Fibretherm FT12: Instruction Manual

Fibretherm FT12
Instruction
Manual
Please read this instruction manual with care before you start operating
the system!
Please observe the safety instructions of this manual marked with in

order to avoid any dangerous handling!
Warnung vor
einer Gefahrenstelle
FT12
13. June 2007_GB
Content
1 Important notes..........................3 9 Methods execution...................25

1.1 How to use this instruction manual................... 3 9.1. Loading of sample carousel.......................... 25
1.2 Explanation of symbols.................................... 3 9.2. Start programme........................................... 26
9.2.1. Functions during the programme run ........ 26
2 Safety...........................................4
10 On-line mode .........................27
2.1 Operation as directed....................................... 4
2.2 Safety instructions............................................ 4 11 Error messages......................28
2.3 Work bench / Authorized user.......................... 5
2.4. Danger spots at the instrument....................... 5 12 Maintenance............................30
3 Technical description.................6 12.1. Service and cleaning................................... 30
12.2. Spare parts.................................................. 30
3.1. Warranty conditions......................................... 6 12.3. Accessories................................................. 31
3.2. Technical data.................................................. 6 12.4. Trouble shooting.......................................... 31
12.5. Disposal....................................................... 32
4 Description of the Fibretherm...7 12.5.1. Information for the Disposal of Electric and
Electronic Instruments within the European Uni-
4.1 Front view Fibretherm FT 12............................ 7 on.................................................................... 32
4.2. Rear view Fibretherm...................................... 8 12.5.2. Ban on Materials according to ROHS Regula-
tion 2002/95/EG.............................................. 32
5 Assembly and installation.........9 12.5.3. Transfer.................................................... 32
5.1. Check for transport damage............................ 9

5.2. Unpack apparatus........................................... 9
5.3. Parts list........................................................... 9
5.4. Installation..................................................... 10
5.4.1. Set up tubing connections.......................... 10
5.4.2. Mains connection....................................... 11
5.5. Setting into operation.................................... 12
6 Description of the Fibretherm 13

7 Control panel............................14
7.1. Keyboard....................................................... 14
8 Methods definition....................15
8.1. Schematischer Überblick Programmierung... 15
8.2. Main menus................................................... 16
8.3. System-Settings............................................ 16
8.3.1. Selection of languages............................... 16
8.3.2. Contrast...................................................... 17
8.3.3. Monitoring of tanks..................................... 17
8.3.4. Settings rinsing........................................... 17
8.3.5. Settings for heating up............................... 18
8.3.6. Menu Service............................................. 20
8.3.6.1. Calibrate pump/ discharge flow............... 20
8.4. Prepare methods– Define programme.......... 22
8.5. Examples for programming........................... 24
Fibretherm FT12
1 Important notes
1.1 How to use this instruction manual

Please make sure that the persons working with the Fibretherm have read and
understood this manual in order to observe all the instructions.
This instruction manual must be accessible to all users at any time and is a part
of the Fibretherm system!
The instrument will be called 'Fibretherm' in the entire document.
This instruction manual only explains the technical details necessary for the ope-
ration of the instrument but is NOT a complete technical description.
The security advises given in this manual have to be observed under all circum-
stances! The symbols at the border of the text emphasize the dangers cited in
the text.
Symbols at the instrument warn of possible dangers and will refer you to this
manual!
The copy right of this manual remains with C.Gerhardt GmbH & Co. KG
Reproduction and copying are only allowed with the permission of C.Gerhardt
GmbH & Co. KG
1.2 Explanation of symbols
Attention! Attention!
Advance notice of danger spots, carefully Read instruction manual!
read instruction manual!
Warnung vor
Hot surface! Use eye protection!
Mains voltage! Use protective gloves!
Warnung vor gefährlicher,

elektrischer Spannung
Beware of hot liquids and vapours! Be careful to avoid injuries of your
hands!
Attention! Advance notice of substances

which might be a health risk or cause
irritation!
Fibretherm FT12
2 Safety
2.1 Operation as directed

Fibretherm is a system for the fully automated boiling and filtration process during
the Crude fibre-, ADF- and NDF-determination. Up to 12 samples can be digested
and filtered simultaneously. Please observe the general regulations and applica-
tions for the determination.
Applications for the various areads of usages can be obtained at Gerhardt on
request.
Make sure to use the instrument according to our instructions, especially:

- all instructions of this manual
- the regulations in place in the country the instrument is used
Warnung vor
All other usage is not recommended!
C. Gerhardt GmbH & Co. KG is not liable for any damages caused due to non
recommended usage
- any modifications are not allowed for safety reasons
Warnung vor
- repairs of electric, electronic or mechanical components may only be done by

authorized personnel!
2.2 Safety instructions

The DUMATHERM corresponds to the technical standard used at this date and
observes the safety rules and regulations in place.
It is understood that the user has to observe
Warnung vor
- the accident prevention regulations in place

- the general accident prevention regulations
- EU-regulations or other country specific instructions
Indicating label and danger symbols must not be taken off!

Warnung vor
Make sure that no liquid gets into contact with cable connections or the interior of
the electrical parts of the unit!
- Danger of electric shock!
In case of an emergency disconnect from mains immediately!

Warnung vor
Always pull the mains plug before opening!

- Danger of electric shock!
Prior to each start of the Fibretherm, make sure that the glass container is closed
tightly. Danger of burns and splashing liquids!
Make sure to wear protective gloves when taking the glass container out and wear
protective glasses as well.
The glass container is very hot and there is the danger of burns!
Attention when handling chemicals! Please observe the manufactures safety

instructions (see label) and your national safety regulations!
Fibretherm FT12
2 Safety
2.3 Work bench / Authorized user

The FIBRETHERM must not be run in damp or hazardous location. The maxi-
mum humidity allowed is 80 %, the maximum room temperature must not ex-
ceed 35 °C!
Warnung vor
The FIBRTHERM has to be placed on a horizontal and stable footprint.

Warnung vor
The FIBRETHERM may only be operated by trained staff or especially trained

persons.
The user has to:
Warnung vor
- read, comprehend, and observe the operation manual

- wear suitable clothes for laboratory work
- deny access to any unauthorized personnel
2.4. Danger spots at the instrument
- Attention, danger of crushing when the hood is put

down on the glass container!
Warnung vor
- Attention, danger of burns on the top of the glass

ceramic-hotplate!
Warnung vor
- Attention, danger of splashing hot or caustic liquids

at the tubing connections at the back of the instru- Warnung vor
ment!
- Attention, danger of burns when taking out the hot

glass container!
Warnung vor
Fibretherm FT12
3 Technical description
3.1. Warranty conditions

The DUMATHERM is manufactured following the high quality guidelines of EN ISO
9001:2000. On the basis of the C. Gerhardt conditions of warranty our products
are guaranteed for 1 year, as long as the apparatus is used in accordance with
the instructions mentioned in this manual.
Please note that the working parts are excluded from warranty.:
- Glass container, order-no. 52826
- Glass-spacer, order-no.: 1772
3.2. Technical data
Fibretherm FT 12
Order-No.: 175000
Type: FT 12
Nominal voltage: 230 V, 50 - 60 Hz
Programs: 9
Cooling water
consumption: ca. 3 l/min
Cooling water pressure: min 0,5 bar
Air pressure: ca. 4,5 bar
Interface: 2 x RS 485
Dimensions (WxDxH): 330 x 650 x 860 mm
Weight: ca. 42 kg (empty)

Fibretherm FT12
4 Description of the Fibretherm
4.1 Front view Fibretherm FT 12
6
5
1 Control panel (key pad), order-no.: 52918

Input of program and control
2 Glass ceramic-heating area, order-no.: 52829

Infrared-heating area, 1800 W
3 Protective hood, can be taken out, order-no.: 52816

Behind the hood there is the glass condenser and tubes
4 Drip tray, order-no.: 52887

After taking out the glass beaker, you can also take out the drip tray and put it
below the protective hood in order to catch any residue of distillate or chemi-
cals. During the analysis you can store the drip tray on the protective hood.

5 Quick clamping handle, order-no.: 52856
Quick clamping handle serves for:
A - Inserting and taking out of the drip tray
B - Inserting and taking out of the carousel
6 Electronic- and pump cabinet

Electronic and pumps are separated from each other and are built in splash
proof.
7 Glass container, Order-no.: 52826

The carousel containing the 12 FibreBags is put into the glass container.
Fibretherm FT12
4 Description of the Fibretherm
4.2. Rear view Fibretherm
10
8
1
6
11
5 12
4 13
3 14
2
1 Ventilator 9 Appliance plug with mains cable

Keeps inside of instrument cool. Connection for mains cable, Order-No.: 1312
2 Drip tray, order-no.: 52189 10 Interface RS 485 (2 x)
Pull it towards the backside when you want to clean Quality control conform to ISO/GLP is possible
it. using the interface RS 485
3 Suction of sample residue 11 Inlet compressed air
Connection for PVC-tube 8x12, Connection for compressed air tubing, order-no.:
order-no.: 22604 52199
4 Cooling water inlet with cleaning sieve 12 Inlet 2 for chemicals (Detergent 2)
Connection thread 3/4 inch for water inlet tube Connection for PVC-tube 8x12,
10/17, order-no.: 22802 order-no.: 22604
5 Inlet 1 for chemicals (Detergent 1) 13 Inlet for cleaning water with cleaning sieve
Connection for PVC-tube 8x12, Connection thread 3/4 inch for cleaning water inlet
order-no.: 22604 tube 10/17, order-no.: 22802
6 Tubing pump 14 Cooling water outlet
Easily accessible for maintenance Connection for PVC-tubing 8x12,
7 Socket for level detector order-no.: 22604
Connection for diode plug, 3-pin or level detector
for set of storage tanks
8 Mains switch with excessive current protection
Order-no.: 52834
Here you turn instrument on / off. The switch turns
off when current consumption is too high.
Fibretherm FT12
5 Assembly and installation
5.1. Check for transport damage

Before assembling the apparatus please check if the content of the box is com-
plete and intact!
In case of any damage, please notify your carrier (post, rail, road) as well as your
supplier!
5.2. Unpack apparatus

You need a connection (cold water pipe) with 1/2 inch thread to connect it to the
water supply.
The FIBRETHERM must not be run in damp or hazardous location. The maximum
humidity allowed is 80 %, the maximum room temperature must not exceed 35
°C!
Warnung vor
Please observe the local water and waste regulations and those of your public
water supply company!
Please note that the length of the inlet and outlet tubing is restricted to 2 metres.
The equipment should be located on a fixed laboratory bench, close to the cold
water connection and the drain. There should be sufficient space for the set of
tanks below the work bench.
Make sure to take a faucet, which can be connected to the inlet tubing perma-
nently.
The water pressure must be at least 0,5 bar in order to activate the integrated
pressure detector.
The Fibretherm comes fully pre-assembled. Please unpack the equipment with
care!
1. Place the equipment on the work bench.

2. Unpack accessories
The exact contents of the delivery can be checked by the following list.
5.3. Parts list
1 x Fibretherm FT 12, ready to use, Order-No.: 1755

12 x Glass spacer, Order-No.: 1772
1 x Bag with 100 FibreBags, crude fibre, Order-No.: 1776
4 x PVC-tubing 8/12, 2 m, Order-No.: 22604
2 x PVC pipe 10 x1 mm, 400 mm long, Order-No.: 25451
2 x Water inlet tubing grey, 10/17, 2 m, Order-No.: 22802
1 x Seal ring, Order-No.: 52891
1 x Tool hook wrench (50 x 25 mm) for seal ring, Order-No.: 19999
1 x Compressed air tubing, Order-No.: 52199
1 x Mains cable, Order-No.: 1312
1 x Instruction Manual
1 x Test report
Fibretherm FT12
5.4. Installation
5.4.1. Set up tubing connections

Put the storage tanks for acids, alkalis as well as sample residue under or next
to the working bench.
Make sure, however, that those containers are not higher than the Fibretherm!
When establishing the tubing connections, make sure to observe the labeling of
the connection at the rear of the instrument. Always make sure that the connec-
tions are sitting tight.
Abb. 5.4.1. Tubing diagram
230 V AC
14
1
0
13
11 1
12
2
8 9 10
4,5 bar
3
7 6 4
5
17 16 15
ater inlet tubings

W
- Connect the water inlet tubing for cooling water (pressure resistant hose 10/17,
pos.1) with the cooling water inlet at the rear of the instrument and your in-
house water supply.
- Connect the water inlet tubing for the rinsing water (pressure resistant hose
10/17, pos.2) with the rinsing water supply at the rear of the instrument and
your in-house water supply.
10 Fibretherm FT12
ater outlet tubing

W
- Put the water outlet tubing (PVC-tube 8/12, Pos. 4) on the corresponding socket
at the rear of the instrument and guide the end of the tube to the drain.
Sample outlet tubing

- Put the sample outlet tubing (PVC-tube 8/12, Pos. 5) on the corresponding
socket at the rear of the instrument and guide the end to the tube to the sample
residue container (Pos. 15).
hemicals inlet tubing

C
- Put the chemicals inlet tubing 1 (PVC-tube 8/12, Pos. 6) on the corresponding
socket at the rear of the instrument and guide the end of the tube to the che-
micals reservoir 1 (Pos. 16). Additionally plug the PVC-tubing on the end of
the tubing.
- Put the chemicals inlet tubing 2 (PVC-tube 8/12, Pos. 7) on the corresponding
socket at the rear of the instrument and guide the end of the tube to the che-
micals reservoir 2 (Pos. 17). Additionally plug the PVC-tubing on the end of
the tubing.
ompressed air connection

C
- Connect the compressed air tube (Pos. 3) with the quick coupling and the com-
pressor or the local compressed air supply. Check the tight fit of the tube and
set the pressure reducer to 4,5 bar. Please make sure to check the instruction
in the manual of the compressor.
Reservoir connection
Tank with level sensor
- Put the diode plugs of the level sensor (Pos. 8, 9, 10) to the connector (Pos.
11) and connect these with the connection socket for the level monitoring (Pos.
12).
Tank without level sensor

- Put the diode-dummy plug (Pos. 13) on the connection socket for the level
monitoring.
5.4.2. Mains connection

Please check the nominal voltage on the product information plate before connec-
Warnung vor
ting to the mains. Should the nominal voltage deviate for more than +/- 10%, then
you must contact your service engineer.
- Make sure that the mains switch at the rear of the instrument is in position
"0"
- Connect the mains cable to the rear appliance plug first
- Connect the mains cable to the shockproof socket
Fibretherm FT12 11
5.5. Setting into operation

Attention when working with acids and alkalis! Make sure you observe the safety
instructions concerning work with hazardous materials!
1. Turn the instrument on using the mains switch.
2. After turning the instrument on, the display shows following messages:
C. Gerhardt - Current date

Nov 14 2006
Fibretherm - Display of actual firmware-version

Version 1X81
Fibretherm - Main menu

Menu
3. You can now start the programming or start a program which was previously
entered. Make sure to read the following chapters!
12 Fibretherm FT12
6 Description of the function Fibretherm
1 Glass ceramic-hotplate, Order-No.: 52829 0 Valve for cleaning water (ON/OFF),

1
Order-No.: 17101
2 Insert rack (carousel), Order-No.: 52805 and 11 Unit injector element for cleaning water, Order-No.:
FibreBags 52813, incl. seal ring, Order-No.: 52891
3 Axis carousel (suction pipe for chemicals) 12 Inlet for cooling water
4 Filter glass, Order-No.: Order-No.: 52846 3 Valve for cooling water (On/Off),
1
Order-No.: 52825
5 Glass condenser small, Order-No.: 52847 14 Glass condenser big
6 Peristaltic pump, Order-No.: 52849 15 Cooling water outlet
7 Pinch solenoid valve, Order-No.:10385 16 Sample waste tank, 20 l
8 Unit injector element 17 Chemicals tank acid, 20 l
9 Inlet for cleaning water 18 Chemicals tank lye, 20 l
Fibretherm FT12 13
7 Control panel
7.1. Keyboard
The Fibretherm can be programmed and controlled via the keyboard of the control
panel
Fig. 7.1.:
Keyboard
Fibretherm FT 12
2 13
Enter + Start
3 14
Menu Lift
4 12
Esc Stop

Fibretherm
5 6 7 8 9 10 11
1. Display Displays all relevant information
2. Key "Enter" Confirms and/or stores the current value
3. Key "Menü" Calls up main-menu fields
4. Key "Esc" Aborts current programmee step,

Return to previous step,
Return to main menu.

5. Key "+" Increases value
6. Key "-" Decreases value
7. Key "Stop" Aborts the running analysis

Return to main menu
8. Key "Start" Starts programme
9. Key "Suction" Chemicals residue are manuelly absaugen
10. Key "Addition" Detergents are added manually
11. Key "Rinsing" Clean glass container manually
12. Key "Lift up" Lift is raised manually
13. Key "Lift down" Lift is lowered manually
4. Status lamps
1 Red = Lift cannot be moved
Green = Lift can be moved
14 Fibretherm FT12
8 Methods definition
8.1. Graphic presentation of the method

In the following illustration you get a graphic presentation of the progarmme.
There are three stages of this programme:
1. Heating up phase
2. Cooling down phase
3. Waschphase
Fig. 8.1.
Heating delay
General method
1. Heating up phase
execution
Addition Intervall Heating up
detergent rotation
Heating Intervall rotation

2. Cool. down phase
Intervall
rotation Cool down
Suction
Addition
water
3. Rinsing phase
Rinsing
Suction
Fibretherm FT12 15
8.2. Main menus
The programme is divided in 3 main menu items which can be accessed by pres-
sing the key "Menu"
Fibretherm - Start window

Menu Is shown after each start of Fibretherm
Menu
Methods - Main menu 1 "Execution"

Execution You start a selected menu with the programme.
Additional detailed information available in chapter
Menu "9. Execute method".
Method - Main menu 2 "Generation"

Definition In this menu you generate and manage pro-
grammes. Detailed information available in chapter
Menu "8.4. Programme method".
System - Main menu 3 "System-settings"

Settings In this menu you determine the basic settings like
e.g. selection of language, contrast, monitoring of
Menu tank etc. Additional detailed information available
in chapter "8.3. System-Settings".
8.3. System-Settings
In the main menu "System settings" the following settings are done: selection of
language, contrast, monitoring of tank, settings elute, Settings heating up and
service.
System Press key "Enter", to activate the first menu level. By

Settings pressing the key "Menu" you can then activate the
other menu items as well.
Enter
8.3.1. Selection of languages

Select language Using this function, you can select the desired lan-
guage.
Menu
Enter
Select language You can choose from the following languages:

<- English +> - German
- English
Enter
+ - French
16 Fibretherm FT12
8.3.2. Contrast
Contrast Using this function you can adapt the contrast of the
display to the conditions of light.
Menu
Enter
<- Contrast +>
Enter
+
8.3.3. Monitoring of tanks

Tank control Using this function you can activate the monitoring of
the set of tanks/ or de-activate (only if you have set of
Menu tanks with level sensor).
Enter
Tank control
<- active +>
Enter
+
8.3.4. Settings rinsing

Settings Using this function you can set the cycle for the rinsing
Rinsing of the glass container.
Menu
Enter
Water filling - Define the amount of rinsing water to be added.

1.30l - Setting range 0 - 4,99 L
Enter
+
Rotation - Define the duration of the rotation of the carou-

Time 30s sel
- Setting range 01 - 59 s
Enter
+
Rotation - Setting for interval

Pause 06s - Setting range 0 -.59 s
Enter
+
Fibretherm FT12 17
Suction - Enter the duration of suction of the rinsing water

1min 28s - Press key "Enter", to switch from minutes to se-
conds..
Enter
+ - Setting range 0 - 3 min, 0 - 59 s
Wash out - Display of duration of an entire cycle

Time 3min 56s - Press key "Enter", to switch from minutes to se-
conds.
Enter - Programming "Rinsing" is finished
- Setting range 0 - 3 min, 0 - 59 s
Settings 8.3.5. Settings for heating up

Preheating Using this function you can define the heating up per-
Menu formance during the programme.
Enter These settings are important e.g. to avoid formation
of foam and to reduce heating up time.
Prior to define the settings for the heating up perfor-
mance, you have to calibrate the pumps.
Make sure to also read chapter 8.3.5.1. Calibrate
pumps/discharge flow.
Rotation - Define the rotation of carousel

Time 05s - Should the samples have excessive foaming; the
formation of foam can be reduced by setting a lon-
Enter
+ ger duration of the rotation. However, it is advisable
to set the rotation as short as possible.
Rotation - Setting for interval

Pause 20s - A longer duration of the interval between the rota-
tions can reduced the heating up time.
Enter
+ - Setting range 01 - 59 s
Heating delay - The delayed heating helps to avoid damaging the

after start 30s glass containers e.g. by heating till dry. Thus, it is
advisable to start the heating process only after
Enter
+ adding the detergents.
Detergent 1 - Please indicate here, at what temperature deter-

Heat up to 80 °C gent 1 will start boiling.
- Setting range 10 - 99 °C
Enter
+
18 Fibretherm FT12
Detergent 2 - Please indicate her, at what temperature detergent

Heat up to 80 °C 2 will start boiling.
Enter
+
H2O-Rinse - Please enter whether you want to heat up the

Heat up to 60 °C rinsing water.
Enter
+
Detergent 1 - Indicate up to which temperature detergent 1 has

Cool dwn to XX°C to cool off, till it can be sucked off.
- The suction is necessary, to extend the life span
Enter
+ of the suction pump.
Detergent 2 - Indicate up to which temperature detergent 2 has

Cool dwn to XX°C to cool off till it can be sucked off.
Enter
+
H2O-Wash - Indicate up to which temperature rinsing water has

Cool dwn to XX°C to cool down till it can be sucked off.
Enter
+
Fibretherm FT12 19
Service 8.3.6. Menu Service

In the menu Service you can define the following
settings:
Enter - Calibrate pump/ discharge flow..
Make sure to do the calibration prior to taking the
instrument into operation for the first time!
- Calling up of amount of hours of operation, call up
statistics.
8.3.6.1. Calibrate pump/ discharge flow

Pump 1 Detergent The discharge flow of the pump depends on the vis-
KOH cosity of the detergents used, the delivery height and
Menu
the other conditions of the ambiance.
Enter Due to this reason, you have to calibrate the pumps
prior to the first run or when switching to a different
chemical.
- Put the glass container on the hotplate and press
key "Lift down".
- Press the key "Enter", if you want to calibrate the
pump
Overview Pump 1 Detergent - Press key "+" or "-", to make your selection from
List of detergents: <-Detergent 1+> the list of detergents.
- You also have the option not to calibrate the pump.
H2SO4 + In that case, select the dashed line from the list.
Enter
KOH - Press key "Enter" to confirm.
NaOH
ADF-Lsg
NDF-Lsg Pump 1 Cal. - Pump delivers for 30 s
Scharrer 30s=0,30l - Please follow the instructions to aerate the hoses
H2O (see marginal note).
Lösung 1 Enter - Press key "Enter", to start process.
Lösung 2
---------------
Pump 1 Cal. - After expiration of the time, you must measure the
Important, aerate! 06/30s delivered amount in litres (determine the dischar-
When connecting the ge volume with measuring cylinder). In order to
hose for the first time or Enter do so, press key "Lift up" and take out the glass
when changing the che- container.
micals, there will be air in - Stellen Sie anschließend den leeren Glasbhälter
the hose. In order to get wieder auf die Heizplatte und drücken Sie die Taste
the air out of the hoses, "Lift runter".
please start process. As
soon as the liquid is pum-
ped evenly in the contai- Pumpe 1 Set - Press key "+" or "-", to enter the actual-discharge
ner, press key "Stop". volume and then press key "Enter", to confirm
Then, you have to start entry.
calibration again. Enter
+
20 Fibretherm FT12
Pump 2 Detergent - Now you can calibrate pump 2. To do so, press

H2SO4 key "Enter".
- The procedure is the same as described for pump
Menu 1
Valve Detergent The addition of the rinsing water is done from your in
H2O-Rinse house water supply. Depending on the pressure in the
pipe, the discharge volume is very different in each
Enter laboratory. This is the reason, why the rinsing water
amount has to be calibrated as well.
Menu Open the water inlet completely, before you start
calibration.
- Put the glass container on the hotplate and press
key "Lift down".
- Press key "Enter", if you want to calibrate the rin-
sing water addition.
- The lift goes to work position
Valve Detergent
10s=0,98l - The current calibration value is displayed.
- Press key "Enter", to start process
Enter
Valve Cal. - Pump delivers for 10 s

06/10s - Then, you must measure the delivered amount
in litres (determine the discharge volume with
Enter measuring cylinder).
Valve Set - Press key "+" or "-", to enter the actual-discharge

10s=xxxml volume and then press key "Enter", to confirm
entry.
Enter
+
Operating time In the menu "Hours of operation" you can call up

statistics for the amount of hours of operation of the
pumps and the entire instrument.
Enter - Press key "Enter", to call up the individual posi-
tions.
Fibretherm FT12 21
8.4. Prepare methods– Define programme
In the main menu "Prepare methods" you can prepare, manage and delete up to
10 programmes. The programmes are stored under method number 0 to 9.
On page 24 you can find some examples for programming. Should you wish to
obtain detailed info as well as sample programmes for the various procedures,
contact us for application notes.
Comment Methods For each method, up to 4 boiling phases (A to D) have

Press key "Esc", to get Definition to be defined.
back to the previous pro- The following programme for the determination of
gramming step.. Enter crude fibre in animal feed gives you an example for
the programming:
Method No X - Enter programme number, which has to be worked

Edit on or prepared (0 - 9).
Example: Methode number 1
Enter
+
Comment <A>: Detergent - Selection of detergents for Boiling phase A by

When selecting the da- <- H2SO4 +> pressing key "Plus" or "Minus":
shed line, the selected Example: Selection H2SO4
boiling phase is skipped. Enter
+
<A>: Add - Amount to be added define detergents

H2SO4: X.XX l - Press key "Enter" , to switch between position
before and after the comma.
Enter
+ - Setting range 0,00 - 4,99 litre
Example: 1,30 l amount to be added
<A> Heating-Pwr - Setting of heating power, which is sufficient to

50% maintain boiling of solution.
- Setting range 0 - 100 %
Enter
+ Example: 50 %
<A> Rotation - Setting of duration of rotation during the simmering

Time 10s period.
Enter
+ Example: 10 s
<A> Rotation - Setting of rotation interval during the simmering

Pause 30s period.
Enter
+ Example: 30 s
22 Fibretherm FT12
<A> Boiling time - Setting of the entire simmering period for the boiling
0h 30min phase.A.
- Press key "Enter", to switch from hours to minu-
Enter
+ tes.
- Setting range 0 - 3 h and 0 - 59 min
Example: 0 h 30 min
<A> Suction - Enter the time for suction of the solution

2m 00s - Press key "Enter", to switch from hours to minu-
tes.
Enter
+ - Setting ranmge 0 to 9 min 59 s
Example: 2 m 00 s
<A> Rinsing - Enter the number of cycles for rinsing the Fibre-
01 cycles Bags. The settings for a rinsing cycle can be found
in chapter "8.2.3. Settings rinsing".
Enter
+ - Setting range 0 - 9 cycles
- Example: 1 cycle
Comment Detergent After that you can define the programme parameter
In order to rinse with hot <- KOH +> for boiling stage B, C and D. The procedure is iden-
water, be kind enough to tical to boiling phase A. The programming of the
set a boiling phase with Enter
+ individual programme steps is done as explained
the selection "H2O-Rin- in boiling phase A.
se". During this boiling
phase, the rinsing water
can be heated up.
Method 1 defined After defining all programme parameter for the

Time: XXh XXmin individual boiling phases, the total duration of the
method is displayed.
- Press key "Enter" to programme further methods.

The programme is stored.
- Press key "Esc" to return to "Fibretherm Menu".
The programme is stored as well.
The programming is finished.
Fibretherm FT12 23
8.5 Examples for programming*
Settings Rinsing ADF NDF Crude Fibre Parameter

Water filling 1,3 1,3 1,3 Liter
Rotation time 9 9 9 Seconds
Rotation pause 4 4 4 Seconds
Suction 1 min 45 s 1 min 45 s 1 min 45 s min / s
Wash out time 1 min 1 min 1 min min / s
Settings Preheating
Rotation time 10 10 10 Seconds
Rotation pause 25 25 30 Seconds
Heating delay after start 30 30 30 Seconds
ADF / H2SO4 heat up to 85 85 °C
NDF / KOH heat up to 85 85 °C
H2O-Wasch heat up to 85 85 85 °C
ADF / H2SO4 cool down to 95 95 °C
NDF / KOH cool down to 95 95 °C
H2O Wash cool down to 95 95 95 °C
Special methods / parameter
Methods definition X Y Z No.
<A> Detergent ADF-Solution H2SO4 Type
<A> Add 1,3 1,3 Liter
<A> Heating power 40 50 - 60 %
<A> Rotation time 10 10 s
<A> Rotation pause 20 30 s
<A> Boiling time 1 h 0 min 0 h 30 min h / min
<A> Suction 2 min 0 s 2 min 0 s min / s
<A> Rinsing 2 2 Cycles
 Detergent NDF-Solution KOH Type
 Add 1,3 1,3 Liter
 Heating power 30 - 40 40 - 50 %
 Rotation time 10 10 s
 Rotation pause 15 25 s
 Boiling time 1 h 0 min 0h 30 min h / min *Settings can vary depending on sample type
 Suction 2 min 0 s 2 min 0 s min / s
 Rinsing 2 2 Cycles
<C> Detergent H2O-Wash H2O-Wash H2O-Wash Type
<C> Add 1,3 1,3 1,3 Liter
<C> Heating power 55 55 55 %
<C> Rotation time 10 10 10 s
<C> Rotation pause 15 15 15 s
<C> Boiling time 0 h 5 min 0 h 5 min 0 h 5 min h / min
<C> Suction 2 min 0 s 2 min 0 s 2 min 0 s min / s
<C> Rinsing 0 0 0 Cycles
<D> Detergent H2O-Wash H2O-Wash Type
<D> Add 1,3 1,3 Liter
<D> Heating power 55 55 %
<D> Rotation time 10 10 s
<D> Rotation pause 15 15 s
<D> Boiling time 0 h 2 min 0 h 2 min h / min
<D> Suction 2 min 0 s 2 min 0 s min
<D> Rinsing 0 0 Cycles
Meth. X defined Time h / min
24 Fibretherm FT12
9 Methods execution
When working with Fibretherm, make sure to always wear protective clothes
(gloves, protective glasses, lab coat).
Warnung vor
When taking out the glass container, wear protective gloves and wear protective
eye glasses. The glass container is very hot and there is the danger of burns!
Warnung vor
Be careful when working with acids and lyes!

Make sure to observe the safety regulations according to the current regulation
of handling hazardous materials!
Warnung vor
9.1. Loading of sample carousel

Please note, that we can only give you a general overview in this manual how to
proceed with FibreBags.
Should you need detailed information for a specific method, contact us for appli-
cation sheets. There, you will find detailed info about sample preparation as well
as programming.
1. Put the sample material in the bags (FibreBags).
2. Put the glass spacer into the bags.
3. Load the bags into the sample carousel at the previewed positions (Position
1 - 12).
Should you analyse less than 12 samples, you have to put a glass spacer in
the positions of the carousel which are not taken. This way, the carousel will
run more evenly during the analysis.
4. Put the sample carousel into the glass container carefully. Always use the quick
clamping handle, order-no. 52856, to set in the carousel. Remove the quick
clamping handle after setting in the carousel.
5. Place the glass container axial on the previewed position of the hotplate. Push
the container all the way back to the catch at the rear end.
6. Now, you can start the programme as described in chapter 9.2.
Fibretherm FT12 25
9 Methods execution
9.2. Start programme

Prior to each start of Fibretherm, make sure to check whether the glass container
is closed tightly. Danger of burns and splashing liquids!
Warnung vor
You can abort the programme at any time by pressing key "Stop".
1. Turn on the instrument
2. You are in the "Fibretherm menu".
3. Press key "Menu", to switch to menu item "Method execution".
Method - Press key "Enter", to select a programme.

Execution
Enter
Method No X - Select a programme between 0 - 9

Run => Enter - Press key "Enter", to start the selected pro-
gramme
Enter
+
A H2SO4 - The programme starts and displays the first boiling

phase.
- The display always shows you the current pro-
gramme steps.
Method No.X - Upon termination of the programme the respective

finished message is displayed.
- Press key "Esc", to get back to main menu of Fi-
bretherm.
9.2.1. Functions during the programme run
1. Polling of actual-temperature
Enter
Turn down key "Enter" to obtain the actual temperature.
2. Stopping programme
Stop
Press key "Stop", to abort programme. Then press key „Enter" to continue
programme or press key "Esc" to confirm abortion.
+ 3. Change heating power
Press key "+" or "-", to change heating power
Menu + 4. Increase remaining time of operation
Press keys "Menu" and "+" simultaneously
Menu 5. Decrease remaining time of operation
Press keys "Menu" and "-" simultaneously
26 Fibretherm FT12
10 On-line mode
The RS 485 interface allows quality assurance conforming to ISO/GLP. It enables

up to 32 different instruments (including other brands) to be connected to each
other. In order to get into the on-line mode, turn on the instrument while pressing
the "+" key simultanously.
The On-line mode provides the following possibilities:
1. Control via PC
Connection of PC for controlling and monitoring in conjunction with a customi-
sed terminal program, i.e., Telix (MS-DOS), Terminal (for Windows). With the
assistance of the interface a program, based on the customer’s needs, can be
written, too.
2. Synchronous mode
Synchronous working of various equipment. The programming and controlling
is effected via a system, which has been appointed semi master.
The working instructions for the synchronous mode are the following:
- Connect all instruments with the interface cables RS 485.
- Provide the last unit connected with the terminator AST.
- The interface of all machines is activated by pressing the keys "Time" and "+"
simultaneously.
- The display shows a " " in the lower part of the display to indicate the system
is On-line. Repeat the last step for all machines involved.
- Now you select one of the machines to be the master, the one that gets all
the key commands (semi-master). This is done by pressing "Prog" and "+"
simultaneously.
The master is indicated by a " " in the upper part of the display.
Programme the semi master as described in chapter 6 "Programming".
- By pressing the "Run" key all machines are started.
- You deactivate the semi master by pressing the keys "Time" and "-" simulta-
neously.
- To go Off-line completely, press the keys „Time“ and „-“ or turn the machine off
and on again.
This procedure is valid for all machines connected in the bus-system.
Further information about GerBus® can either be optained from C. Gerhardt GmbH
& Co. KG or their appointed dealer!
Fibretherm FT12 27
11 Error messages
After the problem is solved, press key "Enter" to continue with current procedure.
Esc Enter Should it not be possible to solve the problem, press "Esc" to abort the proce-
dure.
Error message Reason for error Actions to be taken
Error: Method The programme is not Check programme..

not defined defined.
Error: Micro controller faulty Contact customer ser-

FLASH Checksum vice
Error: Beaker glass for Fibre- Insert glass beaker, check

No sample tube Bags is not inserted. whether it is in correct
position.
Error: Reservoir tank for chemi- Fill up reservoir tank or

Tank control cals is empty or chemical empty the residue tank.
residue tank is full.
Error: Hood Hood- front protective Put front protective hood

or lift-position hood is not put on pro- in correct place..
perly.
Position of lift - Lift is not Check position of the

fitted correctly on the glass beaker
glass beaker.
Error: Water, Water – rinsing water Check rinsing water sup-

or air pressure supply faulty. ply and tubing connec-
tion.
Air pressure – com- Check compressed air

pressed air supply faulty. supply and tubing con-
nections.
Error: Glass container too full Check programming

Beaker full – addition of chemicals and if necessary, redu-
might have been set on ce amount of chemicals
too long. which are added..
Error: Cooling water supply faul- Check cooling water sup-

No cooling water ty. ply and check tubing con-
nections.
28 Fibretherm FT12
11 Error messages
Error message Reason for error Actions to be taken
Error: Temperature sensor faul- Contact customer ser-

Temp. sensor ty vice.
Error: The boiling temperature Let liquid cool down and

Temp. too high set was exceeded continue with procedure.
Should the problem oc-
cur again, call customer
service.
Error: The boiling temperature Re-start procedure.

Temp. too low set was not reached. Should the problem oc-
Maybe heating broken. cur again, call customer
service.
Error: Internal system error Contact customer ser-

Communication vice.
Method stopped The current programme Press key "Enter" to conti-

<Enter> or <Esc> has been aborted due nue with programme.
to a error message or by
pressing key "Stop".
Fibretherm FT12 29
12 Maintenance
Please make sure that only original C. Gerhardt spare parts are used.
To minimize malfunctions of the FIBRETHERM, we recommend having it checked

by authorized service personnel annually.
12.1. Service and cleaning

Make sure to wear gloves at all times when cleaning the components.
Warnung vor
To avoid damage by corrosion, leaking liquids (especially acids and alkali) must
be wiped off and neutralized immediately to prevent damage to casting, lacquer
or housing.
Never use abrasive cleaners! In most cases it will be sufficient after each use
to clean the plates using a moist cloth and some household washing-up liquid.
Subsequently rub dry.
12.2. Spare parts

Order-No.: Description
52826 Glass container, 5,0 l
52887 Drip tray black
52189 Drip tray white
52891 Seal ring for shower
52816 Plastic hood, front cover
52829 Ceramic plate (cooking ranged) 320 x 320 mm

52846 Filter glass, diameter . 42 x 70 mm
1312 Mains cable 3,0 m
52918 Keyboard
52849 Autoclude peristaltic pump
52830 Bearing for carousel

52847 Condenser small
52825 Condenser big
16605 Screw cap GL 45
16608 Silicone-seal for GL 45
16601 Screw cap GL 14

16609 Silicone-seal for GL 14 with connection, straight
16610 Silicone-seal for GL 14 with connection, bent
Tubings
22802 Water inlet tubing 10/17 mm, 2 m
22604 PVC-tubing 8/12 mm, 2 m
52199 Pressure inlet tube, 5 m
30 Fibretherm FT12
12 Maintenance
12.3. Accessories
Order-No.: Description
1776 FibreBags for crude fibre (bag with 100 pcs..)
1775 FibreBags for ADF/NDF (bag with 100 pcs.)
1772 Glass-spacer
52856 Quick clamping handle
52805 Insert rack (carousel) cplt. with quick clamping device
1757 Set of tanks, complete incl. level sensor and connecting cable
4261 Data cable DK 42 for RS 485, 2m

4262 Data cable DK 45 für RS 485, 5 m
4265 Terminator plug AST für RS 485
4260 RS-Adapter
Further accessories and information about the Fibretherm program can be found
in the product catalogue or at your local dealer!
12.4. Trouble shooting

Make sure to handle error messages as described in chapter 11.Error Messa-
ges.
The excess current switch (Mains switch) cuts off in case of excessive current
consumption. Switch on the switch again. If this problem reoccurs, call service!
In case of breakdown or failure of your Fibretherm, please contact your local

dealer or:
C. Gerhardt GmbH & Co. KG

Cäsariusstr. 97
D-53639 Königswinter
Tel.: +49 (0)22 23 - 29 99 0
Fax: +49 (0)22 23 - 29 99 99
[email protected]
www.gerhardt.de
Fibretherm FT12 31
12 Instandhaltung
12.5. Disposal
The disposal of the packaging and the parts used has to be done according to the
rules and regulations which are valid in the country of installation. Should the pro-
duct itself be disposed of, make sure to observe the local rules and regulations..
12.5.1. Information for the Disposal of Electric and Electronic Instruments

within the European Union
The disposal of electrically operated instruments is settled within the European Uni-
on by national regulations, which are based on the EU-directive 2002/96EC about
electric and electronic used-instruments (WEEE). Thus, all instruments delivered
after August 13th 2005 must not disposed into the communal domestic waste.
Since the regulations about disposal of waste might vary from one country to the
other within the European Community, we kindly ask you to contact your supplier
or dealer.
In Germany, this obligation for identification will be valid as of March, 23rd 2006.
As of this date, C. Gerhardt will take back all instruments delivered after August,
13th, 2005 without charges and will dispose of them according to the regulations,
or Gerhardt will come to an agreement with the last user of the unit. For all instru-
ments delivered prior to August 13th, 2005 the last user will be held responsible
for the proper disposal. The only crucial factor accepted, for the chronological
placement, it the serial number at the back of the instrument.
12.5.2. Ban on Materials according to ROHS Regulation 2002/95/EG

Ban on materials from the ROHS regulation 2002/95/EG is not valid for the electro-
and electronic instruments of category 8 and 9 and thus not for those instruments
described in this instruction manual. However, we want to draw your attention to the
fact that we feel obliged to observe the regulations for the RoHs for all our products.
Please be kind enough to contact us if you have any further questions.
12.5.3. Transfer
We kindly ask you to always make sure to add this instruction manual to the product
in case of transferring it to another party.
32 Fibretherm FT12

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Fibretherm FT12

Please observe the safety instructions of this manual marked with in

1 Important notes..........................3 9 Methods execution...................25

5.1. Check for transport damage............................ 9

6 Description of the Fibretherm 13

1.1 How to use this instruction manual

The instrument will be called 'Fibretherm' in the entire document.

1.2 Explanation of symbols

Warnung vor gefährlicher,

Attention! Advance notice of substances

2.1 Operation as directed

Make sure to use the instrument according to our instructions, especially:

All other usage is not recommended!

- repairs of electric, electronic or mechanical components may only be done by

2.2 Safety instructions

- the accident prevention regulations in place

Indicating label and danger symbols must not be taken off!

In case of an emergency disconnect from mains immediately!

Always pull the mains plug before opening!

Attention when handling chemicals! Please observe the manufactures safety

2.3 Work bench / Authorized user

The FIBRTHERM has to be placed on a horizontal and stable footprint.

The FIBRETHERM may only be operated by trained staff or especially trained

- read, comprehend, and observe the operation manual

2.4. Danger spots at the instrument

- Attention, danger of crushing when the hood is put

- Attention, danger of burns on the top of the glass

- Attention, danger of splashing hot or caustic liquids

- Attention, danger of burns when taking out the hot

3.1. Warranty conditions

3.2. Technical data

4.1 Front view Fibretherm FT 12

1 Control panel (key pad), order-no.: 52918

2 Glass ceramic-heating area, order-no.: 52829

3 Protective hood, can be taken out, order-no.: 52816

4 Drip tray, order-no.: 52887

6 Electronic- and pump cabinet

7 Glass container, Order-no.: 52826

4.2. Rear view Fibretherm

1 Ventilator 9 Appliance plug with mains cable

5.1. Check for transport damage

5.2. Unpack apparatus

1. Place the equipment on the work bench.

5.3. Parts list

1 x Fibretherm FT 12, ready to use, Order-No.: 1755

5.4.1. Set up tubing connections

Abb. 5.4.1. Tubing diagram

ater inlet tubings

ater outlet tubing

Sample outlet tubing

hemicals inlet tubing

ompressed air connection

Tank without level sensor

5.4.2. Mains connection

5.5. Setting into operation

1. Turn the instrument on using the mains switch.

C. Gerhardt - Current date

Fibretherm - Display of actual firmware-version

Fibretherm - Main menu