Metal Packing Liquid Distributors
Metal Packing Liquid Distributors
Metal Packing Liquid Distributors
Liquid Distribution Liquid distributors are used in packed columns above each bed of packing. The distributor, depending upon its design features, is elevated between 0 to 8 in. [0-200mm] above the packing. The space is determined by the distributor type and the vertical height required to disengage the vapor phase from the packing before it flows through the distributor gas passage area. An ideal distributor possesses the following attributes, each having a specific effect on the overall performance of the packed tower: Uniform liquid distribution Proper operation through its turn-down range Low vapor phase pressure drop Resistance to plugging or fouling Optimal use of vessel height for proper performance Minimal liquid residence time Mixing capability for redistribution to the next bed The introduction of high performance tower packings in the 1970s and 1980s accentuated the design deficiencies of distributors available at the time. In response, Koch-Glitsch introduced distributors with features to correct these deficiencies. These important features are well understood by Koch-Glitsch and have been incorporated in the family of INTALOX high performance distributors. Koch-Glitsch offers two categories of liquid distributors to meet the requirements of specific applications. In determining which category to choose, it is necessary to know the sensitivity of the process and whether the liquid distribution will significantly affect the overall tower performance. As a general rule: Koch-Glitsch INTALOX high performance distributors are used typically with FLEXIPAC, FLEXIPAC HC, INTALOX and wire gauze structured packings or IMTP, SNOWFLAKE, CMR and -ETA RING high performance random packings in the following services: distillation, processes approaching equilibrium or heat-transfer applications with close approach temperature. Koch-Glitsch traditional distributors are generally used with traditional packings (FLEXIRING and HY-PAK Random Packings, plastic Super INTALOX Saddles, FLEXIGRID and GLITSCH GRID Structured Packings) in general absorption, stripping and heat transfer applications. Traditional distributors take advantage of standardized, pre-engineered design and the optimal use of raw materials. These distributors do not generally provide liquid flow uniformity comparable to INTALOX high performance distributors. As always, there are exceptions to the general rules. Occasionally High performance packing may be used with traditional distributors in cases when only certain aspects of a high performance packing are desired. An example would be to take advantage of the high capacity of IMTP packing or the low pressure drop of FLEXIPAC HC structured packing, when the separation efficiency demands are not high. Traditional packing may be used with high performance distributors in cases when a process is licensed and specified with a certain type of packing. Redistribution The decision of when to install more than one packed bed and redistribute the liquid is somewhat more involved.There are six major reasons to split a packed bed and redistribute the liquid: Feed introduction Product side draw High theoretical stage count Desire to cross-mix the liquid Liquid maldistribution Physical weight of the packed bed
Introduction of a liquid or vapor feed to a column requires a space in the packing and redistribution of the liquid phase. Important factors to keep in mind with the introduction of a liquid feed are the temperature and composition of the feed stream compared to the internal column liquid. Normally, unless the feed rate is small compared to the flow rate of the internal column liquid, it is desirable to mix the feed with the internal liquid to provide compositional uniformity before distributing it to the packed bed below. It is also advisable to mix the feed stream and internal liquid when their temperatures are significantly different. The degree of the thoroughness of the mixing depends upon the magnitude of the differences and to what extent the gradients are expected to affect the overall performance. Liquid cross-mixing and maldistribution correction often go hand-in-hand. When a packed column is designed with a large number of theoretical stages or transfer units, a constant liquid to vapor ratio (L/V) is needed to achieve the best overall column performance. Redistribution of the liquid ensures that the L/V ratio is maintained, while cross-mixing between beds ensures uniform composition. Based on Koch-Glitschs operating experience, a rule-of-thumb is to limit a single packed bed to no more than 20 theoretical stages or transfer units. Consult a Koch-Glitsch technical representative for further details. Note that in some special circumstances, Koch-Glitsch applies more restrictive rules than those discussed above.
The effect liquid distribution quality on tower The Effectofof LiquidbyDistribution Quality performance is shown these actual results: 20 20 18 Actual Actual stages per bed Packing Stages Per Bed of 16 14 12 10 8 6 4 2 0 0 10 20 30 40 50 60 70 80 90 100
Distribution Quality (%) Distribution Quality (%) Stages per Bed with HETP System Base System Base HETP
20
16
16
12
12
8 8
0 30
50
100
150
200 700
25
600
HETP, inches
500 400
15
INTALOX Structured Packing 1T
300 200
10
5 100 0 0 5 10
Drip Points/ft2
0 15 20
HETP, mm
20
Operating Range
A distributor will give its best performance at and around 100% of the design liquid flow rate. As the rate decreases and the liquid head drops, levelness of the distributor as well as gradients in liquid level become a larger percentage of the operating liquid head. At some turndown rate, the flow variation from point-topoint will fall outside of acceptable limits. INTALOX distributors are designed to have a maximum flow variation, defined as the coefficient of variation (Cv), equal to no more than 3% at design rates and no more than 5% at turndown rates. Special designs are available for many INTALOX high performance distributors that will result in even lower flow variation. Typical turndown ranges are given in the description for the various distributor models.
Orifice Size
In gravity-fed distributors, the orifice size is dependent upon the drip point density, the specific liquid rate and the height of the liquid. For a single level orifice, with an operating range of 60 to 120% of the design flow, the approximate orifice size is indicated in the graph below.
150 30
1.00
0.75
20
0.00
] ts/m poin 2 60 ft [ 2] ints/ po ts/m 5.5 poin 2 [85 ts/ft 2 poin 8 /m ] oints p 2 130 s/ft [ point 12
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Liquid Distributors
Depending on the flow rates, column configuration and general mechanical preferences, there are several ways to achieve good liquid distribution. Deck Type Distributors Deck style distributors are clamped on an annular ring that is seal welded to the tower wall. For revamp applications of trayed columns, most often an existing tray ring is utilized and seal welded segments are added as needed. In the case where welding is not permitted, bolt-in segments are available by special request but provide a less reliable liquid seal. Leakage from and around bolt-in support ring segments can be a significant portion of the total liquid flow, resulting in poor distribution quality. In this case, a trough or channel type distributor should be considered. Channel Type Distributors The center channel is designed as a structural member allowing the distributors to rest on a support ring and span columns up to 20 ft [6 m] without the need for additional beams. Locating the distributor on existing support ring in revamp work often makes it easy to determine the tower layout. Supporting a channel type distributor on an annular ring generally requires a more complex design and construction in order to provide drip points at the proper proximity to the tower wall. This increased complexity can be avoided by supporting channel type distributor with the center channel resting on a seat and the channel troughs hung from beams or a ring above. Both beam and ring supported channel distributors can be designed to accommodate uplift conditions.The center channel of a channel type distributor provides cross flow capacity between troughs, to enable liquid head equalization. The addition of covers or hats over the gas riser area provides the ability to turn the device into a redistributor for use between packed beds. This design is especially useful when tower elevation is tight and minimal height for redistribution is required. Trough Type Distributors Trough type distributors are usually hung from beams. When used in conjunction with structured packings, in special circumstances, the trough distributor may be supported from an integral support system resting directly on the packing. Trough type distributors are easily installed and leveled, do not require gaskets and have no annular ring below to interfere with the distribution pattern. Each trough is fed a metered amount of liquid from one or more parting boxes. Because there is no flow communication between troughs, the performance of the parting box is critical. Koch-Glitschs years of experience ensure parting box designs for proper flow metering. When used between packed beds for redistribution, a trough type distributor requires the use of a collector to catch the liquid from the bed above. The use of a separate collector provides complete cross mixing of the liquid before redistribution and also allows mixing of feed streams with the internal column liquid. A separate collector requires more column height than a channel type redistributor.
Construction Details
Standard connection to the tower wall is by bolting to clips. As an option, the distributor can be suspended from clips or a ring trapped between body flanges. Setting the distributor on an annular ring is not recommended. All joints in multi-piece pans are gasketed. The standard design for a Model 107 redistributor includes gas riser covers and a weld-on wall wiper.
Design Options
Orifice strainers Expandable and gasketed wall wiper (Model 107) Suspended mounting Raised tube metering for high turndown or fouling concern Anti-migration bars
Construction Details
The Model 116/117 distributor is clamped onto an annular ring that is seal-welded to the tower wall, with clamps provided. Hence, distributor levelness is determined by the ring levelness. Design of the Model 116/117 distributor takes into account support ring levelness tolerances within ASME code or as otherwise specified. All joints are gasketed. For redistribution between beds, a separate liquid collector is not required. The standard design for a Model 117 redistributor includes gas riser covers to collect liquid.
Model 126 INTALOX Channel Distributor with Bottom Orifices ( Model 127 Redistributor)
Diameters greater than 36 in. [900 mm] Liquid rates between 2 - 16 gpm/ft2 [5 - 40 m3/m2 h] Orifices in channel base Limited fouling resistance Structural center channel provides flow equalization Orifices in the base of the channels are positioned to optimize distribution quality. Vapor passage is provided by the space between the channels. Rates lower than 2 gpm/ft2 [5 m3/m2 h] can be accommodated but a Model 136 sidewall orifice distributor should be considered first. For systems with liquid rates in excess of 12 gpm/ft2 [30 m3/m2 h] a Model 116 deck style distributor should be considered. The channel-type construction allows easy liquid sealing and distributor leveling, which is essential in large diameter towers. Because this distributor normally handles intermediate liquid flow rates, the orifices are usually large enough to allow low to moderate fouling resistance. The standard turndown range is 2 : 1.
Construction Details
The Model 126/127 distributor rests on an annular ring or is suspended from a ring or beams. All joints are gasketed. The standard design for a Model 127 redistributor includes a weld-on wall wiper and bolted gas riser covers, used to collect and redistribute liquid. The redistributor design uses less column height than a separate collector/distributor layout and is valuable where space is limited and total cross mixing of liquid between beds is not critical.
Design Options
Model 127 cross-mixing capability (extent is dependent on diameter and rate) Orifice strainers Leveling screws Expandable and gasketed wall wiper (small diameter Model 127)
Model 136 INTALOX Channel Distributor with Drip Tubes (Model 137 Redistributor)
Diameters greater than 10 in. [250 mm] Liquid rates between 0.3 - 12 gpm/ft2 [0.75 - 30 m3/m2 h] Structural center channel provides flow equalization Liquid overflow protection Side-wall orifices Fouling resistant Orifices in the sidewalls of the channels are positioned to optimize distribution quality. Vapor passage is provided by the space between the troughs. The fouling resistance of this distributor is higher than that of deck-type distributors because it features a debris collection zone below the sidewall orifices. The center channel of the distributor provides structural support as well as equalization of liquid between troughs. The liquid from each drip point is conducted into the lower vapor velocity region below the distributor troughs. This results in low entrainment levels. In addition, overflow holes are provided at each conductor tube to ensure that if the maximum flow range of the distributor is exceeded, the liquid will be conducted to the packing in a controlled manner rather than to randomly spill over the troughs. The standard turndown for a single sidewall orifice is 2 : 1. Using multiple orifices at two or more levels of the same discharge conductor can extend the turndown range. Turndown ratios up to 10 : 1 are achievable. The flow variation will be higher throughout all or part of the operating range with multi-level orifices.
Construction Details
The Model 136/137 distributor are usually constructed as pans for diameters below 30 in. [750 mm] and as channels for diameters above 30 in. [750 mm]. The Model 136/137 distributor rests on an annular ring or is suspended from beams or clips. All joints are gasketed. The standard design for the Model 137 redistributor includes a weld-on wall wiper and bolted gas riser covers to collect and redistribute liquid. The redistributor design uses less column height than a separate collector/distributor layout and is valuable where space is limited and total cross mixing of liquid between beds is not critical.
Design Options
Cross-mixing capability (extent is dependent on diameter and rate) Orifice strainers Leveling screws Multi-level orifices Expandable and gasketed wall wiper (small diameter Model 137) Removable drip tubes
Construction Details
As the standard, the Model 141 distributor is supported and leveled from an integral distributor support grid (Model 883). For redistribution between packed beds, a separate liquid collector is required. The use of a separate liquid collector provides total cross mixing of the liquid between beds.
Design Options
Turndown ratio greater than 2 : 1 Non-standard mounting arrangements Diameters exceeding standard range
Construction Details
The Model 156 is suspended from beams. The troughs are continuous across the column diameter and are fed with one or more parting boxes. Details of baffle arrangement are variable depending upon specific liquid rates and are determined at the time of design. There are no joints to seal, therefore, no gaskets are required for this distributor. For redistribution between packed beds, a separate liquid collector is required. The use of a separate liquid collector provides total cross mixing of the liquid between beds.
Design Options
Mount on packing with the Model 883 bed limiter/support Metering boxes
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Construction Details
As the standard, the Model 186 distributor is suspended from beams. By special request, and within a limited range of diameters, provisions can be made for the distributor to rest on an existing support ring. Model 186 troughs are continuous across the column diameter and are fed with one or more parting boxes. There are no joints to seal, therefore, no gaskets are required. For redistribution between packed beds, a separate liquid collector is required. The use of a separate liquid collector provides total cross mixing of the liquid between beds.
Design Options
Orifice strainers Multi-level orifices Metering Boxes Mounted on support ring or supported by Model 883 bed limiter/support
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Construction Details
This distributor is supported either by a full support ring or by lugs. Gasketed joints are standard for multi-piece pans when liquid rates are below 4 gpm/ft2 [10 m3/m2 h].
Design Options
One-piece construction for body flanged columns
Construction Details
This distributor is supported either by a full support ring or by lugs. Gasketed joints are standard for multi-piece pans when liquid rates are below 4 gpm/ft2 [10 m3/m2 h]. This device is not available in a design suitable for use as a redistributor.
Design Options
One-piece construction for body flanged columns Gasketing for liquid rates above 4 gpm/ft2 Raised tube metering for high turndown or fouling concern Anti-migration bars
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Model 916 Deck Distributor with Bottom Orifices (Model 917 Redistributor)
Diameters greater than 12 in. [300 mm] Liquid rates between 1 - 50 gpm/ft2 [2.5 - 120 m3/m2 h] Orifices in deck The deck-type construction gives liquid level balance around the periphery of the distributor and additionally across the mid-span beam in large diameter columns. Vapor passage is provided through long, rectangular gas risers. At lower liquid rates, as distribution orifice diameters get smaller, this distributor provides minimal fouling resistance. If fouling resistance is important a trough type distributor with sidewall orifices should be considered. The maximum turndown range is determined by the size of the manway access. The standard turndown range is 2.5 : 1.
Construction Details
The distributor rests on an annular ring and is secured with tray clamps. For redistribution between beds, a separate liquid collector is not needed. The standard design for a Model 917 redistributor includes gas riser covers to collect liquid. Distributors in services with liquid rates below 4 gpm/ft2 [10 m3/m2 h] are gasketed as standard.
Design Options
Gasketing for liquid rates above 4 gpm/ft2 Parting box
Model 926 Channel Distributor with Bottom Orifices (Model 927 Redistributor)
Diameters greater than 36 in. [900 mm] Liquid rates between 1 - 20 gpm/ft2 [2.5 - 50 m3/m2 h] Orifices in base Limited fouling resistance Structural center channel provides flow equalization The Model 926 distributor is a channel type distributor providing good cross flow and liquid handling capacity with low leakage compared to a deck style (Model 916) distributor. The structural center sump allows this distributor to be used in large diameter columns, up to 26 ft [8 m], without the need for additional support beams. The standard turndown range is 1.8 : 1.
Construction Details
The Model 926/927 distributor rests on an annular ring. Gasketed joints are standard for liquid rates below 4 gpm/ft2 [10 m3/m2 h]. The Model 927 redistributor includes gas riser area covers to collect liquid as well as a wall wiper to be welded to the column wall.
Design Options
Cross mixing (Model 927) Clamped to support ring for uplift resistances Leveling screws
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Construction Details
As the standard, the Model 976 distributor is suspended from beams. Within a limited range of diameters, provisions can be made for the distributor to rest on an existing support ring. For redistribution between packed beds, a separate liquid collector is required. The use of a separate liquid collector provides cross mixing of liquid between beds. There are no joints to seal for this distributor, therefore, no gaskets are required.
Design Options
Orifice strainers Mount on support ring
Construction Details
The Model 985 distributor rests on a full annular ring. For redistribution between packed beds, a separate liquid collector is required.
Design Options
Clamped to support ring Uplift resistant Distribution notch shape Guide channels
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Construction Details
As the standard, the Model 986 distributor is suspended from beams. Upon special request, and within a limited range of diameters, provisions can be made for the distributor to rest on an existing support ring. For redistribution between packed beds, a separate liquid collector is required. The use of a separate liquid collector provides total cross mixing of the liquid between beds.
Design Options
Orifice strainers High turndown ratio Metering boxes Mount on support ring or supported by Model 883 bed limiter/support
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Construction Details
The header section is flanged for standard horizontal feed from the side of the tower. Inlet flange mates to a 150 psi [PN 10] flange. The end of the header opposite the flange connection as well as the lateral ends are supported by clips as required. Laterals attach to the main header with flanged connections as standard. When an external column feed is not present and for using this device as a redistributor, a total draw-off liquid collector with an external pump loop is required.
Design Options
Threaded header and laterals (4" [100 mm] and under) Vertical-feed header, on tower centerline Bayonet-style construction for small towers
Construction Details
The header section is flanged for standard horizontal feed from the side of the tower. The flange mates to a 150 psi [PN 10] flange. Laterals attached to the main header with flanged connections are standard. For small diameter columns, the ends of the header and laterals are supported by clips as required. For larger diameter columns, laterals are attached to beams.
Design Options
Maximum free passage nozzles for fouling services Special piping design for fouling service
Full cone spray nozzles with an angle of 90 or 120 are the standard design for most applications. Spray nozzles providing maximum free passage
and special distributor configurations to prevent liquid stagnation are typically recommended for refining column wash beds or other applications where complete wetting is critical to avoid fouling. Turndown ratio is limited to 2 : 1 by the range of effective operation of the spray nozzles.
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Construction Details
This distributor is hung from beams and is securely attached to withstand the rigors of column motion. When located at the top of the column with a reflux stream, the reflux pump pressure is used to provide liquid head. For use as a redistributor, a separate Model 613 liquid collector, (specifically designed for motion column service), is used in conjunction with the Model 961 distributor to provide the necessary liquid head. The column height requirement is dependent upon turndown range and motion dynamics.
Design Options
Dependent on column configuration and requirement.
Testing of Model 961 enclosed channel distributor in the Koch-Glitsch test facility simulating wave motion.
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