Spray Drying 31.8.16

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SPRAY DRYING

SPRAY DRYING
It is the most important kind of air
convection driers.
The development of spray drying
equipment and techniques evolved over a
period of several decades from the 1870s
through the early 1900s.
Spray drying comes of age during World
War II, with the sudden need to reduce
the transport weight of foods and other
materials.
Spray drying is limited to
foods that can be atomized,
like liquids and low-viscosity
pastes & purees. Eg. Milk,
coffee,egg
Liquid to be dried is sprayed
in the form of fine droplets
into a current of hot air,
usually counter current flow
is used.
Atomization into minute
droplets results in drying in a
matter of seconds.
The common inlet air temp.
is 2000C.
STEPS OF SPRAY DRYING
CONCENTRATION-
BEFORE DRYING FEED IS
CONCENTRATED

ATOMIZATION- PROVIDES
OPTIMUM CONDITION
FOR EFFICIENT DRYING

DROPLET-AIR CONTACT-
95% of the moisture is
evaporated
DROPLET DRYING-
OCCURS IN TWO
STAGES

SEPARATION-
CYCLONES, BAG
FILTERS,
ELECTROSTATIC
PRECIPITATORS
DROPLET DRYING
Droplet drying: moisture evaporation takes place
in two stages-

1) During the first stage, there is sufficient moisture


in the drop to replace the liquid evaporated at the
surface and evaporation takes place at a relatively
constant rate
2) The second stage begins when there is no longer
enough moisture to maintain saturated conditions
at the droplet surface, causing a dried shell to form
at the surface. Evaporation then depends on the
diffusion of moisture through the shell, which is
increasing in thickness.
ATOMIZATION
Atomization is one of the
most critical aspects of
the spray-drying process
as it controls the droplet
size and defines the final
particle size.
TYPES OF ATOMIZING
SYSTEMS

Pressure Spray Nozzle


Centrifugal Disc
Compressed Air
PRESSURE SPRAY
NOZZLE
It includes the swirl
nozzle (called whizzer or
centrifugal pressure
nozzle)
Pressures from 1500-
5000 psi are used
Feed is forced under
high pressure through a
small orifice and is
atomized instantly.
Higher the pressure or
smaller the orifice, finer
the particle size of the
mist.
CENTRIFUGAL SPINNING
DISC It has two radial
discs
It may resolve at 50,
000 rpm or 3500
rpm for a small and
large disc
respectively.
The pattern formed
is like that of a
cloud.
It does not have an
orifice which gets
clogged.
Can be used to
COMPRESSED AIR
SPRAY
A Jet of high-temperature
compressed air moves at high
velocity through a stream of pre-
heated milk for eg.
The high velocity jet of very hot
air strikes the milk stream at right
angles, atomizing it.
The droplet size determines the final dried
particle size
Particle size affects solubility rate
During atomization,
The trajectory is important also
As droplets descend through the drying
chamber, they transform from liquid to a
sticky condition and then turn dry
Trajectory generally is designed to prevent
minimize wall contact in the early stages of
drying.
ADVANTAGES
Spray drying process have advantages that
can be designed to virtually any capacity
required.
Feed rates range from a few pounds per hour
to over 100 tons per hour. Operation is
continuous and adaptable to full automatic
control.
It can be used with both heat-resistant and
heat sensitive products.
Nearly spherical particles can be produced.
FREEZE
DRYING

THIS PROCESS IS ALSO KNOWN AS


LYOPHILIZATION.
It important incase of heat sensitive materials.
Process occurs at a very low temperature and at
a very high vacuum.
Water in the material is first frozen to ice and
then ice sublimes to vapour without entering the
liquid phase.
This is known as sublimation due to which
cellular structure is not affected and flavour and
colour is retained.
Lyophilization, or freeze-drying, is used to remove
moisture by sublimation
Products are lyophilized to increase shelf life
Freeze-dried products are reconstituted with water
at time of use
Lyophilization processes are based on the physical
properties of water, as described by the phase
diagram
Sublimation is effected by control of product
temperature and pressure within the lyophilization
equipment.
lyophilization is used to improve the stability of a
perishable product or make the product easier to
store or transport
Many food products (e.g., coffee, fruits,
vegetables, meats, and ice cream) can be freeze-
dried and subsequently stored at room
temperature.
In the lyophilization process, the temperature and
pressure conditions within the lyophilizer are
controlled to enable the sublimation of water.
PHASE DIAGRAM
A phase
diagram for a
substance
describes the
solid, liquid, and
gaseous states
of a substance
as a function of
temperature
and pressure
DRUM DRIER or ROLLER
DRIER

Single
Double- Rotates towards each other
Twin Rotates away from each other

Drums are heated from inside with staem
They are usually made of stainless steel.
Speed of rotation is 10 rpm.
The drums have a nip where the drums
come close together.
This clearance determines the thickness of
the applied food layer.
Each drum has a doctors knife along the
lengthe of the drum.
Temp. is 100-150 0C
As the food layer rotates it loses moisture
and the dry powder is collected in the trays.
liquid food, purees, milk, potato mash,
baby food, sambhar slurry.

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