Ad-A234 566
Ad-A234 566
Ad-A234 566
Geotechnical Laboratory
DEPARTMENT OF THE ARMY
Waterways Experiment Station, Corps of Engineers
3909 Halls Ferry Road, Vicksburg, Mississippi 39180-6199
-P- 3, 1991
March 1991
Final Report
91 4 *2-09
The following two letters used as part of the number designating technical reports of research published under the Repair,
Evaluation, Maintenance, and Rehabilitation (REMR) Research Program identify the problem area under which the report
was prepared:
Problem Area Problem Area
COVER PHOTOS:
TOP - Placing plastic concrete in triaxial mold.
MIDDLE - Plastic concrete test specimen.
BOTTOM - Triaxial compression test chamber.
Form AppOved
REPORT DOCUMENTATION PAGE 0MB No. 0704-0188
COllecion Of information. enuigsgetosfr.ddgUe udn oWsigo eadquarterServices.Ogretorae Infor.monOperatinsan Aporb. 5215 eferson
1. AGENCY USE ONLY (Leave blank) 12. REPORT DATE 993 REPORT TYPE AND DATES COVERED
6. AUTHOR(S)
Thomas W. Kahl
Joseph L. Kauschinger WU 32310
Edward B. Perry
7. PERFORMING ORGANIZATION NAME(S) AND ADORESS(ES) B. PERFORMING ORGANIZATION
REPOUT NUMBER
US Army Engineer Waterways Experiment Station
Geotechnical Laboratory Technical Report
3909 Halls Ferry Road, Vicksburg, MS 39180-6199 REMR-GT-15
for cutoff walls due to limited documentation of field performance of existing cutoff
walls and lack of laboratory test data on plastic concrete under test conditions which
approximate field behavior.
This research was conducted to quantify the stress-strain-strength behavior and
permeability of plastic concrete, and to develop design data for specifying plastic con-
crete for use in a diaphragm cutoff wall for an earth dam. The results of this research
indicate that the addition of bentonite clay to conventional concrete significantly
increases the ductility and plastic deformation of the concrete while simultaneously
reducing its shear strength. The permeability of plastic concrete was found to be the
same or less than conventional concrete, and it decreased significantly with consolida-
tion. A design method is given for determining the mix design of a plastic concrete
cutoff wall based upon the unconfined compressive strength and/or modulus of the embank-
ment soil.
PREFACE
44
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CONTENTS
Page
PREFACE ................................................................ 1
CONVERSION FACTORS, NON-SI TO SI (METRIC)
UNITS OF MEASUREAENT..................................................... 4
PART I: INTRODUCTION ................................................... .5
Purpose .............................................................. 5
Scope of Work ........................................................ 6
PART II: LITERATURE REVIEW ............................................. 10
General Observations of Recent Plastic Concrete Research ......... 10
Major Plastic Concrete Research Programs ............................ 13
Plastic Concrete Cutoff Wall Field Case Studies .................... 17
PART III: LABORATORY TESTING TECHNIQUE .................................. 24
Materials ............................................................ 24
General Concrete Fabrication Procedure .............................. 25
Unconfined Compression Test Procedure ............................... 31
Brazilian Splitting Tensile Test Procedure ......................... 41
Flexural Beam Test Procedure ........................................ 42
Erodability Test Procedure .......................................... 43
Triaxial Testing Equipment .......................................... 46
Q Test Procedure ..................................................... 53
CIUC Test Sample Setup and Consolidation Procedure ............... 55
Permeability Test Procedure ......................................... 62
CIUC Shear Test ...................................................... 66
PART IV: UNCONFINED TEST RESULTS ....................................... 67
Unconfined Compression Test Data Analysis ........................... 67
Results of Unconfined Compression Test Series ...................... 70
Error Analysis of Unconfined Compression Tests ..................... 73
Conclusions from Unconfined Compression Tests ...................... 74
Results of Other Unconfined Tests ................................... 75
PART V- TRIAXIAL AND PERMEABILITY TEST RESULTS ....................... 78
Results of CIUC Tests ............................................... 79
Results of Unconsolidated Undrained Compression Tests ............ 81
Results of Permeability Tests ....................................... 83
PART VI: ANALYSIS AND DISCUSSION ....................................... 85
Relationship of Unconfined Compressive Strength and Splitting
Tensile Strength to Cement Factor and Water-Cement Ratio ....... 85
Relationship of Elastic Modulus and Strain at Failure to
Unconfined Compressive Strength................................... 91
Relationship Between Unconfined Compressive Strength and
Splitting Tensile Strength........................................ 92
Effect of Curing Age and Bentonite Content on Unconfined
Compressive Strength.............................................. 93
Effect of Consolidation on Cement Factor and Water-Cement
Ratio .............................................................. 95
2
Page
Effect of Bentonite Content on Pore Pressure Generation and
Stress Path ........................................................ 96
Relationship Between Triaxial Stress-Strain-Strength
Behavior and Unconfined Stress-Strain-Strength Behavior ........ 103
Comparison of a CIUC Test and a Q Test Having the Same Cement
Factor, Bentonite Content, and Water-Cement Ratio Tested
at the Same Age ................................................... 107
Influence of Bentonite Content, Confining Stress, Consolidation,
and Age on Triaxial Stress-Strain-Strength Behavior of
Plastic Concrete .................................................. 108
Permeability of Plastic Concrete ................................... 113
PART VII: SUMMARY AND RECOMMENDATIONS .................................. 115
3
CONVERSION FACTORS, NON-SI TO SI (METRIC)
UNITS OF MEASUREMENT
Multiply By To Obtain
cubic feet 0.02831685 cubic metres
cubic yards 0.7645549 cubic metres
4
PLASTIC CONCRETE CUTOFF WALLS FOR EARTH DAMS
PART I: INTRODUCTION
Purpose
plastic concrete for use as a remedial diaphragm cutoff wall material in earth
dams to control seepage. Many of the earth dams in the United States were
constructed during the Depression Era of the 1930's and immediately after
World War II. Today, many of these dams are over 50 years old, and a few have
severe leakage problems due to the erosion of core material. The potential
catastrophic failure of one of these dams due to piping creates a need for
effective and practical remedial seepage control solutions. One solution is
to install a deep, relatively thin concrete diaphragm wall along the axis of
an earth dam using the slurry trench method. This type of cutoff is usually
quite effective in controlling seepage. Examples of this type have been done
at Clemson Lower Diversion Dam, Mud Mountain Dam, Navajo Dam, and Fontenelle
Dam. Problems can arise, however, when conventional concrete is used as a
cutoff trench backfill material because of its inherent brittleness. Deforma-
tions of earth embankments due to fluctuations in impounded reservoir levels
or seismic activity can cause concrete cutoffs to develop cracks. New leakage
cutoff.
consists of aggregate, cement, water, and bentonite clay mixed at high water-
limited and/or poorly documented field performance data for plastic concrete
cutoffs. Thus, this research was conducted to quantify factors which influ-
5
Scope of Work
6
bentonite contents of 0, 20, and 60 percent
ages of 3 to 90 days
6 flexural beam tests
2 erodability tests (high velocity pinhole type)
the filter cake (EM 1110-2-1901, Figure 9-9)). At the completion of the exca-
vation, plastic concrete with a 8-in. slump is tremied into the excavation,
from the bottom upward, displacing the bentonite slurry to form the panel. As
the surface of the tremie plastic concrete rises, it may remove the filter
cake from the sides of the excavation. However, the relatively low permea-
bility of the adjacent soil, which was penetrated with bentonite slurry, will
prevent the free (unabsorbed) water in the plastic concrete panel from drain-
ing laterally. The water will be free to migrate upward through the plastic
concrete. The plastic concrete begins to set as soon as it is placed in the
excavation with stiffening occurring from the bottom of the panel upward. The
set of the panel will occur within a few hours, generally less than I day
(retarding admixtures can be used to prolong the set). Consolidation of the
plastic concrete panel under the vertical stress imposed by the weight of the
overlying plastic concrete (some of this stress will be taken by arching if
the sides of the excavation move laterally) will be completed in a matter of
days, the exact time depending on the depth of the plastic concrete cutoff
wall. After consolidation, the permeability of the plastic concrete will be
kplastic concrete - 10-8 to 10- 9 cm/sec (measured in this study). The plastic
concrete will continue to cure and gain strength following consolidation. Due
to the low permeability of the plastic concrete, very lictle migration of
water will occur within the plastic concrete cutoff wall after consolidation.
7
8. The laboratory stress-strain characteristics and strength behavior,
permeability, and erodability Fhould be obtained under test conditions which
approximate, as closely as possible, those which exist in the field. It was
not feasible (for this study) to form, consolidate, and test tensile strength
samples (Brazilian and Flexural Beam Test) and erodability samples (pinhole
type test) under conditions which would duplicate those existing in the field.
However, for permeability and compressive strength testing, this was feasible,
and plastic concrete specimens were formed in the triaxial chamber after
mixing, isotropically consolidated in the triaxial chamber with ertical
drainage, and cured in the triaxipl chamber under effective confining pres-
sures typical for existing cutoff walls (50 to 300 psi). Permeability tests
were conducted in the triaxial device during the curing phase (once gas gener-
ation within the sample had ceased). Following the permeability test, the
pore water pressure in the sample was given time to equalize, and the sample
was sheared under undrained conditions. In addition to the consolidated-
isotropic undrained compression (CIUC) triaxial tests described above, uncon-
solidated-undrained triaxial compression (Q) tests were conducted to determine
the effects of consolidation on the stress-strain characteristics and strength
behavior of plastic concrete (previous investigators had suggested that the
effects of consolidation could be simulated by forming a Q test sample at the
cement factor and water-content ratio a CIUC test sample would have at the end
of consolidation). Unconfined compression tests were conducted to correlate
with the more time-consuming and expensive CIUC tests.
9. The scope of Phase II tests was as follows:
20 CIUC Tests
6-in.-diam 12-in.-high sample size
cement factor of 300 lb/cu yd
bentonite contents of 0, 20, and 40 percent
effective confining pressures of 50, 100, 200, and 300 psi
ages of 3, 7, and 14 days
permeability tests
20 Q Tests
6-in.-diam 12-in.-high sample size
cement factor of 300 lb/cu yd
bentonite contents of 0, 20, and 40 percent
total confining pressures of 50. 100, 200, and 300 psi
ages of 3, 7, and 14 days
8
10. As a control, two unconfined compression tests and a splitting
tensile test were performed on the same material molded for each pair of CIUC
9
PART II: LITERATURE REVIEW
11. Although plastic concrete has been used to produce cutoff walls
with greater ductility than conventional concrete, relatively little published
13. Table 1 was constructed in order to compare mix designs and scopes
of work of various test programs. Different methods of describing plastic
concrete batch designs are used throughout the literature. To make compari-
sons of mix design possible, all of the mix design parameters of the research
programs listed in Table 1 were converted to cement factor, percentage ben-
inch.
14. For each test program listed in Table i, mix design parameters
percentage bentonite, cement factor, and water-cement ratio are presented
first along with slump and fine-coarse aggregate ratio. The scope of each
testing program is then summarized according to the type of tests performed,
number of tests performed, curing ages tested, and, if applicable, the range
15. The body of work lacks critical data necessary to evaluate the
range of behavior possible in plastic concrete for design in a cutoff wall.
The most glaring deficiency is the lack of CIUC testing. CIUC tests are
10
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12
Major Plastic Concrete Research Programs
19. This section contains summaries of each of the major plastic con-
crete research programs listed in Table 1. Some of the programs described
consisted of laboratory testing only. Other programs were conducted to
develop mix designs for specific earth dam cutoff walls. In addition, some of
the programs also examined the influence of adding other materials to
concrete.
13
a-a3 (kPa) 03= 300 kPa
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14
designs in Table Al are summarized in Tables A4 through A6. The permeability
of the mix designs tested was 4-40 *10-8. Other major conclusions were:
a. Permeability is independent of gradient and no significant
piping occurred at gradients up to 280.
b. The shear strength and initial tangent modulus increase as the
water-cement ratio decreases and as the effective consolidation
stress increases.
C. Strain at failure increases as consolidation stress increases.
15
Table 2
Summary of Batches Designs and Corresponding Shear Strength
and Strain Data from Bucknell University Research
Program (Evans 1987)
Propert0
1I 0.5 08 1 20 3.2 18 1-
H draulhc 3.5
Conducti' ity (Xt0"' Cm 'sec I
338 3427 1455 1214 903 1110 545 _t
Shear 400
Strength (kPa)
20 37 10.0 55 9.8 54 12.2 168 96
Axial Strain
at failure (%)
425-ft high earth and rockfill flood control dam located on the White River
near Enumclaw, WA. In 1982 piezometric studies conducted at the deepest point
16
of the center of the dam's clay core showed that the water level within the
core responded very quickly to changes in elevation of the impounded reser-
voir. These observations suggested zones of deterioration within the core.
Subsequent borings confirmed zones of soft and loose material having the
potential to allow excessive seepage (Peck 1986). The Corps then conducted a
research program to evaluate the possibility of installing a plastic concrete
diaphragm cutoff wall in the core as a seepage barrier. Table A7 in Appen-
dix A contains a summary of the plastic concrete mix designs examined and the
results of unconfined compression, flexural beam, Q, pressure, and erodability
tests (US Army Engineer Division, North Pacific 1987). The pressure tests
were nonstandard tests conducted in lieu of CIUC tests to evaluate the influ-
ence of consolidation on the stress-strain-strength behavior of plastic con-
crete. Wet samples were formed in open ended steel cylinders, and pressure
was applied to the samples with a hydraulic loading device. Water was allowed
to drain from the samples through vertical slots in the steel cylinder. When
drainage ended (25 to 45 min), the pressure was removed, and the samples were
cured under atmospheric pressure and later tested in a triaxial chamber.
28. Important general conclusions from the tests series are:
a. Unconfined compressive strength, flexural strength, and elastic
modulus decrease dramatically with the addition of bentonite.
b. Strain at failure increases dramatically with the addition of
bentonite.
c. Maximum deviator stress and elastic modulus increase with
confinement.
d. Maximum deviator stress increases with consolidation.
17
England. The shell is crushed shale and the central core is composed of com-
pacted boulder clay. The core is connected to the foundation bedrock by a
conventional concrete cutoff. A profile of the dam is shown in Figure 2.
lvel 3 .23 - -
-a.1mom
oseervoi,
Cwshod flawoe flifO,
- . . . . . . -:- ......-. *
Subsequent studies showed seepage through the core was reduced from 60 2/sec
to 5 I/sec.
Convento Viejo Dam
33. Convento Viejo Dam (Alvarez and Mahave 1982) is a 38-m high earth
embankment dam located on the Tinguiririca River in Chile's central valley
18
constructed in 1977. Figure 3 shows an upstream elevation view of the dam.
The original design called for a 14-m deep compacted clay cutoff to be
installed beneath the embankment to control underseepage. During construction
of the cutoff, however, it was discovered that underseepage occurred to a
depth of 57 m. To remedy this, a continuous plastic concrete cutoff was
installed to bedrock in front of the clay cutoff. The mix design used was as
follows:
Subsequent pump test have determined seepage across the dam to be 29.1 I/sec,
and the hydraulic efficiency of the plastic concrete cutoff to be
93.5 percent.
Z23m
270
260 LEGEND
200
19
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PLAN OF DAM
PLAN DU 8kA'-GE
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LEGEND
20
select the best mix design to meet these criteria (see paragraph 22). The mix
design selected was as follows:
21
90 DAYS
a Kg/cm2 28 DAYS
32 a Kg/cm2
32 16 3
28 2
2 12 1
24 1 0
8 2
20 03
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16 20
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8 2
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m cutoff wall
Triaisial ts au'in situ-
fI ailtire 415
4 1 31-0 60t "'0
V I adiiire 579 kg/crn'
1- 7S I" 2,8(0) kg/L.ni' E 3,200-5,s00 kg crn'
mI i h, 4ii1 k g. Cin
22
loin
* .. S' * of S. * ,
TYPICAL SECTION
Figure 6. Profile of Verney Dam (Tardieu 1987)
o1
a(MP*) St)- 174 Ps
So li~ePs BLOCK 13
4f,
6 BX I
0 ( *(%)
23
PART III: LABORATORY TESTING TECHNIQUE
consolidate wet 8-in. slump plastic concrete for the CIUC tests required the
development of some nonstandard procedures. In the following sections the
procedure for each type of tests performed in the research is described, and
where applicable, references to ASTM standards are given. In addition, where
nonstandard test procedures are described, any related ASTM standards are
Materials
Cement
41. Ironclad brand type I portland cement was used throughout the test
program. Chemical analysis performed by the US Army Engineer Waterways Exper-
iment Station (WES) confirmed that this cement conformed to ASTM designation
C-150 (Appendix B, Table B2). For batch design, the specific gravity of
24
Bentonite
42. Volclay brand low yield (90 barrel*), untreated Wyoming grade
sodium montmorillonite was used throughout the test program. This is the same
material typically used for cutoff wall trench slurry. The results of a chem-
ical analysis performed by WES are located in Appendix B, Table B3. Index
properties are:
G, = 2.75
LL = 530 %
PL = 41 %
PI 489 %
Aggregates
43. Masonry sand (SP) and minus 3/4 in. well rounded gravel (GP) were
used. Phase I aggregate was obtained from Lakeville Crushing, South Carver,
MA. Phase II aggregate was obtained from Boston Sand and Gravel, Boston, MA.
The grain size distribution of both sets of aggregates conformed to ASTM spec-
ification C 33-86 and are shown in Appendix B, Figures Bl through B4. Com-
parison of Figures BI and B2 to Figures B3 and B4 shows very little difference
between the grain size distributions of the two sets of aggregate.
Water
44. Potable tap water from the Geotechnical Laboratory at Tufts Univer-
sity was used for all batches.
45. One of the primary criteria for tremie placement of plastic con-
crete in a slurry trench is flowability. In order to prevent clogging of
tremie pipes, and to provide for uniform plastic concrete distribution along
trench bottoms, an 8-in. slump is recommended (Tamaro 1988). In light of
this, all of the plastic concrete batches produced in this research were
designed for a nominal 8-in. slump. This section describes the procedures
used for batching, mixing, and wet testing of all of the concrete batches
* One ton of clay will yield 90 barrels (42 gallons-US petroleum) of material
with a dynamic viscosity of 15 centipoise.
25
produced in this research program. The fabrication and curing procedures for
conventional test cylinders and flexural beams are also included.
Batch design
46. All batches were proportioned by the absolute volume method
described in ACI Standard 211.1-81 (CRD-C 99-82). Consistent with this
method, the following batch proportion parameters were used to describe the
plastic concrete batches:
Cement factor - The cement factor was defined as the total amount,
by weight, of cement and bentonite in a cubic yard of plastic
concrete:
26
their volumes. The weights of all the constituents were then corrected for
hygroscopic moisture content and scaled to produce the desired batch volume.
After the batch was made, the cement factor and water-cement ratio were cor-
rected for any additional water added during mixing (see Paragraph 48). An
illustrative batch design example can be found in Appendix B, Table B4.
Plastic concrete mixing procedure
48. All plastic concrete batches were mixed at 25 revolutions/min in a
stone brand six cubic foot power concrete mixer. The procedure which was
generally followed corresponded to ASTM specification C 192-81, para-
graph 6.1.2 (CRD-C 10-81). The modified procedure used is a follows:
a. Water content tests were performed on cement, bentonite, sand
and gravel to determine hygroscopic moisture. Figure 8 shows
typical quantities of materials used for water content test.
b. The bentonite and the cement were mixed together dry in a 5-gal
bucket.
c. Approximately one-half of the sand, gravel, and water were
added to the mixer and mixed for approximately 15 sec.
d. Approximately one-half of the cement-bentonite mix was added to
the turning mixer.
e. The remaining sand, gravel, and cement-bentonite mix was added
to the turning mixer, along with enough of the remaining water
to produce an 8-in. slump upon visual inspection.
f. Batches containing bentonite tended to "stiffen" in the mixer
over time as the bentonite absorbed water. To counter this,
the remaining water and, if necessary, additional water was
added approximately every 10 min to maintain an 8 -in. slump.
Additional water was added until the mix no longer "stiffened,"
generally about 45 min.
g. Total mix time was approximately 10 min for batches with 0 per-
cent bentonite and 45 min for batches with 10 to 60 percent
bentonite.
49. An attempt was made to premix the bentonite and water in a bucket
to form a slurry, as is commonly done in slurry trench field operations. This
was unsuccessful due to balling of the bentonite. A special colloidal mixer
would have been necessary to overcome this problem, but was deemed beyond the
scope of this project. Therefore, the bentonite was dry mixed with the cement
before being added to the mixer (as described above) to help ensure uniformity
of the mix. In addition, the water content required for pumpable slurry is
approximately twice the liquid limit, or 100 percent for the bentonite used in
this research program. Based on estimated water-cement ratios, the use of
27
Figure 8. Samples of sand, gravel, bentonite, and
cement (clockwise, from right) for water content
tests to determine hygroscopic moisture
such a high water content would have limited the bentonite contents evaluated
to 10 percent and less.
50. Because the hydration of bentonite in a mixer is time dependent, it
was necessary to continue to add water to a mix until there was no longer a
loss of slump with increased mixing. Trial batches reached this point after
approximately 45 min, but more or less time may be taken if visual inspection
determines that slump loss has ended. Any water added in addition to that
specified in the batch design during this time period was figured into the
recalculation of the batch design (see batch design example, Table B4).
Concrete fabrication equipment
51. All scales hand tools and mix pans used for concrete fabrication
conformed to ASTM specification C 192-81 (CRD-C 10-81). Calibrations of the
scales are presented in Appendix C, Figure Cl.
Tests performed c wet concrete
52. The following tests were performed:
a. SlumR -- Tests were performed according to ASTM specification
C 143-78 (CRD-C 5-86). Typical values ranged between 7-1/2 and
8-1/2 in.
b. Unit weight -- For Phase I batches ASTM standard C 138-81 was
followed using the air content test sample bowl as a measuring
28
container. For Phase II batches, the actual concrete cylinder
specimens were used as measuring containers. This method
allowed for multiple independent unit weight calculations (as
many calculations as specimens formed), and therefore provided
a measure of batch consistency. Typical values ranged between
125 and 145 lb/cu ft. Unit weight decreases with increasing
bentonite content because water comprises a larger fraction of
total batch weight as bentonite content increases.
c. Air content -- Air content tests conformed to ASTM specifica-
tion C 231-82 (CRD-C 41-84) for a type B air content meter.
Typical air content values ranged between 0.2 percent and
2 percent.
d. Water content -- Oven-dry water content tests were performed on
wet concrete to develop a correlation between calculated water
content and oven dry water content. Calculated water content
is the ratio of weight of water to combined weight of other
materials (cement, bentonite, and aggregate) used to form the
batch. Oven dry water content tests were performed in accor-
dance with ASTM standard D 2216 for soils. Typical values of
oven dry water content ranged between 8 percent and 22 percent
and the ratio of oven-dry to calculated water content ranged
from 0.53 to 0.92 and averaged 0.74. This ratio can be used
for field quality control to estimate the wet water content of
tremie concrete from a sample taken from the top opening of the
tremie pipe.
e.pH -- The pH of wet concrete was determined for some Phase II
batches with quantitative pH paper to ensure the proper suspen-
sion of bentonite in the mix. Typical values ranged between 11
and 12 (pH range for suspension of bentonite = 9.5 to 12)
(Sliwinski and Fleming 1975).
f. Temperature -- Temperature measurement of wet concrete con-
formed to ASTM specification C 1064-88 (CRD-C 3-87). Tempera-
ture was usually measured by inserting a thermometer into the
concrete mound left by a slump test. Typical values ranged
between 64 and 700 F.
Fabrication of conventional
plastic concrete test cylinders
53. The formation of 6- by 12-in. cylindrical tests specimens for all
unconfined compression, splitting tensile, and unconsolidated undrained com-
pression (Q) tests conformed to ASTM C 192-81 (CRD-C 10-81). Specimens were
2
formed using standard 6-in. diam by 1 -in. high molds in three layers of
approximately 4 in. thick. Each layer was rodded 25 to 30 times and vibrated
by hand to ensure proper consolidation. Figure 9 shows test cylinders being
formed.
29
Figure 9. Six in. by twelve in. plastic
concrete cylinders being formed
54. Initially, cylinder molds made of plastic were used to form all
specimens in Phase I. However, scarification problems were encountered when
extracting the first high bentonite content (BEN = 40 and 60 percent) speci-
mens from the plastic molds after the recommended ASTM period of 2 days.
Thereafter, ASTM approved peel-off wax coated cardboard cylinder molds were
used for all high bentonite specimens formed in Phase I. Due to general ease
of use and better specimen quality, it was subsequently decided to use the
cardboard molds exclusively for all Phase II specimens.
Fabrication of flexural beam specimens
55. All flexural beam specimens were formed in 6-in.-wide by 6-in.-high
by 24-in.-long rectangular steel molds in accordance with ASTM specifica-
tion C 192-81 (CRD-C 10-81).
30
Curing of concrete test specimens
56. All plastic concrete test specimens were cured in either a wet room
or cure box environment. Figures 10 and 11 show specimens in the wet room and
cure box, respectively. The wet room lacked temperature control, but humidity
control was provided by an air/water mist system. During Phase I testing,
specimens from the same batches were stored in both locations to evaluate
their performance. Comparison of unconfined compression test results showed
that curing location had no effect on the mechanical properties of the cylin-
ders, as shown in Figure 12. Each data point represents cylinders of the same
age and batch composition.
57. Monitoring of both locations over 60 days produced the following
performance criteria:
a. Wet room:
31
Figure 10. Six in. by twelve in. plastic concrete
cylinders curing in wet room
0.
.1750
E
0
0
X 1500 0
1250
C
1000
0
7500
I-) 0
L
E
o 500
c) 250-
addition, two companion unconfined compressions were performed for each of the
20 CIUC batch designs tested in Phase II.
59. For all of the 291 unconfined compression tests performed in both
phases, continuous load and deformation readings were recorded in order to
evaluate the stress, strain, and strength characteristics of each specimen. A
compilation of the data is presented in Appendix D, Table Dl and will be dis-
cussed more fully in Part IV. All tests were performed using ASTM C 39-86
(CRD-C 14-87) and ASTM C 469-83 (CRD-C 19-87) as guidelines, but some
procedure and equipment modifications were made as noted. All tests were
performed at a deformation rate of 0.05 in./min +/- 0.005 in./min.
Measurement of uncon-
fined compression test samples
60. After curing in either the cure box or wet room for a specified
amount of time, samples were removed and examined for signs of damage. Speci-
mens too damaged to cap were discarded. Typically, the high bentonite content
(BEN - 40%, 60%) specimens were most likely to be damaged during mold
33
Table 4
Summary of Nominal Batch Designs for Phase I Unconfined Compression Tests
34
stripping and handling because of their low strength. Any loose aggregate on
the sample ends was removed.
61. The length and the diameter of samples were measured as follows:
a. Length: All Phase I samples were measured with a 12-in.
vernier, precise to +/- 0.0005 in. All Phase II samples were
placed vertically on a piece of plate glass and measured with a
24-in. machine scale, precise to +/- 0.008 in.
b. Diameter: All Phase I samples were measured at top, middle,
and bottom with a 6-in. micrometer, precise to +/- 0.0005 in.
All Phase II samples were measured at top, middle, and bottom
with a double carpenters scale, precise to +/- 0.008 in.
35
T
a
3"
Measurement of axial load
for unconfined compression tests
65. All unconfined compression tests were performed with a constant
rate of deformation Riehle Model FS-300 testing machine. This machine has a
screw-driven loading platen with a minimum deformation rate of 0.04 in./min
and a maximum load capacity of 300,000 lb. Loads are measured internally with
a beam-type reaction system and displayed on a large analog dial gage. The
dial gage has six loading ranges:
Range, lb Precision, lb
0-3,000 5
0-15,000 25
0-30,000 50
0-63,000 100
0-150,000 250
0-300,000 500
66. Figures 16 and 17 show the Riehle testing machine and a close up of
its load head crushing a 6- by 12-in. sample. Calibrations of the Riehle
testing machine are located in Appendix C, Figures C2 and C3.
67. Loads were read manually by the operator of the Riehle testing
machine and hand recorded. Corresponding deflections were read manually by an
assistant from a dial gage attached to the test specimen and hand recorded.
Accurate reading of peak loads was ensured by a dial pointer follower. In
order to develop complete stress-strain curves, deflection readings were taken
at least six loads prior to peak load and, in most cases, at least two loads
after peak.
Measurement of deflection
for unconfined compression tests
68. During Phase I, strain was initially calculated from the gross
deflection of the load head of the testing machine as measured by a dial gage
rigidly mounted to the loading platform. This gage had a precision of
+/- 0.0005 in. Midway through Phase 1, a compressometer conforming to ASTM
specification C 469-83 (CRD-C 19-87) was purchased for measurement of
deflection. The gage mounted on the compressometer had a precision of
+/-0.0005 in. Schematic diagrams of the gross deflection system and com-
pressometer are shown in Figures 18 and 19.
69. Subsequent Phase I tests were performed using both the gross
deflection method and the compressometer method to establish the
37
Figure 16. Riehle testing machine and general
testing equipment setup
38
P
LOAD HEAD
NOTE: G - 12 in.
SPECIMEN
SPECIMEN DIAL GAGE (A)
PIVOT
COMPRESSOMETER 41(
FIXED
77 7777777 //77
Figure 19. Schematic diagram of compressometer system
39
relationship between the two. For a given batch design and age, three samples
were typically broken to ensure statistical confidence. Two of these samples
were tested using the gross deflection method, and one sample was tested using
the compressometer. If less than three cylinders were available for a given
batch design and age, at least one test was performed using the
compressometer.
70. A comparison of the strain at failure of specimens of the same age
and batch design calculated with gross deflection and compressometer data is
shown in Figure 20. Figure 20 shows that the scatter in strain at failure
1
data is greater than any difference caused by the different deflection mea-
surement systems. Only the compressometer was used to measure the deflections
of unconfined compression tests performed in Phase II.
0.006 . . .. .
0
.
S0.0040
0
o Oi 0
00
0 0
c0.002 00
O
0.002 0oOI
U0
40
72. After compression testing, one cylinder from each test group of the
same age and batch design was broken into pieces less than 1 in. in size, and
a water content was performed on pieces taken from the core. Standard oven-
dry soils testing water content test procedure (ASTM D 2216) was used.
Measurement of Brazilian
splitting tensile test specimen
75. After the specified curing time, test samples were examined,
cleaned, and measured as described in Paragraph 60. Two diametrical lines in
41
the same plane were then drawn across both sample ends to use as guides to
align the specimen with the test apparatus.
Positioning of Brazilian
splitting tensile test specimen
76. A 1-in. wide by 1/8-in, high by 12-in. long plywood strip was
placed across the lower bearing block. The test cylinder was then placed
horizontally on the plywood strip so that the lines marked on the ends of the
cylinder were vertical and centered over the plywood strip. A second plywood
strip was then placed lengthwise across the top of the cylinder and centered
on the lines marked on the ends of the cylinder. A supplementary bearing bar,
as described in ASTM specification C 496-85, was then placed on top of the
upper plywood strip. The load head was then brought into contact with the
supplementary bearing bar.
78. One 6-in. wide by 6-in. high by 24-in. long flexural beam was cast
in a steel mold for each preliminary Brazilian tensile test batch and tested
in single-point simply supported flexure at an age of 28 days, in accordance
with ASTM specification C 293-79 (CRD-C 17-80). All tests were performed with
the Riehle testing machine at a deformation rate of 0.05 in./min. +/-
0.005 in./min.
Measurement of flexural test sample
79. After curing, the length, width at center, and thickness at center
were measured to a precision of +/- 0.008 in. Post test measurements of the
width and thickness of the beam at the point of rupture were taken and, if
different from the initial measurements, recorded for use in calculation of
the modulus of rupture.
80. The span length was then calculated using the equation:
42
L - 3D
where
L - Span length
D - Beam thickness
Support point marks were then drawn on the beam at distances of L/2 from the
beam center line. A line was also drawn at the center line to locate the
single center point load.
port was lined up with a span mark on the beam, and the center point load
block was lined up with the center line of the beam and the center line of the
load head. Beams were then loaded and the peak load was manually recorded by
the testing machine operator. Modulus of rupture was then calculated as
82. Two tests were performed to measure the resistance of plastic con-
crete to erosion by seepage through cracks. Both tests were performed accord-
No. 87-C-329 for their preliminary plastic concrete testing program. Crack
conditions were simulated by casting a 3/16-in. hole through each sample and
flowing water through it at a velocity of 17 ft/sec. One test had a bentonite
taken continuously between ages 3 and 8 days with a No. 200 sieve.
43
3/16 A. DLtA*ETER ALtAAM ROD
I I. WIDE ALLWMM
'CENTERING PLATE*
SETS IN SLOTS
7- IN CARDBOARD MOLD
6 .DAMTRB
12I.HIHSADR
CADORDCLNDRML
NUT
im
GEL
AO. SBW
U KHEA Awv mw B TTO
4AD4R YLNE ~
b. A 1/4-in. Swagelok pipe thread fitting was installed in a hole
drilled in a I- by 8- by 1/4-in. piece of aluminum.
c. The piece of aluminum with the pipe thread fitting was then
installed into 1/4-in, slots cut into opposite sides near the
top of the mold. The piece of aluminum was adjusted until both
fittings were on the same axis.
d. A 3/16-in. aluminum rod was then inserted through both
fittings. The rod was coated with vacuum grease to help seal
the bottom fitting and make later removal of the rod easier.
FROM TAP --
SAMPLE
WIRE MESH
MILK CRATE
-. FLOOR
GRATE/
7,S.777.777
SUMP DRAIN
45
b. The cylinder was allowed to cure in the open laboratory, for
fear that moving the specimen might cause excessive cracking,
To prevent drying of the specimen, the mold was left on so that
the entire curing period and the top would keep moist. The
aluminum rod was gently rotated periodically to prevent it from
adhering to the concrete.
C. At the required age, the mold was stripped and the aluminum rod
removed. A 1/4-in.-diam hose carrying city water at 75 psi was
then attached to the top fitting and a No. 200 sieve was placed
beneath the bottom fitting.
d. The water was turned on and flow rate calculated.
e. The No. 200 sieve was periodically checked for eroded material.
If significant material was observed, the test was stopped and
the material weighed.
f. The test was continued until it was determined that there was
not change in the erosion rate.
85. Most of the equipment used in the triaxial test program was stan-
dard soils testing equipment. Some pieces of equipment, however, were special
made for this test program.
Triaxial cell and accessories
86. The following contains a listing of equipment used in the tests.
a. Triaxial cell. Two Geotest brand model S5050 high pressure
triaxial cells were used to perform all tests. A photograph
and schematic diagram of one of the triaxial cells are shown in
Figures 23 and 24. Extensive modification was done to the
control valve system in order to make it simpler to operate and
to accommodate pressure transducers. A schematic representa-
tion of the final valve scheme is included in Figure 24. All
deflection measurements were corrected for the machine deflec-
tion of the triaxial cells. Critical features of the cells
are:
46
Figure 23. Geotest triaxial cell
47
TEFLON BEARING SLEEVE
GORINGS
FILTER PAPER
HOOD POROUS STONE
SAMPLE
o'--- MEMBRANE
POROUS STONE
PEDESTAL "
FILTER PAPER
--- GRINGS
CLAMPING RINGN
48
mounted on the pedestal. Halves were held together during
tests by standard duct tape. Swagelok fittings were attached
to each half to permit application of vacuum to hold the mem-
brane to inner wall during sample formation.
h. Pore pressure transducers. Validyne brand model DPI5 variable
reluctance differential pressure transducers were used to mea-
sure cell pressure and head difference during permeability
testing for all CIUC tests. Voltage output was read by a
multimeter. Transducers were calibrated, on average, every
other test using a Refinery Supply Company model 35260-4 dead
weight tester. The dead weight tester was calibrated annually.
solidation, two accumulators were used for each triaxial cell, one controlling
the top cap and the other controlling the pedestal. Each accumulator consists
of 25 ml graduated pipette, precise to +/- 0.05 ml, and a 100 m (approxi-
mately) ungraduated annulus. The annulus and pipette can be used to measure
volume change either alone or together, depending on flow requirements and
OWN
1 .
49
I-- Pressure Positions --
1 2 3
Re dout 1 12 8 - J R 0
Section r' ofg .3I
1 1'eg c q
Reunto orc 0
R egulator 2 Regulator 3
reo .
Panel
Control
Section supply press
AQ
master
regulator
"fi ,dra
in n 2 id,=,
I~.,
E off off off
deird 2o
nqh2o
5
0drain
drain h2o 1rnh2odan
in drat 0 o
50
88. Back pressure for each accumulator was independently controlled by
a Fairchild bleeding regulator. Maximum allowable back pressure was 200 psi.
Back pressure for CIUC test program was provided by an air compressor
operating at 120 psi delivery pressure. Back pressure was measured in two
ways:
a. Panel board mounted transducer attached to bleeding regulators.
b. Pressure transducer mounted on cell pedestal drainage port(s).
89. All fluid used for application of back pressure and permeability
testing was de-aired tap water stored under vacuum.
Triaxial cell pressure control
90. For all CIUC and Q tests, cell pressure was applied using a gas
pressure over water system. Gas pressure was supplied by high pressure
(2,300 psi) nitrogen bottle fitted with a two-stage, non-bleeding union
carbide regulator rated at 3,000 psi. The gas-water interface was located in
a high pressure stainless steel reservoir, as shown in Figures 27 and 28.
51
-.*TE-GAS PRESSURE
FROM NITROGEN
GAS BOTTLES
ON/OFF 1/4 IN.
WHITNEY BALL VALVE
GAS-WATER INTERFACE
TO TRIAXIAL CELL
FLUID VALVE
Figure 28. Schematic diagram of
stainless steel reservoir con-
taining cell pressure gas-water
interface
52
Cell pressure was measured continually using a pore pressure transducer
mounted on the triaxial cell pedestal. The observed drift over 7 days at
400 psi cell pressure was +/- 5 psi.
0 Test Procedure
Table 5
Test Schedule for CIUC and 0 Test Groups by Batch Design,
Age and Effective Consolidation Stress
Batch ID
Percent Age Effective Consolidation Stress, psi
Bentonite Days 50 100 200 300
3 -- 080288 091488 *
0 7 -- 030189 * *
14 -- 102688 * *
Note: All batches have nominal cement factor of 300 lb/cu yd.
* Tests could not be performed because sample strength was beyond the
capacity of the triaxial cell piston (85,000 ib).
53
C 801-81 (CRD-C 93-83), except as noted below. Tests were performed at a
strain rate of 0.05 in./min. Deformations were measured using a 0.0001-in.
precision dial gage.
0 test sample fabrication and curing
93. All samples were fabricated and cured as described in paragraphs 53
through 58.
54
The problem of seating deflections during Q tests is examined in greater
detail in Paragraph 143.
0 shear test procedure
97. The following procedures were used for all Q tests:
a. A double membrane was placed over the Q test sample. The sam-
ple was then positioned on the triaxial cell base, and the
membrane ends were sealed to the sides of the pedestal and top
capped with O-rings and vacuum grease.
b. The cell hood was placed over the sample and attached to the
base with a clamping collar. Care was taken not to crimp the
top cap water lines. The piston was then seated against the
top cap and locked into place.
C. The cell was filled with tap water via the stainless steel
reservoir bottle and cell pressure hose. The cell hood bleed
valve was kept open during filling to purge all air from cell.
d. The cell pressure transducer was attached to the cell base and
purged of air. The triaxial cell was then positioned under the
load head of the Riehle testing machine, and a brass loading
block was placed on top of the piston. This loading block
prevented the piston from stamping the testing machine load
head during loading.
e. The cell pressure was applied and the pedestal valve was opened
momentarily to check for leaks across the membrane. If no
significant leaks (more than a few drops of water) were
observed, the load head was brought into contact with the
loading block and the piston was unlocked. The deflection dial
gage was then adjusted on the piston to provide maximum travel.
f. A loading scale was chosen based on prior testing experience.
Shear testing was begun and load and deformation readings were
taken often enough to develop a complete stress-strain curve.
As many post-peak load and deformation readings as possible
were taken. The deflection dial gage was reset on the piston
as necessary.
g. After completion of shear testing, the Q test specimen was
removed from the cell and its height and diameter measured and
recorded. The specimen was then marked with its batch number
and stored in the wet room.
98. CIUC tests were performed to simulate the behavior of plastic con-
crete in a cutoff wall following tremie placement. The CIUC test procedure
for soils outlined in Appendix X of EM 1110-2-1906 (Headquarters, Department
of the Army 1986) was used as a guideline for developing the procedure
described below. In order to form a 6-in.-diam by 12-in.-high test specimen
55
from wet 8-in. slump concrete, it was necessary to partially consolidate the
specimen under a vacuum in a split mold prior to full consolidation in a
triaxial chamber. Granular, cohesionless soils are often consolidated in a
similar manner. The following procedure was developed by trial and error on
preliminary batches made during May, June, and July 1988. Subsequent refine-
ments in procedure made during Phase II testing are also included here. Nota-
tions are made, when relevant, explaining why and when each refinement was
done.
56
Figure 29. Presaturation of pedestal and top cap
porous stones and filter paper
5/
Figure 30. Spil1t mold(1cmsol idomot er with mcwhirali
inside just prior to formaI.tionI Of CIUC -,,-MPI(
f. The inside depth of the membrane/consolidometer was then mea-
sured and recorded. The inside diameter of the membrane/
consolidometer was then estimated by filling the
membrane/consolidometer with a known quantity of water, mea-
suring the depth of the water and using the equation:
1 /2
D = (4V/ifH)
where
D = average diameter
V - volume of water
H = height of water
59
%M
Figure 32. Plastic concrete CIUC Figure 33. CIUC sample after
sample being vacuumed vacuuming with consolidometer
removed
60
.01
f. The cell was filled with tap water via the stainless steel
reservoir bottle and cell pressure hose. The cell hood bleed
valve was kept open during filling to purge all air from cell.
g. The cell pressure transducer and the pedestal pore/pressure
transducer were attached to the cell base and purged off air
(Figure 35). The top cap and pedestal were than resaturated
via the panel board accumulators in order to eliminate any
void space caused by vacuuming.
61
Figure 35. Close-up of pore pressure
transducer setup
62
Table 6
Summary of Changes in Volume of CIUC Samples
During Vacuum and Consolidation
Water Water
Initial Initial Volume Removed Removed
Total of Water During During
Volume in Sample Vacuum Consolidation
Ben. cc of Sample % of % of % of
Batch ID % P..-j cm3 ml. total ml. total ml. total
082088-1 0 100 5478 1488 27.2 279 5.1 163 3.0
091488-1 0 200 5521 1396 25.3 215 3.9 149 2.7
030189-1 0 100 5584 1482 26.5 236 4.2 157 2.8
102688-1 0 100 5564 1492 26.8 225 4.0 159 2.9
082688-1 20 50 5701 1884 33.0 226 4.0 180 3.2
080588-1 20 100 5916 1917 32.4 242 4.1 135 2.3
091088-1 20 200 5394 1900 35.2 121 2.2 359 6.7
081088-1 20 100 5593 1875 33.5 180 3.2 294 5.3
082388-1 20 200 5397 1882 34.9 83 1.5 466 8.6
090188-1 20 300 5518 1943 35.2 77 1.4 428 7.8
111688-1 20 300 5393 1911 35.4 208 3.9 357 6.6
091588-1 40 50 5551 2259 40.7 193 3.5 178 3.2
090988-1 40 100 5449 2151 39.5 128 2.3 546 10.0
091988-1 40 200 5377 2183 40.6 239 4.4 428 8.0
101488-1 40 300 5494 2255 41.0 239 4.4 537 9.8
083188-1 40 100 5790 2247 39.1 136 2.4 232 4.0
092888-1 40 300 5490 2328 42.4 178 3.2 576 10.5
102888-1 40 100 5509 2304 41.8 208 3.8 367 6.7
022289-1 40 100 5714 2291 40.1 64 1.1 406 7.1
100688-1 40 300 5537 2225 40.2 215 3.9 546 9.9
63
0 _
CL
-100
*SAMPLE ID: 100688-1
.10CEMENT FACTOR: 300 LB/CU YD
.15
LiBENTONITE: 40%
-200
250 -C
0
w -300
> -350
z
-400
-55 0
1.0 L
0 5 10 15 20 25 30 31
SOUARE ROOT OF TIMIE. F'
Table 7
Summary of CIUG Samples for which Permeability Tests were Performed
64
a guide. Using this procedure, permeability was determined using Darcy's law
for flow of through soil:
q = kiA (1)
where
q rate of flow of water through soil with cross-section A
k = coefficient of permeability
i =hydraulic gradient
rearranging
k = q (2)
iA
by definition
q=- qt (3)
and
i = h2 - h (4)
L
where
Q = quantity of water flowing through cross-section A in time t
h2 - h, = difference in head across sample
h 2 -h = 2 - P-
YW
(5)
where
65
k = QLy (6)
tA(P, - P,)
103. Since L , A , and 7w are known constants only time, flow and
pressure difference need to be measured during testing. The pressure differ-
ence was established by reducing the back pressure on the top cap. Flow
through the sample was then measured by periodically reading the water level
in the pedestal accumulator and recording the corresponding time. Approxi-
mately 12 hr prior to shear testing, the permeability test was stopped, and
the top cap back pressure was returned to the original back pressure to allow
the pore pressure within the sample time to equalize.
104. All CIUC shear tests were performed with the Riehle testing
machine at a deformation rate of 0.05 in./min. Deformation readings were read
from a 0.0001 in. precision dial gage attached to the piston. The actual
procedures used for all tests were as follows:
a. The triaxial cell was positioned under the load head of Riehle
testing machine and a brass loading block was placed on top of
the piston. This loading block prevented the piston from
indenting the test machine load head during loading.
b. The load head of the testing machine was brought into contact
with the loading block and the piston was unlocked. The
change in height of the sample due to consolidation was mea-
sured by loading the piston until it reestablished contact
with the top cap, and then taking a dial reading. The differ-
ence between this dial reading and the initial dial reading
taken in Paragraph 100 was the change in height due to consol-
idation. The deflection dial gage was then adjusted on the
piston to provide maximum travel.
c. A loading scale was chosen based on prior testing experience.
Shear testing was begun and load and deformation readings were
taken often enough to develop a complete stress-strain curve.
As many post-peak load and deformation readings as possible
were taken. The deflection dial gage was reset on the piston
as necessary. In addition, pore pressure readings were taken
for samples 080288-1 and 022289-1.
d. After completion of shear testing, the test specimen was
removed from the cell and its height and diameter measured and
recorded. The specimen was then marked with its batch number
and stored in the wet room.
66
PART IV: UNCONFINED TEST RESULTS
251 UC tests
cement factors 230 to 450 lb/cu yd.
bentonite contents of 0, 10, 20, 40, and 60 percent.
ages of 3 to 660 days.
2 erodability tests
106. Summary tables of each test program are presented in Appendix D
and discussed in the paragraphs below. The cement factors and water-cement
ratios for all of the plastic concrete batches presented in each test series
summary table are corrected for actual batch composition as described in Para-
107. Load and deflection measurements were taken for all unconfined
67
- ULTIMATE COMPRESSIVE STRENGTH
- STRAIN AT FAILURE
E - YOUNG'S MODULUS
-- -
/,)
,/1
i//
STRAIN, PERCENT
Al (7)
where
- strain, in./in.
Al - vertical deformation of specimen, in.
directly with a dial gage and 1. equals initial height of the specimen. For
strains measured with a compressometer, Al equals one-half the dial gage
deflection and 1, equals gage length and distance between top and bottom
connection points. The gage length of the compressometer used in this test
program was 8 in.
68
110. Stress was calculated by dividing load by specimen cross-sectional
area, corrected for strain:
(8)
A,/ (I-e)
where
a - stress, psi
P = load, lb
E (9)
eb -C a
where
ab - maximum stress on the linear portion of the stress-strain curve,
psi
a. - minimum stress on the linear portion of the stress-strain curve,
psi
Lb - maximum strain on the linear portion of the stress-strain curve,
psi
69
the use of neoprene end caps results in lower ultimate stresses when compared
to specimens tested with sulphur end caps. This lowering of ultimate
strengths is the result of the reduction of cross-sectional area caused by
spalling of specimen ends. Spalling is caused by shear stresses developed at
the neoprene-specimen interface caused by the deformation of the neoprene.
The failure mode for all neoprene-capped tests was vertical splitting while
diagonal failure occurred with the specimens with sulphur end caps. In order
to include ultimate strengths from neoprene-capped specimens in analyses in
Part VI, a plot was developed to correct ultimate strength to sulphur-capped
values. The plot and its use are described in Paragraph 148.
113. No elastic modulus and ultimate strain values for specimens tested
with neoprene end caps are included in Table Dl. These values are inaccurate
because they include the deformation of the neoprene end caps. A correction
procedure for elastic modulus and ultimate strain could not be developed
because the deformation of the neoprene end caps could not be measured sepa-
rately. No ultimate strain and elastic modulus data from neoprene-capped
samples were used in any analyses.
70
460-........
44 Slump= 8 +/- I in.
360- 010
0
t340- 60%
320- 0
C
E 300 8A
U8
280 0
00
260- A A
240 0 0
220-, r-- .4 ~
0.8 1.0 1.2 14 1.6 1.8 20O 2.2 2.4 2.6 2.8 3.0 3.2
Water-cement ratio. w/c
00000 0% bentonite
00000 10% bentonite
0 -&a 20% bentonite
aL 1000- a. 10% 00000 40% bentonite
- 4 02esee 60% bentonite
V.0
0%)8
0)>
100
00
440
C
C
0
1)
C
D 60%
71
Each data point corresponds to one test specimen. Boxes are drawn around
groups of data points with the same bentonite contents. Figure 39 shows that
unconfined compressive strength decreases with the addition of bentonite for
the 8-in. slump mixture.
117. Figure 40 shows the relationship between unconfined compressive
strength and elastic (Young's) modulus for all ages and bentonite contents.
Separate regression lines are drawn through data points with elastic moduli
calculated from strain values obtained with both the compressometer and by
gross deflection. Figure 40 shows that elastic modulus increases with
increasing unconfined compressive strength. The influence of bentonite on
elastic modulus is expressed indirectly by the influence of bentonite on
unconfined compressive strength. For example, a low unconfined compressive
strength corresponding to a high bentonite content obtained from Figure 39
corresponds to a low elastic modulus in Figure 40.
00000 CA bentonite
00o0 10% // 0/
&a&&&20% bentonite /o 00
QOO0000 60%
0oo .1000 bentonite
40% bentonite /o/
- /
C /
/4 C
gross deflection /
0. U.X& /', t( /
0) 0
E 100 7'
0
0)compressometer
C
C/
0
C-)
C
1 10 100 1000
Unconfined Elastic Modulus, ksi
Figure 40. Unconfined compressive strength
versus unconfined elastic modulus for all
bentonite contents
72
tests were performed for each Phase II batch. Complete stress-strain curves
for each test are shown by batch in Appendix E. The Phase II unconfined com-
pression tests were performed as companion tests to the CIUC and Q tests to
ensure repeatability within a batch (i.e. that batch constituents were uni-
formly mixed). This was important because the estimates of initial propor-
tions of batch constituents in CIUC samples were based on the assumption that
constituents were uniformly mixed throughout the batch. In addition, the
Phase II unconfined compression tests were performed to ensure that batches
with the same cement factor and bentonite content (but which were formed at
different times) were the same. Statistical analysis of the unconfined com-
pressive strengths reported in Table D2 shows that the average standard devia-
tion of unconfined compressive strength within batches is 1.7 percent with a
maximum standard deviation of 6.1 percent for batch 080288-1. The standard
deviations of unconfined compressive strengths between batches of the same
bentonite content and age are less than 5 percent, except between batches
080288-1 and 091488-1 which have a standard deviation of 30 percent.
73
(1) strain measured by gross deflection 160
(2) strain measured by compressometer 71
(3) neoprene end caps used 20
c. Total number of test specimen groups (I to 100
3 specimens from the same batch tested at same age)
d. Number of test specimen groups with only 13
one test specimen
e. Average standard deviation of ultimate 4 % +/- 3 %
compressive strength within test specimen
groups containing more than one specimen
f. Number of test specimen groups with standard 4
deviations from test group average greater than 10%
g. Maximum standard deviation within a test 14 %
specimen group
The above analysis indicates that the values of unconfined compressive
strength obtained in Phase I testing are accurate.
121. The actual degree of accuracy of any given test group is also
dependent on the precision to which the stress-strain-strength parameters (q.,
E, and cu) can be calculated. The precision of each parameter depends on the
combined precision of the measured values each parameter is dependent upon
(see Paragraphs 107-113). The following is a summary of the precision of
E , and e. as a function of reading error during testing:
74
a. Ultimate compresssive strength (q,.) and elastic modulus (E)
(1) qu and E decrease with increasing bentonite content
(Figures 39 and 40).
(2) qu and E increase with increasing cement factor (Fig-
ures 38, 39, and 40).
(3) q, and E increase with curing age (Tables Dl and D2).
b. Strain at failure (c)
(1) e. increases with increasing bentonite content
(Tables D1 and D2).
(2) c,, decreases with curing age (Tables Dl and D2).
(3) e. decreases slightly with increasing cement factor
(Tables DI and D2).
c. Water-cement ratio (resulting in 8 in. slump)
(1) Water cement ratio increases with increasing bentonite
content (Figure 38).
(2) Water cement decreases with increasing cement factor
(Figure 38).
d. Air content of wet concrete
Air content decreases with increasing bentonite content
(Table Dl).
Brazilian splitting
tensile test series
124. Brazilian splitting tensile tests were performed on 45 specimens
from six batches of plastic concrete to evaluate the effect of bentonite con-
tent, cement factor, and age on splitting tensile strength. Batches with
nominal cement factors of 250 and 350 lb/cu yd and bentonite contents of 0,
20, and 60 percent were chosen in order to bracket the preliminary unconfined
compression series data as well as possible with a minimum number of tests.
125. A summary of the batch design and tensile strength of all Phase I
test specimens is contained in Table D3. Most specimens were tested at
nominal ages of 3, 7, 28, and 90 days. All specimens from the 60 percent
bentonite, 250 lb/cu yd batch (062288-1), were too weak to test correctly and
75
were thrown out. A summary of the batch design and tensile strength of all
Phase II test specimens is contained in Table D4.
126. The tensile strength of all splitting tensile tests was calculated
according to the procedure outlined in ASTM designation C 496-85 (CRD-C
77-85). The peak load for all tests recorded and splitting tensile strength
was calculated as follows:
T -2P (10)
7tId
where
T - Brazilian splitting tensile strength, psi
P - peak load, lb
1 - cylinder length, in.
d - cylinder diameter, in.
127. Conclusions on the effect of bentonite content, cement factor, and
age on splitting tensile strength observed in Tables D3 and D4 are listed
below in order of relative influence:
a. Splitting tensile strength decreases with increasing bentonite
content.
b. Splitting tensile strength increases with increasing cement
factors.
. Splitting tensile strength increases with specimen age.
Results of flexural beam series
128. One flexural beam was cast from each Brazilian tensile test batch
and tested in single-point simply supported flexure at an age of 28 days. A
summary of the batch designs and modulus of rupture of these tests are con-
tained in Table D5. For each test, the peak load was recorded and
the modulus of rupture calculated:
R =3P1 2
2bd
where
R - modulus of rupture, psi
P - peak load, lb
76
1 - length of beam span, in.
b - width of beam at point of rupture, in.
d - depth of beam at point of rupture, in.
129. Conclusions observed in Table D5 from these tests are similar to
those of the unconfined compression and brazilian tensile series:
a. Modulus of rupture decreases with increasing bentonite
content.
b. Modulus of rupture increases with increasing cement factor.
Results of erosion test series
130. Two tests were performed to measure the resistance of plastic
concrete to erosion by seepage through cracks. Crack conditions were simu-
lated by casting a 3/16-in. hole through each sample and flowing water through
it at a velocity of 17 ft/sec. One test had a bentonite content of 0 percent
and the other had a bentonite content of 60 percent. Both tests had cement
factors of 300 lb/cu yd and were tested continuously between ages 3 and
8 days.
131. For all practical purposes, the tests showed that neither specimen
was susceptible to piping. The 0 percent bentonite batch showed no signs of
erosion over the 5-day test period. The 60 percent batch lost material at an
average approximate rate of 0.05 percent of initial sample weight per day.
This number is a rough estimate, however, because the amounts of material
eroded on some days were too small (<0.1 grams) to measure precisely on the
scale used (precise to 0.1 gram). More erosion tests need to be conducted on
plastic concrete before any definitive conclusions can be drawn.
77
PART V: TRIAXIAL AND PERMEABILITY TEST RESULTS
132. Plastic concrete mixes with cement factors of 300 lb/cu yd and
bentonite contents of 20 and 40 percent in addition to a 0 percent bentonite
was decided that samples would be tested at 3, 7, and 14 days age. Table 5
content is 20 percent, effective confining stress is 100 psi, and curing age
is 58 days) test was performed but finished too late to incorporate into this
report. The results of CIUC test 031889-1 are usEd only in the discussion of
pore pressure generated during shear presented in Paragraph 163.
133. For each combination of bentonite content, age, and confinement,
d. 1 T test.
consistency within and betweet, batches with the same bentonite content. A
different confining stresses would have been cast simultaneously from the same
batch into three triaxial chambers and tested as a group. This would have
tice, however, thi- procedure was unworkable for two main reasons:
78
136. Companion UC tests were also done to determine if correlations
could be developed between CIUC, Q, and UC shear strength. In addition, com-
panion Brazilian splitting tensile tests were performed to determine if a
correlation could be developed between unconfined compression and splitting
tensile strength. A summary of the results of the companion splitting tensile
tests is presented in Table D4 and discussed in Paragraph 123.
79
w1
0000 0000 0 0 a,0
0 - 44 O r*.i c'J C1 Ln e
a4a f eJ.4 .4 OO
0
ON Y0 0'% 04C r M, .4 -4 -4 M, C-4j
V) 4o c -4 .- 4 ,-4 0
4J-
-) I
Q U V)00D 0 n000000 0
04
-4 u
w . -"- 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0
W4. 0 41
r. 0)
14 14 C
4U40
4-4 40)-)
0 41 4] -. 4
C
0141
xU l
0000000000000000000 r- 4wr-m 140
0. o0 1.) 01, Ln ID n t;)- " ) 0,) ciU CUD
'4 ' -44- -4'4 4 -r-C4 - 4- - 4- C2-4 - -4'J -4W 4
-40 ".4
1 1.0 1 1 " 1 1 0.
00-14O 40 ~ D- ~ 4 r
40 C40 )( -4 - -400 -4 4 10 bo C41 w0
4J.. -4 - 14 144
4.) 4.J1 if
0+ b -4 'A cc
NN. -... .. N. 4J 3t 0 E
r". mr- 4) 4J."4
.41 41 -OO .
0 u- r- m-
b -o I r 4--44 - -4-4.-4.- -4.I-4 4 4 -4 01
00 4 J4 0m
C00 -Q-C U -4 4
~- 4 (A (D V) .-I w- >
Li~ 41)
C0
c M0 4J " e -.
r-0 nr rI nM0 40I00r n0 DIr D0 14C
0 to I4W U8 L,
r. 11 4~ J Cs 44 114 D1Dr Dk U OQ 00 b~j
a
CU
01 0 ) C 4.) 140
0 1 0
E 4- 0 1
co4cy m 0~~~/
coc h oc - 7 (,400 0(, '
80
, WAxial stress, psi
03- Confining stress, psi
(a,-q/2 - S, - Shear strength
e -Strain at falure
E - Young's modulus
I-I
w
I)
STRAIN, PERCENT
Table 9. Shear strength, elastic modulus, and strain at failure are defined
as described in Paragraph 137. Individual stress-strain curves for each Q
test are presented by batch in Appendix E. All strain data were corrected for
the machine deflection of the triaxial cells. There is no Q test for
batch 101488-1 because the sample was accidentally broken during setup. In
addition, the strain at failure of the Q test specimen of batch 083188-1 could
not be measured because the dial gage jammed during shear testing.
140. Comparison of Q tests in Table 9 of the same age and effective
81
Cn
r4 00 %o Co
r- I Lr) )%Cr- A' -4 0 0
C14 C
In
U) In 42
112 L4n4
0 0c
c - r0"a'oo '0r00 -00 C'0~
ul L 04
"D%.1 0\004a' ma'a00 ls '100 D00
0.) 4I 4 -4'J 4 - 4J 4 14 r- r ,-4 C-4-r C
~
-4 4r4r4- ~ ~ '- 4)
41)
04 4.344 '0 t- C4OMC -4
C - r- .- 4 V .D M 0 It a'D
y C)0
2-4 r* n % 4 1 o n - - - % ) I %
bO) r,) Ul -4C4MC1 n0 n 4- 4- 40-
2-4 4) ,-,-
0 0UJ m )C)) >C mC >0 *- UY
En V.fU)0
444
E 1-1 0
0.
4- '4 % lCJC 0r C4 00C-4 0 04 C 'J4M-.?L "C MUr'.,,4
r-4 4 . (.3 -4
a\ ul W.4- 1
4)4). 40l-.40 4) 2
E--4 4) 0
C4141)- 0c
0. 4)ca-4" 4)0
tX-C9-4 4 .) 4.3o
+ - - P
0000 000
0000 000 00 4-) ~ 0. v2
bo 4 4 r4 4 - ( ) -4--4 C-a. 41
41-l1 -4 x -
U.- r0. ca -4 -
0J 040
co ~~I
E -
4. 0 4 C14& 0W
ooU0 0 0 CO co o o c 0 4-bO co ) CL 4
04. .44 .. 44 4 440 2- -'- ) i r -4 -4
0A 4) 2-i bO
-3 0 )& 4.34
E 00- 4). 4) cz)
4)4- co 14 ) Q..r
41
w .4 - .Q
r. 0 > C n4r ", N0t ' n no w >04 _(
-
" :3 o.4-0mC mmoo0ooC c\c )ob -r\
U 0U00
( C4 000000M4C04.-400'-40-4
(14 t- I e l)MCJCIe ~l4 d- -
Wcol w . w l82
141. However, all Q elastic modulus values listed in Table 9 are less
than corresponding UC elastic modulus values listed in Table D2. This sug-
gests that elastic modulus, and hence, material stiffness decrease with con-
finement, a conclusion not consistent with the results of the CIUC test
series. Concrete subjected to confining stress should become stiffer. The
most likely cause of this anomaly is lack of planeness of Q test specimen
ends. Seating deflections probably occurred in the early stages of compres-
sion due to crushiiug of high points on specimen ends. These seating deflec-
tions resulted in higher than actual strains, and thus lower than actual
elastic moduli. The Q test strain and failure values were probably influenced
very little by any seating deflection. Most of the strain at failure occurs
during plastic deformation, at almost constant load, long after sample seating
during elastic deformation. These broad zones of plastic deformation are
shown in the Q test stress-strain curves in Appendix E.
142. An attempt was made to eliminate seating deflections by sulfur
capping Q test specimen ends, as described in Paragraph 94. Q test specimens
111688-1, 022289-1, and 030189-1 were sulfur capped. Comparison of the
stress-strain curves of Q specimens 022289-1 and 102888-1 (same batch design,
confining stress, and age of 022289-1 capped; 102888-1 uncapped) shows that
sulfur capping increased elastic modulus from 25 to 43 ksi or by 72 percent.
However, the Q elastic modulus of 022289-1 is still significantly less than
its companion UC elastic modulus (43 ksi compared to 207 ksi or 79 percent
less). This suggests that seating deflection problems still existed between
the sulfur caps and the pedestal and top cap of the triaxial chamber. Thus,
the Q elastic moduli values listed in Table 9 are probably incorrect and
should not be used for design. The Q strain at failure values listed in
Table 9 are probably nearly correct; however, they should not be used for
anything except rough approximation until the Q tests are reproduced and the
seating deflection problems solved.
83
Permeability values were calculated using the following equation, which is
derived from Darcy's law for flow through soil:
K = QLYw (12)
tA(P 2 - PI)
where
k - coefficient of permeability
Q - quantity of water flowing through cross-section A in time t
84
PART VI: ANALYSIS AND DISCUSSION
plex and time-consuming (expensive) triaxial tests to simple and quick (less
expensive) unconfined tests. This allows designers to estimate triaxial
148. Figures 42, 43, and 44 are companion plots for selecting a plastic
concrete batch design (cement factor, water-cement ratio, and percent
splitting tensile strength at a particular age. For a given cement factor and
bentonite content, there is a unique water-cement ratio which will produce an
8 in. slump plastic concrete. Figure 42 shows cement factor as a function of
water-cement ratio and bentonite content. Figure 42 was initially developed
from the Phase I unconfined compression test series data (Figure 38) and was
subsequently used to specify batch designs for the preliminary splitting ten-
sile test series and the triaxial test series. In addition, Figure 43 can be
used in conjunction with Figure 40 to specify unconfined elastic modulus.
content are presented in Figures 44 to 48. These figures allow more precise
85
46 0 . . . . . . . . . . . . . . . . . . . . . . . .. . . . . . . . . . . . ..
440 Slump= 8 /-1 in.
420-
lo 400-
40%
u380 20%
0_0% 10%
360-
0260
S340-
0
-. 320-
Q)
E 300-
U
280-
260-
240-
220
0.8 1.0 1.2 1.4 1.6 .8 20 2.2 2.4 2.6 2.8 3.0 3.2
Wter-cement Ratio. W/C
Figure 42. Cement factor versus water-cement ratio and
bentonite content
365 +
28
10%
.1000- 7
3* 28 365+
0%+
V)
(I)
L100-
0 1
Q) ~40% 9
c 60%
86
I*T
Bentonite= N%
0 28
4)1000 7
(0
0)
0.
E
C
Bentonite= 10%
Slump= 8 in.
In
~ioo
10I-
T--r--
1a
Wae cmntrto /
Fiue4.UcnieCopesiesrnt esswtr
ceen rai oa0pretbnoiecnetwt ie
benUsbaso urn g
487
Bentonite= 20%
6- Slump= 8 in.
365
a-
U
0)
D)
0 0 Vi -
1.E. . . . . .
0ae-e etrto /
C
2
1 I , I I
1.C. . . . .
Wae-eetFto /
1 4 11um6 8 24 in2.
8
2 1 1
Bentonite= 60%
Slump= 8 in.
O)
365t
09
0 9
c0 5
plete, however, because of the limited number of tensile batch designs and
curing ages.
150. A designer who needs plastic concrete of a certain unconfined
strength of 210 psi. Figure 43 then shows a choice exists at 210 psi between
bentonite mix at a curing age of 365+ days. Since the criterion is long-term
stiffness, the designer chooses the 40 percent bentonite mix. The designer
89
2 28 0 Slump= 8 inches
7
3
S-
Q. 6
C 3
100- 28
2 1) 1
4 -
e 60%
0.8 1 . 8 . 2 0 2 2 52 , , . .
designer thus has all the mix design parameters necessary to proportion a
batch (see batch design example, Table B3). An identical procedure can be
used to specify a batch design based on splitting tensile strength using
Figure 49.
151. A comparison between actual unconfined compressive strengths of
specimens from the (triaxial companion) unconfined compression test series and
90
50-
4o
3cI
S20
o
- 1 5
C _ 10 ~y=_48.53e
0
strengths than sulphur caps for the same specimen. An example of how
Figure 50 was used is as follows:
91
observed between E/qu and bentonite content. This suggests that the addi-
tion of bentonite has an equal effect on both unconfined elastic modulus and
unconfined compressive strength. However, E/qu as a function of age yielded
the following relationship:
4
_----- 00logtA + 1,000 (13)
qu
where
E p= elastic modulus, psi, calculated from strains measured with a
compressometer at age tA
92
1500
1400 QgQQQ 0 bentonite Slump= 8 in.
oQ.SL::P 10% bentonite
1300 4A&" 20% bentonite
0 40% bentonite
S1200 Otamt 60% bentonite
1100
1000
u900
0
800
: 700
g 6000
U0
2 400 0 1M 0-
o
300 o
5 200 - 2o
200 0
~~60
Age, days
157. From Figure 52 it appears that T/US is about constant at 0.26 and
300 lb/cu yd and ages 3 to 14 days. Further study must be conducted before
this equation can hold for the full range of cement factors and ages contained
in Figure 43.
function of curing age and bentonite content. Regression lines are drawn for
93
1.00 ... . . . .
0.9 Slump= 8 in.
0.90 Cement Factor= 300 pcy
.S 0.60
C
0
Cu050
-E 0.40
C
0 0
~0.30 @ 0 T/US- 0,26
nr 'C
00
.0.2000
L'. 10
C.
0 100 zoo 303 430 503C C
Unconifined Smear Strengtn, ps'
QC10007
S900-
ID 800 0
v) 700
P0 109%
"L600
E00
UO500 A 0
-o 40020
C 300
3O
00 - __ _ _ __ _ _ __ _ _ 40__
C
D100- 60%
0- 54I 769
5
27'6'9" S9 2 31 4 567,8,91 2 3
1 10 100 1000
Curing Age, days
94
each bentonite content. All the data points shown are averages of 1
to 4 tests and were corrected to a cement factor of 300 lb/cu yd using Fig-
ure 43. The equations for the regression lines are as follows:
qu, 01 - 278*log(age) + 580
qu,1oz - 95.6*log(age) + 340
qu,2 0 Z - 45.6*log(age) + 280 (14)
q., 40- 40.0*log(age) + 100
q.,602 26.1*log(age) + 0
where q is in units of pounds per square inch and age is in units of days.
The percent increase in unconfined compressive strength between ages of
3 and 600 days for each bentonite content are:
Percent
Increase
Bentonite in qu ,
Content 3-600 days
0% 90%
10% 58%
20% 36%
,to% 85%
60% 300%
160. For all CIUC tests the amount of water removed during consolida-
tion was carefully measured in order to better understand the influence of
consolidation on the stress-strain-strength behavior of plastic concrete.
Table 6 summarizes the amount of water removed during consolidation for each
CIUC test. The cement factor and water-cement ratio of a CIUC sample are
defined as:
95
1 cu vda
o
CF - weight of cement+bentonite in sample * volu
volume of sample
163. Pore pressure readings were taken for the CIUC tests of batches
080288-1 (bentonite content at 0 percent), 031889-1 (bentonite content at
20 percent) and 022289-1 (bentonite content at 40 percent). Plots of deviator
stress (al-a 3 ), change in pore pressure (Au), and pore pressure coefficient A
(Au/Aal) versus axial strain (c) are shown in Figures 56, 57, and 58. The
effective and total stress paths for each test are shown in Figures 59, 60,
and 61. Figures 56 through 61 show that greater pore pressures are developed
for higher bentonite contents. All of the tests have values of Ama, less
than 0.1, indicating that pore water carries relatively little of the load
applied during shear. Figure 59 shows that the total and effective stress
paths for 0 percent bentonite content samples are essentially identical.
However, Figures 60 and 61 show the excess pore pressures generated during
96
380.
370
360
J:ul 350
2340 01
0
ZE 330
E0
320
310
380.........................
All CIuC tests start at CF= 300 lbs/yd'
Ox
3707A
360
20S
350
.2340 a 0
U
00
Z 330- 0
E0
320
310
300 .T---r1~mTr-T-J
o. 80.9. 1.0U 1.1 1.2 1.3 1.4 1.5 1.6 1.7 1 81.9 2.0 2.1 2.2
Water-cement Ratio
Figure 55. Cement factor versus water-
cement ratio during consolidation
97
1500 .. .. .. .. .
1400
in1300
1200I
cn 800=
S700
C/) 600
1.- 500
0
c) 4001 Bentonite: 0%
~ 3QQAge: 3 days
300 CCOII 120 psi
o 200 abk: 20 psi
100
000.5 1.01.20
Axial Strain,
10
( 5
-10
000.5 1.01.20
Axial Strain,
0.0 10
'.0.000
- 0.0 10
98
1 5 0 0 ... .. l....ll l llf lll l ll l |I l ll l l ll ll l l
.........
l ll l ll l
1400
a 1300
1200
C1100
-1000
- 900
800
09700
Ln 600
500
400 Bentonite: 20%
Age: 58 days
3 00 r. 1 : 200 psi
r 200 r-"k: 100 psi
100
25
0.05
-0.00
-0.05- . ,I
99
1000 1 1 1 11 11111t I 7I I
MI I rr to it1 11 I Ii II I I if III, I I I I III I I III ." i
S900
800
I700
600
in 500
0I 400
0 .300
.2 Bentonite: 40S
> 200 Age: 14 days
C) O',,': 200 psi
100 ab.Ck: 100 psi
40-
~i20-
0.10 -TT__TrT~T .
0.06
<~ -0.02
-0.06
100
1000-
Batch: 080288-1 acau= 120 psi
900- Bentonite: 0% awx 20 PSI -j
Age: 3 days Auh4~x= 12.5 psi.
800Aq~x 0.01
700
6005
- ~effective stress p(a t hl
to 500-
400
300-
100
0 1CO 30040050'06070
200'6 300 900 1-000
p= ac-,-a
3 /2
1000-
:Batch: 031889-1 aCELL= 200 psi
900- Berntonite: 20% aa~zx= 100 psij
-Age: 58 days Auwm= -44 psi
aoA,,.. -. 09
700
600
C'J
400-
200
100 /
0~
0 160 2(03,0 ' 7 5060066 0 30 C00 00C
p= a,+j 5 /'2
Figure 60. Total and effective stress paths for GIUG
test 031889-1
101
6OO
Batch: 022289-1 CELL= 200 psi
Bentonite: 405 aWK= 100 psi
Age: 14 days tuv =46.8 psi
500 Am 0.08
400
C-4
200
Total Stress Path
100
shear for the 20 and 40 percent bentonite content samples are great enough to
content. Each failure envelope was constructed from two points, a CIUC test
and its corresponding UC test. For the 0 percent failure envelope, the CIUC
data point is the effective failure point of test 102688-1. For the 20 and
40 percent failure envelopes, the CIUC data points are the effective failure
points of tests 031889-1 and 022289-1 (Figures 60 and 61). The values of
angles were developed from so few points they are only rough estimates. They
are presented only for use in obtaining preliminary approximations of CIUC
shear strength. More CIUC tests with pore pressure measurements are required
to better define plastic concrete friction angles.
165. Additional testing was planned to study the effect of strain rate
on pore pressure generation but was unable to be performed because the testing
102
2000 ................
Curing ages of tests: On- 14 days
1800 20%- 58 days
40%- 14 days
1600
1400
205
1200
C-, CIUC tests with pore 405
J 1000 pressure m-jasurements
800
/,
- 2.o = 50 .
600 T"= 42
400
200 uCompanionUC
tests
0-
0 200 400 600 800 1000 1200 1400 1600 1800 2000
p= aT+a 3/2
machine could not deflect at a rate significantly slower than the 0.05 in./min
deflection rate used for the tests described above.
103
from the design charts presented in Figures 42 and 43 or from an actual UC
tests. For example, a designer needs an estimate of the 7-day CIUC shear
strength of a sample with a 20 percent bentonite content at a confining stress
of 200 psi. First, an estimate of the UC, 7-day, 20 percent bentonite shcar
strength is obtained from Figure 43. Then the normalized shear strength value
corresponding to 200 psi confinement and 20 percent bentonite content is
obtained from Figure 63. Finally, the unconfined shear strength is multiplied
by the normalized shear strength value to obtain the CIUC shear strength.
15.0 ....IIIIIIIIIl
5,14.0 O.ap 0% bentonite A
3
C P- -0-02 0% b e nt o n it e
-o
13.0 ____ 40% bentonite 40X
12.0 7
5 111.0
10.0
A14
C 9.0
C
o 8.0
Z) 7.0
6.0
C7
a! 5.0 140
S4.0
30
3.
2.0
21.0
0.0 I I I I, , l i ' I l IT I l 250i
i l, I I I300~l,
,l I , I
effective confining stress. Because CIUC elastic moduli were calculated from
strains measured by gross deflection and corresponding UC moduli were calcu-
same age with deflection measurements taken with both the compressometer and
104
00000o Ox bentonite
0000OC0 20% bentonite 6
6.0 AAAAA 40% bentonite
5.0
4.0
OM A3 40
2.0$
1.07cA
0~ 50 101020 25 230N5
12.0 tt
~- 14.0
11.07
1
950 0 15 00% 0 5
17.0000 05 etne
16.0A14030 20 etne
5.0 4059 betoit
14.0
15 3.0 3
.S 12.0
Q1.0
80
07.00 00 20 20 30 5
105
2500 . . . . . . . . . . . . . . . .
. 2000
C
1500
V 1000.
00
00
o 0 0
.2 500, 0
0-0
0 500 1000 1500 2000 2500
Elastic Modulus. Cornpressometer, ksi.
Figure 66. Unconfined elastic modulus measured by gross
deflection versus unconfined elastic modulus measured
by compressometer
106
3 .5 0 .. .. . .. ... ... . .. .. ... .. . ... ... . .... .. .. .. ... 1 , ,, , , ,, ,,, , ,, ,, ,, ,
oQQQ 0% bentonite
Eo3o 20% bentonite
3.00 a&&&& 40% bentonite
o14
C
5 2.50 3 44
.7
2.00
03
1.5 0
A7
1 00
o 0.50
107
a. CIUC Test 091488-1. at Time of Shear Test
Bentonite content 0 percent
Cement factor 328 lb/cu yd
Water-cement ratio 1.0
Confining stress 250 psi
Back pressure 50 psi
Test age 3 days
Slump at mixing 8 in.
Void ratio, after consol 0.217
b. Comparison 0 Tests, at Time of Shear Tests
Bentonite content 0 percent
Cement factor 326 lb/cu yd
Water-cement ratio 1.0
Confining stress 200 psi
Test age 3 days
Slump at mixing 8 in.
Void ratio 0.252
174. Much of the difference in elastic moduli and strain at failure can
probably be attributed to the seating deformation problems with Q tests
described in Paragraph 139. The difference in shear strength, however, is due
entirely to differences in internal structure of the specimen. Because they
were not consolidated, the void ratios of the Q tests were higher than that of
the CIUC test. A higher void ratio implies greater spacing of particles
within the concrete matrix. This greater spacing allows more interparticle
movement in the Q tests which in turn results in lower shear strengths and
elastic moduli and higher strains at failure.
108
3 00 0 .......
.................. . ..............
. ............ .......
2750 cuC (Son.- O. CF- 328. W/CF- 1 0. slump- 8 in.)
2500
2250
,2000
1750 1
0 1500
to0
q 1250
a-TEST (Ben' On0.CF- 326. w/CF-I 0. siumQ=- 0 n -
-
0 1000
S 750 -
-4
500
250
The effects of bentonite, confining stress, and age are each addressed below.
curves for each triaxial batch contained in Appendix E and test summaries in
Tables 8 and 9.
The influence of
bentonite content on triaxial
stress-strain-strength behavior
176. Bentonite content has the most dramatic effect on the triaxial
109
Bentonite S.. Rsi
percent CIUC 0
0 695 450
20 479 254
40 351 146
The percent drop in elastic modulus between 0 and 40 percent bentonite content
is 77 percent for CIUC tests and 83 percent for Q tests. These decreases are
more dramatic than those of shear strength and indicate that the addition of
bentonite reduces stiffness more than it reduces shear strength. Strain at
failure generally increases with the addition of bentonite. This increase.
however, is much greater between 20 and 40 percent bentonite than between
0 and 20 percent bentonite. This indicates that a threshold exists somewhere
between 20 and 40 percent bentonite where the space between aggregate parti-
cles in the concrete matrix becomes great enough to allow particle movement.
In addition, the increase in strain at failure is greater for Q tests than for
CIUC tests, most probably because the Q tests have higher water-cement ratios
and lower cement factors. However, comparisons of Q elastic modulus and
strain at failure may be incorrect due to the seating deflection problems
discussed in Paragraph 139.
110
The influence of confin-
ing stress on triaxial
stress-strain-strength behavior
178. In general, shear strength, elastic modulus, and strain at failure
all increase with confinement. These increases with confinement are greater
with increasing bentonite content. A comparison between any batches at the
same age and confining stress shows that the ratios of CIUC shear strength and
Q shear strength to companion unconfined shear strength increase with increas-
ing bentonite content, as shown in Figures 63 and 67, respectively. This is
also true of the ratios CIUC elastic modulus and strain at failure to compan-
ion unconfined elastic modulus and strain at failure as shown in Figures 64
and 65, respectively. These trends suggest that confinement has a greater
effect on the looser matrices of higher bentonite mixes. The rate of increase
of shear strength, elastic modulus, and strain at failure decreases above
100 psi effective confining stress, particularly for Q tests. For CIUC tests,
this phenomena is the result of the reduced effects of consolidation on cement
factor, water-cement ratio, and void ratio as consolidation/confining stress
is increased (Paragraph 160). As consolidation stress is increased, incre-
mental gains in shear strength, elastic modulus, and strain at failure are
more a function of confinement than of changes in cement factor and water-
cement ratio. At a certain consolidation pressure, no additional consolida-
tion can occur because the particles in the concrete matrix cannot be pushed
any closer together. Gains in shear strength, elastic modulus, and strain at
failure at confining pressures above this point are only a function of
confinement.
111
180. For CIUC tests at 100 psi effective confining stress:
* Age - 8 days.
** Average of two tests.
strength between 3- and 7-days age. In contrast, at the same effective con-
fining stress, 20 percent bentonite concrete experiences a 27 percent increase
above; however, the magnitudes of the changes are much less. For Q tests at
* Age - 8 days.
** Average of two tests.
The increases in shear strength between 3- and 7-days age are 12 and 6 percent
for 0 and 20 percent bentonite concrete, respectively. The values of strain
at failure and elastic modulus of the Q tests are too variable to draw any
specific conclusions.
112
Permeability of Plastic Concrete
113
10~ *-0
0 00 0 2 0% b e n .
AAAAA 40% ben.
0
.00
'00
100
0 1A 0 0
Age, days 0
114
PART VII: SUMMARY AND RECOMMENDATIONS
185. Part VII summarizes the important findings of the research pro-
Summary
186. This research program has shown that the addition of bentonite
Stress-strain-strength
behavior of plastic concrete
187. A summary of the stress-strain-strength behavior of plastic con-
115
Permeability and
erodibility of plastic concrete
188. Permeability and erodibility of plastic concrete are as following:
a. The permeability of plastic concrete at an age of 10 days is
between 10-8 and 10-9 (Figure 69).
Recommendations
116
angles. Additional CIUC tests should also be performed over a greater range
of cement factors to expand the scope of the design data. In addition, all of
the Q tests in this test program should be repeated to better evaluate Q elas-
tic modulus and strain at failure. Specific additional triaxial testing
should include the following:
a. Mix designs of 250 and 400 lb/cu yd.
b. More CIUC shear tests with pore pressure readings to evaluate
CIUC stress paths and friction angles.
C. Triaxial shear tests at strain rates cf 0.005 in./min or less
to confirm independence of pore pressure generation from
strain rate.
d. Long-term triaxial testing, i.e. 28 and 90 days, to confirm
age independence of normalized CIUC and Q stress-strain-
strength parameters.
e. Long-term permeability testing, i.e. 1 year or more, to obtain
design permeability values.
191. In addition, a Phase III test program should be conducted to eval-
uate the behavior of plastic concrete under different loading and environ-
mental conditions. This program should include the following:
a. Creep testing to evaluate the long-term strain behavior of
plastic concrete under constant load.
b. Cyclic triaxial testing to simulate the changes in stress an
earth dam cutoff wall might experience due to fluctuations in
reservoir level.
C. Permeability tests with typical ground water pollutants to
evaluate plastic concrete performance in an aggressive subsur-
face environment.
d. Additional erosion tests should be conducted to quantify the
erodibility of plastic concrete.
117
REFERENCES
Alvarez, L., and Mahave, G. 1982. "Convento Viejo's Plastic Concrete Cut-
off," Proceedings. Fourteenth International Conference on Large Dams.
pp 339-353.
Amsler, D. E., and Grygiel, J. S. 1977. "Capping Concrete Cylinders with
Neoprene Pads," Research Report No. 46, New York State Department of
Transportation, New York.
Evans, J. C., Stahl, E. D., and Drooff, E. 1987. "Plastic Concrete Cutoff
Walls," Proceedings, Specialty Conference, Geotechnical Practice for Waste
Disposal, Geotechnical Division, American Society of Civil Engineers, Special
Publication 13, pp 462-472.
Fenoux, G. Y. 1985. "Filling Materials for Watertight Cutoff Walls,"
Fifteenth International Conference on Large Dams, Bulletin 51.
Habib, P. 1977. "Grout Mixes and Plastic Concretes for Impervious Cutoffs,"
Proceedings of the Ninth Conference of International Conference on Soil
Mechanics and Foundation Engineering pp 89-91.
Hankour, R. (Translator). 1979. "Interface Between a Dam and It's Abutments
and Foundations-Continuity of Sealing Works," Proceedings of Thirteenth Inter-
national Conference on Large Dams, p 4.
Peck, R. 1986. "Report on Seepage Control Measures," Mud Mountain Dam for
Seattle District, Corps of Engineers, pp 1-21.
118
US Army Engineer Division, North Pacific. 1987. "Report of Tests on Plastic
Concrete," North Pacific Division, Corps of Engineers Memorandum W.O
No. 87-C-329.
Woodward-Clyde Consultants. 1981. "Data from Laboratory Testing Program,
Colbun Main Dam," Clifton, NJ.
119
APPENDIX A: DETAILED TEST DATA FROM COLBUN MAIN DAM LABORATORY
PROGRAM AND MUD MOUNTAIN DAM LABORATORY PROGRAM
Table Al
Summary of Batch Designs for Colbun Main Dam Research
Program (Woodward-Clyde Consultants 1981)
The batches prepared, and their components and quantities used are as
follows:
The batches prepared, and their components and quantities used are as
follows:
A3
0
E E0
0 0 ) 001
C: 0." f
0
)u0 II
0
L. 0*0.
4) 0'
(~ 0 cc 10
'.0 '0
02t '1: -
(N a,
I-''
oo 0 (N(N coN
- .0 .0 'D '0w
ID'. 0~ ' C ' co'
00
W r
0o'0
4) L4
m 0o
&N .0 !
0~
.00
21 E
4)d
.00
w 40
'-A4
4) ..... . . ...
00Ccc
. - .1 0 .0 .
0 0 n -- ,
O.*L
Go . 0.
0 r0 0
0 ~ u .. u. 0 .
-0 0-1C 0
bo ., bo l MO4
X".- Nd1 - w 4-.1a
0 0 3t 0
(4 0 ( 0 0 0 In
0 C 0 ~ 0
-~~0 .--.
0 -- - 4D ' 0
u 4d (A(N
'~- C~ 1
$4 (4 c , - ,
In, 01 a,-
04 .
14 - CU ID0
4)
.oA5
Table A4
Summary of Colbun Main Dam Research Phase I Permeability Tests
(Woodward-Clyde Consultants 1981)
ke 200 C
Batch ac Stage Hyd. cm/sec
Identification k/cm2 No. System II- x 108
Proposed Mix 2.980 1 Closed 42 43.1
2.980 2-1 Open 45 42.9
2.980 2-2 Open 45 43.2
2.980 2-3 Open 45 40.7
2.980 2-4 Open 45 41.0
2.973 3-1 Open 84 41.4
2.973 3-2 Open 84 41.7
2.973 3-3 Open 84 42.3
2.973 3-4 Open 84 41.8
2.973 3-5 Open 84 37.4
Alternate Mix A 2.994 1 Closed 36 3.7
2.987 2-1 Open 45 4.1
2.987 2-2 Open 45 3.8
2.987 3-1 Open 84 3.6
2.987 3-2 Open 82 3.6
Alternate Mix B 2.973 1 Closed 35 3.5
2.973 2-1 Open 45 4.0
2.973 2-2 Open 45 3.2
2.966 3-1 Open 84 3.0
2.966 3-2 Open 82 3.2
A6
Table A5
Summary of Colbun Main Dam Research Phase II Permeability Tests
(Woodward-Clyde Consultants 1981)
ke 20oC
Batch ac Stage Hyd. cm/sec
Identification kg/cm 2 No. System i,.- x 10-8
Proposed Mix AD 3.001 1 Closed 20 17.2
3.001 2-1 Open 100 17.8
3.001 2-2 Open 100 17.5
3.001 2-3 Open 100 17.8
2.994 3-1 Open 200 18.2
2.994 3-2 Open 200 18.1
2.994 3-3 Open 200 17.8
2.994 3-4 Open 200 18.2
Mix No. 1 2.994 1 Closed 24 17.4
2.987 2-1 Open 100 17.0
2.987 2-2 Open 100 17.3
2.987 2-3 Open 100 17.3
2.994 3-1 Open 200 17.4
2.994 3-2 Open 200 17.4
2.994 3-3 Open 200 17.2
2.994 3-4 Open 200 17.2
Mix No. 2 3.001 1 Closed 19 9.6
3.001 2-1 Open 100 9.4
3.001 2-2 Open 100 9.7
3.001 2-3 Open 100 9.9
3.001 3-1 Open 200 9.5
3.001 3-2 Open 200 9.8
3.001 3-3 Open 200 9.7
3.001 3-4 Open 200 9.6
A7
Table A6
Summary of Colbun Main Dam Research Phase III Permeability Tests
(Woodward-Clyde Consultants 1981)
ke 200 C
Batch ac Stage Hyd. cm/sec
Identification k/Lcm 2 No. System Io X 10 -8 Remarks
Mix No. 2 2.99 1-1 Closed 20 7.3
2.99 2-1 Closed 40 7.2
2.99 3-1 Open 100 7.0 Initial
W/C - 5.56 2.99 3-2 Open 100 6.9 After overnight
2.99 3-3 Open 100 7.1 After overnight
2.99 4-1 Open 200 7.2 After overnight
2.99 5-1 Open 282 7.9 At maximum io
2.99 5-2 Open 281 7.5 At maximum i.
2.99 5-3 Open 282 7.4 At maximum io
Mix No. 1 3.00 1-1 Closed 20 11.9
3.00 2-1 Closed 40 11.8
3.00 3-1 Open 100 12.1 Initial
W/C = 5.97 3.00 3-2 Open 100 11.7 After overnight
3.00 4-1 Open 200 12.5
3.00 5-1 Open 282 13.5 At maximum io
Took specimen down and installed No. 4 screens
3.07 1A-1 Closed 20 11.8
3.00 2A-l Open 100 11.8
3.00 3A-1 Open 200 12.2
3.00 4A-1 Open 282 13.6 Initial at maximum
io
3.00 4A-2 Open 282 10.0 After 24 hr
Mix No. 3 3.00 1-1 Closed 20 12.9
2-1 Closed 40 12.9
3-1 Open 100 15.5 Initial
W/C - 6.4 3-2 Open 100 13.7
3-3 Open 100 13.5
3-4 Open 100 13.5 After overnight
4-1 Open 200 14.1
5-1 Open 280 9.9 Initial
5-2 Open 280 15.1 After overnight
5-3 Open 280 16.0
A8
Table A7
Summary of Plastic Concrete Mix Designs and Tests
Mix No
NPDL No. A B C D
3097 3098 3099 3100
(Control)
1. Mix Characteristics
Cement + Bentonite 300 + 0 180 + 120 120 + 180 60 + 240
(C + B),* lb/cu yd
Unit water, lb/cu yd 354.2 535.1 682.6 1050.0
W/(C + B) ratio, by weight 1.18 1.78 2.28 3.50
Sand content, percent 50.0 48.0 48.0 48.0
Slump, in. (measured) 7 1/2 8 8 8 1/4
Air, percent (measured) 1.2 0.5 0.5 0.6
A9
Table A7 (Concluded)
Mix No
NPDL No. A B C D
3097 3098 3099 3100
(Control)
Young's modulus,
E x 103 psi 295.7 102.6 41.2 20.7
5. Presure Test **
Time, min
24 -- 0.2 0.0 2.6
48 -- .-- 3.8
A1O
APPENDIX B: CHEMICAL ANALYSIS OF CEMENT AND BENTONITE FINE AND
COARSE AGGREGATE GRAIN SIZE DISTRIBUTION
AND BATCH DESIGN EXAMPLE
Table BI
ComRarison of Grain Size Distribution of Tufts University
Aggregate to Grain Size Distribution of MUD Mountain
Dam Research Aggregate (NPSEN)
50 79 -- 86 -- 85 --
100 91 -- 96 -- 95 --
B3
Table B2
Chemical Analysis of Cement Used in Research
P 20 5 0.26 --
Insoluble Residue 0.25 0.75
Free CaO 0.34 --
Fineness (Air permeability) 375 m2 /kg 160
3
Density 3.12 Mg/m --
Calculated Compounds
C 3A 15
C3 S 52
C 2S 14
C4AF 6
(Continued)
B4
Table B2 (Concluded)
Calculated Compounds
C3 A 15
C3 S 55
C2 S 13
C4 AF 6
B5
Table B3
90 Barrel Bentonite
Sample 4
Analys is Result
Si0 2 55.8
A1 20 3 16.2
Fe2 0 3 3.5
CaO 2.9
MgO 3.0
S03 0.1
Na 2 0 2.02
K20 0.61
B6
Table B4
Batch Design Example
Gravel - 1.5 %
(Continued)
(Sheet 1 of 6)
B7
Table B4 (Continued)
(Bl)
V. W
where
W, - dry weight of material
G. - gravity of solids of material
1. - unit weight of water
therefore
570
Volume water - 62.
62.4 - 9.14 cu ft
Total = 10.71 cu ft
(3) The remaining volume of the cubic yard is made up to equal volumes of
sand and gravel:
I cu yd - 27 cu ft
27 - 10.71 - 16.29 cu ft
16.29 _ 8.15 cu ft
2
(Continued)
(Sheet 2 of 6)
B8
Table B4 (Continued)
(4) The dry weight of sand and gravel is then calculated using equation
BI to solve for W.:
Ws - N 5 7w
therefore
Weight sand - (8.15)(2.65)(62.4) - 1,348 lb
Weight gravel - (8.15)2.65)(62.4) - 1,348 lb
Bentonite - 60
Sand - 1,348
Gravel - 1,348
Water - 570
e. The dry weights are then corrected for hygroscopic moisture content:
Total weight - dry weight + weight of water
or
WT = +w (B2)
by definition
W
Water content, W -
Ws
therefore
(B3)
w.= w7W.
(Continued)
(Sheet 3 of 6)
B9
Table B4 (Continued)
WT - Wa + Wc Ws
or
WT = W(1+W,)
Corrected weights:
Cement - 240 (1.005) - 241.2 lb
Bentonite = 60 (1.10) - 66.0 lb
Bentonite - 66.0 lb
Sand - 1,388.0 lb
Gravel - 1,368.0 lb
Water - 502.8 lb
(Continued)
(Sheet 4 of 6)
BlC
Table B4 (Continued)
These are the weights of materials that were actually added to the mixer.
g. After batch was made weights were corrected for any differernce in water
added and for actual hygroscopic moisture content:
Suppose an additional 0.9 lb of water were needed to achieve
an 8-in. slump and that the following actual hygroscopic
moisture contents were calculated for the materials:
Actual Water Content, W c
Cement - 0.3 %
Bentonite - 10.3 %
Sand - 1.9 %
Gravel - 0.8 %
Summary of Actual Weights Added
29.36 lb
h. The values of the dry weights are then calculated and actual cement
factor, bentonite content, and water-cement ratio back calculated.
Volumes were again calculated using equation Bl.
Weight Volume
Components lb cu ft
Cement 12.46 0.063
Bentonite 3.05 0.018
Sand 70.63 0.427
Gravel 70.33 0.425
Water 29.36 0.471
Total 185.83 1.403
(Continued)
(Sheet 5 of 6)
BI1
Table B4 (Concluded)
185.83 lb
Theoretical unit weight - 1.403 lft - 132.5 lb/cu ft
29.36
Water-cement ratio - (12.46 + 3.05) - 1.893 - 1.89
(Sheet 6 of 6)
BI2
LMO&M AS 8MM3O AD~ VW
w
:Izz
oo
CD
a. 0U)i
o - 0
a)
200
of
mow la
IB13
-#IL
ZU AS- &DH
w _U L 2- -n-
> -a
0 00
L
co co
D CO -
o :6O
CD
UO - -- - - -
< ~ I
I 0
-4- 1 0
s 3t
LHW Al NaHDV
K:
zRJ~B14
wL A"EuM All VISIV02 LHO aIM
0 0 0 -0
z X,
'
CL
z Ln
of ~C*)
00
Z-
<-
cn,
ca
-4
B15
WU AWgV4% At 1US#VOD 1041: li
I
< CD w-t4
-a
DD
> C)--i
~C/
00
-4
~ 0
.00
"-4
B161
APPENDIX C: CALIBRATIONS OF RIEHLE TESTING MACHINE
AND 1,000 LB BEAM BALANCE SCALE
TESTING MACHINE CALIBRATION REPORT AND DATA
AMERICAN CALIBRATION & TESTING CO.
176 Wolnut Street
Lawrence, MA 01841
Machine Povi j
OMER Reading Readlng Mbchine trro- P. 1k,
lb lb lb Code
xam-
Tufts University 1 1 0 0 3
Location
Anderson Hall C 2 2 0 0 3
Platform Balance 10 10 0 0 3 F 5
Zapaclty _____
Bureau of Wts.
Bureau of Wts. ii
A1l-- 0-150 lb & m___q_ _ _
C3
CrrtifiraIr of Urrifirntion
178 Walnut Street Lawrence, Mt, C1E41
11 ,500 1 5,0,30 1b l
0
C. V. PMCecry
C4
Americar Calibration & Testirn; Co.
178 Walnut St.
Lawrence, MA 018JI
Mae hi no Provi ri
OWNER Reading Reading Nktbhie bror P. K
wI lb lb 2 Czde
UTfts
University 299.0 3f'3 -! .0 C. 3 1 &2
(5
American Calibration & Testing Co.
178 Walnut St.
Law.rence, MA 0181
OWK
Reingeeading rc Irror P. R
lb lb 2b Code
Raw
Tufts University 1I,0C5 i',Oo- S 03 1 & 3
Locat ion
Anderson hall 30,016 3o,000 !6 0.05 1 & 4
Civil Engineering Div. t 6C,052 60,000 V2 0. 0: TI & 4
PROVING RINGS
P. R Serial Loadine Verif. Date -
Code Nn. Ran e Lab. No. _-
5-27-86
1046 Cal. Ind. SJ1.0] /103221
5-2;-85
2 18248 0-2,400 lb Si.-2 1-0822
5-21-8b
10234 0-24,000 1 SJiT.01 /103221
5-21-Sb
140796 0-240S000 1 SJT.O1 /103221
5
I - __ _ __ --- _
C6
QCrtifirate of Urhrifiration
Awma UaIhrujm & Ugrsiinz (Co.
176 Walnut Street Lawrence, MA 01841
0-30,000 lb
0 3,000 -30,000 lb ______
'0Cal. j
Ind. Serial No. (9) of
1046 j18248
testin d es(s) used for ca~iwation:
110234 40796
Date($) of certificatio
Compan-s_
C7
TESTING MACHINE CALIBRATION REPORT AND DATA
Nochne Proving
OWNER Reading Reading Machine Zrror P. A,
lb lb lb % Code
Tufts University 298.3 300 -1.7 0.57 1 & 2
Locat ion
Anderson hall 596.7 600 -3.3 0.55 1 &2
C8
TESTING MACHINE CALIBRATION REPORT AND DATA
mahne Proving
OWNER Reading Readlng mhine 2 P. P
lb lb 2b Code
Name
Tufts Unviersity 15,005 15,000 5 0.03 1 & 3
Location
Anderson Hall 30,027 30,000 27 0.09 1 & 4
PROVING RINGS
P. R!erial Loading Vert. Date
Code No. Range Lab. Nc,
6-1-88
1046 Cal. Ind. SJT.01/103817
6-1-88
18248 0-2,400 lb SJT.01/103817
6-1-88
3 10234 0-24,000 11 SJT.01/103817
6-1-88
140796 0-240,000 SJT.01/103817 __
6
-puted Loads Corrected For
.emn'n. 70 F
Service Engineer Date
G. W. momy Aug. 29,1988
ASY'M SPee. Ul Calibration frequency =1 year
C9
APPENDIX D: SUMMARY TABLES OF UNCONFINED COMPRESSION TESTS (PHASES I
AND II), BRAZILIAN TENSILE TESTS (PHASES I AND II), AND
FLEXURAL BEAM TESTS
Table D1
Batch ID CFben v/c SL G %air cylinder ID age storage strain water qu I eu AVG STO %SID
060387-1 266 0 1.43 7.25 142 0.5 060317-1-DS 5 cure bot gross - 603 0.0035 603
206
060317-I-A 7 cure box gross - 674 129 0.0025 674
060317-1-8 62 cure box gross - 774 432 0.0022 774
060387-1-C 131 wet room gross 9.4 797 492 0.0025 797
060387-2 311 0 1.31 8.75 Il 0 060307-2-J 5 wet room gross - T60 382 0.0035 656 75 11%
060387-2-L 5 wet room gross - 585 320 0.0029
06037-1-! 5 wet room gross - 623 251 0.0033
060387-2-G 7 wet room gross - 691 603 0.0020 697 69 10%
060317-2-N 7 wet root gross - 785 406 0.0029
060317-2-D 7 cure box gross 616 60 0.0034
060381-2-F 62 wet room gross 8.9 919 538 0.0023 891 28 3%
060387-2-B 62cure box gross 864 469 0.0028
061687-1 413 0 0.91 7.75 142 1.8 061687-1-1 3 cure box gross 8.3 1379 586 0.0035 1379
01687-1-1 7 wet room gross 8.8 1716 954 0.0024 1722 133 81
06107-1-L 7 wet room gross - 1536 10970.0020
(Continued)
(Sheet I of 7)
D3
Table Dl (Continued)
D4
Table D1 (Continued)
110387-1 229 10 2.13 7.75 139 - 110387-1-A 3 wet room gross - 150 59 0.0052 155 3%
110317-1-3 3 wet room gross - 158 104 0.0031
110387-1-C 3 wet room camp - 158 244 0.0031
110317-1-1 7 wet room gross - 240 619 0.0026 255 9
110387-1-1 7 wet room gross 14.8 264 937 0.0020
110387-1-G 28 wet room comp 296 507 0.0012 297 2 it
110387-1-0 28wet room gross 14.2 301 358 0.0026
110387-1-D 28 wet room gross - 295 417 0.0022
110387-1-J 75 wet room gross 14 322 181 0.0035 316 5 it
110387-1-1 75wet room gross - 312 209 0.0027
110387-1-L 75 wet room camp - 313 707 0.0014
110387-1-P 90 weL room cop - 286 373 0.0024 295 7 21
110387-1-0 90 wet room gross 13.7 301 312 0.0032
110387-1-1 90 wet room gross - 299 365 0.0029
110387-1-J 542 wet room camp 0 288 1059 0.0021 291 3 1%
110387-1-K 487 vet room camp 12 293 826 0.0026
110387-2 275 10 1.75 8 138 - 110387-2-A 3 wet room gross 12.5 244 295 0.0033 246 2 it
110387-2-B 3 vet room gross - 248 311 0.0026
113087-2-C 3 let root gross - 245 i34t.5046
110387-2-G 7 wet room gross - 414 500 0.0027 411 7 2t
110387-2-F 7 wet room gross - 18 311 0.0027
110387-2-1 7 wet room gross - 402 361 0.0023
110387-2-N 28wet room comp - 529 S20 0.001f 490 28 5%
110387-2-P 28 wet room gross 12.5 475 444 O.024
110387-2-J 28 wet room groft - 466 375 0.0024
110387-2-I 90wet room camp - 483 716 0.0019 504 15 31%
110317-2-L 90 wet room groas- 519 625 0.0018
110387-2-0 90wet room gross 12.8 510 456 0.0021
110387-2-H 529 wet room coup 0 473 1264 0.0021 481 14 3%
110387-2-1 487 vet room comp 11.1 501 i11 0.0018
110381-2-1 542 wet room coup 0 470 1059 0.0019
110387-3 319 10 1.5 8 138 - 110387-3-A 3 wet room gross 14.1 379 310 0.0026 374 5 it
110387-3-B 3 wet room ;rcss 359 358 0.0032
110317-3-G 7 let room gross - 558 783 0.0017 575 16 3%
110317-3-1 7 wet room gross - 597 626 0.0019
110317-3-1 7 wet room grca - 569 570 0.0011
110317-3-F :8wet room comp 636 593 0.0025 670 41 61
110387-3-1 28 wet room gross 12.7 647 290 0.0030
110387-3-M 28wet room grcst - 728 932 0.1019
110311-3-1 90 wet room gross - 695 717 0.0016 121 37 5%
110387-3-J 90 wet room gross - 773 663 0.0021
110387-3-0 90 wet room coim - 696 1325 0,0019
(Continued)
(Sheet 3 of 7)
D5
Table Dl (Continued)
110317-3-H 487 wet room comp 10.4 711 1402 0.0015 635 87 14%
110387-3-1 542 wet room coop 0 681 1404 0.0017
110387-3-0 529 wet room coup 0 514 1239 0.0006
Blatch
ID C!ben u/c SL G %air cylinder ID age storage strain water qu I ev
111087-1 353 10 1.4 7.25 138 - 111087-1-A 3 wet room gross 13.5 531 415 0.0034 552 19 3%
111087-1-B 3 wet room gross 547 518 0.0030
111087-1-C 3 wet room coop - 577 741 0.0028
111087-1-! 7 wet room gross 14.3 '64 566 0.0029 790 26 3%
111087-1-D 7 wet room comp - 916 702 0.0024
111087-1-I 29 wet room coop - 978 1379 0.0017 962 16 2t
111087-1-J 29 wet room gross 14.3 967 1070 0.0019
111087-1-G 29 wet room gross - 941 932 0.0024
111087-1-L 94 wet room copm 14.1 931 1289 0.0018 900 15 6%
111007-1-1 94 wet room coop - 821 466 0.0021
111087-1-H 94 wet room coop - 939 1153 0.0016
111087-1 480 wet room coup 11.3 997 1552 0.0021 976 22 21
111087-1-N 522 wet room coup 0 904 1671 0.0018
111087-1-P 535 wet room coup 0 946 16810.0016
060487-1 268 20 2.03 9.25 133 0.6 060487-1-A 4 cure box gross - 163 6o 0.0042 160 3 2%
060487-1-D 4 cure box gross - 158 67 0.0043
060487-1-B 33 cure box neop 12.9 215 214 1%
060487-1-C 33 cure box neop - 213
060587-1 300 20 2 9.25 130 0.2 060587-1-C 7 care box gross - 160 43 0.0053 159 1 2%
060587-1-A 7 cure box gross -158 9 0.0055
060587-1-D 32 wet room neop - 176
176
060587-1-n 60 care box gross 16.5 171 82 0.0042 172 1 1%
060587-1-1 60 care box gross - 172 82 0.0033
060587-1-1 129 wet room gross 19.3 182 96 0.0040 182
061887-1 369 20 1.53 6.75 132 0.7 061887-1-G 4 wet room gross 13.8 361 199 0.0031 367 2 0%
061887-1-0 4 wet room gross - 368 152 0.0032
061887-1-1 7 wet room gross 14 441 257 0.0031 440 9 2%
061837-1-1 7 wet room gross - 428 234 0.0031
061087-1-1 7 wet room gross - 450 243 0.0032
061887-1-3 29wet room neop - 431 401 23 6%
061187-1-0 28wet room neop 13.8 396
061117-1-1 28 wet room neop - 376
061817-1-I 50 wet room gross - 533 264 0.0030 540 5 1%
061117-1-1 50 wet room gross 12.7 545 420 0.0022
061687-1-L 50 wet room gross - 542 363 0.0026
061817-1 660 wet room comp 0 521 1096 0.0024 529 15 3%
061867-1-4 559wet room comp 0 512 10580.0013
061817-1-? 655 wet room cop 13.4 540 1097 0.0011
D6
Table Dl (Continued)
(Continued)
(Sheet 5 of 7)
D7
Table Dl (Continued)
061287-1 321 60 2.23 7.75 122 0.8 061287-1-B 3 cure box gross 20.1 37 18 0.0091 35 3 at
061287-1-1 3wet room gross - 32 15 0.0117
061287-1-A 7 cure box gross 22 45 12 0.0098 40 5 12
061217-1-J 7wet room gross - 35 11 0.0098
061287-1-0 28 cure box neop 18.8 37 35 1 4%
061287-1-1 28 wet room neop 20 35
0612187-1-KS 28let room aeop - 33
061287-1-c 54wet room gross - 50 19 0.0085 50 1 21
061287-1-B 54 wet root gross 20.5 49 16 0.0062
061207-1-I 54wet room gross - 51 26 0.0074
061287-1-C 122 wet room gross 28.1 73 20 0.0094 73
(Continued)
(Sheet 6 of 7)
D8
Table Dl (Concluded)
072717-1 231 60 2.19 6.5 127 0.9 072787-1-1 3 cure box gross 17.4 25 6 0.0101 25 0 1%
072717-1-I 3 let room gross - 25 7 0.0096
072787-1-0 3 vet room gross 14.1 25 7 0.003
072717-1-1 7 vat room gross - 25 13 0.0077 26
072717-1-0 7 cure hot gross 17.9 26 9 0.00i4
072717-1-1 7 vet room gross 16.7 28 13 0.0077
072707-1-1 77 met room gross 22.2 53 13 0.0092 56 3 5%
072787-1-C 77 vet room gross 21.1 59 12 0.0096
072787-1-J 94 vet room gross - 52 35 0.0065 49 2 4%
072787-1-1 94 let room gross 21.2 49 39 0.0053
072787-1-1 94 vet room gross - 48 29 0.0067
072717-1-9 586 vet room cop 21.5 85 147 0.0044 85
(Sheet 7 of 7)
D9
Table D2
Summary of Phase II Unconfined Compression Test Program
sample I Sample 2
080288-1 290 0 3 8 1.5 144.6 442 642 0.33 391 975 0.28
091488-1 302 0 3 7 1/2 1.4 146.5 793 - 759 1042 0.27
030189-1 299 0 7 7 1.4 145.2 760 1627 0.19 717 1477 0.23
102688-! 295 0 14 8 1.5 243.9 979 1750 0.15 945 188 0.16
082688-1 304 20 3 8 1/2 1.8 133.4 282 467 0.32 :6 446 0.33
080588-1 297 20 3 8 1.9 128.8 295 695 0.38 302 572 0.39
091088-1 302 20 3 8 1.9 139.7 290 446 0.41 297 446 0.44
081088-1 306 20 8 8 1/2 1.8 139.2 375 464 0.26 342 464 0.29
082388-1 289 20 7 8 1/4 1.9 138.8 - 245 466 0.35
090188-1 299 20 7 8 1/2 1.9 138.1 336 512 0.27 340 519 0.28
111688-1 300 20 14 8 1.9 138.8 408 619 0.33 397 565 0.31
091588-1 305 40 3 81/4 2.1 133.2 117 199 0.78 117 215 0.9
090988-1 306 40 3 8 2.1 133.3 127 114 0.78 127 103 0.61
091988-1 305 40 3 8 1/2 2.1 132.9 116 162 0.88 116 137 1.02
101488-1 302 40 3 8 1/4 2.2 134.3 124 179 0.92 121 161 0.7
083188-1 305 40 7 8 1/4 2.1 129.5 146 159 0.67 144 180 0.76
092886-1 296 40 7 8 2.3 133. 134 241 0.64 128 255 0.73
102880-1 301 40 14 81/2 2.2 135.0 152 209 0.66 150 214 0.74
022289-1 308 40 14 7 1/2 2.1 132.9 155 190 0.72 153 223 0.49
10088-1 300 40 14 8 2.2 129.7 157 277 0.73 164 279 0.77
D10
Table D3
Summary of Phase I Brazilian Splitting Tensile Test Program
Slup: 8 inches
test ID then age CF I/C length diameter Load tensile
strength
days lbs/cu. yd. in. in. lbs. psi
053088-1-C 0 3 261 1.56 12.136 6.016 8850 77
053088-1-8 0 3 261 1.56 12.034 6.039 9050 79
053088-1-A 0 3 261 1.56 12.074 6.022 9775 86
053088-1-1 0 7 261 1.56 12.153 6.040 14550 126
053088-1-9 0 7 261 1.56 11.987 6.048 14800 130
D53088-1-J 0 7 261 1.56 11.987 6.037 16600 146
053068-1-G 0 2s 261 1.56 12.020 6.000 17850 158
053088-1-L 0 28 261 1.56 12,120 6.051 17100 148
053088-1-F 0 28 261 1.56 11.980 6.051 19150 168
053088-1-N 0 92 261 1.56 12.078 6.031 17700 155
053088-1-K 0 92 261 1.56 12.094 6.047 17200 150
053088-1-I 0 92 261 1.56 12.016 6.000 17500 155
060288-1-8 0 7 346 1.18 12.104 6.029 23950 209
060288-1-A 0 7 346 1.18 11.973 6.034 21650 191
060288-1-! 0 7 346 1.18 11.903 6.040 19950 177
060288-1-D 0 28 346 1.18 12,094 6.022 26200 229
060288-1-J 0 28 346 1.18 11.938 6.042 26800 237
060288-1-1 0 28 346 1.18 11.969 6.034 23750 209
060288-2-3 20 7 255 2.22 12.093 6.042 5475 48
060288-'-1 20 7 255 2.22 11.835 6,062 5125 45
060288-2-N 20 7 255 2.22 12.094 6.058 4650 40
060288-2-D 20 28 255 2.22 12.188 6.037 6050 52
060288-2-3 20 28 255 2.22 12.250 6.064 5625 48
060288-2-L 20 28 255 2.22 12.047 6.051 6725 59
060288-2-8 20 92 255 2.22 12.156 6.036 5400 47
060288-2-C 20 92 255 2.22 12.156 6.052 6275 54
060288-2-G 20 92 255 2.22 12.125 6.063 6300 55
061988-1-A 20 3 362 1.44 12,036 6.076 9600 84
061988-1-8 20 3 362 1.44 12.073 6.057 7450 65
061988-1-P 20 7 362 1.44 12.170 6.045 11250 97
061988-1-L 20 7 362 1.44 12.120 6.044 11575 101
(Continued)
DI I
Table D3 (Concluded)
D12
Table D4
Summary of Phase II Brazilian Splitting Tensile Test Results
DI 3
Table D5
Summary of Flexural Beam Test Program
1:3P1/2bd^2
D14
APPENDIX E: PHASE II CIUC, Q, AND UC STRESS-STRAIN CURVES BY BATCH
3 2 50 -............. ............ ........... .
Bentonite: 0%
3000- Age: 3 days
ar~e,: 120 psi
2750- abCk: 20 psi
S2500
2250-
2000-
S1750-
1500
. cluc
o 1250
750
500
uc
250
3250- _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _
Bentonite: 0%
3000--cu Age: 3 days
- OCol 250 psi
2 750 Crbok: 50 psi
CL 2500
0
2250
2000-
S1750
0
o1250-
Vo 1000
750
UC
500,-
250
0-
0.00 0.50 1.00' 1.50 2.0062.50 3.00 3.50 4.00 4.50 5.00
Axial Strain, %
Deviator Stress vs. Axial Strain
Batch: 091488-1
E3
3250-
Bentonite: 0%
3000- Age: 7 days
O'cel: 200 psi
2750 abac: 100 psi
'~2500-
A ~ cluc
b
2250-
2000
1750-
1500-
0
.21250-
o1000-
0 (sulfur end cops)
750-
500-U
250
0.00 0.50 1.00 1.50 2.00 2.50 3.00 3.50 4.00 4.50 5.00
Axial Strain, %
Deviator Stress vs. Axial Strain
Botch: 030189-1
3250 -
Bentonite: '0
3000 Age: 14 days
Cluc 20psi
2750- Crbk: 1 Opsi
S2500
2250-
2000
C,,
S1750-
1500
.2 1250-
0 1000-- uC
750
500
250
0- ......... "I "'
...... ..... ~
' ' " " I
.......... "
.... "....
0.00 0.50 1,00 1.50 2.00 2.50 3.00 3.50 4.00 4.50 5.00
Axial Strain, %
Deviator Stress vs. Axial Strain
Batch: 102688-1
E4
2 7 50 -.. . . . . . . . . . . . . . . . . . . . . . . . . . . . .
Bentoriite: 20%
2500 Age: 3 days
or,,: 70 psi
.6 2250 ao.,: 20 psi
C2000-
U
S1750
(I)
500
1250
250
0-0
6 2000-
S1750-
~j1500-
if)
8, 1250
> 1000-
750-
500-
E5
2750 Bentonite: o
2500- Age: 3 days
- crU. : 2 50 ps i
u~ 2250O~k. 50
225
6 2000-
b 1750
V)
U)
~?1500 cu
01250
1000-
750
500-
250- uc
07
0.0 2,0 40 6.0 8.0 10.0 12.0
Axial Strain. %.
Deviator Stress vs. Axial S5:-an
Batch: 091088-1
27 5 0 . . . .. . . . . . . . . . . .v.. .
Beitonite- 20%
2500 Age: 7 days
c", 120 psi
2250 (back: 20 psi
62000-
~'1750
LO,
1 1500-
125ED0-
-
0 ~ uc
I1000)
750 -
asoo 2
E6
2 7 5 0 . .......... ......... ......... .......... .........
Bentonite: 20%
2500- Age: 7 days
- Cceii: 250 psi
.6 2250 aback: 50 psi
A~
&2000
S1750-
S1 500-Cu
1250-
0
> 1000-
750-
500-
250 uc
0.0 20 .0 60 80 1.0 20
Axia; Strain. %
Deviator Stress vs. Axial Strain
Batch: C82.388-1
2750-
- Bentonite: 20%
2500 -Age: 7 days
12750
S1500-
1250-
> 1000-
750
500
250 u
Lc
E7
2 75 0 .. . . ... .. ... ... .. ... ... .. ...
Bentonite: 2059
2500Age: 14 days
ciuc c. 400 ps I
cluc ak: 100 Psi
Cri 2250
tS 2000-
01750
a! 1500
750-
UC
250
1100
S1000
Lni -4
cn900
7()o
600
500
300
2007
130-
0 TT '" .. ......
E8
16 0 0-: ............... .... ........ 1 ..... ....
1500- Bentonite: 40%
- Age: 3 days
1400 aw 120 psi
CrbOk: 20 psi'
cn1300-
*1200
I1100-
tD 1000
U'900-
07 800
o 00 cluc
.0 600
S500-
400-
300-
2 000
100 uc
1600-
Bentonite: 40%
1500 Age: 3 days
1400- Cci 250 psi
-ar 3 k: 50 psi
1300
1200
t 1 100
100
800
700
6 00
5 00'
4 00
30)
2 00
300 aC
E9
16 00 ..... .... ... .... ... .
1500
1400 CiUC
ji 1300Benton'te: 40%
1200- Age: 3' days
acl 350 psi
ab~.50 psi
'000
U)
U' 00
U1 00
-'0
400
30
~00 - u
0-
0.0 2.0 40 6.0 8.0 10.0 12.0 14.0 16.0
Axial Strain, %
Deviator Stress vs. Axial Strain
Batch: 101488-1
16 00 -........ ...........
1500Bentonite: 40%
1500Age: 7 days
1400 arc.1: 120 psi
CrbOCk: 20 psi
~1300
1200-
I1100-
t:1000
in 900-
(J800
o700-
.0 600_________ __
o500-
400-
300-
200Q
1140
10.0 20 4 60 8.0 10042 16.0
Axial Strain.
E10
1600- .........
1500-
1400
cluc
u1300
Bento'nite: 40%
120Age: 7 days.
1100- crel 350 psi
tD 10 0-UbOCk: 50 psi
V)900-
S800
o700-
0
>~ 6007
S500-
400-
z00 --
100 iJC
S900'
S800 CU
S700-
.0 600
0 500-
400
300 a
200-
100 uC
0-.
00 2.0 4.0 80 .. 0.0... ..
0 12.0
I.....
14.0
. ...
16..
Axial Strain, %
Deviator Stress vs. Axial Strain
Batch: 102888-1
Eli
1 6 0 0 ,.,.... ,,,,....... ,..... ,.,, ,,,..,..,.........,,.,,,,..........,.,,.,
S900
LOO
co 520
=0
0 (sulfur end cops)
-_30/
UC
16 0 0 ...........
........................... .................
1500 Bentonite: 40%
Age: 14 days
1400 oc,,.: 400 psi
S1300 ciuc b
Oa 100 psi
1200
1100
o 1000 /
i~800
S700-
. 600
r 500
400 a
300
200 '
100 Ur
1_00 O 4,? 0 8
0 10.0 12.0 14.0 !.
20 1 . 16.0
Axial Strain, %
Deviator Stress vs. Axial Strain
Batch: 100688--l
E12
APPENDIX F: SUMMARY TABLES OF PERMEABILITY TESTS
Specimen Dimensions:
Height, ft.: 0.96
Area, sq. cm.: 176.4
Head
Elapsed Cell Gage Gage Diff. loss Grad. Flow Perm.
Date Time Time Press. Press. Press. Press. across across thru
sec. psi. Ped. Top Cap psi. sample sample sample
psi. psi. ft ml. cm/sec
Specimen Dimensions:
Height, ft.: 0.98
Area, sq. -.a.: 174.5
Head
Elapsed Cell Gage Gage Diff. loss Grad. Flow Perm.
Date Time Time Press. Press. Press. Press. across across thru
sec. psi. Ped. Top Cap psi. sample sample sample
psi. psi. ft ml. cm/sec
F3
Batch ID: 030189-1
Cement Factor: 325 lbs./cu.yd.
Bentonite: 0 %
Fabrica. Date: 3/1/89
In Pipette #: 5
Out Pipette #: 6
Specimen Dimensions:
Height, ft.: 0.95
Area, sq. cm.: 183.6
Head
Elapsed Cell Gage Gage Diff. loss Grad. Flow Perm.
Date Time Time Press. Press. Press. Press. across across thru
sec. psi. Ped. Top Cap psi. sample sample sample
psi. psi. ft ml. cm/sec
3/4/89 11:45 0 198 100 50 49.5 114.2 120.4 0.0
3/4/89 16:30 17100 200 99.7 49.9 48.8 112.5 118.6 4.8 1.3E-08
Specimen Dimensions:
Height, ft.: 1.01
Area, sq. cm.: 173.2
Head
Elapsed Cell Gage Gage Diff. loss Grad. Flow Perm.
Date Time Time Press. Press. Press. Press. across across thru
sec. psi. Ped. Top Cap psi. sample sample sample
psi. psi. ft ml. cmjsec
11/2/88 16:20 0 201 100 50 50 114.6 113.8 0.0
11/3/88 10:30 65400 200 100 50 50 115.3 114.6 2.2 1.7E-09
11/4188 14:54 167640 201 100 50 50 115.8 115.0 3.1 1,5E-09
11/6/88 15:03 340980 203 100 50 50 116.2 115.4 4.9 1.4E-09
F4
Batch ID: 080888-1
Cement Factor: 313 lbs./cu.yd.
Bentonite: 20 %
Fabrication Dat 8/5/88
Specimen Dimensions:
Height, ft.: 0.98
Area, sq. cm.: 183.1
Head
Elapsed Cell Gage Gage Diff. loss Grad. Flow Perm.
Date Time Time Press. Press. Press. Press. across across thru
sec. psi. Ped. Top Cap psi. sample sample sample
psi. psi. ft ml. cm/sec
Specimen Dimensions:
Height, ft.: 0.96
Area, sq. cm.: 167.8
Head
Elapsed Cell Gage Gage Diff. loss Grad. Flow Perm.
Date Time Time Press. Press. Press. Press. across across thru
sec. psi. Ped. Top Cap psi. sample sample sample
psi. psi. ft ml. cm/sec
F5
Batch ID: 081088-1
Cement Factor: 351 lbs./cu.yd.
Bentonite: 20 %
Fabrication Dat 8/10/88
Specimen Dimensions:
Height, ft.: 0.98
Area, sq. cm.: 169.8
Head
Elapsed Cell Gage Gage Diff. loss Grad. Flow Perm.
Date Time Time Press. Press. Press. Press. across across thru
sec. psi. Ped. Top Cap psi. sample sample sample
psi. psi. ft ml. cm/sec
8/12/88 13:30 0 119 20.2 9.8 11.0 25.5 25.9 0.0
8112/88 14:45 4500 119 20.2 9.8 11.1 25.7 26.1 0.1 7.5E-09
8112/88 22:32 32520 119 20.1 9.8 11.0 25.5 25.9 1.5 1.2E-08
8/13/88 19:56 109560 119 20 9.6 11.0 25.4 25.8 2.8 8.3E-09
8/15/88 00:59 214140 119 20 9.6 11.0 25.3 25.8 1.7 3.7E-09
Specimen Dimensions:
Height, ft.: 0.96
Area, sq. cm.: 164.8
Head
Elapsed Cell Gage Gage Diff. loss Grad. Flow Perm.
Date Time Time Press. Press. Press. Press. across across thru
sec. psi. Ped. Top Cap psi. sample sample sample
psi. psi. ft ml. cm/sec
F6
Batch ID: 090988-1
Cement Factor: 365 lbs./cu.yd.
Bentonite: 40 %
Fabrica. Date: 9/9/88
Specimen Dimensions:
Height, ft.: 0.95
Area, sq. cm.: 165.1
Head
Elapsed Cell Gage Gage Diff. loss Grad. Flow Perm.
Date Time Time Press. Press. Press. Press. across across thru
sec. psi. Ped. Top Cap psi. sample sample sample
psi. psi. ft ml. cmlsec
Specimen Dimensions:
Height, ft.: 0.94
Area, sq. cm.: 165.0
Head
Elapsed Cell Gage Gage Diff. loss Grad. Flow Perm.
Date Time Time Press. Press. Press. Press. across across thru
sec. psi. Ped. Top Cap psi. sample sample sample
psi. psi. ft ml. cm/sec
F7
Batch ID: 092888-1
Cement Factor: 364 lbs./cu.yd.
Bentonite: 40 %
Fabrica. Date: 9/28/88
Specimen Dimensions:
Height, ft.: 0.95
Area, sq. cm.: 164.1
Head
Elapsed Cell Gage Gage Diff. loss Grad. Flow Perm.
Date Time Time Press. Press. Press. Press. across across thru
sec. psi. Ped. Top Cap psi. sample sample sample
psi. psi. ft ml. cm/sec
1011188 20:57 0 340 50 24.9 25.1 57.9 61.1 0.0
10/3/88 17:18 159660 340 50 24.9 25.1 57.9 61.1 2.2 1.4E-09
Specimen Dimensions:
Height, ft.: 0.96
Area, sq. cm.: 168.9
Head
Elapsed Cell Gage Gage Diff. loss Grad. Flow Perm.
Date Time Time Press. Press. Press. Press. across across thru
sec. psi. Ped. Top Cap psi. sample sample sample
psi. psi. ft ml. cm/sec
F8