CDS CS-InstrumentConfig
CDS CS-InstrumentConfig
CDS CS-InstrumentConfig
ChemStation Edition
Instrument Configuration
Guide
ChemStation Edition Instrument Configuration
Agilent Technologies
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This guide describes how to configure your instruments to work with Agilent
OpenLab CDS ChemStation Edition. It includes instructions on how to add
instrument modules and configure them.
Throughout this guide, the term ChemStation always refers to Agilent
OpenLab CDS ChemStation Edition and Control Panel refers to the Agilent
OpenLab Control Panel.
5 Troubleshooting
This chapter summarizes helpful hints for troubleshooting potential problems
you might see during the configuration process.
Contents
5 Troubleshooting 87
Troubleshooting the Network 88
LC Instrument Start-up Problems 91
1
Quick Configuration Guide
Configuration using the Control Panel 6
Quick Configuration Guide 6
The figures in this chapter show the Windows 7 user interface. If you have installed
NOTE Windows 10, your user interface is different, but the instructions are still applicable.
Agilent Technologies 5
1 Quick Configuration Guide
Configuration using the Control Panel
To create and edit locations, refer to the Control Panel online help.
NOTE
6 Navigate to the new instrument and click the Configure Instrument icon or
right click on the instrument name and select Configure Instrument.
2
Overview of Instrument
Communications
Overview of Instrument Communications 12
Network Communication 13
About Networks 13
Upgrading to Network Communication 14
Installing Network Communication 14
Instrument configuration using the Agilent BootP service 16
Configuring the Agilent BootP Service 18
Instrument Connections 22
Connecting an Agilent GC system 22
Connecting an Agilent LC system via the Network 22
Connecting an Agilent Integrated LC System via the Network 23
Connecting a 35900E ADC 23
Connecting an Agilent 7100 CE System 24
Agilent Technologies 11
2 Overview of Instrument Communications
Overview of Instrument Communications
Network Communication
About Networks
Each device on the network requires a unique IP address, a subnet mask, and
an optional gateway.
If installing on a site network, contact the site network administrator. If
installing on an isolated network, Agilent recommends the following
addresses:
Device Address
PC 10.1.1.100
GC, LC, CE or ADC 10.1.1.101 through 10.1.1.255
Subnet mask 255.255.255.0
Gateway 10.1.1.100
PC 1 10.1.1.100 255.255.255.0
Use the IPCONFIG utility to verify the PC's TCP/IP settings by opening a command
NOTE window and typing
ipconfig /all
• IP Address
• Comment, if desired
• Subnet Mask
• Gateway address (optional)
f Click OK.
g Leave Edit BootP Addresses by pressing Close.
h Use the PING utility to verify the LAN connectivity by opening a
command window and typing
ping <ip.adress> (e.g. ping 10.1.1.101) “Verify that the IP Address is
correct” on page 89 .
i Exit BootP Settings by pressing OK and power cycle the instrument.
If changing the IP address, it will be necessary to power cycle the
instrument for the changes to take effect.
3 Add an additional instrument or device to the network.
a Repeat step 2 on page 17 for each instrument or device on the network
that requires the Bootp service.
b When finished, click Exit Manager.
c Click OK.
Figure 6
Configuring logging
1 Do you want to log BootP requests?: Check to enable logging
OR
Uncheck to stop logging.
A default log file was created at installation and is located at C:\Program
Data\Agilent\BootP\LogFile. It contains an entry for every time a device
requests configuration information from Bootp.
2 Click OK to save the values or Cancel to discard them. The editing ends.
Instrument Connections
Be sure to set up the communication channel between the instrument and the
PC prior to operating the system.
We recommend that you connect the network (LAN) cable to an Agilent Modular LC
NOTE detector (mandatory for DAD and MWD detectors). If no Agilent detector is used, please
contact your Agilent representative for information about the insertion point of the
communication card.
The 35900E dual channel interface uses APG remote, but the two remote
connectors are not pass-through connections. When you operate the 35900E
with both channels simultaneously, only the A-channel remote is connected;
the B-channel acts in synchronization with the A-channel and reacts to the
remote signals from the A-channel remote connector. If you wish to operate
the B-channel independently, you connect a remote cable to the B-channel
remote connector. In this mode, one instrument may start and stop the
A-channel while another instrument has control of the B-channel.
3
General Instrument Configuration
Considerations
Adding Instruments to a ChemStation Installation 26
Number of Instruments Supported 28
Printer Configuration 31
Configuring Physical Printers in Distributed Systems 31
Agilent Technologies 25
3 General Instrument Configuration Considerations
Adding Instruments to a ChemStation Installation
If you want the instruments allocated to a specific instrument number (for example, if you
NOTE are upgrading from a previous ChemStation revision) you must configure the instruments
in the required sequence. The first instrument you configure will be allocated to
instrument 1 (..\Users\Public\Documents\ChemStation\1\), the second to instrument 2
(..\Users\Public\Documents\ChemStation\2\) and so on. However, the Control Panel
lists the instruments in alphabetical order.
GC, LC (2D)1 4 10 2 1
LC (3D)2, 3 2 5 2 1
CE 2 5 2 0
1100/1200 LC mixed-module The 35900E Dual Channel Interface counts as the equivalent of
combinations: one 1100/1200 module.
configuration for very complex systems. The following list outlines some
considerations:
• 1100/1200 chromatography instrument configurations that do not include
diode array detectors (DADs) on a single workstation are limited to a total
of around 18 individual modules, configured as up to four instruments with
a limit of four detectors per instrument.
• The maximum number of 18 modules can consist of about 12 modules such
as pumps, detectors and injectors, and about six can-slave modules such as
valves and UIB interfaces. The maximum number depends on the exact
module configuration and the LAN connection point.
• If detectors of the same type are used in one stack, two detectors of the
same type are supported, or, in the case of the VWD, up to three. If DADs
are included in the configuration, there is a limit of two DADs and about
eight modules that may be configured as two separate instruments.
• When an instrument configuration includes an LC/MS, there is a limit of
one LC/MS and one DAD on the instrument; no additional instruments are
supported on the workstation.
• When an instrument configuration includes a CE/MS, there is a limit of one
CE/MS including the DAD on the instrument. No additional instruments are
supported on the CE/MS or CE ChemStation.
Printer Configuration
Print Limitations
The maximum number of pages for one print job is 1500; for example, a
sequence summary report is one print job.
When printing Multi-Page chromatograms (specified in the Specify Reports
dialog box), the maximum number of pages that can be printed properly
depends on the resolution of the printer. 300 dpi allows ten pages per
chromatogram, 600 dpi allows up to six pages per chromatogram.
4
Adding and Configuring Instruments
Adding an LC System 34
Configuring a Device Cluster 40
Adding an ELSD to an LC System 46
Adding an Agilent 7100 CE System 48
Adding an Agilent GC System 53
GC ChemStation demonstration methods and data files 58
Adding an Agilent 490 Micro GC 59
Adding an Agilent Headspace Sampler 65
Adding a Standalone ADC 66
Configuring the Agilent ADC Instrument - Dual Channel 66
Configuring the Agilent ADC Instrument - Two Independent
Channels 73
Adding a 35900E ADC to an LC or GC System 76
Adding an Agilent PAL-xt or PAL3 Sampler with LC or GC 78
Adding a PAL3 Sampler for GC 78
Adding a PAL-xt Sampler 79
Adding an LC/MS or CE/MS System 81
This chapter describes how to add instruments using the Agilent OpenLab
Control Panel.
The figures in this chapter show the Windows 7 user interface. If you have installed
NOTE Windows 10, your user interface is different, but the instructions are still applicable.
Agilent Technologies 33
4 Adding and Configuring Instruments
Adding an LC System
Adding an LC System
The G1315C/D DAD and the G1365C/D MWD are equipped with on-board LAN
NOTE communication, and require a LAN connection. These detectors must be the
communication entry point to the PC when they are used in an 1100/1200 stack.
1 In the Navigation pane of the Agilent OpenLab Control Panel, select Instruments.
3 Click the Create tool in the top toolbar and select Create instrument from the
menu.
OR
Right-click Instrument and select Create instrument.
f Enter details of the contact person in the Contact field. The contact
details are optional.
5 Click OK.
The new instrument is created in the Instruments tree.
6 In the Instruments tree, select the newly created instrument.
8 If Auto Configuration is offered, accept it. Enter either the IP address of the LC
or the Host name; all recognized modules will be copied from the Configurable
Modules panel to the Selected Modules panel.
Use Auto Configuration if possible. If you use manual configuration, you must enter all
NOTE configuration parameters correctly; if the configuration does not match the module
exactly, the module will not be recognized.
OR
Select the module(s) that you want to configure from the Configurable
Modules panel and click > to copy them to the Selected Modules panel.
9 Specify the instrument's LAN access parameters either by IP address or by
instrument Hostname.
For manual configuration of instruments with multiple modules, specify the LAN access
NOTE parameters for each module.
10 Complete the configuration dialog box(es) for the module(s) you have
selected.
If you skip this step, you will be asked to configure your new LC system the
first time you launch it.
11 Add and configure any additional modules from the Generic Modules section
of the Configurable Modules panel.
12 Click the Method load on startup down-arrow and select which method to load
when ChemStation is started.
13 Mark the check box(es) for the Options that you want to install.
Select Enable Intelligent Reporting to enable expanded reporting features. Clearing the
NOTE check box will not install these features for this instrument and they will never be
available.
If you enable Intelligent Reporting, the classic Report Layout will not be available for this
instrument. However, existing classic reports can be used in parallel with Intelligent
Reports.
14 To specify the size of the software window, select Additional configuration >
Initial screen window size and select the window size from the menu.
15 Click OK to complete the instrument configuration.
When you expand the Details section of the instrument information in the
Agilent OpenLab Control Panel, the new configuration data and details are
shown.
1 In the Navigation pane of the Agilent OpenLab Control Panel, select the
Instruments tree.
3 Click the Create tool in the top toolbar and select Create instrument from the
menu.
OR
Right-click Instrument and select Create instrument.
8 If Auto Configuration is offered, accept it. Enter either the IP address of the LC
or the Host name; all recognized modules will be copied from the Configurable
Modules panel to the Selected Modules panel.
Use Auto Configuration if possible. If you use manual configuration, you must enter all
NOTE configuration parameters correctly; if the configuration does not match the module
exactly, the module will not be recognized.
OR
Select the module(s) that you want to configure from the Configurable
Modules panel and click > to copy them to the Selected Modules panel.
9 Specify the instrument's LAN access parameters either by IP address or by
instrument Hostname.
For manual configuration of instruments with multiple modules, specify the LAN access
NOTE parameters for each module.
The cluster is created using the marked modules; the individual modules in
the Available Modules panel are replaced by the cluster, and a configuration
dialog box is displayed that allows you to configure the cluster.
You can decluster the cluster into its individual modules by right-clicking on the cluster
NOTE and removing all components from the cluster. Note that declustered fraction collectors
are not supported; only the last one may be used as a recovery collector).
Depending on the module, the ELS detector is fitted with a LAN or standard
RS232 3-wire serial interface.
An ELS Detector that is connected via LAN interface can be configured
simularly as an LC module, see “Adding an LC System” on page 34.
Some older ELS detectors only have an RS232 serial interface though.
Autoconfiguration does not detect these ELSDs. The device must be
configured manually, since it has a separate network connection. This
procedure describes how to add an Agilent ELSD to an LC instrument that has
already been configured.
1 Create and configure the LC system to which the ELSD is connected. See
“Adding an LC System” on page 34 for full details.
2 In the Instruments tree, select the newly created instrument.
1 In the Navigation pane of the Agilent OpenLab Control Panel, select the
Instruments tree.
3 Click the Create tool in the top toolbar and select Create instrument from the
menu.
OR
Right-click Instrument and select Create instrument.
8 If Auto Configuration is offered, accept it. Enter either the IP address of the LC
or the Host name; all recognized modules will be copied from the Configurable
Modules panel to the Selected Modules panel.
Use Auto Configuration if possible. If you use manual configuration, you must enter all
NOTE configuration parameters correctly; if the configuration does not match the module
exactly, the module will not be recognized.
OR
Select the module(s) that you want to configure from the Configurable
Modules panel and click > to copy them to the Selected Modules panel.
10 Complete the configuration dialog box(es) for the module(s) you have
selected.
If you skip this step, you will be asked to configure your new LC system the
first time you launch it.
11 Add and configure any additional modules from the Generic Modules section
of the Configurable Modules panel.
12 In the upper pane of the Configure Instrument dialog box, click the Method load
on startup down-arrow and select which method to load when ChemStation
is started.
13 In the Configure Instrument dialog box, mark the check box(es) for the Options
that you want to install.
14 To specify the size of the software window, select Additional configuration >
Initial screen window size and select the window size from the menu.
15 Click OK to complete the instrument configuration.
When you expand the Details section of the instrument information in the
Agilent OpenLab Control Panel, the new configuration data and details are
shown.
This section is applicable to the Agilent 9000, 78xx and 68xx GC systems. For
490 Micro GC please see “Adding an Agilent 490 Micro GC” on page 59.
Beginning with OpenLab CDS ChemStation C.01.09, the instrument types used
for a new installation are either Agilent GC System or Agilent GC Core System (VL).
For upgrade installations, the following instrument types, Agilent 9000, Agilent
78xx, or Agilent 68xx GC Systems are used.
1 In the Navigation pane of the Agilent OpenLab Control Panel, select the
Instruments tree.
3 Click the Create tool in the top toolbar and select Create instrument from the
menu.
OR
Right-click Instrument and select Create instrument.
5 Click OK.
The new instrument is created in the Instruments tree.
6 In the Instruments tree, select the newly created instrument.
7 Click Configure Instrument in the toolbar or right-click the instrument name
and select Configure Instrument.
• Click the Keypad Lock down-arrow and make a selection from the
drop-down list.
• Select the Prep Run on Manual Request check box if required.
10 Click OK.
The new instrument is shown in the Selected Modules panel of the Configure
instrument dialog box.
11 In the upper pane of the Configure Instrument dialog box, click the Method load
on startup down-arrow and select which method to load when ChemStation
is started.
12 Mark the check box(es) for the Options that you want to install.
Select Enable Intelligent Reporting to enable expanded reporting features. Clearing the
NOTE check box will not install these features for this instrument and they will never be
available.
If you enable Intelligent Reporting, the classic Report Layout will not be available for this
instrument. However, existing classic reports can be used in parallel with Intelligent
Reports.
13 To specify the size of the software window, select Additional configuration >
Initial screen window size and select the window size from the menu.
14 Click OK to complete the instrument configuration.
When you expand the Details section of the instrument information in the
Agilent OpenLab Control Panel, the new configuration data and details are
shown.
For the 7890, if you use the 35900 for additional signals, it replaces two of the four native
NOTE signals (the maximum number of signals is still four).
100FID.M This method can be used to display the three 100FID files.
100FID5.D These are examples of the Ultra column test mix run on a
100FID20.D 10m x 100µM id x 0.17µM film HP-5 column in an 6890
100FID50.D Series GC. They were collected at 5, 20, and 50 Hz data
rates, respectively.
1 In the Navigation pane of the Agilent OpenLab Control Panel, select Instruments.
3 Click the Create tool in the top toolbar and select Create instrument from the
menu.
OR
Right-click Instrument and select Create instrument.
9 In the IP address field, enter the IP address of the 490 Micro GC and click
Activate communication to register the system access parameters.
The GC's details are added to the Instrument Information field.
10 Complete the instrument configuration.
a Enter the hardware parameters in the Instrument Hardware tab.
b Click the Instrument configuration tab and enter the configuration
parameters.
c Click the Automation and remote control tab and specify the remote control
and automation parameters. You can also configure the VICI valve here.
d Click OK to complete the 490 Micro GC configuration.
11 Click the Method load on startup down-arrow and select which method to load
when ChemStation is started.
12 Mark the check box(es) for the Options that you want to install.
Select Enable Intelligent Reporting to enable expanded reporting features. Clearing the
NOTE check box will not install these features for this instrument and they will never be
available.
If you enable Intelligent Reporting, the classic Report Layout will not be available for this
instrument. However, existing classic reports can be used in parallel with Intelligent
Reports.
13 To specify the size of the software window, select Additional configuration >
Initial screen window size and select the window size from the menu.
14 Click OK to complete the instrument configuration.
When you expand the Details section of the instrument information in the
Agilent OpenLab Control Panel, the new configuration data and details are
shown.
2 In the Agilent OpenLab Control Panel, select the GC to which the headspace is
to be configured.
3 Select Configure instrument by right-clicking on the GC.
OR
Click Configure Instrument in the toolbar.
4 Select the headspace module to configure from the Configurable Modules
panel and click > to copy the module to the Selected Modules.
The Agilent Headspace Sampler Configuration dialog box opens. If it does not
open automatically, select Configure or double-click on the Configured
module to open the Agilent Headspace Sampler Configuration dialog box.
5 Select the Preferences tab to specify Method Editor and Instrument Actuals for
how information should appear when editing the method and reviewing
headspace sampler (HS) status.
6 Enter the IP Address or Hostname on the Connection tab.
7 Select OK.
This establishes a connection and uploads the Configuration.
8 Select OK to complete configuration.
1 In the Navigation pane of the Agilent OpenLab Control Panel, select the
Instruments tree.
3 Click the Create tool in the top toolbar and select Create instrument from the
menu.
OR
Right-click Instrument and select Create instrument.
The serial number and firmware version are updated upon successful
connection to the 35900E.
11 Mark the check box(es) for the channel(s) that you want to use.
Two channels can be assigned to different instruments when using the 35900 RC.Net
NOTE driver.
13 Specify the actions of the 35900E buttons in the Front Panel Buttons.
14 Click the Events button for each channel to assign the TTL digital I/O states.
15 Enter a unique descriptive label you want to use to define the instrument's
energized state (high) and de-energized state (low). You may use any
combination of characters and numerals (maximum of 20). Refer to Help
and the 35900 User's Guide for more information on the Digital I/O
connection.
For example, if you are going to control a normally closed valve (a valve that opens only
NOTE when energy is applied), you could assign the events like the one shown in the figure. This
event indicates that the valve is normally closed (Low state) and when energy is applied it
goes to the opened state (High state).
You could also use the more descriptive labels, such as Open Nitrogen Valve and Close
Nitrogen Valve, if you prefer.
4 Click Configure.
5 Enter the IP address.
6 Select only Channel A, then click OK.
For Instrument 2:
1 Create the instrument in Agilent OpenLab Control Panel.
2 Select either Agilent ADC LC System or Agilent ADC GC System.
3 Move the 35900E from Configurable to Selected.
4 Click Configure.
5 Enter the same IP address as for Instrument 1.
6 Mark the check boxes for the channel(s) that you want to use.
7 Click OK to complete the instrument configuration.
When you expand the Details section of the instrument information in the
Agilent OpenLab Control Panel, the new configuration data and details are
shown.
When configured as part of a GC system, the 35900E adds two signals to a 68xx and
NOTE replaces two signals for the 78xx.
There are two different Agilent PAL Sampler models, PAL3 and PAL-xt.
Ensure that you install the correct software driver and firmware for your
instrument configuration.
The Tool Configuration and Tray Configuration tabs are now available in the PAL3
Configuration dialog box.
OpenLab CDS ChemStation Edition offers Script Manager, Tray Map, and PAL3
Configuration within an online session.
For Agilent Customer Engineers or Field Service Engineers, insertion of the FSE serial key
NOTE at this point offers access to programmatic cycle modification for a single session ONLY.
Methods for the PAL-xt are based on installed or imported cycles and
syringes that are configured within the control module of the instrument.
OpenLab CDS ChemStation Edition offers PAL Configuration, the ability to
Import Cycle... and Reset PAL within an online session.
This task shows you how to add an LC/MS system or a CE/MS system to a
standalone ChemStation workstation.
If you want to use an Agilent PAL Sampler with your LC/MS system, install the Agilent
NOTE PAL Control software before you configure your LC/MS system. See Adding an Agilent
PAL Sampler for details (“Adding an Agilent PAL-xt or PAL3 Sampler with LC or GC” on
page 78).
When secure file I/O is ON you can start the ChemStation of an MSD instrument, only if
NOTE the new MSD tune directory is protected.
To protect the MSD tune dir do the following:
1 Open the CSAdmin tool
2 Look for the new MSTune directory for MS instruments.
3 Set the checkmark to protect this directory.
4 Close CSAdmin tool.
1 In the Navigation pane of the Agilent OpenLab Control Panel, select the
Instruments tree.
3 Click the Create tool in the top toolbar and select Create instrument from the
menu.
OR
Right-click Instrument and select Create instrument.
Do not click OK to close the Configure Instrument dialog box at this stage.
NOTE
9 From the Generic Modules section of the Configurable Modules panel, add
Single Quad MSD to the Selected Modules.
The Configure Selected Module dialog box is displayed.
You can choose to set the LC/MS or CE/MS access by either the host name
or the IP address.
10 To set the system access by host name:
• Select the Identify by Host Name option.
• Enter the network name of the LC/MS or CE/MS in the Host Name field.
OR
To set the system access by IP address:
• Select the Identify by IP Address option.
• Enter the IP Address name of the LC/MS or CE/MS in the IP Address field.
See the documentation that came with your LC/MS or CE/MS for more
information about network parameters.
11 Add and configure any additional modules from the Generic Modules section
of the Configurable Modules panel.
12 In the Configure Instrument dialog box, mark the check box(es) for the Options
that you want to install.
13 Click OK to complete the instrument configuration.
When you expand the Details section of the instrument information in the
Agilent OpenLab Control Panel, the new configuration data and details are
shown.
5
Troubleshooting
Troubleshooting the Network 88
Troubleshooting Network Connections 89
Troubleshooting Network Communication 89
LC Instrument Start-up Problems 91
System remains in a wait-state waiting for a module that has been
taken out of the configuration 91
Data File is empty (contains no signal) 91
Devices report “Buffer Overflow” in the logbook 91
Agilent Technologies 87
5 Troubleshooting
Troubleshooting the Network
General Information
DHCP cannot be used to assign IP addresses to Agilent instruments used with
ChemStation. The ChemStation computer and all connected instruments must
use static IP addresses assigned at the PC, instrument front panel, or in the
G1369 network card.
Each computer and instrument uses a Network Interface Card (NIC) to
provide network communications. In some instruments, such as the 7890
Series GC, the NIC is built-in. For other instruments, the NIC is a separate
accessory or “card” that is installed. In either case, the NIC provides
communications programming and the physical connector for the network
cable.
To increase stability of communication, it is recommended to disable the Aero
look on the AIC, install the SP1 for Windows Server 2008 R2 and disable the
Application Experience Service. See also
http://support.microsoft.com/kb/902196
G1369A/B LAN card is inserted and scroll down to the IP address of the
G1369A/B LAN card.
When the MIO dialog box is opened on the Agilent 1100/1200 control module,
NOTE ChemStation cannot communicate with the Agilent 1100/1200 system.
In This Book
*M8300-90009*
*M8300-90009*
M8300-90009
Rev. B
Agilent Technologies