate the display of "CURRENT TEST".
• Select <Flame test> to identify the igniter at any point during the test.
5 - SAFETY FEATURES
All Analyzer parts with voltages exceeding 24 V are not accessible to the operator. The handles on the test cup and
cover allow both to be lifted without danger of burns.
Any failures trigger an audible alarm. The origin of failure, error or report alarms may be displayed. Certain failures
switch the Analyzer to standby. If the detection of one of these failures (refer to the list in PART II - section 3 -
ALARMS page II-67) does not result in the power circuits being switched off, the operator must immediately switch
off the Analyzer and disconnect it from the mains supply.
The system is equipped with a fire detector. On detection of fire, the system switches the Analyzer to standby. A
continuous audible alarm is triggered and remains activated until the Analyzer is switched off. The user may connect
an extinguishing accessory to the system’s safety relay. It is also possible to connect an external alarm device (refer
to the PART III - section 0page III-110).
• Control of the gas supply Solenoid Valve, the igniter and the bath cooling fan is disabled. The alarm continues
until the Analyzer is switched off.
5.1.3 - Failures preventing the start of a test and stopping running tests
These failures trigger a continuous audible alarm. Press (ALARM STOP) to display the type of alarm.
The selection of access levels is covered in section 4.3 - ACCESS CONTROL - PASSWORDS page I-37.
Once an access level has been confirmed by entering the correct password, it remains available until a lower access
level is explicitly requested (refer to the PART II - section 2.2.1 - Power on parameters page II-59 to configure the
access level). When the system is switched on, it defaults to access level 0.
• Avoid rubbing the screen with hard objects which may result in scratching.
Moisture/water
• Water on the surface of a functioning LCD screen can cause damage. Wipe with a clean soft cloth or leave to dry
before switching on.
Dirt
• The screen can be stained by fingerprints, saliva, starch, oil and fat. If it is stained, wipe with a clean soft cloth.
• LCD modules are sensitive to high temperatures. Follow the operating and storage recommendations given in the
"Technical specifications " section of this chapter.
Vacuum cleaners
If the laboratory is cleaned using a vacuum cleaner, keep it away from the LCD (risk of electrostatic discharge).
To ensure that the results are reliable, your Analyzer’s results can be quickly checked. These checks must be
performed at regular intervals, in compliance with your organization’s quality system.
• Disconnect the temperature probe from its connector (see Picture 4 page I-20) and replace it with the probe
simulator.
• From the "RUN MENU" screen, select <Display>.
• Set the PS 100 switch to - 50°C.
• Wait for the temperature measurement to stabilize and check that it is - 50°C.
• Now set the PS 100 switch to 100°C and, after the temperature display has stabilized, check that it is 100°C.
If calibration is necessary, consult the PART III - section 2.1 - SAMPLE TEMPERATURE MEASUREMENT
ADJUSTMENT page III-89.
These checks must be performed at regular intervals, in compliance with your organization’s quality
system.
If calibration is necessary, refer the PART III - section 2.4 - ATMOSPHERIC PRESSURE MEASUREMENT
CALIBRATION page III-93.
7.1.1 - Definition
The flash point is the lowest temperature, corrected to a barometric pressure of 101.3 kPa (760 mmHg), at which the
application of a test flame causes ignition of a part of the sample’s vapors under specified test conditions.
1st flame application EFP - 9 °C EFP - 10°C EFP - 5°C (10 °F)
7.2.1 - Sampling
To avoid the loss of vapors from the test sample and to protect the test sample from contamination by humidity, do
not open the sample container. Do not handle the sample at temperatures above the EFP - 10°C (20°F). The flash
point test must be the first test subjected to the test sample.
7.2.2 - Preparation
The operator must be informed about the dangers relating to flash point testing. Some of these
dangers are indicated in the standards. Handle test samples and waste solvents in compliance with
applicable regulations.
The flame (gas ignition) is lit automatically at the start of the test. A device allows flame extinction to
be detected. In the event of extinction, the flame is automatically re-lit.
• The flash point tests should be performed in a draft-free room (or in a fume cupboard). If the unit is equipped with
an anti-draught screen (supplied as an accessory), install it before starting the test.
• Make sure that the Analyzer is placed on a stable and horizontal benchtop.
• Thoroughly clean and dry all parts of the cup and its accessories before starting the test.
• Carry out the checks described in the preceding chapter regularly. See also chapter 8 - REGULAR
MAINTENANCE page I-48.
Several test start procedures are indicated in section 7.4 -TEST MODES page I-45. The operator can choose that
which best corresponds to his/her needs.
Between two tests, the cover and the probe can be cleaned together - after disconnecting the probe.
In this way, the probe can be positioned in its holder before placing the cover on the cup.
The glow plug current should be around 10 to 13 A, see section 2.2.4.2 - Electrical igniter page I-22.
If the glow plug current is not within the limits (< 3A and > 15A), a failure alarm is triggered and the
test is abandoned.
The default test may be used without further configuration. From the initial screen:
• Enter the EFP or use the "EFP recall" function (to recall the previous EFP).
• Select "RUN START".
Before a test in Run Menu can be started, Main menu must be exited by selecting "END OF MAIN
MENU".
When the igniter is applied, the large size temperature display is locked. The display is unlocked only if the flash
point is not detected.
In this way, when the flash point is detected, the temperature at which the flash point was detected remains displayed
after the test has been automatically stopped.
The operator can manually apply the igniter at any time during the test (or in standby mode) by selecting <Flame
test> in the "TEST RUNNING" screen.
• Cooling of the heating block is started depending on the temperature indicated in the program.
• The temperature of the flash point remains on display after the test has been stopped. The
observed/corrected/rounded result, depending on the program (see in PART II - section 1.2 - TEST PROGRAM
PARAMETERS page II-51), is displayed to the nearest first decimal.
The detected flash point temperature is replaced by the current temperature reading when one of the following is
done :
• The expected flash point (EFP) which is displayed at the end of the test is the valid EFP at the first programmed
igniter application. After detection of the flash point, the first line under the large size display indicates the EFP,
the number of igniter applications, "FLASH" and an indicator of "in spec" results (see in PART II - section 4.2 -
RESULTS page II-75 for interpretation of this indicator). "FLASH" indicates that the flash point was correctly
detected. This information is also shown at the bottom of the "TEST RUNNING" screen until unlocked by one of
the actions listed above.
7.7 -CLEANING
Clean the cup, cover, shutter, stirrer (FP170 5G2), flash point detector and sample temperature probe with a
suitable solvent.
In general, all accessories which may have an effect on the result, including the test flame nozzle or the flash point
detector must always be clean and the shutter must always be able to move freely.
Depending on the state of the various accessories, they may be disassembled for a thorough cleaning.
If it is necessary to remove the flash point detector or the stirrer (FP170 5G2), refer to the PART III - section 5 -
STRIPPING DOWN – COMPONENT LOCATION AND REPLACEMENT page III-103.
The stand for the cup/cover (standby) can be removed for cleaning.
If the operator wishes, it is possible to dismount the stirrer propeller. The propeller blades must be held and the
driving pinion at the other end of the shaft unscrewed: the propeller can then be removed from below (FP170
5G2).
8 - REGULAR MAINTENANCE
It is preferable that the maintenance checks and operations described in this chapter and in chapter 6 -
MEASUREMENT CHECKS AND SETTINGS page I-42 be performed by the operator. In this way, the operator
better understand the Analyzer.
It is recommended to carry out maintenance at regular intervals. The ideal interval will depend on the environment of
the Analyzer and its frequency of use and also will depend on the applied Quality Assurance System of the customer.
The following environmental conditions may need more maintenance.
Optimum periodicity for checks and maintenance is determined by the experience of the responsible for the
Analyzer.
• Adjustment of the test flame: check at the start of a test and, if necessary, adjust gas flow using the regulator (refer
to the PART I - section 3.4.2.1.3 page I-30).
• Check temperature measurement (refer to the PART I - section 6.1 - page I-42).
• Check atmospheric pressure measurement (refer to the PART I - section 6.2 - page I-42).
• Clean the cup, cover and accessories after each test. The flash point detector must always be clean (refer to the
PART I - section 7.7 - page I-47).
• Setting of real time clock (refer to the PART II - section 2.6 - page II-65).
• Replacement of temperature probe (refer to the PART III - section 5.3.1 - page III-106).
• Replacement of the flash point detector (refer to the PART III - section 5.3.2 - page III-106).
• Replacement of the glow plug (refer to the PART III - section 5.3.3 - page III-106).
• Transfer of service parameters to a PC (refer to the PART III - section 4.5 - page III-100).
• Test of the fire detection device (refer to the PART III - section 5.4.3 - page III-110).
• Replacement of paper and ribbon in printer. See the printer user manual.
The customer can of course replace unneeded test programs by test programs specific to the laboratory. Any
modifications applied to an existing standard can be immediately applied by the customer by making modifications
to the corresponding test program, without having to wait for a software upgrade.
Having created test programs corresponding to the various standard and non-standard methods, up to 20 pre-
programmed sample types (defined by the laboratory manager) can be created. A test program can be associated with
each sample type created. Pre-programmed samples are saved with an identifier and under a number from 1 to 20.
Thus, when a pre-programmed sample type is selected by the user, the associated test program is called. Editing of
pre-programmed sample types is explained in the section 1.5 - SAMPLE EDITING (access level 1) PAGE II-56.
TEST DISPLAY
Selected test: _
Show test list
• Select "SHOW TEST LIST" and the list of existing tests is displayed (1 to 20). Select one of the tests, e.g., test 1.
The previous display returns and "1" is displayed on the "SELECTED TEST" line.
* FP56 5G2 :
DISPLAYING A TEST
Name: ASTM D 56 Tmp unit: °C
Bath setpoint at EFP - 10 °C
Barometric correction: 1 Rounded: N
Heating rate: LOW if EFP < 60 °C
Heating rate: HIGH if EFP \ 60 °C
<Down>
* FP170 5G2 :
DISPLAYING A TEST
Name: ISO 13736 Tmp unit: °C
Bath setpoint at EFP - 17 °C
Barometric correction: 1 Rounded: N
Heating rate: ISO if EFP < 19 °C
Heating rate: ISO if EFP \ 19 °C
Stirring: ISO <Down>
Test name: This parameter allows the test to be identified. The user can thus check if the displayed test is that which
he/she intends to run before starting . A maximum of 12 characters may be entered.
Temperature units: Depending on whether you wish to work in Celsius or Fahrenheit, enter "C" or "F". Parameter
entry during creation is flip-flop.
Heating block set-point at EFP - °C: Depending on the standard used, the heating block must be at EFP - °C.
Barometric correction: An automatic barometric correction can be requested, which will be applied during the
calculation of the results. Entry of "1" or "2" or “none” is by flip-flop.
Rounded: there are 2 possible entries: "Y" (Yes: rounded to the nearest 0,5°C or 1°F) or "N" (No: no rounded).
Entry is by flip-flop.
Heating rate:
• FP56 5G2:
There are 2 possibilities: " Low" (1 °C/min or 2 °F/min) or " High"(3 °C/min or 5 °F/min).
• FP170 5G2:
There are 3 possibilities: « NF » (0.5 °C/min), « ISO » (1°C/min) or « RAPID » (3 °C/min). Entry
is by flip-flop.
Stirring speed (FP170 5G2): There are 3 possibilities "None" - "ISO" (30 rpm), "NF" (75 rpm). Parameter entry
during creation is by flip-flop.
<Down>
Test every: This parameter defines test flame frequency. It can be programmed from 0,5 °C to 999.9 °C.
Tests start: If the initial phase is used, this parameter defines the temperature at which the flame is first applied.
This function is inhibited by the value 999.9.
For this phase, it is possible to define only one flame presentation at the beginning of the test, the following test
being the first of the standard phase. To achieve this, enter the following parameter:
• FP170 5G2
STANDARD PHASE <Up>
Test every 0.5 °C if EFP < 19 °C
Test every 0.5 °C if EFP \ 19 °C
Start tests at EFP - 9 °C if EFP < 19 °C
Start tests at EFP - 9 °C if EFP \ 19 °C
<Down>
Test every: this parameter defines test flame frequency. It can be programmed from 0,5°C to 10°C.
Test start: This parameter defines the temperature at which the flame is first applied. Tests start at - 5°C (FP56
5G2) or - 9°C (FP170 5G2) before the EFP. This function is inhibited by the value 999.9.
• Press <Down>.
<Exit>
GO-NO GO: To program a single test flame at the EFP, this parameter must be "Y" for yes. Enter "N", for no, to
allow several flame presentations, depending on the standards. When this parameter is "Y", the test start temperature
(initial phase and standard phase) is not taken into account. Entry is by flip-flop.
Pre-safety alarm at EFP+: An intermittent audible alarm can be programmed for a given temperature above the
EFP.
Safety alarm at EFP+: An intermittent audible alarm can be programmed to switch the Analyzer to standby at a
given temperature above the EFP. For the consequences of the Analyzer switching to standby mode, refer to the
PART I - section 5 - SAFETY FEATURES page I-40. The red alarm indicator is illuminated.
CUSTOMIZE A TEST
Selected test: 1
Show test list
New one
• Select "NEW ONE" and the first page of program entry is displayed. Enter the parameters for the various phases as
indicated in section 1.2 - TEST PROGRAM PARAMETERS page II-51.
When all the parameters have been entered and "FINAL PHASE" is displayed:
<Cancel> <Ok>
<Exit>
• Select "SAVE AS" and the list of existing tests is displayed (1 to 20).
Save as...
1: 6:
2: 7:
3: 8:
4: 9:
5: 10:
<Exit> <Down>
• Select the number of the program displayed and the "TEST DISPLAY" screen appears. The test number which you
have just selected is displayed.
• To return to the first display of the section C without saving the program, select <Exit>.
The new program has therefore been saved under the displayed number. If, in the future, the user modifies the
program, "SAVE" can simply be selected to save the program under the same number.
CUSTOMIZE A TEST
Selected test: 1
Show test list
New one
• Select the program to be modified from the list and the previous screen is displayed. The "Prog No." must display
the selected number.
The modification and the saving of an existing program is carried out in the same way as for a new program, see
section 1.3 - PROGRAM CREATION (access level 1) page II-54. It can be saved under the same program No.
(modification) or under a new program No.
• Select <Edit> to go into editing mode. The screen title then becomes "SAMPLES EDIT"
• Select "Prog No.". The program selected must correspond to the selected sample type.
• Enter the name and the EFP (-30 to 110°C). The displayed temperature units is selected during test program
creation.
• Enter "in spec" and "out of spec" pages. The "out of spec" page can be either the same as the "in spec" page or
page 21.
The user must now save the sample. The principle is the same as for saving a test program.
Editing of a specification page consists of entering a maximum permissible result and a minimum permissible result.
When a test is performed using a pre-programmed sample, the result (observed, corrected and/or rounded -
depending on program configuration) is compared with its limits.
If the result is "in spec" when compared with the associated results page, it is stored in this page.
If the result of a test using a pre-programmed sample is "out of spec", it is stored in the page defined during sample
editing. If no page has been specified, the result is stored in page 21 - the failure page for all "out of spec" results.
Select "PAGES EDIT" from the "RUNS ENVIRONMENT" menu to display a "OUTPUT PAGES EDIT". Select
<Show list> to display the list of "OUTPUT PAGES NAMES".
To display the list of existing pages, select <Show list> the select the page number.
• Select <Edit> to go to editing mode. The screen title changes to "RESULTS PAGE"
• Enter the title, "Spec. min.", the "Spec. max." and the maximum number of results spaces reserved for the page.
For further information on these spaces, refer to chapter 9, "RESULTS..."
• After displaying all entries, select <Ok> and save the page under a number (1 to 20).
• Select "OPERATOR EDIT" from the "RUNS ENVIRONMENT" menu to display the first page of the operators
list (<Down> to display the second page).
• Select the operator number and enter the operator name as explained in the PART I - section 4.2.1 - Text editing
(text entry) page I-36.
After validating the entry by pressing (ENT), the name is saved in the list. Select <Exit> to return to the previous
display.
• Select "OPERATORS DISPLAY" from the "RUNS ENVIRONMENT" menu to display the first page of the list of
operators.
• Select "CUSTOMIZE RUN MODE SCREEN" from the "RUNS ENVIRONMENT" menu.
• Select “Y” or “No” opposite the function concerned to modify the screen display configuration ("Yes" to display
and "No" to hide). The selection is by flip-flop.
• Select “Y” or “No” opposite the function concerned to authorize or not the operator (level 0) to modify the field.
• Sample ID
• Sample No.
• Test ID
• Operator name
• Second screen displaying (the <Down> key can be removed)
• Analyzer configuration,
• Service settings,
• Calibrations,
• Quality,
• ISL configuration.
Only service parameters accessible at access level 1 are covered in this part. The factory-set passwords for the
different access levels are indicated in the "TECHNICIAN SERVICING" chapter of the Service Manual.
With the exception of the ISL configuration, the other parameters accessible at access level 2 are covered in the
PART III - of this manual.
• Select " ANALYZER SETUP" from the main menu. The following screen is displayed:
ANALYZER SETUP
PRINTER SETUP
The values indicated are valid only for printers supplied by ISL. For other printers, refer to the
printer user manual.
Power on parameters
Safety parameters
<Exit>
CAUTION ! The preconfigured duration, 4 min, is convenient for most of products. Increasing this
value could be dangerous.
Each of these communication modes is specialized (refer to the section PART I - 3.3.3 - FP page I-26) and
parameters linked to them must be set.
By means of the RS 232 C or the RS 485 link, the FP can send test results to a data processing system. If the RS
232C link is used, result messages including test programme parameters (conditions of run) and the program (if
they are selected, refer to the section 2.3.1.1 Transmitted data page II-61) are sent under the form of character
strings in delimited ASCII format (refer to the section 5 - RS 232C STANDARD INTERFACE page II-80 for the
meaning of the content of the message sent).
The Service port enables the upgrading of the control software by downloading. It also allows to upload /
download the content of the non-volatile safe memory (NVRam, refer to the PART III - section 4.5 - page III-
100).
<Exit>
The ALAN/RS-232C adapter must be connected to allow the access to the «RS-232 LINK SETUP»
menu.
The access to the external link setup is possible with the access level 1.
• Select "ANALYZER SETUP" in the MAIN menu.
• Select "EXT. LINK SETUP" in the "ANALYZER SETUP" menu.
• Select "RS 232 link setup" to display the submenu of the same name.
Transmitted data
Hardware setup
Software setup
Data flow control
Computer on-line: N
<Exit>
The different commands displayed in this way are treated in the following sections.
<Exit>
As well as the result message, 2 other optional messages can be sent: the “test programme parameters” and the
programme. Messages are transmitted under a character string form in ASCII code. Refer to the section 5 - RS 232C
STANDARD INTERFACE page II-80 for the meaning of the content of the message sent).
All the selections are in Flip-flop mode and the possibilities are "Y"/"N", yes or no.
• Select "Hardware setup" in the "RS 232 LINK SETUP" submenu to do display :
<Exit>
All the parameter keys are of the flip-flop type with 2 or more possibilities.
• Select "Software setup" in the "RS 232 LINK SETUP" submenu. The display becomes:
Analyzer ID (0 - 99): NN
Automatic validation of results: N
End of transmission character: 0
<Exit>
• Select "Analyzer ID" and type in the Analyzer ID number (0 - 99) and confirm with (ENT). This number is sent
with each result message.
If another result is recorded before "validation for transmission" the result will be lost.
See the chapters 4.2 -RESULTS page II-75; 4.3 -LAST RUN RESULTS page II-78 and 4.4 -PRINTOUT page II-78
for more information.
• Select "End of transmission character" (EOT), type in the numerical value and confirm with (ENT).
The EOT character falls into 2 categories : "0" or "> 0" (1 - 99).
EOT Character = 0
There is no EOT character at the end of transmission.
• Select "Data flow control" in the "RS 232 LINK SETUP" submenu. The display becomes :
The first 3 parameters keys, for protocol selection, are Flip-flop with "Y"/"N" as choices. Only one of them can be
configured "Y".
• Select the desired configuration. which is automatically taken into account on selection.
• Select the 4th parameter key and enter the value in seconds (see the screen above).
The time between each message will be as configured. It is not possible to request a second transmission of any
message.
The external computer uses the ENQ code (05H) to ask the Analyzer if any results are ready to be sent.
If the Analyzer has no results to send, it replies ACK (06H). If it has, the results are sent.
If there are several fruitless communications, the computer may decide to abort transmission by sending an EOT
(04H) character.
On receiving ACK, the computer need not reply. On receiving a results message, the latter must be checked
(checksum) and the computer must reply ACK (06H) or NAK (15H), depending on whether the message was correct
or not.
For the external link to be operational the "Computer on-line" parameter of the "RS-232 LINK SETUP" menu must
be set at "Y".
• Use the Flip-flop selection key to set the parameter "Y" / "N".
See in PART III - section 3.2 - DIFFERENT DIAGNOSTICS page III-96 for the procedure. If the message is very
rapid, don't forget that when there isn't any protocol used, the time between successive messages can be set (see
section 2.3.1.4 - Data flow control page II-62 of this chapter).
<Exit> <Init>
The configuration of this link needs to have the level one access authorization.
• Select "ANALYZER SETUP" in the MAIN menu.
• Select "EXT. LINK SETUP" in the "ANALYZER SETUP" menu.
• Select " PC link setup " to display the submenu of the same name.
The different commands displayed in this way are treated in the following sections.
• Select « Analyzer network address”, enter the Analyzer address number in the Alan network.
The address is the number allocated for the Analyzer in the network. This number can be from 1 to 31 inclusive. (the
maximum number of AD86 5G2 Analyzers on the network is 20). This number is then used to identify and control
the Analyzer from the PC.
Note: The operator should beware of entering the same address number for 2 Analyzers on
the same network. This will lead to incomprehensible messages being received by the PC.
2.3.3.1.3. PC on line
For the external link to be operational the "PC on-line" parameter of the "PC LINK SETUP" menu must be set at
"Y".
Use the Flip-flop selection key to set the parameter "Y" / "N".
It is thus possible for the "Laboratory Manager" to modify the level 1 password.
The master password is given in the PART III - section 4.1 - page III-99.
The date and time should then be entered to correspond to the formats chosen. See the following example.
When all the entries are correctly displayed, press <OK> to confirm them. If there are any incoherent entries, they
will be indicated at this stage.
3 - ALARMS
A continuous alarm is triggered and the red indicator light on the keypad is illuminated. As long as the alarm
condition continues, even if the alarm has been acknowledged, the red indicator remains illuminated.
In both cases, an intermittent audible alarm is triggered and the red indicator light on the keypad is illuminated. The
active buzzer pulse duration can be configured. When the alarm is acknowledged, the red indicator is extinguished.
An intermittent alarm is triggered and the red indicator light on the keypad is illuminated. The active buzzer pulse
duration is half that defined for error alarms. When the alarm is acknowledged, the red indicator is extinguished.
A warning number can be displayed - "Warning: NN". The list of warning numbers is given at the end of this
chapter.
In the case of failure or report alarms, the cause of the alarm is displayed. For example:
"FIRE DETECTION",
"FLASH ON FIRST FLAME TEST",
"END OF TEST: FLASH".
• Select <ACQUIT> to stop the audible alarm and return to the previous screen. Note that in the case of failure
alarms, if the failure is still present, the red "ALARM" indicator remains illuminated.
However, this does not mean that an instrument of this type is not dangerous or that, if the Analyzer does not switch
to standby, there is no danger for the operator and/or the Analyzer. It is always important, in the event of an alarm, to
check what has happened.
For example, because of a failure component, a failure alarm which normally switches the Analyzer to standby may
not do so. In this case, the operator must intervene to switch off the Analyzer.
In general, when an audible alarm is triggered, the operator must display the cause
of the alarm to check that the unit is operating normally.
To stop the audible alarm, the Analyzer must be switched off. After intervention of a qualified technician, replace the
fire detection thermofuse.
If this failure is signaled switch off the Analyzer and then switch it on again. If the failure still exists, call the ISL
Service Department.
Switch off the Analyzer and then switch it on again. If the failure still exists, call the ISL Service Department.
The life duration of the Ram non-volatile memory (NVRam) memory battery is approximately 7 to 8 years. This
alarm may be due to a failure battery.
The content of NVRam, where the Service Parameters are stored, is checked by the microprocessor. If an error
exists, the Analyzer automatically goes into download mode to restore the back-up memory content by loading a
backup file from a PC.
For this, a diskette containing the service parameters configuration (necessary if any upload had been carried out)
and an upload/download PC programme is provided with the standard FP 5G2 Analyzers. Refer to the PART III -
section 4.5 - UPLOAD / DOWNLOAD page III-100.
When uploading the service parameters configuration, do not use the same file name as the file on the diskette
delivered with the Analyzer.
The glow-plug is first used to light the test flame and the pilot light at the beginning of the test.
In this case, if the glow plug is defective, the system tries to relight the test flame for 10 minutes. If during this time
the test flame is still not detected (manual lighting) the system stops the test.
The glow plug is also used to relight the test flame and the pilot light in the case of an unexpected loss of test flame
during the test. In this case the system tries to relight the test flame for 1 minute. After that duration, if a test flame is
not detected the system stops the test.
If the current is outside the specified limits (< 3A et > 15A) the alarm is triggered but the test is not aborted.
Pressing (ALARM STOP) displays the cause of the alarm, indicated by a warning No. Refer to the following table
to find the corresponding alarm.
In the event of a warning alarm, the displayed warning number is the sum of the numbers of all the signaled warning
alarms. For example, if the safety temperature is too high and the presentations frequency too high, the displayed
warning number will be the sum of 1 + 2, therefore "3".
During sample editing (see section 1.5 -SAMPLE EDITING (access level 1) page II-56), the laboratory manager
selects the results page associated with the pre-programmed sample. A minimum specification and a maximum
specification are entered during "SPECIFICATION PAGE EDITING" (see section 1.6 -EDITING
SPECIFICATION PAGES (access level 1) page II-56). When a test performed with a pre-programmed sample, the
result (observed/corrected and/or rounded - depending on configuration defined during program creation) is
compared with the specifications (min. and max.).
If the result is "in spec", it is saved in the "IN SPEC" page defined for the pre-programmed sample (see section 1.5 -
SAMPLE EDITING (access level 1) page II-56).
If the result is "out of spec", it is saved in the "OUT OF SPEC" page defined for the pre-programmed sample as for
the tests stopped on "SAFETY" (see section 1.5 -SAMPLE EDITING (access level 1) page II-56).
The "out of spec" page can be the same page as the "in spec" page or it can be page 21. If no page is specified, the
results page will be page 21 by default.
In addition to the "out of spec" results sent to page 21, and the results received by default, page 21 receives all
results from tests not using pre-programmed samples.
The storage of results in all pages is governed by the FIFO principle (first in first out). No warning is given when a
result is deleted form a page.
When, on a given page, the maximum number of results is reached, the first result saved there will be
deleted from the page when a new result arrives. The tests for which no flash point was detected will
not be saved - for example when the pre-safety and safety alarms have been triggered (without flash
point detection).
4.2 -RESULTS
• Select "PAGES RESULT ALLOCATION DISPLAY" to display the results pages from 1 to 21.
• Select a results page from the list - <Down> to display the 2nd page from the list. After selecting a page, the
previous screen is displayed with "SELECTED PAGE" indicated.
• Select <Show result> and the last result saved in this page is displayed.
1. The results page identifier (n/N) indicating the page number of the current results page out of the total
number of results pages available.
2. The runs environment:
Sample ID, Sample No., operator name, test No., Program No., the atmospheric pressure and the type of
igniter used ("G" for gas and "E" for electrical).
3. The EFP, the observed result and the corrected result,
4. Information concerning comparison with specification - "Yes", "No" or "SAFETY" ("_" indicates page
21) and the "*" indicator is shown if:
• The probe measurement values have been manually adjusted, i.e., without using the automatic
adjust function (refer to the PART III - section 4.4 - page III-100).
• The programmed date for the "next" adjustment has already passed.
5. The maximum, minimum and mean results for the page.
• To display other results from this results page, use <Previous> or >Down>.
• Select "STATISTICS".
• Use "SELECTED ITEM" to make a flip-flop selection (for the displayed page) of one of the following:
STATISTICS
Page: 2 Items: All results
Selected items: 8
In spec: 8 Out of spec: 0
Min. result: 62.0 Max. result: 64.0
Average: 63.00 Deviation: 0.71
<Exit>
Tests stopped on "SAFETY" are not taken into account by the statistics.
The "STATISTICS" screen indicates the selected results page and the type of results on which statistical analysis has
been performed. Indicated statistical details are:
(xi - xa)2
( Dms )2 = ________
N
xi = all results
xa = mean result
N = number of items
Dms = standard deviation
Printing statistics
After selecting ("SELECTED ITEM"- see above) the type of results on which statistical calculations are to be
performed, the user can select <Print> to make a printout:
• Statistics only
• Select a results page from the list. The pervious screen appears.
<No> <Yes>
• Select <Yes> to delete the pages contents and the page name.
The "LAST RUN RESULT" menu allows the operator to display, print and validate the result of the last run for
transmission on the RS-232C interface. It is also possible to re-transmit the result (in the event of a failure, for
example).
• To re-transmit the last run result, select "VALIDATE EXTERNAL LINK TRANSMISSION".
• The sample ID, sample No., program name, program No., operator name and EFP,
• The flash point (observed and corrected), date, time and atmospheric pressure,
• The probe measurement values have been manually adjusted, i.e., without using the automatic adjust
function (refer to the PART III - section 4.4 - page III-100)
• The programmed date for the "next" adjustment has already passed.
• Select "VALIDATE EXTERNAL LINK TRANSMISSION" from the "LAST RUN RESULT" menu.
4.4 -PRINTOUT
The Analyzer is equipped with a standard Centronics printer interface with a 25-pin connector. An Epson compatible
printer (80 or 40 columns) can be connected.
4.4.1 - INITIALIZATION
Printer initialization allows the printer and its interface to be re-programmed.
The following lists can be printed by selecting the corresponding function key.
• Sample list,
• Page list,
• Tests list,
• Operators list.
• Select "SHOW TEST LIST" and select a test program from the list.
• The operator can check the program by selecting <Display>. The selected program is displayed. Select <Exit> to
return to the previous screen.
The ISL FP56 5G2 and FP170 5G2 Analyzers standard versions are equipped with a simple RS-232C serial interface
for the results to be collected on a PC and sent to a LIMS (refer to the section 2.3.1 - RS 232C link setup page II-60
for the RS 232C link configuration).
Use the adapter supplied with the unit. This one has on the same side 2 RS485 series ports to be connected
simultaneously to the inlet and outlet of the ALAN network and a RS 232C series port to be connected to a PC.
When the Analyzer is connected to the Alan network, the direct connection to a LIMS is no longer possible, it must
be done via the PC.
The RS 485 connector of the adapter is a 9-pin connector. The pin configuration is as shown below.
RTS
FP170 5G2:
( 1,"R ","CYCLO-HEXANON","090498#1 ", 1,99,"C", 43.7, 43.7, 44.3,999.9,999.9,10," ")AD
( 1,"C ","LG ",21,21,"-", 98.7, 1,"G",999.9,"09/04/98 ", 0,"13:16 ")64
( 1,"T ","ISO 13736(C)","N", 1, 1, 0,999.9,999,999, 1, 0.5, 34.7,"N", 53, 58,999)4F
Heating rate
Frequency
Test start
Test end
Stirring
The value 999 indicates that the field is not being used or is reserved for a future use.
( XY, " R" ," SSSSSSSSSSSS" ," NNNNNNNNNNNN" ,P P ,9 9 ," T " ,EEE.E,FFF.F,CCC.C,9 9 9 .9 ,
9 9 9 . 9 ,ZZ," A" ) CK CR LF
XY = Analyzer number
R = Result
S...S = Sample ID
N...N = Sample No
PP = Test No
99 Non used
EEE.E = Expected Flash Point
FFF.F = Flash point
CCC.C = Corrected flash point
999.9 = Non used
ZZ = Test stopped by flash point detection.
10: flash detection
13: flash safety detection
A = Calibration indicator
FP56 5G2:
Number of
Identification Description
characters
Analyzer number 2
Type of message identifier 2 «T» (for test)
Program name 12
Rounded 2 0, 1, 2 (None, ASTM D93 or ISO/NF/EN)
Barometric correction 1 «O» or «N»
Non used 2
Non used 2
"Test every" of initial phase 5
Start test temperature of initial phase 3
Non used 3
Heating rate standard phase 2 0, 1, 2 or 3 (low, A, B, or high)
"Test every" of standard phase 5
Start test temperature of standard phase 5 (the real temperature value is sent)
Go-No Go 1 «Y» or «N»
Pre-safety alarm 3 «Y» or «N»
Safety alarm 3 «Y» or «N»
Non used 3 Always 999
FP170 5G2:
Number of
Identification Description
characters
Analyzer number 2
Type of message identifier 2 «T» (for test)
Program name 12
Rounded 2 0, 1, 2 (None, ASTM D93 or ISO/NF/EN)
Barometric correction 1 «O» or «N»
Stirring speed 2 0: None / 1: ISO / 2: NF
Non used 2
Heating rate initial phase 2 0, 1 or 2 (None, A or high)
"Test every" of initial phase 5
Start test temperature of initial phase 3
Non used 2
Heating rate standard phase 2 0, 1, 2 or 3 (low, A, B, or high)
"Test every" of standard phase 5
Start test temperature of standard phase 5 (the real temperature value is sent)
Go-No Go 1 «Y» or «N»
Pre-safety alarm 3 «Y» or «N»
Safety alarm 3 «Y» or «N»
Non used 3 Always 999
Example
Reception of result and test context messages. Translation to delimited ASCII format using Wedge software (Version
3.0 Professional Edition).
If hardware flow control is used, connect the PC COM port RTS to the Analyzer CTS.
• Select the "CONTINUE" button and choose "Multiple fixed length data fields".
• Select "CONTINUE". A maximum of 40 fields are allowed. In the example, 32 fields will be entered.
• Click on the "NEXT FIELD" button to go to the next field. There is also a "PREVIOUS FIELD" button.
The resulting file is delimited ASCII format, read by spreadsheets and database software (the fields are delimited by
commas, alphanumeric chains are in inverted commas and the end of record is by CR/LF).
The fields "None" above can be replaced by "Ignore this field", if they are not required.
1 - GENERAL
Cleaning the cup, the cover and their accessories (in PART I - section 7.7 - page I-47)
Adjusting the test flame and the pilot light (in PART I - section 3.4.2.1.3 page I-30)
The temperature measurement check (in PART I - section 6.1 - page I-42)
2 - QUALITY
After checking sample temperature measurements and atmospheric pressure, as described in PART I - chapter 6 -
MEASUREMENT CHECKS AND SETTINGS page I-40, it may be necessary to perform adjustments on the
corresponding measurement circuits.
QUALITY
Temperature measurement calibration
Next calibration date: DD/MM/YY
TEMPERATURE MEASUREMENT
Temperature measure calibration
Calibration frequency: 365 days
Next calibration date: DD/MM/YY
Start test refusal: N
<Exit>
Entry in this menu requires that the entire calibration procedure be completed.
Consequently, before starting this procedure, make sure that you are in possession of the ISL
PS 100 probe simulator or certified resistors.
<Exit>
If the probe simulator has not been certified -50°C/+100°C, the resistance values must be certified
and the exact values must be entered. This certification can be performed by ISL or any other
authorized organization.
<Exit>
• Enter the exact values (with 2 decimal places) of the resistors placed in the -50 et 100°C positions. Typical values
for ISL probe simulator resistance values are given in the screen reproduction below.
• Select <Ok> to validate the values.
<Exit>
Temperature: 0.X
A/D: CCCCC
• Wait for the "TEMPERATURE" and "A/D" displays to stabilize and select <OK>.
Temperature: XXX.X
A/D: CCCCC
• Wait for the "TEMPERATURE" and "A/D" displays to stabilize and select <OK>.
As indicated in the screen, probe correction is calculated by subtracting the probe temperature from
the temperature reading on the reference thermometer.
To modify the temperature units, use the "TMP. UNIT" key to display the correct units.
There are 21 correction values between - 80°C / - 112°F and 320°C / 608°F at intervals of 20°C or 36°F. These
values are displayed over 2 pages. To display the second page, select <Down>.
The sign of the correction value (+/-) must be indicated and can be entered with one decimal place. A linearization
calculation is performed between the 21 values of the table.
For example:
At 110°C the corrected value will be 109.9°C (determined by a linearization calculation between 100 and 120°C).
CORRECTION TABLE
• To enter a correction, select a value, enter probe correction and select (ENT).
• For the second page of values, select <Down>.
If sample temperature is below - 50°C (- 58°F), the - 50°C temperature correction will be used. If the
sample temperature is 100°C (212°F), the 100°C temperature correction will be used. This
correction is applied during test only.
• In the run menu, select another program than the one displayed that will lead to the EFP deleting and will stop the
bath temperature regulation or enter the value 999 as regulation temperature to inhibit the regulation function (refer
to the PART II - section 2.2.1 - Power on parameters page II-59).
• Select “BATH TEMPERATURE CALIBRATION” in the “QUALITY” menu:
<Exit>
• Use the sample temperature probe to measure the bath temperature: insert the probe in the drilling located at the
bottom of the bath.
• Press the “Measure” key of the “BATH TEMPERATURE TMP CALIBRATION” menu and wait for the sample
temperature measure stabilize.
• Read the sample temperature when it is stable.
• Press the <Exit> key to return to the previous screen.
• Select <Ext read temperature> and enter the value measured by the sample temperature probe.
• Select <Exit> to return to the “QUALITY” menu.
• Select "QUALITY" in the main menu and then select "ATMOSPHERIC PRESSURE CALIBRATION".
<Exit>
• Select "ATMOSPHERIC PRESSURE" and enter the value of atmospheric pressure read on the reference
barometer. Validate with (ENT).
This chapter describes how the "DIAGNOSTICS" sub-menu can be used to check the operation of the various parts
of the Analyzer. Refer also to the chapter 6 - TROUBLESHOOTING IDEAS page III-111 for additional
troubleshooting hints.
Any diagnostics cannot be performed on the Analyzer when a test is in progress. Similarly, a test
cannot be started on the Analyzer when in diagnostics mode.
SERVICE
<Exit>
When the "DIAGNOSTICS" screen is displayed, the Analyzer is in diagnostics mode. The Analyzer remains in
diagnostics mode until <Exit> is selected.
FP56 5G2:
DIAGNOSTICS <Measures>
Printer
Flame RS-232 link: Off
Heating: Off Heating: 0 %
Cooling: Off Cooling: 0%
<Exit>
FP170 5G2:
DIAGNOSTICS <Measures>
Stirrer Printer
Flame RS-232 link: Off
Heating: A Heating: 0 %
Cooling: A Cooling: 0 %
<Exit>
When a diagnostic command is given, the operator can press <MEASURES> to check the device in question.
When the heating and ignition devices (heating elements, gas supply SV, gas igniter and glow plug) are activated in
the diagnostics mode, they remain activated for 4 minutes.
MEASURES
Display of "MEASURES" allows rapid verification of the various data and the corresponding A/D conversion. This
allows the detection of any anomalous values due to a faulty sensor or component.
The "FLAGS" display in the "MEASUREMENTS" screen allows rapid verification of the status of the various input
circuits.
A flag can have the value "0" or "1". The interpretation of flag values is as follows:
3.2.1 - Heating
• Select "HEATING" on the right of the screen and enter a value corresponding to the power in percent to apply to
the heating block - between 50 and 100 in order to detect an increase in the measured temperature.
• Use "HEATING" on the left of the screen to display "ON", for power-on (Flip-flop).
• Select <MEASURES> to display the "MEASURES" screen and check the heating block temperature, "BATH
TMP" - the "HEATING" value (in %) will be the same as that entered in the "DIAGNOSTICS" screen.
An increase in the heating block temperature should be observed and the red heater light (see Picture 4 page I-20)
should be illuminated for the percentage of time requested for "HEATING" on the right of the screen in the
"DIAGNOSTICS" screen.
3.2.2 - Cooling
• Select "COOLING" to display "ON" (Flip-flop): the cooling solenoid valve of the heating block should be heard to
operate.
• Select <MEASURES> to display the "MEASURES" screen : the temperature displayed for "BATH TMP" should
fall.
3.2.3 - Printer
• Connect the printer and set to On-line.
• Select "PRINTER".
Printer test
or
Printer test
or
3.2.6 - Ignition
• Select "FLAME" in the "DIAGNOSTICS" screen. The "FLAME DIAGNOSTIC" screen appears:
Each diagnostic function is independent, but before lighting the test flame or energizing the glow plug, cup and cover
must be in place and the igniter arm must be in the test position.
To light the test flame, the gas supply must be connected at the rear of the Analyzer.
• Select "Gas SV" to display "ON". The sound of the solenoid valve clicking open should be heard.
• Press the "GLOW PLUG" key to display "ON". The glow plug should light the pilot light and the test flame. After
lighting the test flame, select "OFF" to extinguish the igniter flame.
• To apply the flame, select "EXECUTE FLAME TEST".
• Select "OFF" at solenoid valve to extinguish the flame.
• Press the "GLOW PLUG" key to display "ON" to energize the glow plug.
• Select <MEASURES> and check the displayed "GLOW PLUG" current. It should be about 7A and the "A/D"
conversion should display about 7000.
• To apply the igniter, select "EXECUTE FLAME TEST".
SERVICE PRINTING
<Exit>
3.3.2 - Measures
To printout the current measures, select "MEASURES" in the "SERVICE PRINTING" sub-menu.
The current measures may be displayed and also printed by selecting "MEASURES DISPLAY" in the "SERVICE"
menu or by selecting “MEASURES” in the “DIAGNOSTIC” menu (refer to the section 3.1.2 - Measurement display
page III-95).
This chapter covers service parameter configuration and service parameter functions specific to access level 2. If
access is denied, the system displays the required access level.
Service parameter configuration for access levels 0 and 1 is explained in PART II - section 2.2.2 - Safety
parameters page II-59.
On reception of the Analyzer, it is recommended to make a printout of the internal parameters (refer to the previous
section 3.3.1 - Internal parameters page III-98).
• Select "ANALYZER SETUP" from the main menu.
• Select "TECHNICAL SETUP" in the "ANALYZER SETUP" menu.
TECHNICAL SETUP
Service password:
Regulation parameters
Buzzer pulse width: W
Sample temperature calibration values
Upload / Download
<Exit>
REGULATION PARAMETERS
Kp: pp
Ti: iii s
Td: d s
Delta t: xx s
<Exit>
• Select "BUZZER PULSE WIDTH" and enter a value between 1 and 100. Validate using (ENT).
If these values are manually modified, it will be indicated by the appearance of an asterisk when results are displayed
or printed out. Refer to section B of the "RESULTS AND PRINTING" chapter.
Modem signals are not provided during downloading. If necessary, transfer by modem should be carried out in 2
steps:
1. Transfer between 2 PCs by modem
2. Local transfer between PC and Analyzer without modem signals.
The transfer mode (uploading / downloading) is a specific Analyzer mode. The Analyzer switches to this mode:
Either by automatic detection of a transfer requirement (signaled on the PC screen),
Or on request by the operator from the Analyzer keypad.
In the former case, the Analyzer cannot leave transfer mode until it has succeeded in linking with the host PC.
In the latter case, it is best not to try to quit the transfer mode. If the downloading process has begun, then some of
the memory has probably been deleted. If an error has been made, the best method is to let the transfer continue its
course and start the transfer over again. When the Analyzer is switched off during downloading, on switching on
again, it will detect a transfer requirement and will signal this requirement to a connected PC on which the transfer
program is running.
UPLOAD / DOWNLOAD
<Exit>
• Select the required command (the upload is performed towards the PC).
On the PC
• Start the transfer program on the PC as explained in the "Read.me" file - refer to the section 4.5.2 - page III-101.
• Enter the communications serial port (COM) as requested (1 or 2). Confirm by (ENT).
Analyzer Program and Texts Software Downloading
• Type in the name and extension of the information file named FP93.Vxx (xx being the software version) and
confirm by (ENT).
Service Parameters Uploading/Downloading
• Input the file name requested (the name and extension must be given) and press (ENT) to confirm.
During uploading of service parameters to the PC, do not use the original filename. A name
containing the date could be used, for example, SPDDMMYY.NVM.
When the Analyzer is waiting for a download, the red LED will flash every second.
A downloading in progress is indicated by rapid flashing which is related to the rate of data transfer.
Switch off the Analyzer and disconnect it from the mains before removing the housing.
If the service operations require you to switch on the Analyzer, switch it off again before
disconnecting or removing any electrically powered components.
Securing screws of
the rear plate
Inlet / outlet of
Stainless steel
the heat
rear plate
exchanging liquid
• Loosen the 2 securing screws of the stainless steel rear plate and remove it
• Pull the lateral end-plate towards the rear to remove it
• If necessary, unscrew the top ring of the bath
• Pull the stainless steel cover backwards then lift
Use the relevant photographs to locate the various components. Indications for the “side” of the Analyzer are given
when looking from the front of the Analyzer.
The spare part list, DOCV208X200, is attached to the user Manual. Open this file from the contents.
Acquisition
board
Safe Ram
memory
battery
Connector (J1)
for external fire
alarm
Control unit
board
Central Unit
Board +
Acquisition
Board
Electronic
boards power
supply box
Bath Fuse
Heating
regulation board
• Remove the Control Unit housing cover (refer to the section 5.1.1 - page III-103).
• On the Acquisition board, disconnect the connector for the magnetizing coil power supply wires (J17) for the
cooling solenoid valve (refer to the Picture 12 page III-104).
• Remove the screw or the clip securing the magnetizing coil (1) on the solenoid valve to separate them.
• Remove the magnetizing coil, wires and connector and replace it by a new one.
• Reassemble the new magnetizing coil proceeding in the reverse order.
• Cut the gas supply and disconnect the gas inlet tube from the rear of the Analyzer.
• Remove the Control unit housing cover (refer to the section 5.1.1 - page III-103).
• Remove the securing nut for the gas tube on the solenoid valve.
• Remove the 2 securing screws for the solenoid valve support accessible from the rear of the Analyzer.
• Extract the solenoid valve and its support.
• Remove the screw or the clip securing the magnetizing coil on the solenoid valve to separate them.
• Remove the solenoid valve from its support.
• Install the new solenoid valve on the support then proceed in reverse order to re-install the various components.
Switch off the Analyzer and disconnect it from the mains before removing fuses.
Use only fuses of the correct type and rating as indicated in the list of spare parts, DOCV208X200 (see attached file
accessible from the content).
5.3.5.1. Thermofuse
• Disconnect the thermofuse located on the lateral right side connection panel of the test unit (see Picture 4 page I-
20).
• Replace the damaged thermofuse by a new one.
The 2 general fuses are situated at the rear of the unit under the power supply socket. To remove them:
• Use a screwdriver to open (downwards) the small protection cover. Use the screwdriver to unlock the
corresponding fuse holder.
• Remove the fuse holder and replace the fuse: 6,3A / 230V - 10A / 115V.
The power supply box K01069 for electronic boards contains a fuse. To replace it:
• Remove the control unit housing cover (refer to the section 5.1.1 - page III-103).
• Locate the power supply box for electronic boards under the Central Unit board and the Acquisition board (see
Picture 13 page III-105).
• Remove the 3 securing screws for the power supply box accessible from under the Analyzer.
• Extract the box without disconnecting it.
• Unscrew the 6 securing screws for the power supply box: 2 screws in the top of each side.
• Remove the fuse from its holder and replace it: 6,3A / 230V
The electronic board Y20801 controlling the heating contains a fuse. To replace it:
• Remove the stainless steel rear plate then the lateral end plate (refer to the section 0page III-104).
• Locate the Heating control board next to the bath and the fuse (see Picture 14 page III-105).
• Remove the fuse from its support and replace it: 10x38 8A
Do not replace the battery before printing or uploading (towards a PC file) the internal
parameters of the Analyzer.
Before handling the processor board or any other electronic components, touch a grounded
metallic element to discharge yourself.
Then:
• Remove the control unit housing cover (refer to the section 5.1.1 - page III-103).
• Locate the safe Ram memory battery on the Control unit board (see Picture 12 page III-104) and replace it.
• Reassemble the Analyzer control unit housing cover.
• Power on the Analyzer: the alarm is triggered on.
• Display the origin of the triggered alarm: “Low battery” and acknowledge it.
• The following screen appears:
- Press the “Analyzer serial number:” key and enter the Analyzer serial number.
- Press the “Set default values” key: parameters are initialized.
- Check Analyzer parameters compared with ones printed (refer to the PART II - section 3.5.19 - “Low battery”
page II-72) and complete them.
• Carry out an automatic adjustment for sample temperature measurement, for bath temperature measurement and for
atmospheric pressure measurement.
Connector J1
1 2 3
NF Com NO
To test the Fire Detection alarm, switch off the Analyzer and remove the thermofuse by unplugging it. Switch on the
Analyzer without the thermofuse. The Fire Detection alarm should be triggered.
6 - TROUBLESHOOTING IDEAS
Q1 I pressed the (STOP) key before noting the result. How can I recover the result?
A1 Select "Last run result" in the main menu and choose "Display" to display the last result.
Q2 There was a printer problem during automatic result printing at the end of the test. What can I do?
A2 Select " Last run result" in the main menu and choose "Print" to print out the result again.
Q3 Can I validate results before they are transmitted on the RS232 link?"
A3 The Analyzer must be configured to request validation before transmission, you can then simply select
"Last run result" from the main menu for each test.
Q4 Can I lock the Analyzer so that it performs only one given test, ISO 13736 for example? Is it
possible to make this test the failure test at power up?
A4 The failure test at power up can be configured (numbers 1 to 20). The test used in Run Menu can be
locked using "Customize Run Menu Screen".
Q5 I created a test in Main menu, can I use it whilst locking access to the Analyzer (i.e., access level 0)?
A5 It is possible if the test has been saved before leaving Main menu.
Q6 I am creating a test in Main menu. Can I run this test or another test in Run Menu?"
A6 It is always possible to leave Main menu to return to Run Menu. In all cases, it is necessary to save a test
created in Main menu if you wish to use it in Run Menu or simply keep it.
Q7 I have a sample which is seldom tested. Can I limit the memory allocation for saving this sample?
A7 Select the "Pages edit" function which allows the definition of the maximum number of results (5, 10, 15,
20, etc.) which can be saved in each of the pages. Select the "Results pages allocation" function to display
the current configuration.
Q8 I do not want to save results which our outside of the specifications I defined in the corresponding
results page. How can I do this?
A8 During creation of the pre-programmed sample, specify your page number as "in spec" and specify 21 as
the "out of spec" page number.
Q9 If I use an "in spec" page and define page 21 as the "out of spec" page, will I still get an end of test
alarm if the result is out of spec?
A9 Yes. The "End of test: flash" alarm will be triggered as usual. In addition, the test which allows detection
of the "Result out of spec" alarm is performed on the basis of the specifications in the "in spec" page.
Both alarms will be displayed on pressing (ALARM STOP).
A10 The specification test is related to a page from 1 to 20. This test can only be performed if such a page has
been defined, a consequence of which is that the results will be saved there. Saving of results is an
Analyzer option which you can choose not to use. Results will be saved, the most recent overwriting the
oldest without any intervention required from the user.
Note: If you want to allocate the maximum space for saving results from other samples, you can limit the
allocation for this page to the minimum value of 5 results.
Q11 Is it possible in Run Menu to select a pre-programmed sample then change the test program
number on the Run Menu screen?
A11 A pre-programmed sample is always associated with a test program and possibly with a specification
(defined by an "in the spec" page). If the test program number is modified as suggested, the sample
identifier and the results page numbers will automatically be deleted.
Q12 Can I use the same results page for different samples?
A12 Yes. However, this may limit the relevance of the "Statistics" function, which would become redundant.
A14 For the same reason given above, use of the "Statistics" function on results saved in page 21 would be
meaningless.
Q15 Can I configure the Analyzer for pressure units other than those used during the automatic
correction of atmospheric pressure?
A15 Yes. For example, if automatic correction is performed in mmHg, it is possible to run the Analyzer using
kPa.
• Remove the test unit lateral end-plate (refer to the section 5.1.2 - Dismounting the facing cover of the control unit
page III-103) on the right side of the Analyzer.
• Install the draught protection accessories following the diagram below:
• Re-install the end-plate assembly of the Plexiglas protection on the side of the Analyzer proceeding in reverse
order.
INDEX
Symbols
(ALARM STOP) 29
(PRINT STOP) 29
(ENT) 29
(RESET) 29
(BACKSPACE) 29
(STOP) 29
Flash point................................................................. I-22
A Diagnostics .................................................................... I-23
Dimensions .................................................................... I-24
Abnormal atmospheric pressure ................................... II-71 Display........................................................................... I-36
Abnormal heating rate .................................................. II-70 Download
Access codes ................................................................. I-41 Service parameters................................................ III-100
Accessories Download
Available for analyzer ............................................... I-23 Principle of transfer .............................................. III-101
Installation / using.................................................III-113 Download
Of the cover .............................................................. I-19 Installation and starting of program...................... III-101
Adjustment check........................................................III-98 Download
Adjustments Transfer requested by the operator ....................... III-101
The Quality menu ...................................................III-89 Download
ALAN............................................................................ I-26 Software code / Software texts...........................III-101
Alarms .......................................................................... II-67 Download
Error and signalization.............................................. I-40 Service parameters .............................................III-101
Types........................................................................ II-67 Download
Analyzer Unsuccessful transfer............................................ III-102
FP56 5G2 / FP170 5G2 ............................................ I-17 Draught
Arrow keys .................................................................... I-35 Protection ............................................................. III-113
ASTM D 56 (FP56 5G2) EN/ISO 13736, NF T 66-009
(FP170 5G2) E
Standards summary................................................... I-16
Electric
C Ignition ...................................................................... I-22
End of test
Calibration flash ..........................................................................II-73
Periodicity...............................................................III-89 End of test
Sample temperature measurement...........................III-89 no flash .....................................................................II-73
Cleaning ........................................................................ I-47 End of Transmission (EOT) Character
Computer on-line RS-232 .....................................................................II-62
RS-232 ..................................................................... II-64 ENQ/ACK protocol
Conditions of a test run RS-232 .....................................................................II-63
RS-232 ..................................................................... II-82 Entry
Configuration Flip-flop .................................................................... I-37
Software.................................................................... I-23 Environnement
Connections................................................................... I-26 Printing.....................................................................II-79
Control unit ................................................................... I-18 Examples of transmitted messages
Cooling.......................................................................... I-24 RS-232 .....................................................................II-81
Diagnostics .............................................................III-96 External link .................................................................. I-25
Cooling system.............................................................. I-21 External link test
Correction table...........................................................III-92 RS-232C...................................................................II-64
Customize
Run mode screen...................................................... II-57 F
D Failure
Safe memory.............................................................II-69
Data flow control Failure
RS-232 ..................................................................... II-62 Other alarms .............................................................. I-40
Definitions Failure
EFP Expected Flash Point ........................................ I-16 Glow plug current failure .........................................II-70
Flash point ................................................................ I-16 Failure
Delete Flat battery............................................................ III-108
Page contents ........................................................... II-77 Familiarization
Page name and contents ........................................... II-77 Utilization.................................................................. I-38
Detector Final phase