Designation: A1014/A1014M − 16

Standard Specification for

Precipitation-Hardening Bolting (UNS N07718) for High
Temperature Service1
This standard is issued under the fixed designation A1014/A1014M; the number immediately following the designation indicates the
year of original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last
reapproval. A superscript epsilon (´) indicates an editorial change since the last revision or reapproval.

1. Scope* Worked Nickel Alloy Bars, Forgings, and Forging Stock

1.1 This specification covers precipitation hardening bolting for Moderate or High Temperature Service
material (UNS N07718) and bolting components for high B880 Specification for General Requirements for Chemical
temperature service. See Specification A962/A962M for the Check Analysis Limits for Nickel, Nickel Alloys and
definition of “bolting.” Cobalt Alloys
E112 Test Methods for Determining Average Grain Size
1.2 The following referenced general requirements are in- E292 Test Methods for Conducting Time-for-Rupture Notch
dispensable for application of this specification: Specification Tension Tests of Materials
A962/A962M.
2.2 ASME Standards:3
1.3 Supplementary requirements are provided for use at the B1.1 Screw Threads
option of the purchaser. The supplementary requirements only 2.3 SAE Standards:4
apply when specified individually in the purchase order or AS 7467 Bolts And Screws, Nickel Alloy, UNS N07718
contract. Tensile Strength 185 KSI [1275 MPa] Stress Rupture
1.4 This specification is expressed in both inch-pound and Rated Procurement Specification
in SI units. However, unless the purchase order or contract
specifies the applicable M designation (SI units), the inch- 3. Ordering Information
pound units shall apply. 3.1 Ordering—It shall be the responsibility of the purchaser
1.5 The values stated in either SI units or inch-pound units to specify all requirements that are necessary for product under
are to be regarded separately as standard. Within the text, the this specification including any supplementary ones and those
SI units are shown in brackets. The values stated in each included in the ordering information required by Specification
system may not be exact equivalents; therefore, each system A962/A962M.
shall be used independently of the other. Combining values
from the two systems may result in non-conformance with the 4. Common Requirements
standard. 4.1 Common Requirements—Bolting material and bolting
components furnished to this specification shall conform to
2. Referenced Documents Specification A962/A962M, including any supplementary re-
2.1 ASTM Standards:2 quirements indicated on the purchase order. Failure to comply
A962/A962M Specification for Common Requirements for with Specification A962/A962M constitutes non-conformance
Bolting Intended for Use at Any Temperature from Cryo- with this specification. If the requirements of this specification
genic to the Creep Range conflict with those of Specification A962/A962M, then the
B637 Specification for Precipitation-Hardening and Cold requirements of this specification shall prevail.

5. Manufacture
1
This specification is under the jurisdiction of ASTM Committee A01 on Steel, 5.1 Melting Process—Bolting material alloy shall be
Stainless Steel and Related Alloysand is the direct responsibility of Subcommittee multiple-melted using consumable electrode practice in the
A01.22 on Steel Forgings and Wrought Fittings for Piping Applications and Bolting remelt cycle or shall be induction melted under vacuum. If
Materials for Piping and Special Purpose Applications.
Current edition approved May 1, 2016. Published May 2016. Originally
approved in 2000. Last previous edition approved in 2015 as A1014/A1014M – 15.
3
DOI: 10.1520/A1014_A1014M-16. Available from American Society of Mechanical Engineers (ASME), ASME
2
For referenced ASTM standards, visit the ASTM website, www.astm.org, or International Headquarters, Two Park Ave., New York, NY 10016-5990, http://
contact ASTM Customer Service at [email protected]. For Annual Book of ASTM www.asme.org.
4
Standards volume information, refer to the standard’s Document Summary page on Available from Society of Automotive Engineers (SAE), 400 Commonwealth
the ASTM website. Dr., Warrendale, PA 15096-0001, http://www.sae.org.

*A Summary of Changes section appears at the end of this standard

Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United States

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 A1014/A1014M − 16
consumable electrode re-melting is not performed in vacuum, 6.2 Product Analysis—If a product (check) analysis is per-
electrodes produced by vacuum induction melting shall be formed by the purchaser, the bolting material shall conform to
used. the product (check) analysis variations prescribed in Specifi-
5.2 Heat Treatment: cation B880.
5.2.1 Solution Treatment—Bolting material shall be solution 7. Mechanical Properties
heat treated at a temperature within the range of 1725 to 1850
°F [940 to 1010 °C], held at the selected temperature for a time 7.1 Tensile and Hardness—All testing shall be performed
commensurate with cross-sectional thickness, and cooled at a after aging. The test specimens shall meet the requirements of
rate equivalent to an air cool or faster. Table 2.
5.2.1.1 Temperature Variation—Solution treating tempera- 7.2 Stress Rupture—Stress rupture testing shall be con-
tures shall be controlled in the range of 6 25 °F [6 14 °C]. ducted in accordance with Table 2 using a combination test bar
5.2.2 Precipitation Heat Treatment—Bolting material shall in accordance with Test Methods E292. Rupture must occur in
be heated to 1325 °F [720 °C], held at temperature for eight the smooth section of each test specimen.
hours minimum, furnace cooled to 1150 °F [620 °C] at 100 °F 7.3 Headed Bolting Components—In addition to 7.1 and
[55 °C] per hour, held at temperature for eight hours, and 7.2, headed bolting components such as bolts, studs, or screws
cooled to room temperature. Alternatively, bolting material with a body length three times the diameter of the component
may be furnace cooled to 1150 °F [620 °C] at any rate provided or longer shall be subjected to full size tensile test and shall
the time at 1150 °F [620 °C] is adjusted so the total precipi- conform to the tensile strength shown in Table 2. The minimum
tation heat treatment time is 18 hours minimum. full size breaking strength (lbf) for individual sizes shall be as
5.2.2.1 Temperature Variation—Precipitation treatment follows:
temperatures and cooling rates shall be controlled in the range
Ts 5 UTS 3 As (1)
of 6 15 °F [6 8 °C].
where:
5.3 Straightening—When straightening is necessary it shall
be done after solution treating and prior to aging. Straightening Ts = tensile strength,
after aging is prohibited. UTS = tensile strength specified in Table 2, and
As = stress area, square inches [square millimetres], as
5.4 Threads—Threads shall be formed by rolling in one pass shown in ASME B1.1 or calculated as follows:
after oxides have been removed from the area to be threaded.
As 5 0.785 ~ D 2 ~ 0.974/n ! ! 2 (2)
5.5 Dimensions and Tolerances, Bolting—Fully heat treated
bolting material shall meet the dimensional requirements of where:
Specification B637 for UNS N07718. D = nominal thread size, and
n = the number of threads per inch.
6. Chemical Composition @ As 5 0.785 ~ D 2 0.9382P ! 2 # (3)
6.1 Remelt Ingots—The chemical analyses of each remelted [where:
ingot used for bolting material shall conform to the require- D = Nominal thread size, and
ments for chemical composition prescribed in Table 1. P = Thread pitch, mm.]

8. Metallography
8.1 Microstructure—The microstructure of the bolting ma-
TABLE 1 Chemical Requirements terial shall be free of freckles, white spots, and Laves phases.
UNS N07718 Threads of bolting components may show evidence of cold
Element
(Formerly Grade 718)
Carbon, max. 0.08
Manganese, max. 0.35 TABLE 2 Mechanical Properties
Silicon, max. 0.35
Tensile and Hardness
Phosphorus, max. 0.015
Tensile strength, min, ksi [Mpa] 185 [1275]
Sulfur, max. 0.015
Yield Strength, min, ksi, [Mpa] 0.2 % offset 150 [1035]
Chromium 17.0–21.0
Elongation in 2 in., or 50 mm (or 4D) min % 12
Cobalt, max.A 1.0
Reduction of area, min, % 15
Molybdenum 2.80–3.30
Hardness, Brinell 331–444
Columbium + 4.75–5.50
Stress Rupture Requirements
Tantalum ...
Temperature, °F [°C] 1200 [650]
Titanium 0.65–1.15
Stress, ksi [Mpa] 100 [690]
Aluminum 0.20–0.80
Hours, min 23
Boron, max. 0.006
Elongation in 2 in., or 50 mm (or 4D), min % 5
IronB Remainder
Elevated Tensile Requirements
Copper, max. 0.30
Temperature, °F [°C] 1200 [650]
NickelC 50.0–55.0
Tensile strength, min, ksi [Mpa] 145 [1000]
A
If determined. Yield Strength, min, ksi, [Mpa] 0.2 % offset 125 [860]
B
Determined arithmetically by difference. Elongation in 2 in., or 50 mm (or 4D) min % 12
C
Nickel + Cobalt. Reduction of area, min, % 15

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 A1014/A1014M − 16
working as a result of rolling. The average grain size shall be 9.5 Headed Bolting Components—One tensile test per lot.
determined in accordance with Test Methods E112 and found
to be ASTM No. 5 or finer. Up to 20 % of the structure may 10. Bolting Quality, Condition, and Finish
have a grain size as large as a No. 3 due to the presence of 10.1 Bolting Material—Shall be uniform in quality and
non-crystallized grains. condition, smooth, commercially straight or flat, and free of
8.2 Macrostructure—Bolting components produced from injurious imperfections.
forgings shall exhibit continuous flow lines in the threads and 10.2 Bolting Components—Multiple laps on thread flanks
in any shank to head or fillet and/or bearing surface areas. are prohibited. Seams, laps, notches, slivers, or oxide scale in
9. Number of Tests the root area of threads are prohibited. Cracks are prohibited.
9.1 Chemistry—One test per remelt ingot of bolting mate- 11. Product Marking
rial.
11.1 Marking—Bolting components shall be marked with
9.2 Mechanical Properties—The number of tests shall be in “718” and the manufacturer’s identification symbol.
accordance with Specification A962/A962M except that for
stress rupture one test shall be run per lot. For headed bolting 12. Certification
components with a body length less than three times the 12.1 Report—In addition to the requirements of A962/
diameter of the component, a separately forged test bar may be A962M, certification shall include the solution treatment cycle
used for tensile and stress rupture testing provided it is time and temperature and the aging cycle time(s) and tempera-
heat-treated with the components. Separately forged bars shall ture(s).
be approximately the same diameter as the headed bolting
component they represent. 13. Keywords
9.3 Grain Size—One test per lot. 13.1 bolting; bolting materials; bolting components; Inconel
9.4 Flow Lines—One test per lot on forged bolting compo- 718; nickel alloy; precipitation hardening; temperature service
nents after final machining. application – high

SUPPLEMENTARY REQUIREMENTS

These requirements do not apply unless specified in the purchase order and in the Ordering
Information, in which event the specified tests shall be made before shipment of the product.

S1. Protective Atmosphere S4. Forged Heads

S1.1 Heat treatment shall be performed under suitable S4.1 Heads for bolts, screws, or studs shall be forged.
protective atmosphere.
S5. Marking
S2. Cleaning
S5.1 Marking on bolting components shall include heat lot
S2.1 Bolting components shall be cleaned with nitric acid as
identification.
stated in AS 7467
S3. Fillet Rolling S5. Thread Rolling
S3.1 The fillet area of the head of bolts, screws, or studs S5.1 Thread rolling shall be performed before precipitation
shall be rolled. heat treatment.

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 A1014/A1014M − 16
SUMMARY OF CHANGES

Committee A01 has identified the location of selected changes to this specification since the last issue,
A1014/A1014M–15, that may impact the use of this specification. (Approved May 1, 2016)

(1) Removed reference to A370.

Committee A01 has identified the location of selected changes to this specification since the last issue,
A1014/A1014M–10, that may impact the use of this specification. (Approved November 1, 2015)

(1) Removed the word “fasteners” and replaced it with “bolting (2) Expanded the words “material” or “bolting” to be specific
components” in accordance with the definition of bolting in as to context whether they are bolting materials or components
Specification A962/A962M in 7.3, 8.2, 9.2, 9.4, 9.5, 10.2, 11.1, in 1.1, 4.1, 5.1, 5.2.1, 5.2.2, 5.5, 6.1, 6.2, 8.1, 9.1, and 10.1.
13, S3.1, and S5.1.

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