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    حسن كنزي
    This document describes an experiment to determine the concentrations of Ca2+ and Mg2+ ions in bottled mineral water through titration with EDTA. The titration reaction involves Ca2+ or Mg2+ ions binding to the EDTA ligand. The endpoint is indicated by a color change from wine red to blue. The document provides procedures for titrating a water sample against a standard HCl solution and calculating the hardness in terms of CaCO3 concentration. Experimental results found 400 mg/L hardness for tap water and 40 mg/L for RO water.

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    تقرير

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    حسن كنزي
    42 views8 pages
    This document describes an experiment to determine the concentrations of Ca2+ and Mg2+ ions in bottled mineral water through titration with EDTA. The titration reaction involves Ca2+ or Mg2+ ions binding to the EDTA ligand. The endpoint is indicated by a color change from wine red to blue. The document provides procedures for titrating a water sample against a standard HCl solution and calculating the hardness in terms of CaCO3 concentration. Experimental results found 400 mg/L hardness for tap water and 40 mg/L for RO water.

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    This document describes an experiment to determine the concentrations of Ca2+ and Mg2+ ions in bottled mineral water through titration with EDTA. The titration reaction involves Ca2+ or Mg2+ ions binding to the EDTA ligand. The endpoint is indicated by a color change from wine red to blue. The document provides procedures for titrating a water sample against a standard HCl solution and calculating the hardness in terms of CaCO3 concentration. Experimental results found 400 mg/L hardness for tap water and 40 mg/L for RO water.

    Copyright:

    © All Rights Reserved
    Download as PDF, TXT or read online from Scribd
    Download as pdf or txt
    42 views8 pages

    تقرير

    Uploaded by

    حسن كنزي
    This document describes an experiment to determine the concentrations of Ca2+ and Mg2+ ions in bottled mineral water through titration with EDTA. The titration reaction involves Ca2+ or Mg2+ ions binding to the EDTA ligand. The endpoint is indicated by a color change from wine red to blue. The document provides procedures for titrating a water sample against a standard HCl solution and calculating the hardness in terms of CaCO3 concentration. Experimental results found 400 mg/L hardness for tap water and 40 mg/L for RO water.

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    of 8

    #7 HARDNESS OF WATER

    *Objectives
    1. To determine the concentrations of Ca2+ (aq) and Mg2+(aq) ions in a commercial sample of
    bottled mineral water.
    2. To compare experimental results with the concentrations of the metal ions claimed by the
    manufacturer.

    *Theory

    The ions involved in water hardness, i.e. Ca2+(aq) and Mg2+(aq), can be determined by titration
    with a chelating agent, ethylene-diamine-tetra-acetic acid (EDTA), usually in the form of
    disodium salt (H2Y2-). The titration reaction is

    Ca+2{aq}+ H2Y2- Ca2-{aq}+2H+{aq}

    HOOC COOH
    N___CH2 ___ CH2__N
    -OOC COO-

    As the stronger ligand EDTA is added, the CaIn+ (aq) complex is replaced by the CaY-(aq)
    complex, which is blue. The endpoint of titration is indicated by a sharp color change from wine
    red to blue.
    Rocedure
    1.Fill the burette with HCl Solution (Known concentration from previous Exp

    . 2. Take with cylinder (40 ml) of water sample and put it in a conical flask.

    3. Add 2 drops of M.O and titrate with HCl until the color change from yellow to pink.

    4. Repeat the experiment three times and record the average of volume of HCl consumed

    5. Find the CaC03 Concentration as water hardness

    * Calculations: (to TAP WATER)

    N(HCl)=0.02
    V(HCl)=4ml
    N(tap water)=?
    V(Tap water)=10ml
    V1=4ml
    V2=4ml
    V3=4ml

    VAVRG=4+4+4/3=4ml
    N (tap water).V (tap water) =N(HCI).V(HCl)
    N10=0.02x4
    10N=0.08N=0.08/10=0.008
    ppm=NxN(wt)x1000
    =0.008x50x1000
    =400mg/L

    Calculations: to(R.O WATER)


    N(HCl)=0.02N
    V(HCl)=2ml
    N(R.O)=?
    V(R.O)=50ml
    V1=2ML
    V2=2ML
    V3=2ML

    VAVRG=2+2+2/3
    =2ml

    N(R.O)xV(R.O)= N(HCl)xV(HCl)
    Nx50=0.02x2
    N=0.04/50=0.0008N
    ppm=Nxeq(wt)x1000
    =0.0008x50x1000=40mg/L

    Discussion

    1_How do we determine the concentration of iron in its ores?

    _Determination of molarity and concentration of iron in its ores or in a sample


    solution containing iron by titration with a standard solution of 0.101N potassium
    permanganate

    2_Why in this experience we use H2SO4 instead of HCL?

    _Because H2SO4 dissolves in the water and the reaction does not A repellent
    heat when it melts in the water as we use because we are in this experiment we
    need heat to increase the speed of the reaction either HCL shall reaction
    exothermic when solubility in water

    3_Why in this experiment do we add water?

    We add it for relief


    Tools and materials used:

    1-Buret

    2-spatula

    3-wash bottle

    4-erlnmeryer flask

    5-volum etric flas

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