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    A Micro-Method of Determining The Boiling Point of

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    Dekace pohuwato
    This document describes a micro-method for determining the boiling point of liquids. The method involves placing a liquid in a micro test tube attached to a thermometer and suspended in a beaker of water or glycerol heated on a tripod stand. Bubbles form when the liquid reaches its boiling point. Students determine the boiling points of acetone, chloroform, and isopropyl alcohol using this method. The document also provides exercises asking students to explain advantages of the method and differences in reported versus measured boiling points.

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    A Micro-Method of Determining The Boiling Point of

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    Dekace pohuwato
    109 views8 pages
    This document describes a micro-method for determining the boiling point of liquids. The method involves placing a liquid in a micro test tube attached to a thermometer and suspended in a beaker of water or glycerol heated on a tripod stand. Bubbles form when the liquid reaches its boiling point. Students determine the boiling points of acetone, chloroform, and isopropyl alcohol using this method. The document also provides exercises asking students to explain advantages of the method and differences in reported versus measured boiling points.

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    A Micro-method of Determining the Boiling Point Of

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    This document describes a micro-method for determining the boiling point of liquids. The method involves placing a liquid in a micro test tube attached to a thermometer and suspended in a beaker of water or glycerol heated on a tripod stand. Bubbles form when the liquid reaches its boiling point. Students determine the boiling points of acetone, chloroform, and isopropyl alcohol using this method. The document also provides exercises asking students to explain advantages of the method and differences in reported versus measured boiling points.

    Copyright:

    © All Rights Reserved
    Download as PPTX, PDF, TXT or read online from Scribd
    Download as pptx, pdf, or txt
    109 views8 pages

    A Micro-Method of Determining The Boiling Point of

    Uploaded by

    Dekace pohuwato
    This document describes a micro-method for determining the boiling point of liquids. The method involves placing a liquid in a micro test tube attached to a thermometer and suspended in a beaker of water or glycerol heated on a tripod stand. Bubbles form when the liquid reaches its boiling point. Students determine the boiling points of acetone, chloroform, and isopropyl alcohol using this method. The document also provides exercises asking students to explain advantages of the method and differences in reported versus measured boiling points.

    Copyright:

    © All Rights Reserved
    Download as PPTX, PDF, TXT or read online from Scribd
    Download as pptx, pdf, or txt
    of 8

    A MICRO-METHOD OF

    DETERMINING THE BOILING


    POINT OF A LIQUID

    KELOMPOK 2
    Discussion
    The boiling point od a liquid is the temperature
    at which it’s vapour pressure equals the
    atmospheric pressure exerted on it. As pure
    organic compounds have definite boiling points,
    their determination provides valuable information
    for the identification of organic compounds.
    Boiling points can also indicate the state of purity
    of compounds.
    In this experiment, we use a micro-method of
    determining the b.p. of a compound.
    Procedure

    Fill a 100 cm3 beaker with 60 cm3 of water (or glycerol) and
    place it over a wire gauze supported by a tripod stand. Next, tie a
    micro* test tube to a thermometer with a rubber band (see Figure
    2). Introduce five or six drops of aceton (b.p. = 56.2 ˚C) into the
    test tube. Clamp the thermometer so that the bulb of the
    thermometer and part of the micro test tube are immersed in the
    water (or glycerol). Place a sealed capillary tube in the micro test-
    tube as shown in the diagram.
    Heat the beaker and stir constantly. When a steady stream of
    bubbles comes out of the capillary tube, remove the flame.
    Continue stirring until the aceton begins to enter the capillary
    tube. Note the temperature. This is the b.p. of aceton.
    Repeat the procedure with chloroform (trichloromethane)
    (b.p. = 61 ˚C) and isopropyl alcohol (propan-2-ol) (b.p. = 83 ˚C).
    Exercise

    What adventages does this method of b.p. determination


    give ?
    In an experiment, a student found that the b.p. of acetone
    was 2 ˚C higher than it’sreprted value whereas those of
    chloroform (trichloromethane) and carbon tetrachloride
    (tetrachloromethane) were nearly the same as the reported
    value. Can you give an explenation ?
    Why is the b.p. of a liquid containing a little dissolved solid
    higher than the b.p. of the pure liquid itself ?
    What experiment would you carry out to show that constant
    boiling HCl is a mixture and not a pure compound ?
    Translate

    METODE MIKRO
    DARI PENENTUAN
    TITIK DIDIH
    SUATU CAIRAN
    Diskusi

    Titik didih cairan adalah suhu di mana tekanan


    uapnya sama dengan tekanan atmosfer yang diberikan
    padanya. Karena senyawa organik murni memiliki
    titik didih yang pasti, penentuannya memberikan
    informasi yang berharga untuk identifikasi senyawa
    organik. Titik didih juga dapat menunjukkan keadaan
    kemurnian senyawa.

    Dalam percobaan ini, kami menggunakan metode


    mikro untuk menentukan titik didih dari suatu
    senyawa.
    Prosedur Kerja

     Memasukkan 60 cm3 gliserol kedalam gelas beaker berukuran 100 cm3 ,


    kemudian letakkan gelas beaker yang sudah terisi larutan di atas tripod yang di
    lapisi dengan kasa kawat.
     Mengikat tabung uji mikro dengan termometer menggunakan karet gelang
    (lihat gambar 2)
     Menambahkan 5 atau 6 tetes aseton (titik didih 56,2 ˚C)
     Menjepit termometer sehingga bohlam termometer dan bagian dari tabung uji
    mikro terendam dalam gliserol
     Tempatkan tabung kapiler tertutup dalam tabung uji mikro.
     Panaskan gelas kimia yang berisi larutan dengan di aduk secara terus menerus.
     Saat aliran gelembung yang stabil keluar dari tabung kapiler, matikan
    pemanas.
     Lanjutkan mengaduk sampai aseton mulai memasuki tabung kapiler.
    Perhatikan suhunya. Ini adalah titik didih dari aseton.
     Ulangi prosedur 1-8 dengan kloroform (triklorometana)(titik didih 61˚C) dan
    isopopil alkohol (propan-2-ol) (titik didih 83˚C)
    Latihan

     apa kelebihan dalam metode penentuan titik didih ini ?


     Dalam percobaan, seorang siswa menemukan bahwa titik didih aseton adalah 2
    ˚C lebih tinggi dari nilai yang dilaporkan, sedangkan kloroform
    (triklorometana) dan karbon tetraklorida (tetraklorometana) hampir sama
    dengan nilai yang dilaporkan. Bisakah Anda memberi penjelasan?
     Mengapa titik didih cairan yang mengandung padatan terlarut sedikit lebih
    tinggi dari titik didih cairan murni itu sendiri?
     Percobaan apa yang akan Anda lakukan untuk menunjukkan bahwa HCl
    mendidih konstan adalah campuran dan bukan senyawa murni?
     
     
    Bacaan yang Disarankan
    Glasstone, S. Dasar Kimia Fisik. Edisi 1 (London: Macmillan, 1956) hlm. 144-146

    Shiner, R, L., Fuson, R. C, dan Curtin, D.Y. Identifikasi Sistematik Senyawa


    Organik. Edisi ke 4 (New York: John Wiley & Sons Inc., 1956) hlm.32.34

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