Model CFA3018

PDS 71-Hydrazine3018/rev.B

Product Data Sheet

September 2011

On-Line Hydrazine Analyzer

One Button Operation. One button starts, calibrates, and puts the analyzer on-line. Multiple Sample Option. Measure as many as six sample streams sequentially. Routine Maintenance takes five minutes every three months. Self-Diagnostics. The analyzer monitors critical functions and alerts the user when a problem exists. Pre-Packages Reagents and Standards. No messy chemical solutions to prepare and standardize. Reagents and standards come from the factory ready-to-use.

Analyzer shown with front covers removed

Applications
The Model CFA3018 Hydrazine analyzer is intended for the determination of hydrazine in boiler feedwater.

Features and Benefits

Simplicity, ease-of-use, and reliable operation characterize the Model CFA3018 Valve-Pump hydrazine analyzer. Place colorcoded reagent straws in color-coded reagent bottles, place the blank and standard straws in the appropriate bottles, and press a button. The analyzer automatically calibrates and puts itself in service. Once in service, the analyzer runs a blank and full scale standard twice a week. Routine maintenance is simple. Replace reagents and standards every three months. Replace the valve pump, the key to the reliable performance and low maintenance of the Model CFA3018, every two years. Total maintenance time is at most one hour per year.

Using an optional built-in stream selector, the Model CFA3018 can measure as many as six sample streams sequentially. A single analog output is standard. A stream identification marker indicates the start of each new sample. A multiple output option in which a separate analog output is assigned to each sample stream is also available. With the multiple output option each output holds the last value until updated. The Model CFA3018 Hydrazine Analyzer has a pumped reagent delivery system. Instrument air, needed for pressurized systems, is unnecessary. The Model CFA3018 uses a batch measurement technique. The update rate is approximately every 12 minutes.

Model CFA3018

September 2011

Principles of Operation
The heart of the CFA3018 Hydrazine analyzer is the valve pump. The valve pump has separate pumping elements for sample, reagents, and standards. Each pump element consists of a chemically inert flexible membrane in a cavity. Cavity volumes are 5 mL for sample and standards and 0.2 mL for reagents. A vacuum/ pressure pump pushes and pulls on the membrane. Vacuum causes the chamber to fill. Pressure pushes the liquid out of the cavity into the reaction chamber. Check valves prevent backflow. A stream of air pumped into the reaction chamber mixes the sample and reagents. After the reaction time has passed, the treated sample is pumped to the measurement cell. Light at 460 nm from an LED passes through the sample and a photodiode measures the light intensity. The analyzer automatically calculates the absorbance and translates the results into a hydrazine concentration reading. Once the measurement is complete, repeated flushes with fresh sample remove the treated sample from the measurement and reaction cells.

Specifications
Ranges: 0-100 ppb, 0-200 ppb Method: Hydrazine is determined colorimetrically using the p-dimethylaminobenzaldehyde method. Sampling Method: Batch; update rate is approximately every 12 minutes. Precision: 1% of full scale Detection limit: 1% of full scale Calibration standards: zero and full-scale standard for each measurement range. Automatic calibration: Blank and full scale: every 72 hours, requires about 40 min. Reagent consumption: 5 L of each reagent every 3 months Standard consumption: 5 L of standard and 5 L of baseline solution every 3 months Sample requirements: Flow: 10-15 mL/min (minimum) Pressure: <10 psig (<170 kPa) (overflow cup must drain to atmosphere) Temperature: 0-50C (32-122F) Filter: 8 micron filter in sample inlet line is recommended. Multiple sample option: Up to six sample streams, measured sequentially. Single output (standard): Output corresponds to sample currently being measured. A stream identification marker on a chart recorder indicates the start of each new sample. Multiple output (optional): Each sample has its own output. The output holds last value when the analyzer changes to the next sample stream.

Outputs: 4-20 mA or 0-5 Vdc (non-isolated). Isolated output is optional. Load requirements for 4-20 mA output: 450 W (minimum), 1200 W (maximum). Load requirement for 0-5 Vdc output: 10kW (minimum). Outputs are not scalable. The range of the outputs is the same as the measurement range. Parallel output for printer. Standard on multi-stream instrument. Optional on single stream instrument. RS232C output is standard on multi-stream instrument, optional on single stream instrument. Alarms: General: process alarms for streams 1 through 6, leak detection, LED failure, and calibration in progress. Stream 1: separate high and low alarm relays; contacts are rated 2 A at 250 Vac or 3 A at 30 Vdc; delay on/off time is 1 min. Streams 2 through 6 (multiple output option): one alarm relay for each stream; alarm can be configured as high or low; contacts have dc ratings only: 100 Vdc (maximum), 10 VA (maximum), 1.0 amp (maximum - carry only), 0.5 amp (maximum - switched); delay on/off time is 1 min. Display: Single line LCD; 4 1/2 digits; readout in concentration units. For multi-stream option, display remains at last value until new stream reading is stable. Status LEDs: for leak, source LED failure, hours remaining before maintenance, and calibration in progress; for multi-stream analyzers, status LEDs show the sample stream currently valved in and the sample stream for which data is being displayed.

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September 2011

Model CFA3018
Panel mounting: Allow 12 in. (305 mm) on both sides for access to input/output panel and overflow sampler. Weight: 117 lb (53 kg). Add up to 60 lb (27 kg) for full weight of reagents and standards. Shipping Weight of Analyzer: 147 lb (67 kg) Shipping Weight of Reagents: 64 lb (29 kg) for three months supply Power: Standard: 115 Vac (10%), 60 Hz, 3 Amp Optional: 230 Vac (10%), 50 Hz, 1.5 Amp Agency Approvals: IEC 61326

Environmental: Install in a clean, indoor environment. Ambient temperature: 10-45C (50-113F). Avoid temperature swings greater than 5C (10F) over a twelve-hour period. Humidity: 5-95% (non-condensing). Not for outdoor use. Dimensions: Height of analyzer cabinet: 25.75 in. (654 mm) Height of reagent cabinet: 18.25 in. (464 mm) Width: 18 in. (457 mm) includes hinges Depth: 16 in. (406 mm) includes rear mounting bracket Space Requirements: Wall mounting: Allow 18 in. (457 mm) on one side for swing out access to rear panel. Allow 12 in. (305 mm) on the other side for access to input/output panel and overflow sampler.

Ordering Information
Model CFA3018 is a batch analyzer suitable for the determination of hydrazine in the range 0-100 ppb or 0-200 ppb. Range must be specified at time of ordering. A single, non-isolated output is standard. Isolated outputs and multiple outputs (one output for each sample stream) are available as options and must be specified at time of ordering. 115 Vac, 60 Hz is standard; 230 Vac, 50 Hz must be specified at time of ordering. The analyzer is shipped with a three-month supply of reagents and standards. Model 185 CODE 185-A015 CODE 01C 02C 03C 04C 05C 06C CODE -N1 CODE -N2 CODE -N3 CODE -N4 185-A015 On-Line Analyzer Measurement ( required selection) On-line analyzer for hydrazine Number of Sample Streams (required selection) One stream Two streams Three streams Four streams Five streams Six streams Output isolation No isolation Isolated outputs Outputs Single output Multiple outputs equal to number of sample streams RS232C interface No RS232C interface RS232C interface for remote communications Power 115 VAC 60 Hz 230 VAC 50 Hz -01C -N1 -N4 Example

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Rosemount Analytical 3 3

Model CFA3018
PDS 71-Hydrazine3018/rev.B

Product Data Sheet

September 2011

Parts and Accessories

Part Number 185-3018-30 185-3047-61 185-1341-08 NOTE: Description CFA-3018 hydrazine reagents and standards, 3 months, 0-100 ppb CFA-3018 hydrazine reagents and standards, 3 months, 0-200 ppb Disposable cartridge filter (for overflow assembly)

A biannual reagent and valve pump service contract is available and is recommended. To order the reagent and pump service contract, provide a blanket purchase order for eight reagent and standard kits (two-year supply). The kits will be sent in regular intervals over the 24-month period. Once during the 24-month period you will be entitled to a valve pump refurbishment. Contact Rosemount Analytical for details concerning the valve pump refurbishment.

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Emerson Process Management Rosemount Analytical 2400 Barranca Parkway Irvine, CA 92606 USA T 949 757 8500 F 949 474 7250 http://www.raihome.com 2011 Emerson Process Management. All rights reserved.

The Emerson logo is a trademark and service mark of Emerson Electric Co. Rosemount Analytical isa mark of one of the Emerson Process Management family of companies. All other marks are the property of their respective owners. The contents of this publication are presented for information purposes only, and while effort has been made to ensure their accuracy, they are not to be construed as warranties or guarantees, express or implied, regarding the products or services described herein or their use or applicability. All sales are governed by our terms and conditions, which are available on request. We reserve the right to modify or improve the designs or specifications of our products at any time without notice.