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    Lab Report: Edvair Paula Moreira Filho 000837578

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    Edvair Filho
    This lab report summarizes the preparation of a potassium hydrogen phthalate (KHP) standard solution and the titration of sodium hydroxide (NaOH) and citric acid solutions. The student weighed KHP to determine its molarity, then titrated NaOH against KHP to calculate the NaOH molarity. Next, the student titrated NaOH against a citric acid sample and calculated the citric acid percentage. The student reported their results and noted that the NaOH titration trials had a large range, indicating a potential error in their citric acid calculation.

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    Lab Report: Edvair Paula Moreira Filho 000837578

    Uploaded by

    Edvair Filho
    48 views7 pages
    This lab report summarizes the preparation of a potassium hydrogen phthalate (KHP) standard solution and the titration of sodium hydroxide (NaOH) and citric acid solutions. The student weighed KHP to determine its molarity, then titrated NaOH against KHP to calculate the NaOH molarity. Next, the student titrated NaOH against a citric acid sample and calculated the citric acid percentage. The student reported their results and noted that the NaOH titration trials had a large range, indicating a potential error in their citric acid calculation.

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    Acid-Base Titrations

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    This lab report summarizes the preparation of a potassium hydrogen phthalate (KHP) standard solution and the titration of sodium hydroxide (NaOH) and citric acid solutions. The student weighed KHP to determine its molarity, then titrated NaOH against KHP to calculate the NaOH molarity. Next, the student titrated NaOH against a citric acid sample and calculated the citric acid percentage. The student reported their results and noted that the NaOH titration trials had a large range, indicating a potential error in their citric acid calculation.

    Copyright:

    © All Rights Reserved
    Download as DOCX, PDF, TXT or read online from Scribd
    Download as docx, pdf, or txt
    48 views7 pages

    Lab Report: Edvair Paula Moreira Filho 000837578

    Uploaded by

    Edvair Filho
    This lab report summarizes the preparation of a potassium hydrogen phthalate (KHP) standard solution and the titration of sodium hydroxide (NaOH) and citric acid solutions. The student weighed KHP to determine its molarity, then titrated NaOH against KHP to calculate the NaOH molarity. Next, the student titrated NaOH against a citric acid sample and calculated the citric acid percentage. The student reported their results and noted that the NaOH titration trials had a large range, indicating a potential error in their citric acid calculation.

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    CHEM PH108 Experiment 2 (Summer, 2021) – Report Form

    Lab Report
    Name Edvair Paula Moreira Filho Student ID 000837578

    KHP Standard Solution Preparation

    Table 1: Weighing of KHP

    Container +
    Container + Solid (g) Mass of KHP (g)
    Residue (g)

    5.5543 2.0395 3.5148

    Calculation of KHP Molarity in the space provided below. Show your work.
    Report the answer to the correct number of significant figures.

    g∗mol
    ∗1
    204.22 g
    ∗1000 mL
    250.0 mL
    KHP Molarity=3.5148
    L

    KHP Molarity=0.0688 4 mol/ L

    NaOH Standardization

    Table 2: Titration Volumes


    At Least Three Trials are Mandatory
    Additional Trials Only if Necessary
    Indicator
    Trial 1 Trial 2 Trial 3 Trial 4 Trial 5
    Blank

    Final Volume (mL) 0.22 18.47 35.81 45.73

    Start Volume (mL) 0.15 1.16 18.47 31.43

    Titration Volume
    0.07 17.30 17.34 14.30
    (mL)
    Indicator Blank
    0.07 0.07 0.07 0.07
    Volume (mL)
    Blank-Corrected
    0.00 17.23 17.27 14.23
    Titration Volume (mL)

    Page 1 of 7
    CHEM PH108 Experiment 2 (Summer, 2021) – Report Form

    Mean Titration Volume (three best trials): ________16.24_________ mL

    Range (three best trials): _______3.05_________ mL

    Calculate the NaOH molarity in the space provided below. Show your work.
    Report the answer to the correct number of significant figures.

    mL∗1 L
    ∗mol NaOH
    1000 m L
    ∗1
    mol KHP
    ∗1000 mL
    0.06884 mol KHP 16.24 mL
    NaOH Molarity= ∗25.00
    L 1L

    NaOH Molarity=0.106 0 mol /L

    Citric Acid Analysis

    Table 3: Titration Volumes


    At Least Three Trials are Mandatory
    Additional Trials Only if Necessary
    Indicator
    Trial 1 Trial 2 Trial 3 Trial 4 Trial 5
    Blank

    Final Volume (mL) 0.24 9.68 18.25 26.83

    Start Volume (mL) 0.13 1.10 9.68 18.25

    Titration Volume
    0.11 8.58 8.57 8.58
    (mL)
    Indicator Blank
    0.11 0.11 0.11 0.11
    Volume (mL)
    Blank-Corrected
    Titration Volume 0.00 8.47 8.46 8.47
    (mL)

    Mean Titration Volume (three best trials): ________8.47_________ mL

    Page 2 of 7
    CHEM PH108 Experiment 2 (Summer, 2021) – Report Form

    Range (three best trials): _______0.01_________ mL

    Calculate the %(w/v) concentration of citric acid. Show your work.


    Report the answer to the correct number of significant figures.

    mL∗1 L
    ∗mol C . A .
    1000 mL
    ∗192.1 g
    3 mol NaOH
    ∗1
    0.1060 mol NaOH mol C . A .
    % C . A .= ∗8 . 47 ∗100
    L 10.00 mL

    % C . A .=0.575 %

    Conclusions This experiment showed that 0.575% of the solution mass


    : was composed of citric acid. It is important to emphasize
    that the three titrations for NaOH standardization had a
    range greater than 0.20 mL, then one of the samples
    should have been replaced by another titration to reduce
    this range and reach a more precise and reliable mean.
    Therefore, we can say that the final result has a
    considerable analysis error. This error could be eliminated
    by following some important steps, such as eliminating any
    bubbles at the burette tip, rinsing the beaker walls and the
    burette tip to recover any spilled reagent, and wait 30s to
    make sure the end-point was reached.

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    CHEM PH108 Experiment 2 (Summer, 2021) – Report Form

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    CHEM PH108 Experiment 2 (Summer, 2021) – Report Form

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    CHEM PH108 Experiment 2 (Summer, 2021) – Report Form

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    CHEM PH108 Experiment 2 (Summer, 2021) – Report Form

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