Priyadarshini college of engineering

Inventys Reasearch Company Pvt Ltd

From: - 05/07/22 to 22/07/22

Internship report
Submitted by
Mr.

Co-ordinator HOD
Miss/Mr: Dr. Swarda Mote
 CERTIFICATE

This is to certify that __________________________________________________

Student of final year B.tech Chemical engineering has completed the internship
programme at Inventys Research Company Pvt. Ltd.
Nagpur during the academic session 2021-22.

HOD Principal
Dr Swarda Mote Mr S A Dhale
Head of chem . Engg department PCE, Nagpur
PCE, Nagpur
 INDEX
1. Introduction
2. Objectives
A. Brief literature survey Equipment
B. Utilities
C. R & D
D. QUALITY CONTROL
E. QUALITY ASSURANCE
F. EHS

3. METHODOLOGY
A. DISTILLATION COLUMN
B. GLASSED LINE REACTOR
C. AUTOCLAVE
D. HEAT EXCHANGER
E. CENTRIFUGE
F. SCRUBBER
4. CONCLUSION
5. REFERENCES
 ACKNOWLEDGEMENT

With the depth of my heart, I feel immense pleasure in expressing my views for all
correspondence for his valuable guidance, constant encouragement and
enlightened comments for preparing this “INTERNSHIP REPORT “. Apparently, I
am very thankful for the thought provoking discussion, invaluable inspiring and
scholastic guidance, constructive and rational criticism during this course of
seminar report work.
I would also like to thank Head of the Department , Chemical engineering Dr. S. R.
Mote mam for providing his valuable guidance and extending the departmental
facilities for the completion of the " Industrial Training Report " work .
It gives us immense pleasure to pass on our special thanks to our Training in
charge Mrs Bhagyashri Mankar for their all - time guidance to me during the
training and active encouragement due to which I was able to complete my In -
plant training ..
I should express my most valuable thanks to all section in charges, QC Officers,
Production Co - ordinator, and HR who helped me in many ways by guiding me
with their working tips and practical knowledge they gave to me.

(Final Year Chemical Engineering)

 INTRODUCTION

Inventys Research Company – India’s Leading Custom Manufacturer Of

Actives, Advanced Intermediates, & Specialty Chemicals:
A research- driven Custom Chemicals Manufacturing company from India -
with a heritage of demonstrated excellence in process development , process
scale - up , process engineering , project management , and finally in consistent
reliable custom manufacturing of chemicals for Crop Protection , Pharmaceutical ,
and other Fine / Specialty applications . Inventys advanced technologies ensure
innovative , cost effective , and safe processes .
The product portfolio is focused on advanced intermediates and active
ingredients for the crop protection and pharmaceutical sector, as well as
numerous specialty chemicals which find use in electronics and performance
materials . Several catalog products are also available for various applications on
an MTO basis .

Laboratories
R&D
QC & QA
 OBJECTIVES
The objectives of this internship is to study and looking to gain relevant skills and
experience in a inventys research field. Also we want to study various unit
operation & unit process.
➢ Internships are generally thought of to be reserved for college students
looking to gain experience in a particular field. However, a wide array of
people can benefit from Training Internships in order to receive real world
experience and develop their skills.
➢ An objective for this position should emphasize the skills you already
possess in the area and your interest in learning more
➢ Internships are utilized in a number of different career fields, including
architecture, engineering, healthcare, economics, advertising and many
more.
➢ Utilizing internships is a great way to build your resume and develop skills
that can be emphasized in your resume for future jobs. When you are
applying for a Training Internship, make sure to highlight any special skills
or talents that can make you stand apart from the rest of the applicants so
that you have an improved chance of landing the position.
 Brief literature survey

Inventys was founded in 2005. Today, Inventys has the capability (expertise and
capacities) of conducting a broad range of chemical reactions at a commercial scale
including Cyanation, Hydrogenation, Halogenation, Sulfonation, Hydroxylation from kg
to multi tons scale. On site Inventys infrastructure allows it to handle critical materials
like Sodium Cyanide, Hydrazine Hydrate, liquid ammonia, various Alkylating agents,
Oleum/Chlorosulphonic Acid, Hydrogen on site.

Inventys is an established reliable responsible member of global chemical supply

chains. Inventys manufactures high quality chemicals for its customers across the globe.
These commitment to top class enables Inventys to generate the predominant turnover
of the CSM business with leading Multinationals in their segments having revenues of
more than $1 billion/yr.

Inventys has more than 300 employees. The manufacturing facilities are
based on 15 automated production sections – consisting of over 90 reactors,
numerous isolation, drying and recycling equipment. The extensive utilities match
with this production setup. Inventys facilities are completely automated with
advanced automation techniques applied to ensure quality and safety at highest
standards.

Spectacular growth at Inventys has been made possible solely by Inventys

commitment to state-of-the-art Manufacturing facilities, and excellence in
Process Engineering Design, and its commitment to innovative Process Chemistry.
EQUIPMENTS:

A)reactor:

1) Glass lined reactor:

2) Stainless steel reactor

3) Autoclave glass lined reactor

B) Condenser

C) Heat exchanger

1. Plate type heat exchanger

2. Shell and tube heat exchanger

D)HCN generator

E)falling film evaporator

F)centrifuge

G)lipquid vapour separator

H)dryer

1. Vacuum tray dryer

2. Fluidised bed dryer

3. Rotary cone vacuum dryer

I)distillation column

J)automatic valve

K)pumps
 1. Centrifugal pump

2. Reciprocating pump

L)agitator

M) scrubber

UTILITIES:
Any Chemical Plant requires raw materials in order to produce final
products. It also requires various other services called Utilities for smoothly
carrying out the processes. Utility is neither a reactant nor a product, But Utilities
are required for maintaining adequate conditions of a manufacturing unit. Utility
area is an important area of a Chemical Plant. This may house various Boilers,
Large Compressors, Refrigeration systems, Air Conditioning systems, Water
Treatment Plants, Cooling Towers etc. Utilities are situated outside plant limits
should not give any wrong impression that utilities are any less important than
the main process, because it is the Efficient Management of Utilities that generate
Profits. The utilities help to maintain proper process conditions like pressure,
temperature etc., without which it will be impossible to carry out the process.
Now a days most of the Engineering practices are aimed at reducing the
consumption of utilities, because the production of utilities whether it is
compressed air, steam etc., requires energy and energy is becoming costlier day
by day. Efficient Utility Management doesn't end at cost cutting, if utilities supply
is not proper the equipment may not last their full life. For example, if Steam at
higher temperature than desired enters Heat Exchangers, the Exchangers may get
damaged. Air, water, steam, refrigeration, fuel, furnace, insulation etc
Following are some main and basic utility used in Chemical industry.
➢ Electricity
➢ Scrubber
➢ Nitrogen
 ➢ Vacuum
➢ Steam
➢ Hot water
➢ Thf
➢ Air
➢ cooling
➢ Chilling water
➢ Chilling brine
➢ Fuel
➢ refrigeration

Research and development:

(R&D) includes activities that companies undertake to innovate and
introduce new products and services. It is often the first stage in the
development process. The goal is typically to take new products and services to
market and add to the company's bottom line.

➢ Key takeaways:

• R&D represents the activities companies undertake to innovate and

introduce new products and services or to improve their existing offerings.
• R&D allows a company to stay ahead of its competition by catering to new
wants or needs in the market.
• Companies in different sectors and industries conduct R&D—
pharmaceuticals, semiconductors, and technology companies generally
spend the most.
• R&D is often a broad approach to exploratory advancement, while applied
research is more geared towards researching a more narrow scope.
• The accounting for treatment for R&D costs can materially impact a
company's income statement and balance sheet.
 ➢ Important R & D:
Given the rapid rate of technological advancement, R&D is important for
companies to stay competitive. Specifically, R&D allows companies to
create products that are difficult for their competitors to replicate.
Meanwhile, R&D efforts can lead to improved productivity that helps
increase margins, further creating an edge in outpacing competitors. From
a broader perspective, R&D can allow a company to stay ahead of the
curve, anticipating customer demands or trends.

Quality control:

Quality Control (QC) may be defined as a system that is used to maintain a

desired level of quality in a product or service. It is a systematic control of various
factors that affect the quality of the product. It depends on materials, tools,
machines, type of labour, working conditions etc. QC is a broad term, it involves
inspection at particular stage but mere inspection does not mean QC. As opposed
to inspection, in quality control activity emphasis is placed on the quality future
production. Quality control aims at prevention of defects at the source, relies on
effective feedback system and corrective action procedure. Quality control uses
inspection as a valuable tool. According to Juran “Quality control is the regulatory
process through which we measure actual quality performance, compare it with
standards, and act on the difference”. Another definition of quality control is from
ANSI/ASQC standard (1978) quality control is defined as “The operational
techniques and the activities which sustain a quality of product or service that will
satisfy given needs; also the use of such techniques and activities”. Alford and
Beatty define QC as “In the broad sense, quality control is the mechanism by
which products are made to measure up to specifications determined from
customers, demands and transformed into sales engineering and manufacturing
requirements, it is concerned with making things right rather than discovering
and rejecting those made wrong”.
Control:
The process through which the standards are established and met with
standards is called control. This process consists of observing our activity
performance, comparing the performance with some standard and then taking
action if the observed performance is significantly too different from the
standards.
The control process involves a universal sequence of steps as follows:
1. Choose the control object
2. Choose a unit of measure
3. Set the standard value
4. Choose a sensing device which can measure
5. Measure actual performance
6. Interpret the difference between actual and standard
7. Taking action.

Objectives of Quality Control

Following are the objectives of quality control:
1. To improve the companies income by making the production more acceptable
to the customers, i.e., by providing long life, greater usefulness, maintainability
etc.
2. To reduce companies cost through reduction of losses due to defects.
3. To achieve interchangeability of manufacture in large scale production.
4. To produce optimal quality at reduced price.
5. To ensure satisfaction of customers with productions or services or high quality
level, to build customer goodwill, confidence and reputation of manufacturer.
6. To make inspection prompt to ensure quality control.
7. To check the variation during manufacturing. The broad areas of application of
quality control are incoming material control, process control and product
control.

Quality assurance:
Quality Assurance (QA) is a management method that is defined as “all those
planned and systematic actions needed to provide adequate confidence that a
product, service or result will satisfy given requirements for quality and be fit for
use”. A Quality Assurance programme is defined as “the sum total of the activities
aimed at achieving that required standard ” (ISO, 1994). Any monitoring
programme or assessment must aim to produce information that is accurate,
reliable and adequate for the intended purpose. This means that a clear idea of
the type and specifications of the information sought must be known before the
project starts, i.e. there must be a data quality objective. Data quality objectives
are qualitative and quantitative specifications that are used to design the system
that will limit the uncertainty to an acceptable level within the constraints
allowed. These objectives are often set by the end users of the data (usually those
funding the project) in conjunction with the technical experts concerned. Quality
Assurance for a recreational water monitoring programme will, apart from
helping to ensure that the results obtained are correct, increase the confidence of
funding bodies.
Environmental health and safety ( EHS ):
Purpose:
To define the responsibility of the company for Environment Health and Safety.
Scope :
This Policy applies to all Employees, Visitors, Venders, Customers and Contractors
etc. in Environment.

EHS Objective :
i. Establish and maintain an EHS management system that facilitates
a structured approach to the management of EHS risk.
ii. Provide adequate human, financial and time resources to ensure
the effectiveness and sustainability of the system.
iii. Keep up-to-date with relevant health and safety legislative
obligations. Achieve and maintain compliance with these
obligations.
iv. Promote a safety culture that encourages people to proactively
manage Environment health and safety risk through education,
instruction, information and supervision.
v. Clearly define and communicate Employees, Visitors, Vendors,
Customers and Contractors responsibilities in relation to
Environment health and safety.
vi. Proactively identify and manage health and safety risk via a
documented hazard identification, risk assessment, risk control
and monitoring process.
vii. Improve processes that ensure that incidents and hazards are
promptly reported, investigated where appropriate, and control
measures are put in place to eliminate or minimize the chance of a
repeat event. viii. Routinely monitor and review EHS performance
to achieve continual improvement.
HAZARD SYMBOL:

PERSONAL PROTECTIVE EQUIPMENT (PPE):

PPE selection should be based on a job hazard analysis (JHA), which includes evaluation of hazards,
specific tasks, procedures and work practices, in consultation with area supervision and EH&S as
needed. See the EH&S Job Hazard Analysis webpage for more information and link to a template JHA.
This PPE selection guidance is not intended to be a comprehensive resource on PPE.

1. Eye and Face Protection

Thousands of people are blinded each year from work-related eye injuries that could have
been prevented with the proper selection and use of eye and face protection.

2. Head Protection
3. Hand Protection

DISPOSAL GLOVE

WIRE MESS GLOVES

4. Foot Protection

5. Skin and Body Protection

APRON

6. Hearing Protection

7. Respiratory Protection

N95 RESPIRATOR.
 CARTRIDGE RESPIRATOR

SCBA

FIRE:
Fire is a chemical reaction in which a combustible material combines with oxygen
in the atmosphere to give out heat and flame. There are three components which
are necessary to cause a fire. Fuel (Combustible material) Oxygen (Combustion
support) Ignition source or heat (Combustion initiator) If any one of these is
absent, fire cannot take place. It can be represented by a triangle known as
triangle of combustion.
FIRE EXTINGUISER :
 METHODOLOGY

➢ DISTILLATION COLUMN:

A distillation column is an essential item used in the distillation of liquid

mixtures to separate the mixture into its component parts, or fractions,
based on the differences in volatilities. Fractionating columns are used in
small scale laboratory distillations as well as large scale industrial
distillations.
A typical distillation contains several major components.

• a vertical shell where the separation of liquid components is carried out

• column internals such as trays/plates and/or packings which are used to
enhance component separations
• a reboiler to provide the necessary vaporisation for the distillation process
• a condenser to cool and condense the vapour leaving the top of the column
• a reflux drum to hold the condensed vapour from the top of the column so
that liquid (reflux) can be recycled back to the column
 GLASSED LINE REACTOR:

A reactor works by allowing the chemicals into a contained space and

agitating them via the centrally mounted agitator. The vessel will typically
have baffles included to ensure the sufficient level of turbulence inside to
mix / blend the chemicals and enable the reactor. Normal chemical
reactions take place given the correct catalysts present, the chemicals and
pressure / temperature conditions and contact time. The end product could
be crystalline or liquid.
Glass Lined Reactors consist of a main body, top section with connecting
nozzles & man way, baffles, dip pipes, agitator with mechanical seal, tank
outlet valve and jacket for thermal transfer. Smaller components such as
bursting discs and sight glasses are also used frequently for pressure relief
and visibility.

AUTOCLAVE:
Autoclave : The autoclave works on the principle of moist heat sterilization where
steam under pressure is used to sterilize the material present inside the chamber
. The high pressure increases the boiling point of water and thus helps achieve a
higher temperature for sterilization .
Parts of Reactor :
a ) Manhole
b ) Sight Glass
c ) Vapour Column
d ) Agitator
e ) Thermic Fluid
f ) Safety Valve
g ) Storage Tank
h ) Tank Outlet
i ) Several Inlets
j ) Jacket
k ) Resistance Temperature Detector ( RTD )

HEAT EXCHANGER:

A heat exchanger is a system used to transfer heat

between a source and a working fluid. Heat exchangers are used in
both cooling and heating
processes.https://en.wikipedia.org/wiki/Heat_exchanger - cite_note-1 The fluids may
be separated by a solid wall to prevent mixing or they may be in
direct contact. The classic example of a heat exchanger is found in
an internal combustion engine in which a circulating fluid known
as engine coolant flows through radiator coils and air flows past the
coils, which cools the coolant and heats the incoming air. Another
example is the heat sink, which is a passive heat exchanger that
transfers the heat generated by an electronic or a mechanical device
to a fluid medium, often air or a liquid coolant.

a) Plate and frame heat exchanger

b) Shell and tube heat exchanger

SCRUBBER:
Scrubbers are air pollution control devices that use liquid to
remove particulate matter or gases from an industrial exhaust or
flue gas stream. This atomized liquid (typically water) entrains
particles and pollutant gases in order to effectively wash them out of
the gas flow.

CENTRIFUGE:

The centrifugal separator features an inlet, outlet, and separator. The

liquid-solid, solid-liquid, or gas-solid mixture is pumped into a cone-shaped
working apparatus in the separator. The separator produces a spinning
vortex, which leads to the filtration of solids from liquids. The separated
solids are collected at the bottom of the separator, and they are purged
from there. High-density liquid flows out of the separator, along with the
contaminant, and low-density component will remain inside. Water is one
of the denser liquids, so it flows outside, and is removed through a
discharged outlet.
AGITATOR:
An Agitator is device or mechanism to put in
something by shaking or stirring. There are several types of agitation machines,
including washing machine agitators and magnetic agitators which contain a
magnetic bar rotating in a magnetic field. Agitators can come in many sizes and
varieties, depending on the application.
In general, agitators usually consist of an impeller and a shaft. An impeller is a
rotor located within a tube or conduit attached to the shaft. It helps enhance the
pressure in order for the flow of a fluid be done. Modern industrial agitators
incorporate process control to maintain better control over the mixing process.
Paddle Agitators:
Paddle agitators consist of two flat paddle-shaped impeller blades extending to
reach the tank walls. They are used if no extensive axial and radial flow is
required. These impellers can produce a laminar low shear flow and are used for
low viscosity liquid mixing, crystallization, dissolution, and heat transfer. They are
typically operated at low speeds and predominantly give a tangential flow
pattern. Secondary blades can be installed on the paddle blades to enhance the
mixing of more viscous materials.

Anchor Agitators:
Anchor agitators have impellers that resemble the shape of an anchor. They
typically have a U-shape that matches the contour of the tank. They generate a
predominantly tangential flow pattern, but angled blades can be incorporated on
their horizontal supports to create an axial flow.

Anchor agitators are used for blending and heat transfer of highly viscous liquids.
Their impellers generate a laminar low-shear flow; hence, they are used to mix
shear-sensitive media. Anchor agitators are considered the most economical
laminar flow agitator. They are suitable for tanks with rounded or conical
bottoms. The impeller can be designed to have a low clearance with the tank wall.

REDUCER:
A reducer is a component in a piping system that changes the pipe
size from a larger to a smaller bore. A reducer allows for a change in pipe
size to meet flow requirements or to adapt to existing piping. The length of
the reduction is usually equal to the average of the larger and smaller pipe
diameters.
 CONCLUSION

In this intership we are studied different equipment’s, process and

operations. Also we are learning about the environment health and safety. In this
industry we Utilizing internships is a great way to build our resume and develop
skills that can be emphasized ours resume for future jobs.