Construction and Building Materials: Md. Safiuddin, J.S. West, K.A. Soudki
Construction and Building Materials: Md. Safiuddin, J.S. West, K.A. Soudki
Construction and Building Materials: Md. Safiuddin, J.S. West, K.A. Soudki
a r t i c l e
i n f o
Article history:
Received 19 January 2010
Received in revised form 19 April 2010
Accepted 19 June 2010
Keywords:
Flowing ability
Flow spread
High-range water reducer
Mortar
Rice husk ash
Self-compacting concrete
Waterbinder ratio
a b s t r a c t
This paper presents the owing ability of the mortars formulated from various self-compacting concretes
(SCCs) incorporating rice husk ash (RHA). The mortars were produced with different RHA contents and
waterbinder (W/B) ratios, as used in their parent SCCs. The owing ability of the mortars was determined with respect to the ow spread at various dosages of a polycarboxylate based high-range water
reducer (HRWR). The effects of RHA, W/B ratio, and HRWR on the owing ability of mortars were
observed. The mortar owing ability decreased with the higher RHA content and W/B ratio, but increased
with the greater HRWR dosage. However, the excessive HRWR dosages were not conducive to the mortar
owing ability due to the segregation problem in the form of bleeding. The overall mortar owing ability
results were useful to examine the suitability of RHA, and to x the HRWR dosages for different SCCs.
2010 Elsevier Ltd. All rights reserved.
1. Introduction
Self-compacting concrete (SCC) is a special concrete that provides excellent owing ability in fresh state [1,2]. The owing ability is a workability property of SCC that allows it to ll the spaces
in formwork and pass between congested reinforcing bars under
self-weight, and without any means of compaction [3,4]. The owing ability of SCC can be assessed based on the ow time and
spread of concrete obtained from different tests [5].
The owing ability of SCC depends on its constituent materials
and mixture composition. In general, high-range water reducer
(HRWR) improves the owing ability of SCC. However, the excessive dosage of HRWR provides a very high uidity that may cause
segregation problems in the form of bleeding, aggregate piling, and
aggregate sedimentation. In such cases, an appropriate supplementary cementing material (SCM) can be used to improve the segregation resistance, while maintaining an excellent owing ability
in fresh SCC. Most common SCMs such as y ash, silica fume, slag,
and limestone powder have been used to produce SCC with a good
owing ability [6,7]. Similarly, rice husk ash (RHA) can be used in
SCC. RHA is obtained by burning rice husks, which are generated in
the rice milling industry as agricultural wastes during the processing of paddy rice. In rice producing countries, about 120 million
metric tons of rice husks are available annually for disposal [4].
* Corresponding author. Tel.: +1 519 888 4567x37128; fax: +1 519 888 4349.
E-mail address: [email protected] (Md. Sauddin).
0950-0618/$ - see front matter 2010 Elsevier Ltd. All rights reserved.
doi:10.1016/j.conbuildmat.2010.06.084
974
Table 2
Mortar formulations and designations.
Series
Mortar type
Parent concrete
W/B ratio
RHA (% B)
M30-RHA0
M30-RHA15
M30-RHA20
M35-RHA0
M35-RHA15
M35-RHA20
SCC30-RHA0-AC6
SCC30-RHA15-AC6
SCC30-RHA20-AC6
SCC35-RHA0-AC6
SCC35-RHA15-AC6
SCC35-RHA20-AC6
0.30
0.30
0.30
0.35
0.35
0.35
0
15
20
0
15
20
M35-RHA10
M35-RHA25
M35-RHA30
M40-RHA0
M40-RHA15
M40-RHA20
SCC35-RHA10-AC6
SCC35-RHA25-AC6
SCC35-RHA30-AC6
SCC40-RHA0-AC6
SCC40-RHA15-AC6
SCC40-RHA20-AC6
0.35
0.35
0.35
0.40
0.40
0.40
10
25
30
0
15
20
M35-RHA0a
M35-RHA0b
M35-RHA15a
M35-RHA15b
M35-RHA20a
M35-RHA20b
SCC35-RHA0-AC4
SCC35-RHA0-AC8
SCC35-RHA15-AC4
SCC35-RHA15-AC8
SCC35-RHA20-AC4
SCC35-RHA20-AC8
0.35
0.35
0.35
0.35
0.35
0.35
0
0
15
15
20
20
2. Experimental studies
2.1. Constituent materials
Pit sand (S), normal (ASTM Type I) portland cement (C), amorphous RHA, normal tap water (W), and a polycarboxylate based HRWR were used to produce various mortars. Pit sand was incorporated in mortar mixtures to act as ne aggregate.
Cement and RHA acted as the binder (B). The RHA was collected from North Carolina, USA. The RHA particles were angular and much ner than cement. The median
particle size of RHA was 6 lm, whereas that of cement was 15 lm. The major physical properties of pit sand, cement, RHA and HRWR are given in Table 1.
Table 3
Mortar mixture proportions (mortar volume: 3 l).
Mortar type
M30-RHA0
M30-RHA15
M30-RHA20
M35-RHA0
M35-RHA15
M35-RHA20
M35-RHA10
M35-RHA25
M35-RHA30
M40-RHA0
M40-RHA15
M40-RHA20
M35-RHA0a
M35-RHA0b
M35-RHA15a
M35-RHA15b
M35-RHA20a
M35-RHA20b
a
b
Sand
(kg)
Cement
(kg)
RHA
(kg)
Water
(kg)
HRWR dosage (% B)
Dsa
D ub
4.03
3.91
3.88
4.25
4.14
4.11
4.18
4.08
4.04
4.41
4.32
4.29
4.31
4.19
4.20
4.08
4.17
4.05
2.36
1.99
1.86
2.06
1.73
1.63
1.84
1.52
1.42
1.82
1.54
1.45
2.02
2.09
1.71
1.76
1.60
1.65
0.00
0.35
0.47
0.00
0.31
0.41
0.20
0.51
0.61
0.00
0.27
0.36
0.00
0.00
0.30
0.31
0.40
0.41
0.71
0.70
0.70
0.72
0.71
0.71
0.72
0.71
0.72
0.73
0.72
0.72
0.71
0.73
0.70
0.73
0.70
0.72
1.25
2.50
3.00
1.00
2.00
2.50
1.50
3.00
3.50
0.75
1.25
1.50
1.00
1.00
2.00
2.00
2.50
2.50
1.002.00
1.503.00
2.004.00
0.751.75
1.252.50
1.503.00
1.002.00
1.753.50
2.504.50
0.501.50
1.002.00
1.503.00
0.751.75
0.751.75
1.252.50
1.252.50
1.503.00
1.503.00
signicant loss of materials and labor. The mortar proportions given in Table 3
are based on this volume, except for the HRWR dosages. HRWR was used in the
mortars as an additive. The dosages of HRWR for the mortars were varied in the
vicinity of saturation dosages. The detailed procedure for determining the saturation dosages of HRWR is given in a previous publication by Sauddin et al. [5].
The HRWR dosages smaller than the lower limits as shown in Table 3 were not used
to avoid the mixing and handling difculties of the mortars.
Table 1
Major physical properties of sand, cement, RHA, and HRWR.
Material
Properties
975
The mortars were prepared using an epicyclic revolving type small mechanical
mixer conforming to ASTM C 305 [17]. The volume of the mortars prepared was 3 l.
Before batching, the water correction was done considering the absorption of sand
and the water contribution of HRWR. Accordingly, the proportions of sand and mixing water were adjusted. These adjustments were required since the air-dry pit
sand and liquid HRWR were used in preparing the mortars. Nevertheless, the sand
and binder (cement alone or with RHA) were taken in the mixing bowl, and drymixed for 60 s using a stainless steel spoon. The mixing water was added into the
bowl and a rest period of 30 s was allowed for absorption by the sand. Then the
mixer was started and the initial dosage of HRWR was gradually added to the mortar within 510 s. The initial wet mixing of mortar was carried out for 60 s. Later the
mixer was stopped, and the mortar was quickly scraped from the side and bottom
of the mixing bowl over a period of 30 s. The mixer was restarted and run for 60 s.
Thereafter, the mixer was stopped again, the mortar from the bottom and side of
the bowl was scraped, and the mortar agglomerates were broken if any over a period of 30 s. The mixer was restarted again and the mixing was continued for 60 s.
Later, the subsequent dosages of HRWR were used to vary the owing ability of
the mortars. For each incremental HRWR dosage, further mixing was conducted
for 60 s. In all stages, the mixing was conducted at a slow speed to minimize the
entrapped air content in mortars.
2.5. Testing of mortars
The mortars were tested to examine the owing ability with respect to ow
spread. The mortar ow spread test is a smaller version of the concrete slump ow
test. The slump ow test is widely used as a standard test for the owing ability of
SCC. A good relationship has been observed between the ow spread of mortar and
the slump ow of concrete [12,13]. Hence, the mortar ow spread test may provide
an indication for the probable slump ow of SCC.
315
310
305
300
295
290
285
280
M30-RHA0
M30-RHA15
M35-RHA0
M35-RHA15
0.5
1.5
2.5
M30-RHA20
M35-RHA20
3.5
4.5
HRWR dosage (% B)
Fig. 2. Flow spread of various mortars under series 1 (W/B = 0.300.35; RHA = 0
20%).
320
315
M35-RHA10
M35-RHA25
M35-RHA30
M40-RHA0
M40-RHA15
M40-RHA20
310
305
300
295
290
285
280
Test setup
0.5
1.5
2.5
3.5
4.5
HRWR dosage (% B)
Fig. 3. Flow spread of various mortars under series 2 (W/B = 0.350.40; RHA = 0
30%).
330
325
320
315
310
305
M35-RHA0a
300
M35-RHA0b
M35-RHA15b
290
M35-RHA20a
285
280
M35-RHA15a
295
M35-RHA20b
0.5
1.5
2.5
3.5
4.5
HRWR dosage (% B)
Fig. 4. Flow spread of various mortars under series 3 (W/B = 0.35; RHA = 020%).
976
the mortars increased with the greater dosages of HRWR. It indicates that the deformability of the mortars increased with the
higher dosages of HRWR. This is mostly attributed to the liquefying
and dispersing actions of the HRWR. The liquefying action of
HRWR decreases the ow resistance and consequently increases
the ow spread of mortar. In addition, more free water becomes
available in the mortar due to the dispersing action of HRWR, thus
resulting in a greater ow spread.
The effect of HRWR on the ow spread of the mortars was also
examined by visual inspection. The excessive HRWR dosage (equal
to or greater than saturation dosage) was not conducive to the ow
spread of the mortars. In general, the increase in ow spread was
insignicant beyond the saturation dosage. Furthermore, signicant bleeding (a form of segregation) occurred in most of the mortars and the bleed water appeared at the periphery of the ow
spread when the HRWR dosages exceeded the saturation dosage
(refer to Table 5). In few cases, the bleeding took place when the
HRWR dosage was equal to the saturation dosage. For example,
the onset of bleeding occurred in M40-RHA0 mortar for the HRWR
dosage of 0.75% (saturation dosage), as evident from Fig. 5. Based
on the results of visual inspection, it is recommended that the
use of HRWR at or above saturation dosage should be avoided to
prevent bleeding, thus improving the uniformity of mortar. The
overall results of visual inspection also suggest that a HRWR dosage lower than saturation dosage should be used to improve the
uniformity of concrete without any form of segregation.
3.2. Effect of W/B ratio
The effect of W/B ratio on the owing ability of the mortars was
examined based on the ow spreads obtained at the saturation
dosages of HRWR. The saturation ow spreads of the mortars under series 1 and 2 were noted from Figs. 2 and 3, and are plotted
in Fig. 6 for different W/B ratios. The saturation ow spreads of
the mortars under series 3 were not considered in this gure, because they were formulated from the SCCs containing different
air contents (4% and 8%). Nevertheless, it can be seen from Fig. 6
that the saturation ow spread decreased with the increase in
W/B ratio. This is mostly due to the lower paste volume and greater
sand content. At the higher W/B ratio, the paste volume decreased
Table 5
Results of visual inspection on the ow spread of mortars.
Table 4
Various mixture parameters of mortars.
Mortar type
sa
(10
M30-RHA0
M30-RHA15
M30-RHA20
M35-RHA0
M35-RHA15
M35-RHA20
M35-RHA10
M35-RHA25
M35-RHA30
M40-RHA0
M40-RHA15
M40-RHA20
M35-RHA0a
M35-RHA0b
M35-RHA15a
M35-RHA15b
M35-RHA20a
M35-RHA20b
a
b
c
d
bb
3
m3/m3) (10
514
499
494
542
529
524
533
520
516
563
551
547
549
534
536
521
532
516
249
266
272
218
233
238
228
243
248
193
207
211
214
221
229
237
234
242
Abc
3
pd
486
501
506
458
471
476
467
480
484
437
449
453
451
466
464
479
468
484
a
b
Mortar type
Dsa (% B)
Dub (% B)
M30-RHA0
M30-RHA15
M30-RHA20
M35-RHA0
1.25
2.5
3
1
1.002.00
1.503.00
2.004.00
0.751.75
M35-RHA15
M35-RHA20
M35-RHA10
M35-RHA25
M35-RHA30
M40-RHA0
2
2.5
1.5
3
3.5
0.75
1.252.50
1.503.00
1.002.00
1.753.50
2.504.50
0.501.50
M40-RHA15
1.25
1.002.00
M40-RHA20
M35-RHA0a
1.5
1
1.503.00
0.751.75
M35-RHA0b
M35-RHA15a
M35-RHA15b
M35-RHA20a
M35-RHA20b
1
2
2
2.5
2.5
0.751.75
1.252.50
1.252.50
1.503.00
1.503.00
977
320
310
300
290
280
270
260
250
240
0.275
0.3
0.325
0.35
0.375
0.4
0.425
W/B ratio
Fig. 6. Effect of W/B ratio on the ow spread of mortars.
Mortar type
whereas the sand content was increased, as can be seen from Table
4. The dispersion of the sand particles is hindered with the lower
paste volume and greater sand content. The decreased paste vol-
285
290
295
300
305
310
315
320
978
Acknowledgements
3.4. Use of the owing ability results of mortars
The mortar owing ability results primarily revealed the effects
of various HRWR dosages, RHA contents, and W/B ratios. These results were useful to observe the effects of the saturation dosages of
HRWR, and consequently to decide the appropriate HRWR dosages
for various SCC mixtures. It was understood based on the mortar
owing ability results that a HRWR dosage less than its saturation
dosage should be used to enhance the uniformity of concrete without any kind of segregation. In general, the HRWR dosages in the
range of 7080% of saturation dosage should be used for SCC. The
owing ability results of the mortars were also helpful to examine
the suitability of RHA, and to select the proper RHA contents for
various SCC mixtures.
4. Conclusions
The following conclusions can be drawn based on the results of
the present study for the owing ability of different mortars formulated from various SCC mixtures including RHA:
a. The owing ability of the mortars with regard to ow spread
was increased with the greater dosages of HRWR, which
improved the deformability of mortar by its liquefying and
dispersing actions.
b. The increase in mortar ow spread was not signicant
beyond the saturation dosage of HRWR. The bleeding
occurred in most cases when the HRWR dosage was higher
than the saturation dosage.
c. The owing ability or ow spread of the mortars was inuenced by their mixture composition. Particularly, the sand
content and binder surface area greatly inuenced the ow
spread of the mortars by affecting the availability of free
water in mortar mixture.
d. The owing ability, that is, the ow spread of the mortars
decreased with the increased W/B ratio due to the greater
sand content and lower paste volume that hindered the dispersion of sand particles.
e. The owing ability of the mortars with regard to ow spread
decreased with the increased RHA content due to the greater
volume fraction and surface area of the binder. In particular,
the increased surface area greatly reduced the owing ability by decreasing the amount of free water in mortar.
f. The RHA contents greater than 15% signicantly decreased
the ow spread of mortar. Also, the mixing and handling
difculties were experienced for the mortars with a RHA
content higher than 15%. Thus, a RHA content greater than
15% was not suitable to achieve a good owing ability in
mortar.
g. The mortar owing ability results were useful to select the
proper HRWR dosages and RHA contents for various SCC