3 Astm C110 02

NOTICE: This standard has either been superseded and replaced by a new version or discontinued.
Contact ASTM International (www.astm.org) for the latest information.
Designation: C 110 – 02
Standard Test Methods for

Physical Testing of Quicklime, Hydrated Lime, and
Limestone1
This standard is issued under the fixed designation C 110; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (e) indicates an editorial change since the last revision or reapproval.
This standard has been approved for use by agencies of the Department of Defense.
1. Scope 2. Referenced Documents

1.1 These test methods cover physical testing of quicklime 2.1 ASTM Standards:
and hydrated lime, and of limestone not otherwise covered in C 25 Test Methods for Chemical Analysis of Limestone,
ASTM standards.2 Quicklime, and Hydrated Lime3
C 28 Specification for Gypsum Plasters3
NOTE 1—Quicklime and hydrated lime have a high affinity for moisture
and carbon dioxide. Caution should be taken to protect both hydrated and C 50 Practice for Sampling, Inspection, Packing, and Mark-
quicklime during sampling, storage, and testing (see Practice C 50). ing of Lime and Limestone Products3
C 51 Terminology Relating to Lime and Limestone (as used
1.2 The test procedures appear in the following order:
by the Industry)3
Section
C 91 Specification for Masonry Cement3
C 109 Test Method for Compressive Strength of Hydraulic
iTeh Standards
Air Entrainment 13
Apparent Loose Density of Hydrated Lime, Pulverized Cement Mortars (Using 2-in. or 50-mm Cube Specimens)3
Quicklime, and Limestone 16
C 117 Test Method for Material Finer than 75–Micrometre
(https://standards.iteh.ai)
Apparent Packed Density of Hydrated Lime, Pulverized
Quicklime, and Limestone 17 (No. 200) Sieve in Mineral Aggregates by Washing4
Autoclave Expansion of Hydrated Lime 8 C 136 Test Method for Sieve Anlaysis of Fine and Coarse
Dry Brightness of Pulverized Limestone 15
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Dry Screening by Air Jet Sieve 19 Aggrgates4
Fineness of Pulverized Quicklime and Hydrated Lime by Air C 150 Specification for Portland Cement3
Permeability 18 C 185 Test Method for Air Content of Hydraulic Cement
Limestone Grindability 20
Particle Size of Pulverized Limestone 14 Mortar3
Plasticity of Lime Putty 7ASTM C110-02
C 188 Test Method for Density of Hydraulic Cement3
Popping and Pitting of Hydrated Lime 9
Residue and https://standards.iteh.ai/catalog/standards/sist/4ebe6cd0-7baa-4d9d-a31d-6a9d6ed53d90/astm-c110-02
Sieve Analysis 5
C 204 Test Method for Fineness of Hydraulic Cement by
Settling Rate of Hydrated Lime 11 Air Permeability Apparatus3
Slaking Rate of Quicklime 12 C 207 Specification for Hydrated Lime for Masonry Pur-
Specific Gravity of Hydrated Lime Products 21 poses3
Standard Consistency of Lime Putty 6
Water Retention of Hydrated Lime 10 C 230 Specification for Flow Table for Use in Tests of
Wet Sieve Analysis of Agricultural Liming Materials 22 Hydraulic Cement3
1.3 The values stated in SI units are to be regarded as the C 305 Practice for Mechanical Mixing of Hydraulic Cement
standard. Pastes and Mortars of Plastic Consistency3
1.4 This standard does not purport to address all of the C 430 Test Method for Fineness of Hydraulic Cement by
safety concerns, if any, associated with its use. It is the the 45-µm (No. 325) Sieve3
responsibility of the user of this standard to establish appro- C 472 Test Methods for Physical Testing of Gypsum, Gyp-
priate safety and health practices and determine the applica- sum Plasters and Gypsum Concrete3
bility of regulatory limitations prior to use. C 670 Practice for Preparing Precision and Bias Statements
for Test Methods for Construction Materials4
C 702 Practice for Reducing Field Samples of Aggregate to
Testing Size4
1
These test methods are under the jurisdiction of ASTM Committee C07 on C 778 Specification for Standard Sand3
Lime and are the direct responsibility of Subcommittee C07.06 on Physical Tests. C 1005 Specification for Weights and Weighing Devices for
Current edition approved June 10, 2002. Published August 2002. Originally
published as C 110 – 34 T. Last previous edition C 110 – 00a.
Use in the Physical Testing of Hydraulic Cements3
2
For tests on limestone as aggregate, see Vol 04.02 of the Annual Book of ASTM
Standards. For tests on limestone as building stone, see Vol 04.05 of the Annual 3
Annual Book of ASTM Standards, Vol 04.01.
Book of ASTM Standards. 4
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959, United States.
1
C 110
D 75 Practice for Sampling Aggregates5 5.2.5 Attach a pressure gage to the water faucet and a rubber
E 11 Specification for Wire and Cloth Sieves for Testing tubing to the output side of the pressure gage. On the other end
Purposes6 of the rubber tubing attach the spray nozzle (see 5.2.3).
E 29 Practice for Using Significant Digits in Test Data to 5.3 Residue of Quicklime:
Determine Conformance with Specifications6 5.3.1 Select a representative 2.5-kg (5-lb) sample of the
E 691 Practice for Conducting an Interlaboratory Study to quicklime. Break lime selected for this test so as to entirely
Determine the Precision of a Test Method6 pass a 25.0-mm (1-in.) square mesh screen. Test the pulverized
3. Terminology lime as received. Place the sample in a box of wood or of some
3.1 Definitions—Unless otherwise specified, for definitions material of similarly low thermal conductivity, and an experi-
of terms used in this standard see Terminology C 51. enced operator should slake it with sufficient water at 21 to
27°C (70 to 80°F) to produce the maximum quantity of lime
4. General Procedures putty, carefully avoiding “burning” or “drowning” the lime.
4.1 Sampling—Samples of lime and limestone for chemical Allow it to stand for 1 h and then wash through an 850-µm (No.
analysis shall be taken and prepared in accordance with the 20) sieve by a stream of water having a moderate pressure. Do
requirements of Practice C 50 applicable to the material to be not rub any material through the sieve. Continue the washing
tested. until the residue on the screen appears to consist entirely of
4.2 Calculation: coarse particles, but in no case continue the washing for more
4.2.1 The calculations included in the individual procedures than 30 min. Dry the residue to constant weight at a tempera-
sometimes assume that the exact weight specified has been ture of 100 to 107°C (212 to 225°F) and calculate the
used. Accurately weighed samples which are approximately percentage residue, based on the original weight of the sample.
but not exactly equal to the weight specified may be used 5.4 Sieve Analysis of Hydrated Lime:
provided appropriate corrections are made in the calculation. 5.4.1 Select a 100-g sample of the hydrated lime as received
Unless otherwise stated, weights of all samples and residues and place on a 600-µm (No. 30) sieve, which is nested above
should be recorded to the nearest 0.0001 g.
iTeh Standards
4.2.2 In all mathematical operations on a set of observed
values, the equivalent of two more places of figures than in the
a 75-µm (No. 200) sieve. Wash the material through the sieves
by means of a stream of water from the nozzle attached to a
rubber tubing (see 5.2.5) after adjusting the water pressure to
single observed values shall be retained. For example, if
observed values are read or determined to the nearest 0.1 mg,
10 psi (69 kPa) 60.25 psi (61.7 kPa). Carefully wash the
sample through the sieves without allowing any splashing over
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carry numbers to the nearest 0.001 mg in calculation. the sides of the sieve. After the sample is washed through the
4.3 Rounding Figures—Rounding of figures to the nearest top sieve, separate the two sieves and continue washing
significant place required in the report should be done after the through the 75-µm (No. 200) sieve until the water coming
calculations are completed, in order to keep the final results through the sieve is clear, that is, no particles can be seen in a
free from calculation errors. The rounding procedure should ASTMbeaker
C110-02
of the rinse water, but in no case continue the washing
follow thehttps://standards.iteh.ai/catalog/standards/sist/4ebe6cd0-7baa-4d9d-a31d-6a9d6ed53d90/astm-c110-02
principle outlined in Practice E 29. longer than 30 min. Take care not to let water accumulate on
5. Residue and Sieve Analysis the 75-µm (No. 200) sieve, because the openings will become
5.1 Significance and Use: clogged and the operation cannot be completed in 30 min.
5.1.1 This test method determines the residue obtained from 5.4.2 Calculate the percentage residue retained on each
slaking quicklime. Residue, in this case, is largely unreacted sieve, based on the original weight of the sample. The weight
material such as uncalcined limestone or dolomite, overburned of the material retained on the 600-µm (No. 30) sieve shall be
quicklime, or gross impurities, or a combination of these. added to the weight of the material retained on the 75-µm sieve
5.2 Apparatus: to obtain the correct weight of the material retained on the
5.2.1 The sieves used shall conform to the requirements of 75-µm sieve.
Specification E 11. Preferably the sieves should have a 4-in. 5.5 Sieve Analysis of Limestone and Dry Quicklime:
depth. 5.5.1 Select the desired sieves and nest them with the
5.2.2 If sieve calibrations are required, follow the method as coarsest sieves on top. Weigh a 100-g sample of the material to
outlined in Test Method C 430. be tested and place it on the top sieve. Conduct the sieving
5.2.3 Spray Nozzle conforming to the requirements of Test operation by means of a lateral and vertical motion of the sieve
Method C 430.7 accompanied by a jarring action to keep the sample moving
5.2.4 Pressure Gage shall be 3-in. (75-mm) minimum continuously over the surface of the sieve. Continue sieving
diameter, and shall be graduated in 1-psi (6.9 kPa) increments, until not more than 1 % of the residue passes any sieve during
and shall have a maximum capacity of 30-psi (207 kPa). The 1 min. If mechanical sieving is used, the device shall be such
accuracy at 10 psi (69 kPa) shall be 60.25 psi (61.7 kPa).7 as to impart the type of agitation described in the hand sieving
operation. Continue the shaking for a period of 15 min.
5
6
Annual Book of ASTM Standards, Vol 04.03. 5.5.2 Weigh the residue retained on each sieve to the nearest
7 0.1 g. Report the results of the sieve analysis as follows: (1)
A wet washing spray attachment, Soiltest Model CL-364, or equivalent has
been found suitable for this purpose. Available from Soiltest, Inc., 86 Albrecht total percentages passing each sieve, ( 2) total percentages
Drive, P.O. Box 8004, Lake Bluff, IL 60044-8004. retained on each sieve, or ( 3) percentages retained between
2
C 110
consecutive sieves, depending upon the form of the specifica- 6.2.3 Base Plate—The base plate for supporting the ring
tion for the use of the material under test. mold shall be of plate glass and about 100 mm square.
5.6 Precision and Bias: 6.2.4 Mechanical Mixers .8
5.6.1 No precision data are available due to the limited use 6.3 Standard Consistency Determination:
of these test methods. Therefore, users are advised to develop 6.3.1 Mechanical Mixing Procedure Using the Vac-U-
their own laboratory precision. No statement is being made Mixer—To a measured amount of water contained in an
about the bias of these test methods. 800-cm3 Vac-U-Mix bowl, add 300 g of hydrated lime and
hand mix for 10 s with a stiff spatula (Note 2). Cover putty to
6. Standard Consistency of Lime Putty
prevent evaporation of water. After the applicable soaking
6.1 Significance and Use: period, 30 min maximum for Type S, special hydrated lime,
6.1.1 In order to measure certain physical properties of a and not less than 16 h nor more than 24 h for Type N, normal
lime putty, such as plasticity, it is necessary to have a uniform hydrated lime, insert the paddle assembly and mix the putty for
or standard consistency (viscosity), since the property mea- 30 s with the mechanical mixer. Remove the paddle assembly
surement is affected by the consistency level. and scrape down any putty adhering to it and to the sides of the
6.2 Apparatus: mixing bowl. Remix for 30 s and determine the consistency as
6.2.1 Modified Vicat Apparatus—The apparatus, con- prescribed in 6.3. If the penetration is less than 15 mm, return
structed as shown in Fig. 1, shall consist of a bracket, A, all of the material to the mixer bowl, add additional water, and
bearing a movable brass rod, B, 6.3 mm in diameter and of remix for 15 s. If the penetration is greater than 25 mm, repeat
suitable length to fit the Vicat bracket. A plunger, C, 12.5 mm the test.
in diameter, made of aluminum tubing, shall be attached to the
lower end of the rod. The total weight of the rod with plunger NOTE 2—Most lime hydrates will require 250 to 300 mL of water to
produce a putty of proper consistency for this test if 300 g of lime are used.
shall be 30 g. The lower end of the plunger shall be closed
without shoulders or curvature and the tube may be loaded with 6.3.2 Mechanical Mixing Procedure Using the Hobart N-50
shot to the specified weight. The total weight required may also
Mixer—To a measured amount of water contained in the N-50
iTeh Standards
be obtained by means of a weight, D, screwed into the rod. The mixing bowl, add 600 g of hydrated lime and hand mix for 10
rod can be held in any position by means of a screw, E, and hass with a stiff spatula (Note 3). Cover putty to prevent
a mark midway between the ends which moves under a scale, evaporation of water. After the applicable soaking period, 30
F, graduated in millimetres, attached to the bracket, A.
6.2.2 Mold—The conical ring mold shall be made of a
min maximum for Type S, special hydrated lime, and not less
than 16 h nor more than 24 h for Type N, normal hydrated lime,
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noncorroding, nonabsorbent material, and shall have an inside
diameter of 70 mm at the base and 60 mm at the top, and a
height of 40 mm.
insert the paddle assembly and mix the putty for 1 min at a
slow speed. Stop the mixer and scrape down the paddle and the
sides of the mixing bowl. Remix for 4 min at a slow speed.
Determine the consistency as prescribed in 6.3.3. If the
ASTM C110-02
penetration is less than 15 mm, return all of the material to the
https://standards.iteh.ai/catalog/standards/sist/4ebe6cd0-7baa-4d9d-a31d-6a9d6ed53d90/astm-c110-02
mixing bowl, add additional water, and remix for 15 s. If the
penetration is more than 25 mm, repeat the test.
NOTE 3—Most lime hydrates will require 500 to 600 mL of water to
produce a putty of proper consistency for this test if 600 g of lime are used.
6.3.3 Consistency Determination—To determine consis-
tency, place the mold with its larger end resting on the glass
base plate and fill with the lime putty. Then strike off the putty
flush with the top of the mold. Center the lime putty, confined
in the ring mold resting on the plate, under the rod of the
modified Vicat apparatus (Fig. 1). Bring the plunger end, C, in
contact with the surface of the lime putty and take an initial
reading. Release the rod and take the final reading 30 s after the
plunger is released. The lime putty is of standard consistency
when a penetration of 20 6 5 mm is obtained. Record both the
total amount of water required to bring the putty to standard
consistency and the actual penetration. Proceed with the
plasticity determination in accordance with 7.3.
6.4 Precision and Bias:
6.4.1 The precision and bias of this test method has not been
determined.
8
A Vac-U-Mixer or an N-50 Hobart Mixer, or equivalent, has been found
FIG. 1 Modified Vicat Apparatus suitable for this purpose.
3
C 110
for another 2 h. Then transfer to a receptacle containing
running water for at least 1 h. The plate is then free of acid.
After the removal of excess water, place the plate in an oven
overnight at a temperature of between 100 and 110°C (212 and
230°F) for drying. Before using, cool the plate to room
temperature.
7.2.3 Absorption of Plasticimeter Base Plates:
7.2.3.1 Total Absorption—Plasticimeter base plates when
immersed in water at room temperature for a period of 24 h
shall absorb not less than 40 g of water. Before making the
determination, dry the porcelain plates overnight in an oven at
temperatures of between 100 and 110°C (212 and 230°F) and
permit to cool to room temperature. Dry the plaster plates
overnight over calcium chloride at room temperature. After
immersion and before weighing, wipe off the excess water with
a damp cloth.
7.2.3.2 Rate of Absorption (Note 4)—When tested over an
area 70 mm (23⁄4 in.) in diameter, the water absorbed shall be
in accordance with the following:
Time, min Water Absorbed, mL
1 8 to 14
2 5 to 71⁄2
Constants of the Machine: 3 4 to 61⁄2
Absorption of Porcelain Base Plate—minimum of 40 g in 24 h. For rate of 4 4 to 6
iTeh Standards
absorption of base plates see 7.2.3.2. 5 31⁄2 to 51⁄2
Dimension of Base Plate—25 mm (1 in.) in thickness by 100 mm (4 in.) in
diameter. NOTE 4—A convenient apparatus for determining the rate of absorption
Dimensions of Disk—0.8 mm (1⁄32 in.) in thickness by 76 mm (3 in.) in consists of a buret sealed onto an inverted glass funnel from which the
diameter.
Speed of Vertical Shaft—1 revolution in 6 min, 40 s.
stem has been removed. The diameter of the larger end of the funnel shall
be ground so as to be 70 mm (23⁄4 in.) in internal diameter. The funnel may
be attached to the plate on which the measurement is being made by
FIG. 2 Emley Plasticimeter Document Preview
Torque on Disk when Bob Reading is 100—1.41 N·m.
melted paraffin. The paraffin should not be too hot. A little experience will
indicate when it is of the proper consistency.
7.3 Plasticity Determination:
7. Plasticity of Lime Putty 7.3.1 Lubricate a ring mold such as is described in 6.2.2
ASTM C110-02
7.1 Significance and Use: with a thin film of water, place on a porcelain base plate (see
7.1.1 This https://standards.iteh.ai/catalog/standards/sist/4ebe6cd0-7baa-4d9d-a31d-6a9d6ed53d90/astm-c110-02
test method provides a measure of the degree of 7.2.2 and 7.2.3) or a disposable plaster base plate (see 7.2.3),
stiffening of lime putty of standard consistency as water is fill with the paste which has been adjusted to standard
withdrawn from it by a standard suction base plate. consistency as described in 6.3.3, and strike off level. Remove
7.1.2 Plasticity is an important property when applying the mold by raising it vertically without distorting the paste.
mixtures containing lime putty to porous or absorptive surfaces Center the base plate and paste in the instrument and turn the
such as in plastering, stuccoing, and masonry construction. carriage up by hand until the surface of the paste is in contact
7.2 Apparatus: with the disk and the distance between the disk and the top of
7.2.1 Determine the plasticity of lime putty using the the base plate is 32 mm (11⁄4 in.). Throw the carriage into gear
plasticimeter shown in Fig. 2.9 and start the motor. It is essential that the motor be started
7.2.2 Cleaning and Care of Base Plates— In making the exactly 120 s after the first portion of the paste has been placed
plasticity determinations, much of the success attainable de- in the mold. Record the time when the first portion of paste is
pends upon the condition of the base plates. In the case of placed in the mold as zero time; the motor is therefore started
porcelain plates which are reused, improper cleaning results in at 2 min. Take care to protect the specimen from drafts during
clogging of the pores with reduction in the rate of absorption. the test.
After a plate has been used, wipe the excess lime off and 7.3.2 Record the scale reading at 1-min intervals until the
immerse the plate in clear water for not less than 2 h, after test is completed. Consider the test complete when: ( 1) the
which transfer it without drying to a dilute solution of scale reading reaches 100, (2) any reading is less than the one
hydrochloric acid (HCl, 1 + 9) where it shall be kept immersed before, or (3) the scale reading remains constant for three
consecutive readings (2 min) and the specimen has visibly
9
ruptured or broken loose from the base plate. Note the time and
The sole source of supply of the Emley Plasticimeter known to the committee
the scale reading at the end of the test.
at this time is Geotest Instrument Corporation, 910 University Place, Evanston, IL
60201, USA. If you are aware of alternative suppliers, please provide this 7.4 Calculation:
information to ASTM International Headquarters. Your comments will receive 7.4.1 Calculate the plasticity figure as follows:
careful consideration at a meeting of the responsible technical committee 1, which
you may attend. P 5 =F2 1 ~10T! 2 (1)
4
C 110
where Hydrated lime 8g

P = plasticity figure, Standard aggregate (pulverized limestone) 72 g
F = scale reading at the end of the test, and Blend the mix until homogeneous.
T = time in minutes from the time when the first portion of 8.4.2.2 Standard Tablet—Make up a pressed tablet in ac-
paste was put in the mold to the end of the test. cordance with the procedure outlined in 8.3.1 using the
7.5 Precision and Bias: following mixture for the sample:
7.5.1 There are as yet insufficient analyzed data to permit Standard portland cement 7g
preparation of a precision and bias statement for this test Standard aggregate (pulverized limestone) 16 g
method. When data are collected and analyzed, precision and
bias statements will be proposed. Blend the mix until homogeneous.
8.4.2.3 Autoclave and calculate expansions of the test tablet
8. Autoclave Expansion of Hydrated Lime and the standard tablet in accordance with 8.3.1.
8.4.2.4 Determine the autoclave expansion of hydrated lime
8.1 Significance and Use:
for masonry purposes by subtracting the average percent
8.1.1 Expansion of pressed tablets of hydrated lime gener-
expansion of the standard tablet from the sample tablet.
ally indicates the presence of unhydrated oxides of magnesium
and calcium. The relation of the degree of expansion in this test 8.5 Precision and Bias:
method to field performance has not been determined. 8.5.1 No precision data are available due to the limited use
8.2 Apparatus: of this test method. Therefore, users are advised to develop
8.2.1 Mold and Press—A steel mold capable of producing a their own laboratory precision. No statement is being made
press tablet at least 0.032 m (1.25 in.) in diameter and 0.006 m about the bias of this test method.
(0.25 in.) thick, and able to sustain at least 88.9 kN (20 000
lbf) pressure from a suitable press. It should be provided with 9. Popping and Pitting of Hydrated Lime
a release jig also. 9.1 Significance and Use:
8.2.2 Autoclave, capable of holding 1034 kPa (150 psi) for 9.1.1 Pops and pits are caused by the hydration and expan-
2 h.
iTeh Standards
8.2.3 Micrometer, dial-type, capable of measuring 2.54 µm
sion of coarse particles of unhydrated lime or lime-impurity
reaction products present in the hydrated lime. The level of
(0.0001 in.).
mm.
8.2.4 Microscope, with graduated lens for measuring 0.10
popping and pitting in the sample is indicative of the potential
for the appearance of surface defects in plastering applications.
9.2 Gauging Plaster:
8.3 Procedure: Document Preview
8.3.1 Weigh out 15 g of hydrated sample, place in the mold,
9.2.1 The gauging plaster used for the popping and pitting
test shall conform to the Test Methods section of Specification
and press into a tablet. Press to 33.4 kN (7500 lbf) for 10 s, C 28 and shall have a setting time of not more than 1 h when
then increase pressure to 88.9 kN (20 000 lbf) or more. Hold ASTM C110-02
tested in accordance with Test Methods C 472. Test the
for 10 s before releasing. Press tablet from mold with jig and gauging plaster without lime in the manner described in 9.3 to
draw three diameter lines across the surface of the tablet using ensure its freedom from pops and pits. If any pops or pits are
a lead pencil. Draw two diameter lines normal to each other found, provide another lot of gauging plaster that is free of
and draw the third bisecting the 90° angles of the other two. pops and pits when subjected to this test.
Measure the diameters with a dial micrometer and place the 9.3 Procedure:
tablet on the autoclave rack. Use aluminum foil to protect the 9.3.1 Mix 100 g of hydrated lime with sufficient water to
tablets from water dripping. Autoclave at 862 to 1034 kPa (125 bring to such a consistency as to give a penetration of 20 6 5
to 150 psi) for 2 h. Begin timing when the pressure reaches 345 mm when tested in accordance with 6.3.3. Mix into this putty,
kPa (50 psi). After the autoclaving interval, allow the autoclave 25 g of gauging plaster (9.2.1), adding more water as required
to cool, remove the tablet, and remeasure the diameters. to maintain workable consistency. Spread on a glass plate to
Calculate the average percent expansion of the tablet from the make a pat at least 150 by 200 mm (6 by 8 in.) by
before and after measurements. approximately 3 mm (1⁄8 in.) in thickness. Trowel to a smooth
8.4 Expansion of Hydrated Lime-Portland Cement- finish. Allow to stand overnight.
Aggregate: 9.3.2 Place the specimen and plate on a rack in the steam
8.4.1 Materials: bath so that water is not in contact with the specimen to be
8.4.1.1 Standard Cement—Type I or Type II portland ce- tested. Provide a sloping cover above the specimen to prevent
ment. condensed steam from dripping onto the surface of the speci-
8.4.1.2 Standard Aggregate—Pulverized limestone, minus men. Raise the temperature of the water in the steam bath to
212-µm (No. 70) sieve, having less than 0.5 % silicon dioxide boiling and maintain at boiling for 5 h. Remove the specimens
(SiO2). from the bath and examine for pops and pits.
8.4.2 Procedure: 9.3.3 The pitting potential of hydrated lime can be deter-
8.4.2.1 Test Tablet—Make up a pressed tablet in accordance mined in conjunction with autoclave expansion as in 8.3.1.
with the procedure outlined in 8.3.1 using the following However, it is not necessary to measure diameter, if only the
mixture for the sample: pitting potential is to be determined. After following the
Standard portland cement 14 g procedure for expansion in 8.3.1, examine the pressed tablet
5
C 110
under the measuring microscope, and count and measure the retention test in Specification C 91 (see Figs. 3 and 4).
pits in millimetres. 10.4.2 Procedure:
10.4.2.1 Adjust the mercury relief column or vacuum regu-
10. Water Retention of Hydrated Lime lator to maintain a vacuum of 51 6 3 mm as measured on the
10.1 Significance and Use: manometer or the vacuum gauge. Seat the perforated dish on
10.1.1 This test method measures the ability of the hydrated the greased gasket of the funnel. Place a wetted filter paper in
lime in a plastic mix with sand to retain water, and hence retain the bottom of the dish. Turn the stopcock to apply the vacuum
consistency of the mix, when subjected to an applied suction. to the funnel and check the apparatus for leaks and to
This ability, measured as a percent of the original consistency, determine that the required vacuum is obtained. Then turn the
is indicative of the workability to be expected in a masonry stopcock to shut off the vacuum from the funnel.
containing the lime. 10.4.2.2 Immediately after the final consistency test
10.2 Proportioning and Mixing: (10.3.2), return all of the mortar to the bowl and remix the
10.2.1 Apparatus—The apparatus used shall conform to entire batch for 15 s at medium speed. Immediately after
Practice C 305. remixing the mortar, fill the perforated dish with the mortar to
10.2.2 Proportions—The mortar tested shall be composed slightly above the rim. Tamp the mortar 15 times with the
of 500 g of lime and 1500 g of standard sand conforming to tamper. Apply ten of the tamping strokes at approximately
13.2.4. If hydrated lime putty is used, use that weight of putty uniform spacing adjacent to the rim of the dish and with the
that is equivalent to 500 g of dry hydrated lime. long axis of the tamping face held at right angles, to the radius
10.2.3 Mechanical Mixing: of the dish. Apply the remaining five tamping strokes at
10.2.3.1 Place the dry paddle and the dry bowl in the mixing random points distributed over the central area of the dish. The
position in the mixer. tamping pressure shall be just sufficient to ensure filling of the
10.2.3.2 Place a measured quantity of water in the bowl. dish. On completion of the tamping, the top of the mortar
10.2.3.3 Add the lime to the water, then start the mixer and should extend slightly above the rim of the dish. Smooth off the
mix at slow speed (140 6 5 r/min) for 30 s. mortar by drawing the flat side of the straightedge (with the
iTeh Standards
10.2.4 Add the entire quantity of sand slowly over a 30-s leading edge slightly raised) across the top of the dish. Then cut
period while mixing at slow speed. off the mortar to a plane surface flush with the rim of the dish
10.2.5 Stop the mixer, change to medium speed (285 6 10 by drawing the straightedge with a sawing motion across the
rpm) and mix for 30 s.
10.2.6 Stop the mixer and let the mortar stand for 11⁄2 min.
top of the dish in two cutting strokes, starting each cut near the
center of the dish. If the mortar is pulled away from the side of
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(During the first 15 s of this interval, quickly scrape down into
the batch any mortar that may have collected on the side of the
the dish during the process of cutting off the excess mortar,
gently press the mortar back into contact with the side of the
bowl, then for the remainder of this interval cover the bowl dish using the tamper.
with the lid.) 10.4.2.3 Turn the stopcock to apply vacuum to the funnel.
10.2.7 Finish the mixing for 1 min at medium speed. ASTMAfter C110-02
suction for 60 s, quickly turn the stopcock to expose the
10.2.8 Inhttps://standards.iteh.ai/catalog/standards/sist/4ebe6cd0-7baa-4d9d-a31d-6a9d6ed53d90/astm-c110-02
any case requiring a remixing interval, any mortar funnel to atmospheric pressure. Immediately slide the perfo-
adhering to the side of the bowl shall be quickly scraped down rated dish off the funnel, touch it momentarily on a damp cloth
into the batch prior to remixing. to remove droplets of water, and set the dish on the table. Then
10.3 Consistency: using the bowl scraper (rubber scraper as specified in Practice
10.3.1 Apparatus—The flow table and mold used for the C 305), plow and mix the mortar in the dish for 15 s. Upon
measurement of consistency of the mortar shall conform to completion of mixing, place the mortar in the flow mold and
Specification C 230. determine the flow. Carry out the entire operation without
10.3.2 Procedure—Carefully wipe dry the flow table top interruption and as quickly as possible. Not more than 30 min
and place the flow mold at the center. Immediately after should be required for completion, starting from the comple-
completing the mixing operation, fill the mold with mortar tion of the mixing of the mortar for the first flow determination.
gently pressed into place by the finger tips to ensure uniform 10.4.3 Calculation:
filling free of voids. Smooth off the mortar level with the top of 10.4.3.1 Calculate the water retention value for the mortar
the mold by aid of a trowel, and remove the mold. Immediately as follows:
drop the table through a height of 13 mm (1⁄2 in.), 25 times in Water retention value 5 ~A/B! 3 100 (2)
15 s. The flow is the resulting increase in diameter of the
mortar mass, expressed as the percentage of the original where:
diameter. The mortar may be adjusted, if the flow is below A = flow after suction, and
100 %, by additions of water until the flow is within the range B = flow immediately after mixing.
from 100 to 115 %. Make each adjustment by returning the 10.5 Precision and Bias:
mortar to the original mixing bowl, add water, and then mix at 10.5.1 No precision data are available due to the limited use
medium speed (2856 10 r/min) for 30 s. If the flow of the of this test method. Therefore, users are advised to develop
original mortar is greater than 115 %, prepare a new batch. their own laboratory precision.
10.4 Water Retention Test:
10.4.1 Apparatus—The equipment used to determine water 11. Settling Rate of Hydrated Lime
retention shall conform to either apparatus used for the water 11.1 Significance and Use:
6
C 110
iTeh Standards
FIG. 3 Apparatus Assembly for the Water Retention Test
11.1.1 This test method provides a measure Document

of the rate of
settling of a hydrated lime slurry, a form in which this material
Preview
reactivity of the softer-burned portion of the quicklime. Total
slaking time provides a measure of the overall degree of
is frequently used. In some applications a slow settling slurry reactivity of the material. Total temperature rise is largely
is desirable; in others, fast settling is preferred. ASTM C110-02
dependent on the available lime content of the sample.
11.2 Procedure: 12.1.2 These slaking parameters provide an indication of
11.2.1 Place 10.0 g of lime hydrate in a 100-mL glass- the performance of the quicklime to be expected in industrial
stoppered graduated cylinder (internal diameter about 24 mm). slaking systems. Slaking characteristics have an effect on lime
Wet with 50 mL of carbon dioxide (CO2) free distilled water at slurry properties such as settling characteristics, viscosity,
23 6 1.7°C (73.46 3°F) and mix thoroughly by alternately particle size, and reaction rate.
inverting and righting the cylinder slowly for a period of 2 min. 12.2 Apparatus:
Allow the graduate and contents to stand at 23 6 1.7°C for 30 12.2.1 Mechanical Stirrer ,10 speed 400 6 50 r/min, fitted
min and then dilute to the 100-mL mark with CO 2-free with a special stirring rod.
distilled water at 23 6 1.7°C. Mix contents again thoroughly as 12.2.2 Modified Dewar Flask ,11 665-mL, fitted with special
before and allow to stand undisturbed at 23 6 1.7°C for 24 h. rubber gasket covers.
11.3 Report: 12.2.3 Thermometer, dial-type, 0 to 100°C range in 1°C
11.3.1 Report the sedimentation height in millilitres after 1⁄4, increments or thermocouple with a response time equivalent to
1⁄2, 3⁄4, 1, 2, 4, and 24 h, reading the bottom of the meniscus. or faster than the dial thermometer.
NOTE 5—Slight variations in results of this test method on a sample run
12.2.4 Torsion Balance.
in different laboratories or by different operators are permissible. The test 12.2.5 Sieve, 203-mm (8-in.), 3.35-mm (No. 6), conforming
is not an absolute one, but is designed to distinguish between fast and slow to Specification E 11.
settling hydrates. 12.2.6 An apparatus essentially the same as that illustrated
11.4 Precision and Bias: in Fig. 5 and Fig. 6 shall be used. The apparatus consists of a
11.4.1 No precision data are available due to the limited use covered reaction container fitted with a mechanical stirrer and
of this test method. Therefore, users are advised to develop thermometer. The quicklime charge shall be stirred with a
their own laboratory precision. mechanical stirrer fitted with a stainless steel rod, the end of
which is formed into a loop to follow the contour of the
12. Slaking Rate of Quicklime
12.1 Significance and Use: 10
A Fisher 14-498, or equivalent, has been found suitable for this purpose.
12.1.1 The temperature rise in 30 s is a measure of the 11
A Fisher 10-197, or equivalent, has been found suitable for this purpose.
7
C 110
iTeh Standards FIG. 4 Vacuum Gauge Apparatus Assembly for the Water Retention Test
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ASTM C110-02
8
C 110
iTeh Standards
FIG. 5 Slaking Reactivity Apparatus
12.3 Procedure:
12.3.1 Prepare the sample of quicklime (as rapidly as
possible to prevent sample deterioration) so that a majority of
Documentthe Preview
material passes a 3.35 mm (No. 6) sieve. Place the sample
in an airtight container and allow to come to room temperature
before testing. The slaking rate of lime is significantly affected
ASTM C110-02
by the particle size of the sample and must be as close to a 3.35
mm (No. 6) sieve as possible. It is not necessary that 100 % of
the sample pass a 3.35 mm (No. 6) sieve, but all of the sample,
including the plus 3.35 mm (plus No. 6) fraction, must be used
in the test.
12.3.2 Slaking Rate—Adjust the temperature of about 500
mL of distilled water in accordance with the schedule given in
Table 1, and add the specified amount to the Dewar flask. Set
the agitator revolving at 400 6 50 r/min. The temperature of
the water in the flask must be 60.5°C of the desired tempera-
ture. Quarter and weigh out the required amount of the
prepared quicklime sample. Add the quicklime to the water
without delay and simultaneously begin timing. Put the covers
in place immediately. Take a reading at each 30 s interval.
12.3.3 Continue readings until less than 0.5°C temperature
FIG. 6 Stirring Rod Detail change is noted in each of three consecutive readings. The total
active slaking time will then be the time at which the first of the
reaction container. The vacuum reaction flask shall be provided
three consecutive readings was taken. The temperature at this
with a cover consisting of two circular pieces of gasket rubber
time will be considered the final reaction temperature. Subtract
sheet, approximately 3 mm (1⁄8 in.) thick. The first piece is
provided with a single radial slot that slides over the stirring TABLE 1 Schedule for Slaking Rate
rod and the thermometer. The second piece (top) has a similar Material to Be Tested
slot plus a hole to provide for the dial thermometer. When the Dolomitic High Calcium
Temperature of water,° C 40 25A
two cover pieces are in place, the slot on the lower piece is at Quantity of water, mL 400 400
right angles to the slot on the upper piece with the thermometer Quantity of quicklime, g 120 100
stem extending through the lower slot. The apparatus may be A
Initial temperature of 40°C may be used, provided the report of results states
assembled by any convenient supporting equipment. the initial temperature.
9
C 110
the initial temperature from the final temperature to obtain the TABLE 3 Unit Weights and Apparent Specific Gravities
total temperature rise. Subtract the initial temperature from the Materials
Unit weight, Specific
temperature at 30 s for the temperature rise in 30 s. Subtract the kg/m3(lb/ft3)A Gravity
initial temperature from the temperature at 3 min for the Portland cement 1,504 (94) 3.15
Hydrated lime 800 (50) 2.30
temperature rise in 3 min. Blended Ottawa sand 1,280 (80) 2.65
12.4 Report: A
The unit weight values listed for cementitious materials are assumed values
12.4.1 Record the actual temperature rise and plot a suitable commonly used in construction practice.
curve showing temperature rise as the ordinate and time as the
abscissa. The results may also be reported as: produce a flow of 110 6 5 % as determined by the flow table.
12.4.1.1 Temperature rise in 30 s (or at any other designated Proportions for the generally used batch sizes based on Table 2
time) in degrees Celsius, material unit weight shall contain the weights as prescribed in
12.4.1.2 Total temperature rise in degrees Celsius, and Table 4.
12.4.1.3 Total active slaking time in minutes. 13.3.2 Mixing of Mortars—Mix the mortar in accordance
12.5 Precision and Bias: with the procedure for mixing pastes in Practice C 305.
12.5.1 Twelve laboratories cooperated in the testing of five 13.3.3 Determination of Flow—Determine the flow in ac-
high calcium quicklimes and four dolomitic quicklimes thereby cordance with the Procedure section of Test Method C 109.
obtaining the repeatability (r) and reproducibility (R) (Practice 13.4 Procedure:
E 691) data contained in Table 2. 13.4.1 If the mortar has the correct flow, use a separate
12.5.2 Due to the lack of a recognized industry standard, the portion of the mortar for the determination of entrained air.
bias of this test method has not been determined. The variety of Determine the weight of 400 mL of mortar in accordance with
reporting options also complicates obtaining a suitable bias Test Method C 185.
statement. 13.5 Calculation:
13.5.1 Calculate the air content of the mortar and report it to
13. Air Entrainment the nearest 0.1 % as follows:
13.1 Significance and Use:
iTeh Standards
13.1.1 Hydrated lime, particularly that containing an air-
D 5 ~W1 1 W2 1 W 3 1 Vw!/
@~W1/S1! 1 ~W 2/S2! 1 ~W3/S3! 1 V w# A
entraining additive, used in masonry mortar may contribute to 5 100 2 ~W m/4D!
(3)
the air content of the mortar. Certain specifications and
applications of mortar place a limit on this air content. where:
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13.2 Apparatus: D = density of air-free mortar,
W1 = weight of portland cement, g,
13.2.1 Scales, Sieves, Glass Graduates, Tamper, Measure,
W2 = weight of hydrated lime, g,
Straightedge, Spatula, Tapping Stick, and Spoon, conforming W3 = weight of blended Ottawa sand, g,
to the requirements given in Test Method C 185.
13.2.2 Flow Table, conforming to the requirements pre- ASTM VC110-02
w = water used, mL,
S1 = specific gravity of portland cement,
scribed in https://standards.iteh.ai/catalog/standards/sist/4ebe6cd0-7baa-4d9d-a31d-6a9d6ed53d90/astm-c110-02
Specification C 230. S2 = specific gravity of hydrated lime,
13.2.3 Mixing Apparatus, conforming to the requirements S3 = specific gravity of blended Ottawa sand,
as prescribed in Practice C 305. A = volume % of entrained air, and
13.2.4 The sand shall be a blend of equal parts by weight of Wm = weight of 400 mL of mortar, g.
graded Ottawa sand and standard 20–30 Ottawa sand. The
NOTE 6—For lime/sand mortars, W1 and S1 should be dropped from the
fineness of graded Ottawa sand and standard 20–30 sand may calculation.
be checked by using the methods described in Specification
C 778. 13.6 Precision and Bias:
13.3 Preparation of Mortar: 13.6.1 The single operator within laboratory standard devia-
13.3.1 Proportions for Mortar—Portland cement-hydrated tion has been found to be 0.56 % air content throughout the
lime mortar for measurement of air entrainment shall be range of 8 % to 19 % air content. Therefore results of two
proportioned to conform, in batch size, to the unit weights by properly conducted tests by the same operator on similar
volume of cementitious material and aggregate as shown in batches of mortar should not differ by more than 1.6 % air
Table 3. The portland cement shall conform to Specification content.
C 150, and the hydrated lime to Specification C 207. The 13.6.2 The multilaboratory standard deviation has been
quantity of water, measured in millilitres, shall be such as to found to be 1.0 % air content throughout the range of 8 % to
TABLE 4 Weight of Materials for Mortar Batch
TABLE 2 Precision Data Proportions Portland Hydrated Blended Ottawa
Mortar by Cement Lime Silica Sand
Results in °C Rise
Material Labs r R Type Volume (g) (g) (g)
Time Range Tested
M 1:1⁄4:33⁄4 470.0 62.5 1,500
High Calcium 12 30 s 12.3–44.4 1.56 4.21 S 1:1⁄2:41⁄2 376.0 100.0 1,440
High Calcium 11 3 min 32.1–56.1 1.72 4.72 N 1:1:6 282.0 150.0 1,440
Dolomitic 10 30 s 3.6–12.0 1.38 2.84 O 1:2:9 188.0 200.0 1,440
Dolomitic 9 3 min 21.2–36.4 1.62 3.72 Lime/Sand 1:3 300.0 1,400
10

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Standard Test Methods for

1. Scope 2. Referenced Documents

where Hydrated lime 8g

11.1.1 This test method provides a measure Document

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