Non-Traditional Micromachining Processes: Golam Kibria B. Bhattacharyya J. Paulo Davim Editors
Non-Traditional Micromachining Processes: Golam Kibria B. Bhattacharyya J. Paulo Davim Editors
Non-Traditional Micromachining Processes: Golam Kibria B. Bhattacharyya J. Paulo Davim Editors
Golam Kibria
B. Bhattacharyya
J. Paulo Davim Editors
Non-traditional
Micromachining
Processes
Fundamentals and Applications
Materials Forming, Machining and Tribology
Series editor
J. Paulo Davim, Aveiro, Portugal
More information about this series at http://www.springer.com/series/11181
Golam Kibria B. Bhattacharyya
•
J. Paulo Davim
Editors
Non-traditional
Micromachining Processes
Fundamentals and Applications
123
Editors
Golam Kibria J. Paulo Davim
Department of Mechanical Engineering Department of Mechanical Engineering
Aliah University University of Aveiro
Kolkata Aveiro
India Portugal
B. Bhattacharyya
Department of Production Engineering
Jadavpur University
Kolkata
India
Since the last decade, the major research challenges and developments around the
globe are to manufacture microcomponents with high accurate of microfeatures
which have geometrical dimensions even less than tens of microns. It is obvious
that the demand of microcomponents is diversely increasing day by day in the field
of aviation, automotive, biomedical, optical, electronics, and energy sectors. This
wide range of applications of microcomponents brings the necessity to develop
promising micromachining technologies which can yield high degree of precision,
improved machining rate with accurate geometrical dimensions, reliability, flexi-
bility, and after all environment friendly. Moreover, the developments of material
science provide materials which have enormous material properties especially in
their machinability and hardness. In this situation, it is the task of manufacturer
engineers to develop micromachining processes, both traditional and non-
traditional, which can fulfill the demands of microproduct having several micro-
and nanofeatures.
In the area of non-traditional micromachining processes, few books are avail-
able. These books mostly describe numerical and experimental research details at
different stages. However, it is the most important task at this stage to gain the
fundamental knowledge about different non-traditional micromachining processes.
Not only that, but it is also important to be acquainted with the capabilities and
applications of these micromachining processes in various product manufacturing.
Moreover, several hybrid micromachining processes have also been developed to
improve the surface integrity, geometrical accuracy, and machining efficiency. The
present book entitled “Non-traditional Micromachining Processes—Fundamentals
and Applications” will definitely fulfill the gap between the demand of microfea-
tured components and successful micromachining of these products.
This book starts with introduction of various micromachining processes, espe-
cially, non-traditional, with recent research and developments in each processes.
Further, mechanical type micromachining process such as micro-USM is presented
with mechanism of material removal, types and technologies of micro-USM and
recent research advancements. Then, electro-thermal processes such as
micro-EDM, wire-EDM, micromachining using laser beam (micro-turning,
v
vi Preface
parametric effect on machining rate and spark gap width during machining of glass
fiber epoxy composite.
This book offers a comprehensive treatment of various non-traditional micro-
machining techniques and future directions representing a valuable reference to
engineers and R&D researchers involved in micromachining. The present book can
also be used as a research book for final undergraduate engineering course or as a
topic on micromachining processes at the postgraduate level. Also, this book can
serve as a useful reference for academics, researchers, mechanical, manufacturers,
industrial and materials engineers, professionals in micromachining processes and
related industries. The scientific interest in this book is evident from many
important centers of the research, laboratories, universities as well as industries.
Therefore, it is hoped that this book will inspire and enthuse others to undertake
research in non-traditional micromachining processes.
The editors acknowledge Springer for this opportunity and for their enthusiastic
and professional support. Finally, we would like to thank all the chapter authors for
their availability for this work.
This book has become a reality due to the constant inspirations and encouragement
received from the senior professors and colleagues like Dr. B. Doloi, Dr. D. Banerjee,
and Dr. B.R. Sarkar of Production Engineering Department, Jadavpur University,
Kolkata; Dr. B.B. Pradhan and Mr. I. Shivakoti of Sikkim Manipal Institute of
Technology, Sikkim, India. The editors would like to convey warm regards to
Dr. A. Manna, Dr. S. Dhobe, Dr. V.U. Rathod, Dr. Sandip S. Anasane, Dr. Josephine
Peter, Dr. Mukandar Sekh, Dr. Shamim Haider, and Mr. Omar Faruk Biswas for
constant support and active participation in preparing the manuscripts of this book.
Financial support from the University Grants Commission (UGC), All India
Council for Technical Education (AICTE), Department of Science and Technology
(DST), and Council of Scientific and Industrial Research (CSIR) for carrying out
research in this area has proved to be useful for utilizing research outcomes to
enrich this book.
The editors acknowledge Springer for this opportunity and for their enthusiastic
and professional support. The team members of Springer like Guido Zosimo
Landolfo, Editorial Director; Dr. Dieter Merkle, Springer International Publishing
(Physical Sciences and Engineering); and Dr. Mayra Castro, Applied Sciences
Editorial and Senior Publishing Editor of Springer have put their constant effort in
transforming this book into its final shape. Finally, I would like to thank all the
chapter authors for their availability for this work.
ix
Contents
xi
xii Contents
J. Paulo Davim received his Ph.D. in Mechanical Engineering in 1997, M.Sc. degree in
Mechanical Engineering (materials and manufacturing processes) in 1991, Licentiate degree (5
years) in Mechanical Engineering in 1986, from the University of Porto (FEUP), the Aggregate
title from the University of Coimbra in 2005, and a D.Sc. from London Metropolitan University in
2013. He is Eur Ing and Senior Chartered Engineer by the Portuguese Institution of Engineers with
xiii
xiv Editors and Contributors
a MBA and Specialist title in Engineering and Industrial Management. Currently, he is a professor
at the Department of Mechanical Engineering of the University of Aveiro. He has more than 30
years of teaching and research experience in Manufacturing, Materials, and Mechanical
Engineering with special emphasis in Machining and Tribology. Recently, he has also interest in
Management/Industrial Engineering and Higher Education for Sustainability/Engineering
Education. He has received several scientific awards. He has worked as a evaluator of projects
for international research agencies as well as an examiner of Ph.D. thesis for many universities. He
is the editor in chief of several international journals, guest editor of journals, books editor, book
series editor, and scientific advisory for many international journals and conferences. Presently, he
is an editorial board member of 30 international journals and acts as a reviewer for more than 80
prestigious Web of Science journals. In addition, he has also published as editor (and co-editor)
more than 80 books and as author (and co-author) more than 10 books, 60 chapters, and 350
articles in journals and conferences (more than 200 articles in journals indexed in Web of
Science/h-index 35+ and SCOPUS/h-index 44+).
Contributors
Sandip S. Anasane Department of Production Engineering and Industrial
Management, College of Engineering Pune, Pune, India
B. Bhattacharyya Production Engineering Department, Jadavpur University,
Kolkata, India
S. Das Production Engineering Department, Jadavpur University, Kolkata, India
S. Debnath Production Engineering Department, Jadavpur University, Kolkata,
India
B. Doloi Production Engineering Department, Jadavpur University, Kolkata, India
Golam Kibria Mechanical Engineering Department, Aliah University, Kolkata,
India
A.S. Kuar Production Engineering Department, Jadavpur University, Kolkata,
India
S. Kunar Production Engineering Department, Jadavpur University, Kolkata,
India
Anup Malik Department of Mechanical Engineering, PEC University of
Technology, Chandigarh, India
Alakesh Manna Department of Mechanical Engineering, PEC University of
Technology, Chandigarh, India
S. Mitra Production Engineering Department, Jadavpur University, Kolkata, India
B.B. Pradhan Mechanical Engineering Department, Sikkim Manipal Institute of
Technology, Sikkim, India
Asit Baran Puri Mechanical Engineering Department, National Institute of
Technology Durgapur, Durgapur, West Bengal, India
Editors and Contributors xv
Abstract The high demand and stringent design requirements in developing fields
of microengineering as well as various needs of society and nation require the
utilization of suitable techniques of non-traditional machining processes on dif-
ferent existing and newly developed metals, non metals, alloys, polymers, ceramics,
rubber and composites, etc. Presently, nontraditional machining techniques have
expanded their applicability in the field of micromachining and offer better
opportunities with several inherent advantages that make these processes superior
as well as more efficient than conventional one. Non-traditional mechanical
micromachining processes include abrasive jet machining (AJM), water jet
machining (WJM), ultrasonic machining (USM), ion beam machining (IBM), etc.
Non-traditional thermal micromachining processes include micromachining by
electro discharge machining (EDM), laser beam machining (LBM), electron beam
machining (EBM), etc. Non-traditional chemical and electrochemical microma-
chining processes have been used successfully to generate micro features of high
quality. Hybrid micromachining can also be utilized effectively for generating more
intricate shapes and complex parts. Advanced finishing processes using
non-traditional machining like abrasive flow finishing (AFF), magnetic abrasive
finishing (MAF), etc. are also gaining popularity to cope up the steep demand in
finishing intricate, complex, durable and sophisticated shapes that are highly eco-
nomical and posses better surface quality and property. The opportunities and
challenges of each non-traditional micromachining and finishing processes are to be
1.1 Introduction
without the involvement of sharp cutting tools which are used for traditional
manufacturing techniques [2]. The traditional machining methods such as milling,
drilling, shaping etc. are not suitable for the machining of tremendously hard and
brittle materials. But, the non-conventional machining methods are utilized for the
machining of complex and intricate 3D shapes on harder materials as well as
thinner materials, where usual machining processes are neither feasible nor satis-
factory due to various unavoidable reasons like difficulties in clamping very delicate
materials and machining of very flexible workpiece with complex shapes.
Various types of non-traditional machining processes have been developed for
specific requirements to fabricate desired complex features. The material removal
mechanisms of non-traditional machining processes are basically different than
those in the traditional processes that involves different form of energies, other than
the excessive forces exercised by a cutting tool, (which is in physical contact with
the work piece) that are applied to remove the excess material from the work
surface to generate desired shape. Non-traditional machining processes which are
extensively exercised now-a-days can be characterized by material removal
mechanism, type of energy involved in removal of material, forms of material
removal, type and material of tooling, etc. Moreover, different aspects which are
responsible for the correct selection of non-traditional machining methods include
physical parameters of the processes, capability of the processes in machining
desired material and product with required geometry, dimension and size of product
to be machined, process applicability, feasibility, operational characteristics as well
as economics of the process involved. Physical parameters of the processes involve
machining voltage, current, power, machining gap, work medium and other various
specific parameters for specific techniques. For example, Electrochemical
Machining (ECM) requires power as high as 100 kW, Electron Beam Machining
(EBM) and Laser Beam Machining (LBM) require high voltages in the order of 150
and 5 kV respectively and require careful handling, Electro Discharge Machining
(EDM) and Ultrasonic Machining (USM) require medium power whereas, EBM
and Ion Beam Machining (IBM) require vacuum, etc. NTM processes involve
generation of various shapes on work material. For example, EBM and LBM are
used for micro drilling and cutting of parts having slenderness ratio, l/D < 20. USM
and EDM are useful for sinking cavities and standard hole drilling. ECM is useful
for fine hole drilling and contour machining. Both EDM and ECM processes have
good capability to make shallow and deep pockets as well as contoured surfaces
whereas, AJM is useful for shallow pocketing. As discussed earlier, applicability
and usability of any machining process are other aspects which need to be taken
care of. For example, to machine electrically non-conducting materials, both ECM
and EDM are unsuitable, whereas other various mechanical methods can achieve
the desired results. LBM is not suitable for machining of reflective surfaces
whereas, USM is suitable for machining of refractory ceramic material and AJM
can be used for super alloys also.
The machining characteristics of different non-conventional processes can be
analyzed with respect to material removal rate, tolerance achieved, surface finish
4 S. Debnath et al.
Micromachining generally adopts a top down approach, which may involve various
conventional as well as non-conventional machining techniques [5].
Micromachining can easily generate various microfeatures such as microholes,
microslots, microchannels, etc. as well as microproducts like micro sensors, micro
thermal devices and computer chips even down to nano regime. Approaches
towards micromachining need to be specific and systematic for various methods.
However, these approaches can be correlated and directed towards micromachining
by following two guidelines: (i) concept of unit removal (UR) which is defined as
the material removal per pulse or per unit time for generating the smallest adjustable
dimensions of the micro-product and (ii) requirement of precise machining
equipments to obtain the desired microproduct with higher accuracy by reducing
the dimensional error in proportion to the size of the micro-products.
6 S. Debnath et al.
unique challenges and to keep pace with the rising demand. The fabrication of
miniature parts is not new. Many companies have used various machining tech-
nologies such as EDM and laser to produce micro shapes for many years. Today the
difference lies in the sheer volume of products that require micro machining. Many
manufacturers are developing micro machining technologies and techniques to
minimize this gap. Companies are looking for parts having feature sizes of less than
100 microns, or somewhat larger than a human hair. At this dimensional regime, the
slightest variation in the manufacturing process caused by material or cutting tool,
temperature variations in the machine, vibration and any other phenomenon will
have direct impact on the ability to produce features in micron and submicron
ranges on a large scale. With this continued miniaturization, companies are
developing new products and technologies where the limit of tolerances are mind
boggling and would have been unthinkable just a few years ago. For example, using
end mills of 50 µm diameter and EDM wire of diameter 20 µm or electrodes
smaller than a few tenths micron are becoming more common. The applications
related to micro-meso machining technologies are being employed in the manu-
facture of wide variety of products and devices. The trend is growing continuously
in ultra precision and micromachining domain that still requires a fresh look at new
machining technologies and process mechanics.
From the ancient times people are using tools driven by necessary energy sources to
meet the daily needs and to make the life more comfortable and enjoyable. In the
prehistoric ages tools were made of stones for the item being made. Later, the
invention of iron tools and its implementation lead to the fabrication of more
sophisticated articles of required metals. But with further progress in the field of
sophistication, recent twentieth century products need to be made of most durable
and unmachinable materials. To overcome the difficulties created by these harder
materials, tools are now made of alloy steel, carbide, diamond and ceramics, etc.
where different, newer and more advanced methods are utilized for powering up
these tools.
Each time tools with new material and power sources are used, the effectiveness
and capability of fabricators greatly increase. Since 1940’s, a revolution in fabri-
cation industries has been going on allowing fabricators to cope up high demand for
complicated designs of products made up of tougher and difficult-to-cut materials.
This revolution is centered primarily on implementation of numerous new tools and
types of energy which lead to the introduction of various non-traditional manu-
facturing processes for joining, forming as well as removal of materials. Apart from
this, the conventional techniques of machining depends on electric motors and
harder tool materials for carrying out operations like drilling, sawing, broaching,
8 S. Debnath et al.
etc. Conventional process like forming depends on energy from electrical motor as
well as hydraulics and gravitational forces. Moreover, removal of material can now
be done with electrochemical reaction, high temperature plasmas and high-velocity
jets of liquids and abrasives. Different harder materials can be easily formed with
magnetic fields, explosives and the shock waves from powerful electric sparks.
The non-traditional micromachining processes are not affected by mechanical
properties of material and can generate complex shapes by controlling different
physical parameters of the processes. Based on the type of energy required, medium
of energy transfer, inherent mechanism and basic requirements, non-traditional
micromachining processes can be classified as mechanical micromachining, thermal
micromachining, chemical and electrochemical micromachining, hybrid microma-
chining. Various types of non-traditional micromachining processes have been
shown in Fig. 1.1.
material removal of these micromachining techniques have been stated briefly here
under.
AJM uses kinetic energy of loose abrasives to remove material from workpiece.
Before operation, the workpiece surface is covered with wear resistant mask leaving
the portions on to which machining needs to be carried out. Hence, mask also
determines the geometric and dimensional accuracy of the micro feature to be
produced. During operation the entire workpiece surface remains exposed to par-
ticle beam and gas or air jet containing microscopic loose abrasive particles of
around 50 µm grit size impinges the work material in the unmasked area with high
velocity (typically between 150 and 400 m/s) leading to removal of material by
brittle fracture and formation of desired patterns. Material removal rate during
machining depends on other parameters like the size of abrasive particles, type of
abrasives, abrasive flow rate, pressure of gas, type of work material, etc. which can
also be controlled more effectively than standard sand blasting. Popular abrasives
for AJM include aluminum oxide, silicon carbide, etc. and the erosion action of
AJM can especially be applied for cleaning, cutting, etching, deburring or polishing
of various brittle materials such as glass and ceramics where very fine intricate
features can also be generated [6]. Machining of ceramics by other traditional
process like wet chemical etching is relatively expensive for which AJM is being
used. Furthermore, researchers have fabricated channels and holes on polymer like
polymethyl methacrylate (PMMA) [7, 8] by AJM. Other existing applications of
AJM include machining of devices used in micro-electro- mechanical-systems
(MEMS) [9] and opto-electronics, fabrication of complex 3D and free standing
micro features on glass [10], marking on rubber stencils and electronic equipments,
frosting glass surfaces, engraving codes, numbers on car windows, etc.
Unlike AJM, WJM uses kinetic energy of water to remove material from the
target workpiece. Here, water jet of high velocity (up to 900 m/s) strikes the
workpiece surface which, upon impact, converts to pressure energy. The magnitude
of the pressure generated reaches up to three times than that of normal stagnant
pressure. When the generated pressure is higher enough than the binding force of
the material making up the workpiece, erosion occurs and the material removal
takes place. A typical WJM setup consists of pumping unit for generating high
pressure of water, high pressure hydraulic accumulator to store pressure energy
during idle periods and to provide smoother flow during operations, various types
of nozzles, tube fittings, valves, etc. WJM is not thermally activated and is highly
economical and eco friendly process for cutting porous materials like corrugated
boards, woods, and soft materials like rubber, lead, asbestos, etc. with high surface
finish and straightness. Also, the process is applicable for rock excavation [11],
cutting features on sandstones, cutting fibers and polyethylene for automotive
industries, hydraulic mining and drilling of coals, cleaning and descaling in oil
refineries, chemical plants, etc. Moreover, micro features of higher thickness can be
produced by multi pass cutting whereas, various products of metals like aluminum,
copper and alloys like brass, steel, etc. can be machined, although for such case
very high jet pressure is required which limits its uses for commercial intensifiers.
10 S. Debnath et al.
from the surface by suitable medium. Here no external power is used and anode and
cathode, separated by proper medium, are placed in such a way that the rate of
removal of material by oxidation equals to the rate of reduction of the etchant
species. Material removal by CMM involves sequential steps where very accurate
control of process parameters like composition, temperature and type of solution are
required to enhance the mass transfer.
CMM is highly applicable for fabricating metallic parts such as mask, recording
heads, instrument panels, enclosure screens, etc., printed circuit boards (PCB),
semiconductor device, integrated circuit (IC) and other microcircuit devices to be
used in electronics industry in addition with photosensitive resist. But, further
in-depth research work is needed to be carried out to minimize the limitations of
CMM caused from lower material removal rate, lower accuracy of parts being
produced, inability in machining chemically resistive materials, use of hazardous
materials like highly corrosive electrolyte that may cause a risk to environmental
safety, etc.
Electrochemical micromachining (EMM) is an electrochemical material removal
process that implements the method of anodic dissolution and can easily fabricate
metallic features in micron and submicron ranges by offering enhanced process
control. On the other hand, most of the non-conventional machining processes are
thermally activated; examples include Electron Beam Machining (EBM), Laser
Beam Machining (LBM), etc. Hence, thermal distortion, deterioration of surface
and material property, formation of heat affected zone are of prime concern that
need to be taken care of [21]. CMM and EMM are thermal free processes. But, alike
EMM, CMM cannot be controlled adequately in micromachining domain.
However, accuracy of EMM can be highly improved by controlling required pro-
cess parameter settings and maintaining very narrow gap in the order of less than
fifty microns between microtool and workpiece resulting in generation of ultra
precision micro features with desired dimensions. EMM is a very promising micro
manufacturing process that offers several advantages like higher material removal
rate, greater surface finish, better precision and control, flexibility, reliability,
environment acceptability and can even machine chemically resistive materials and
alloys like titanium and titanium alloys, stainless steel, copper alloys and super
alloys, etc. [22] which have wide use in biomedical, optics, electronics, and MEMS.
EMM can be also used as a cost effective manufacturing process for fabricating
micro parts that were previously produced by CMM.
good property of transferring ultrasonic wave. The cyclic and ultrasonic linear
vibration of microtool gives downward stroke to the abrasive particles. The tiny
abrasive particles accelerate and simultaneously strike the work surface resulting in
removal of tiny chips from the work material in the form of craters. The tool is then
moved into the workpiece with constant force for continuation of machining
operations and generation of required micro feature. A schematic diagram of micro
USM setup has been shown in Fig. 1.2.
However, micro USM can be done in two ways; one is by vibrating the micro
tool and another is by vibrating the workpiece itself which has been introduced
recently. In workpiece vibration method the tool is not vibrated, rather piezoelectric
vibrations are provided on the workpiece. Here, no horn is needed to amplify
vibrations during machining which makes the setup simple and compact. Moreover,
the process eradicates the problem like tool wear which is frequent in first method.
The principle operating parameters that need to be maintained for achieving better
material removal rate, dimensional accuracy and surface finish during micro USM
include frequency and amplitude of vibration, load, rotary motion if it has been
implemented on tool head or workpiece, type of abrasive particles and liquid
component, size of abrasive particles, concentration and flow rate of slurry, type,
geometry and thickness of work material, etc.
1.3.1.2 Opportunities
Micro USM can fabricate micro features both on electrically conductive and non
conductive materials and posses numerous applications in the fields of medical,
electronics, aerospace, etc. The geometric capabilities of micro USM for producing
micro slots, holes and 3D cavities can be enhanced by fabricating in situ micro tool
1 Non-traditional Micromachining Processes … 17
followed by machining by it in the same setup. With this process, researchers have
developed micro holes as small as 20 µm diameter and 50 µm depth on silicon and
quartz [27]. Moreover, rotary micro tool can be introduced which is one of the cost
effective process for fabricating micro holes. Here the tool is given ultrasonic
vibrations as well as rotation. The combination of this grinding mechanism and
rotation leads to sliding and rolling of abrasive grains. As a result, impact and
indentation increase that give better material removal rate [28]. In addition, USM
can be assisted with turning for strain hardening, reducing residual stress of work
material, minimizing machining time, improving surface quality of workpiece,
increment of tool life, etc. [29]. Moreover, researchers have fabricated multi micro
tool and used this tool for drilling micro holes having 20 µm diameter on soda lime
glass by micro USM. For this, a tungsten micro tool was fabricated by wire electro
discharge grinding. With this tungsten micro tool array of microholes was fabri-
cated on copper foil by EDM which was later used for fabricating multi micro tool
for USM by reverse EDM [30]. In addition, the capability of micro USM can be
extended more considering its implementation in the emerging area like micro-
fluidics. Microfluidics extensively uses micro channels and micro cavities for
delivering and storing liquid or gas. Also micro channels are used for micro heat
exchanger applications and for micro sensors. These micro channels and micro
cavities can effectively be produced by micro USM. Micro USM has enough
potential for producing 3D micro channels or 3D micro features on silicon and on
other various newer materials like different types of polymers, ceramics and glass
that can readily be applied for micro-electromechanical system (MEMS).
1.3.1.3 Challenges
Micro USM has extensively been used for different applications like making small
holes in helicopter power transmission shafts and gears, fabrication of 3D micro-air
turbines, machining of watch bearings and jewels, generation of high aspect
ratio micro holes on silicon and glass wafers for pressure and flow sensors [31] and
numerous other micro features which are required in MEMS. Moreover, micro-
features can be generated on the micro tool tip to be used for micro USM.
Researchers have fabricated 3D micro gear which acts as a micro tool during USM
[32]. The patterned surface on the tool replicates itself when fed towards the
workpiece leading to parallel production of identical micro features with lower
machining time. Also, researchers have fabricated high aspect ratio micro pillars on
Lead Zirconate Titanate PZT [33], spiral groove, contoured 3D micro cavity with
tool path designed using CAD/CAM [34], micro feature in alumina to transfer this
pattern for generating intricate shaped micro tool [35], wafers in borosilicate glass,
etc. Micro USM can effectively machine and polish steel tool surface [36], micro
channels for bio-MEMS, whereas semiconductor industries greatly rely on
Micro USM as the industry needs like slicing of semiconductor components and
processing of various characteristically brittle materials. Also, Micro USM can be
utilized on relatively ductile metal-based materials with appropriate alteration,
which is a sheer need in microfluidics and heat transfer industries.
Here, a conductive tool and workpiece are submerged in dielectric medium and are
separated by a small gap. The tool is made cathode and workpiece is made anode
that are connected to a resistance capacitance (RC) circuit. When the tool moves
toward the workpiece, discharge occurs resulting in the formation of plasma col-
umn. The flux of electron generates ample amount of heat which melts the work-
piece material. With the feed of the tool, discharge continues making a replica of
the electrode on the work surface. Micro EDM has similar characteristics as EDM
except that the energy range is lower and size of the tool, discharge energy and
resolution of axis movement are in micron ranges. Micro electro-discharge
machining is an efficient process for producing micron sized shapes even on
extremely hard tungsten carbide and stainless steel as no cutting force is involved
during operation. But as the process is thermally activated, hence it suffers from
limitations like formation of heat affected zones, change in material property and
formation of micro cracks on the workpiece surface. Moreover, during each dis-
charge the tool material also melts which limits its use for further applications.
Figure 1.3 shows basic arrangement and setup of the Micro electro-discharge
machining process.
molecules. The ionization gradually increases to such extent that a narrow channel
of constant conductivity or plasma channel creates leading to continuous flow of
electrons towards anode and ions towards cathode. Upon striking the anode and
cathode surfaces their kinetic energy changes to intense heat energy resulting in
generation of momentarily current impulse forming discharge or spark. These
discharges or sparks generate intense heat leading to melting and evaporation of
workpiece as well as tool material.
Actually, during pulse on time the pressure in the plasma channel gets very high
that restricts the evacuation of molten metal. During pulse off time this pressure
drops instantly leading to evaporation of molten metal from the work surface. The
rate of metal removal from both workpiece and tool is highly dependent on the
kinetic energy of electrons and ions respectively. But, as electrons are lighter in
weight than that of ions; it has been seen that anode workpiece corrodes at faster
rate than cathode if both are made up of same material. Hence, workpiece is always
chosen as anode. As the material is removed from that machining zone; the spark
gap between tool as well as workpiece increases resulting in formation of next spark
at next closest points between tool and workpiece. Thus, the discharges travel all
over the tool surface leading to uniform material removal and generation of
approximate mirror image on the work surface. This phenomenon continues when
the tool is fed into the workpiece leading to formation of required feature on work
surface.
Both straight and reverse polarities can be used during micro EDM, where, in
straight polarity workpiece is made positive and tool is negative which is simply
opposite in reverse polarity. During machining the sparking frequency is very high
whereas, spark radius is small and temperature is very high. As a result, small
amount of material melts and evaporates where a portion of this is removed by
dielectric medium and the remaining portion gets solidified on the workpiece
surface forming recast layer. This thermally activated micro electrical discharge
machining process also forms and leaves small amount of crater on both workpiece
and tool surface which hinders further use of same tool and destroys surface
integrity of the produced micro shapes [38].
The operating principle of micro EDM is almost similar to conventional EDM
process. In micro EDM, for maintaining the tiny spark gap of as small as 1–5 µm
[39], servo controlled feed mechanism of enhanced positional accuracy and supe-
rior sensitivity is used that can be used both for conventional precision manufac-
turing as well as fabrication of various micro features like micro inserts, micro
moulds, etc. in micron and submicron ranges [40]. But the main difference between
macro and micro EDM lies in the process of eroding the material. In macro EDM
the motto is to maximize the erosion and minimize the machining time by setting
the pulse and current parameters accordingly where in micro EDM efforts are made
to increase the erosion efficiency required for micromachining by minimizing the
energy of electro-spark and erosion through single capacitor discharge that also
make the power circuitry of this process different.
1 Non-traditional Micromachining Processes … 21
1.3.2.2 Opportunities
Micro EDM is a popular and efficient process for fabricating various complex micro
features. The setup is simple and the process has added flexibility which can be
modified further with ease in the context of specific requirements and applications.
For fabricating and sharpening of tiny tool electrode in single discharge, researchers
have developed micro EDM setup with two drives of different response frequencies,
one is lower response stepper motor controlled for coarser movement of workpiece
and positioning while another has piezoelectric transducer having higher response
for finer movement of electrode [41]. Moreover, researchers have developed micro
EDM setup with two types of local actuator module. The first module consists of
two electromagnetic actuators for holding the electrode, controlling the thrust and
better positioning, whereas the second module consists of eight electromagnetic
actuators for motion in radial direction for smoother, accurate and stable machining
and minimization of tool wear [42]. In addition, micro EDM has been combined
with other processes like micro USM and micro punching for fabricating micro
holes for MEMS in borosilicate glass and on stainless steel sheet [43, 44].
Newer methods of fabrication by micro EDM involve use of variable capacitance
for minimizing electrode wear, implementation of sequential machining like wire
EDG for in situ fabrication of electrode and generate microfeature with same
electrode in micro EDM followed by electrochemical polishing to enhance geo-
metric accuracy and surface quality, etc. [45]. Furthermore, the efficiency, process
stability, material removal rate, flushing and surface quality of micro EDM can be
enhanced by rotating the electrode, rotating the workpiece, etc. Moreover, micro
EDM, as a potential process for fabricating micro shapes of stronger and wear
resistant tungsten carbide, will aid to modern fabricators in their respective areas
and will be of immense help in understanding the basics and fundamental science of
the process, thereby enlarging its implementation field. But further research work is
still needed to cope up with the challenges that are encountered frequently. For
example, development and implementation of new pulse generator is needed that
can produce lower discharge energy suitable for micro scale productions.
Moreover, micro EDM milling can be automated to cope up the steep needs in
producing micro-molds and dies. But superior control of operating parameters with
involvement of proper optimization technique is required to achieve quality
machining with required dimensions, accuracy and surface finish. Also,
multi-purpose and miniature sized machine tool can be fabricated by micro EDM
which will disclose more advanced research areas in the concerned field.
1.3.2.3 Challenges
micro EDM are still prevalent and need more concentration such as lower material
removal rate found in machining of tungsten carbide micro-structures which make it
time-consuming and difficult to be applied for mass scale production. The diffi-
culties are also there in the circulation of dielectric medium and proper removal of
machining products, particularly when the spark gap is in the order of few microns
during machining a complex shaped micro hole or micro cavity with high aspect
ratio. Such improper flushing will eventually degrade the micro machining effi-
ciency and will restrict the formation of high aspect ratio micro holes.
Wear of micro tool is another problem in micro EDM that can stop the
machining process at the middle, if not taken care of at the first time. For machining
square, rectangular, triangular and specific shaped micro features as well as com-
plex shaped 3D micro mould, rotating electrode cannot be used in die sinking micro
EDM. As a result, the machining products deposit and stick between tool and
workpiece that effect badly on the circulation of dielectric and deteriorate quality of
the machined shapes. Other disadvantage of micro EDM includes formation of
relatively poorer and imperfect surface after machining. The surface roughness
increases with increase in machining current, pulse on time and voltage [46]. The
thermal actions during machining also give rise to micro cracks, residual stress; it
changes the microstructure as well as microhardness of surface and subsurface
layers that leads to hydrogen and carbon diffusion. Moreover, each machining
leaves a crater on microtool as well as on work surface which is influenced by pulse
energy. Furthermore, the generated recast layer on the workpiece after machining
needs additional operations like precision grinding for removal. Due to such
research challenges, micro EDM parameters require to be carefully selected [47]
and further attention and investigations are needed for successful utilization of
micro EDM for fabrication of micro features.
Micro EDM is extensively applied for the fabrication of inject nozzle for bubble jet
color printer, micro-slots, high aspect ratio micro-holes, dies for precision blanking,
micro-gear wheels with complex shape, miniature neurosurgical instruments like
micro-forceps made up of nickel-titanium wire, etc. and several other micro com-
ponents for aerospace industries. Moreover, researchers have fabricated micro-
electrode by block-micro EDM process [48], high aspect ratio WC–Co
micro-structures with gear pattern by combining LIGA with micro EDM [49],
micro compressor and micro turbine impeller by micro EDM milling [50], high
aspect ratio micro array with reverse micro EDM [51], micro ball joint of bio
compatible magnesium alloy for use in medical devices [52], micro electrode by
single spark during micro EDM [53], etc. Presently, micro-EDM is a readily used
technique in industries for high-precision machining and generating micro shapes
with higher accuracy on various types of conductive metals and alloys, graphite and
different harder ceramic materials.
1 Non-traditional Micromachining Processes … 23
In modern days, micro machining using laser radiation has become very popular
and is acting as a versatile fabrication process by means of its different superb
features like contact and wear less machining, better flexibility and possibility for
high degree of automation, etc. As a result, micro laser beam machining is being
widely used for fabricating micro components on various metals, ceramics and
polymer to be applied in medical industries, automobile sectors, etc. Micro laser
beam machining process is also being used for producing semiconductors and solar
cell. Laser for micro machining attributes wide range of pulse duration from
femto-second to microsecond, variety of wavelengths and different pulse repetition
rates from single to megahertz allowing the process to fabricate complex machined
micro parts with high aspect ratio. Various micromanufacturing domains like cut-
ting, drilling, welding, surface texturing also use micro laser beam machining
process for removing the material by rapid heating, melting and evaporation. Also,
the detrimental effects of high heat generation like burr formation, melting, etc.
during micromachining can be minimized to some extent by using lasers of
extremely short pulse duration. Figure 1.4 shows the schematic of laser microma-
chining system.
Micro LBM uses thermal ablation technique to remove material from the workpiece
[54]. Typical laser micromachining setup consists of several features like a CNC
machine tool. It has a central computer for controlling and moving the stages and
positioning the workpiece at exact focal point. Moreover, the controller can halt the
laser pulses as per requirement, adjust the pulse and change the pulse repetition rate
1.3.3.2 Opportunities
Micro LBM is a versatile process for fabricating various simple as well as intricate
micro features in metal, glass, plastic, as well as machining very thin and delicate
foils with desired precision and dimensional accuracy. The process includes
machining of required micro shapes by drilling, cutting, marking, and even involves
operations like threading, turning, grooving by utilizing multiple laser beams. The
process can be utilized for controlled fracture of delicate items. Laser drilling of
high aspect ratio micro holes can be enhanced further by implementing newer
techniques like helical drilling that removes work material in helical pass splitting
the total machining depth into multiple single steps; trepanning that uses moving
laser spot in circular orientation and polarization control that can be achieved by
changing linear laser polarization into circular one [55, 56]. Additionally, helical
drilling can be combined with polarization control for fabricating high quality and
high aspect ratio precise micro holes. Laser cutting can be done by trepanning.
Trepanning is done by optomechanically moving the laser on the work surface in a
predefined path which helps in machining larger sized holes even on ceramics.
CNC cutting is used for machining nonlinear micro holes with programmable shape
whereas laser marking is used to machine very low depth grooves to form desired
patterns.
Micro LBM is well known and flexible process to fabricate microfeatures in
submicron or even in nano ranges where possibilities are still there to carry out
further research works by using fiber laser and also by using very smaller pulse
duration in nano, pico and femto second ranges on different materials. Nano second
laser can further be used for excimer laser, CO2 laser, copper vapor laser, diode
pumped solid state laser, etc. [57]. Other research scopes include study of change in
surface morphology due to heating, successful implementation of lasers for
obtaining high resolution, intricate 3D and high aspect ratio micro features on
numerous materials, generation of micro textured surfaces to be used in micro
fluidics and micro mechanics. Micro LBM is also utilized in areas like biomedical
and processing materials for semiconductor, photovoltaic cell, etc.
1.3.3.3 Challenges
removal. Moreover, some amount of molten material resolidifies and forms recast
layer around the machined feature. Formation of heat effected zone and modifi-
cation of grain structure is prominent in laser machining. Also, the work surface
after machining undergoes thermal and mechanical stress as well as surface and
subsurface cracking. All the above mentioned problems can be encountered by
using ultra short pulse laser. However, formation of recast layer does not disappear
completely even for femto second lasers. But these techniques are not at all eco-
nomical and give rise to optical problems. On the other hand, ultra high laser
intensity generates which leads to strong deformation of laser light in the focal
plane that may affect the machining accuracy [58].
Furthermore, newer techniques like underwater laser machining have been
introduced which need extensive research for confirming its feasibility in encoun-
tering several thermal related issues. Another key problem in laser machining is
fabrication of micro features on reflective surfaces that restricts its application in
fabricating features of copper, aluminum, etc. for which further research works are
needed. Other research issues of micro LBM include engraving lines for larger
areas, minimizing machine-to-machine variation and generation of fumes and
odors, decreasing longer machining time needed by pulsed laser systems, charac-
terizing the ablation behavior and heat conductibility of various fiber reinforced
composites, etc.
Micro LBM processes are being used for micro-texturing as well as machining of
silicon wafers, thin glass sheet [59, 60], micromachining of optical material like
lithium niobate, Gallium Arsenide and lithium tantalite, accurate machining of
fluoropolymers to be used for miniature sized lab-on-chip technologies, drilling tiny
holes in chip packages and polymers used for microcircuit boards, micro-texturing
of magnetic hard disk drives, video heads, scribing, patterning, dicing of developed
optical wafer as well as substrates and other numerous micro as well as nano range
applications like smoothing of synthetic CVD diamond for optical applications like
thermal as well as infrared sensors and detectors, etc. [61]. Micro LBM is also used
in various biomedical applications like fabrication of stents, micro holes in patient
monitoring probes, various micro components in MEMS, rapid prototyping of
micro fluidic channels with optical waveguides, micro-textured surfaces for cell
adhesion [62], etc. Further applications involve texturing of magnetic disk and
diamond films, fabrication of various polymeric micro structures for transferring
these patterns on metallic substrate, patterning and repairing of electronic circuits
and devices, fabricating micro patterns of inorganic, organic and biological mate-
rials, fabricating bio sensors, thin film transistors, OLED display [63] as well as
drilling of meshes in metallic foils, trimming of machined devices, percussion
drilling and underwater ablation of silicon [64, 65], fabrication of nickel intravas-
cular rotor micro turbine [66], mold inserts for photo molding, etc. [67].
1 Non-traditional Micromachining Processes … 27
Micro Ion Beam Machining is another atom by atom material removal technique
for fabricating precise parts in micro as well as nano ranges. In this machining
process, ions of inert gas such as argon are bombarded with very high kinetic
energy of about 10 keV on the workpiece surface resulting in ejection of atoms by
elastic collision. A schematic diagram denoting the micro IBM setup has been
shown in Fig. 1.5. Due to rising demand in fabricating micro and nano components,
micro IBM is gaining popularity in manufacturing semiconductor devices, maskless
implantation as well as failure analysis and other respective fields [68]. Apart from
traditional techniques like X-ray or UV lithography that are used as intermediate
process for primarily producing micro and nano scale features, micro ion beam can
efficiently generate high resolution structures on any conductive component by
direct writing manner. This micromachining process is also helpful to fabricate
microtools, etching of IC-patterns, generation of micro and nano features on silicon
substrates, sharpening of diamond cutting tools, etc.
In micro IBM, ion with specific intensity is moved towards work surface for
fabricating required micro feature. The operation of IBM is carried out in vacuum
by using vacuum pump for avoiding collision with surrounding air molecules and
airborne particles. Other accessories of IBM setup includes stage, detectors, ion
column, liquid metal ion source for providing ion, inlet and containment for gas
1.3.4.2 Opportunities
IBM is a popular process for precise and accurate fabrication of micro as well as
nano features. In contrast to highly precise and conventional lithography for
machining micro/nano features, IBM, as a maskless process [71], offers several
advantages like finer focusing of ion beam, availability of various ion masses, better
energy density, etc. which make the process appropriate even for accurate
1 Non-traditional Micromachining Processes … 29
1.3.4.3 Challenges
The major challenge in micro IBM relies in minimizing the damage caused by ion
beam on the wokpiece surface. With the increase in ion implantation, individual
disordered cascade regions get overlap forming a damaged layer over the surface
that generates residual stress in the component. The ion beam can also amorphize
the workpiece surface by creating point defects, dislocations, phase transformation
and grain size modification; thus requiring further study, extensive research and
systematic investigation in this area. Moreover, samples prepared for characteri-
zation and produced by IBM contains impurities like oxygen, galium, carbon, etc.,
where during machining, oxygen can get into vacuum chamber due to its relatively
poor build quality. Several other problems concerning IBM include ion-beam
30 S. Debnath et al.
Micro IBM has lots of applications in the fields of micro as well as nano manu-
facturing and can even develop feature of about 5 nm size. IBM is very popular in
semi conductor industries for failure analysis and modification of electronic circuits,
debugging ICs, repairing mask, preparing samples for TEM, rapid prototyping of
micro/nano features to be used in MEMS, sensors [77], fabrication of nano pillars,
AFM and SPM tips [78], micro tools [79], fabrication of nano patterns [80], and
several trenches [81], micro gear by FIB-LIGA, etc. Furthermore, researchers have
fabricated nano-hand [82], 3D honey comb structure [83], lens moulds [84], stamps
[85], different types of manipulator like as two pillar, nano actuator with coil
structure, 3D nano rotors [86], nano tools, bio nano tools, various bio metric
structures like glass capillary for bio medical treatment, neural interface for con-
necting nervous system with external devices [87], nano structured thin film
magnetic head, nano cup [88] and other various 3D curved nano structure [89], etc.
Moreover, the process can be used for machining micro cutting tools made up of
diamond, tungsten carbide, high-speed steel and various other harder materials
where cutting dimensions within the range of 15–100 µm [90] can easily be
achieved and other complex geometric features like tool nose radius, rake and relief
angles can also be made within micron range by micro IBM process.
Micro EBM is a thermal activated micro machining process where electrons with
high speed strike the workpiece surface, thereby transferring the kinetic energy into
heat energy that melts and vaporizes the workpiece material. During micro EBM
process, very high velocity (228,478 km/s) of electron beam is achieved by using
voltage of about 150 kV and is focused over a point of 10–200 lm diameter that
results in very high power density in the order of 7000 billion W/sq.mm. This high
power density is enough to vaporize any type of material instantaneously.
1 Non-traditional Micromachining Processes … 31
Whole micro EBM process is conducted in vacuum chamber without any contam-
ination to evade any possible collision of accelerated electrons with air molecules.
This restricts the process to be used over large work pieces as the vacuum chamber is
very confined. But the process has advantages in having very less thermal effects on
the workpiece because the machining zone is very small, typically in the order of
only 25–50 µm. Furthermore, the process is able to generate different intricate
shapes and contours by directing the electron beam using magnetic deflection coil.
A schematic diagram of the micro EBM setup has been shown in Fig. 1.6.
In micro EBM process, high velocity of electron beam is generated from an electron
beam gun which consists of tungsten or tantalum cathode filament. When large
potential difference is applied between cathode and anode, cathode gets heated up
to around 2500 °C and thermo ionic emission of free electron occurs that is further
facilitated by maintaining vacuum inside the beam gun chamber. The negative
biased cathode repels the electrons causing them to move towards annular cathode
grid. The cathode grid is also made negative so that the electrons can approach to
32 S. Debnath et al.
annular anode. Due to the application of potential field and attraction of annular
anode the stream of electrons gets accelerated leaving the anode with very high
velocity that is about half the velocity of light. The cathode grid is made concave
for easy concentration of beam. The beam is then made to pass through a series of
magnetic lenses and apertures that shapes the beam, reduce divergence and
improves the quality of that beam. The beam then comes to electromagnetic lens
and deflection coil. The electromagnetic lens is used to focus the electron beam over
a very tiny spot whereas the deflection coil can maneuver and move this beam in
desired direction. A valve is also situated in the electron beam machine for con-
trolling the beam duration.
The entire EBM process needs to be carried out in a vacuum chamber [91] as
electrons travelling at very high velocity may collide with air molecules in the way
and may lose their energy. Moreover, the beam will get disturbed which will make
the control of required operating parameters difficult and will adversely affect the
machining quality. During machining, the electron beam is focused on the work-
piece. The beam interacts with the work surface and the electrons impinge into the
work material. This penetration depth is highly dependent upon work material
properties like melting temperature, thermal conductivity, vaporization temperature,
etc. and the characteristics of the converging beams [92]. Upon striking the work
surface, the kinetic energy of electron coverts to tremendous heat energy that melts
and vaporizes the localized area of the workpiece in the focal region. Finally the
molten material is wiped off from the machining zone by using high pressure of gas
formed by the reaction of beam and backing material that is applied at the underside
of workpiece. However, if some molten metal is left, it will form a recast layer but
this will not oxidize as the process is carried out in vacuum. The electron beam gun
has the facility to even operate in pulse mode during machining where single pulse
is used to drill holes on thin sheets and multiple pulses are used to drill hole on
thicker plates. Other than the pulse duration, control of various process parameters
is necessary for satisfactory machining which include beam current, working dis-
tance, beam shape and size, incident angle etc.
1.3.5.2 Opportunities
Micro EBM can drill very high aspect ratio (25:1) micro holes on various low
strength materials with very high drilling rates leading to minimization of pro-
duction cost. Moreover, tapered, reverse tapered and barrel shaped holes can also be
fabricated be maneuvering the deflection coil and introducing CNC system [93].
The process is suitable for machining wide range of electrically conductive and
non conductive materials like Ni, Ti and other super alloys, stainless steel, plastic,
aluminum, leathers, ceramics, etc. Also, the detrimental thermal effect like forma-
tion of heat affected zone expands over only few microns due to the application of
shorter pulses. Moreover, in general performance of the machining does not depend
on physical, mechanical or metallurgical property of the work material and requires
very simple work holding due to the absence of any cutting force. As a result,
1 Non-traditional Micromachining Processes … 33
the fixturing and holding cost is lower and the process can be used for machining of
very brittle and fragile materials. The process also offers several opportunities that
can be extended further by applying it in fabricating complex micro components.
1.3.5.3 Challenges
Alike other discussed micro machining techniques, micro EBM process is not
devoid of any difficulties or problems. Though no mechanical distortion is there, but
generation of very high thermal energy in a confined zone may introduce residual
thermal stresses and the quality of the edges may be influenced by thermal property
of the workpiece as well as pulse energy. Moreover, the process is not at all
economical, requires high operating cost, initial investment, regular maintenance
and involvement of skilled operators. Additionally, for creating vacuum the time
required is much more, resulting in increase of non productive idle periods and
overall machining time. However, the influence of this incidence can be minimized
to some extent by introducing vacuum load locks. Though the formation of heat
affected zone is negligible, the formation of recast layer cannot be avoided. Hence,
further research is still necessary in order to encounter various challenges and to
enhance the process feasibility as well as applicability.
Micro EBM has diverse application field starting from the fabrication of bi-metal
saw blades to transmission assemblies. On flat as well as contoured surfaces, CNC
EBM drilling is used for rapid fabrication of large number of holes that are faster
than other processes. Moreover, the technique is capable of drilling micro holes by
single millisecond pulse of electron beam making the total process much faster [94].
Various types and shapes of precise slots and holes like tapered, bowed wall,
straight wall with various contoured internal profiles can be produced by micro
EBM. Moreover, holes can be drilled on workpiece of thickness 9.5 mm and on
harder metals like titanium and its alloy [95] by precisely controlling the beam
energy which can be used extensively in aerospace application. Electron beam
milling can be used for cutting of different shaped apertures in thin foils and wafers.
Also, the process is used for selective etching of thin films on glass or ceramics.
Electron beam drilling can contribute ultrafine filter production for numerous
purposes. Moreover, the holes can be fabricated on different ceramic materials.
Micro EBM can be used for making holes in wire drawing dies, fuel injector
nozzles and fabrication of fine gas orifices in nuclear space reactors, etc. Also,
micro EBM can be used in pattern generation for IC fabrication, polishing of metal
mold [96], repairing of defects in masks [97] and fabricating various other micro
features in chemical, textile, food processing and semiconductor industries [98].
34 S. Debnath et al.
1.3.6.2 Opportunities
1.3.6.3 Challenges
Alike other process, chemical micro machining is not devoid of limitations. This
process is limited to fewer metals as selection and finding of appropriate etchant
and maskant for a range of materials is difficult. In addition, the process is highly
dependent on the availability of required etchant and maskant. The gases produced
during machining may entrap under the masking leading to uneven etching,
decrease in etching efficiency and generation of shapes with poor surface quality.
36 S. Debnath et al.
Moreover, when such gases come out, they may spread and attack other equip-
ments. In chemical micro machining, material removal rate is very low which can
further deteriorate as it gets contaminated with machining products. Other chal-
lenges in micro CM include difficulties in machining sharp corners, thicker as well
as chemically resistive material, limitation in scribing accuracy, degradation of
dimensional accuracy in the final product, etc. The etchants used in chemical micro
machining are toxic and hazardous for environment that require expensive methods
for disposal. For machining of alloys, surface quality gets degraded due to differ-
ential etching that requires further study and research work.
Chemical micro machining is used to machine various types of metals like copper,
aluminum and its alloys, lead, steel, titanium, nickel as well as various types of non
metals like ceramics, glass, plastic, etc. [99]. It is used to produce shallow holes and
cavities over large surface area [100], contours, pockets, depression [101], parts
with stepped features, machining of edges of sheet metal, engraving on metal
workpiece, machining of huge work surfaces like airplane wing to tiny workpiece
like IC chips [102], fabrication of stainless steel edge filter by photochemical
machining [103], and batch size production of various other components in
chemical and missile industries. Other popular applications of chemical micro
machining involves minimizing thickness of walls, ribs, webs of components
produced by conventional process, narrow cuts in large thin sheets applicable in
aerospace industries, etc.
challenges in machining different newer materials with greater accuracy for suc-
cessful generation of more intricate micro features. A schematic diagram of
Electrochemical Micromachining setup is shown in Fig. 1.8.
effective removal of machined products like sludge and hydrogen bubbles from the
IEG during pulse off time [106]. For machining to occur, the micrometer scale tool
electrode is then feed forward or feed toward the workpiece by maintaining a
predefined IEG. From the anodic workpiece, surface metal starts dissolving into
metallic ions generating an approximate mirror image of the tool by corresponding
electrochemical reactions. The corrupting position of the workpiece varies with the
location of tool electrode and anodic dissolution continues during whole the time
resulting in generation of desired feature on the workpiece.
Throughout the material removal process, for maintaining uniform current flow
as well as removal of material and to achieve better machining stability, the feed of
tool is kept balance with the rate of dissolution where increase in gap will hinder the
machining process by increasing electrolyte resistance and decrease in gap will
result in improper flushing and coagulation of reaction products leading to occur-
rence of frequent short circuits in the machining zone. However, still during
machining, machining products like gas bubbles, sludge, etc. resulting from
ongoing electrochemical reactions may stick between the microtool and the
workpiece which can clog the small IEG that may lead to formation of micro sparks
and deterioration of machining quality and accuracy. For such cases, to remove the
electrolysis products from the IEG and to supply more fresh electrolytes, use of
rotary electrodes and vibrations by piezoelectric transducer (PZT) [107] may be
used either in tool or in workpiece which generates pressure waves that can clean
the machining gap and maintain machining efficiency. Other parameters which
effect the dissolution process involve concentration of electrolyte, duration of each
pulse as well as pulse on time [108], applied frequency, temperature of electrolyte,
etc.
1.3.7.2 Opportunities
machining of micro features in same setup that leads in reducing the tool handling
and fixing issues. Another advantage of EMM is the use of multi micro tool which
can machine arrays of micro feature simultaneously and decreases the production
time. But, this material removal process offers several opportunities which are still
unexplored and require extensive research, further investigation and detailed study
[24]. Hence, researchers are concentrating towards appropriate designing and
development of various types of microtools, proper selection of suitable electrolyte,
improvement of micro tool feeding system, proper control and monitoring of IEG
during machining and achieving better material removal rate, elimination of micro
spark generated in IEG, achieving better surface finish and dimensional accuracy,
etc.
1.3.7.3 Challenges
conventional grinding process that includes cracking and heat distortion. ECG can
produce sharp edges within the range of 0.001–0.005 lm radius by varying the
power settings. The process can machine thin and delicate metal sheets with better
machining accuracy and feature characteristics. Very less tolerance can be acquired
in the order of 0.005 mm by controlling the micro ECG characteristics such as type
of material being cut, its size and depth of cut. But, this process is applied only for
conductive materials i.e. stainless steel, aluminum, hastelloy, inconel, etc.
Presently, researchers are concentrating to increase the machining rate, machining
accuracy, wheel life, etc. with the development of proper ECG set up. Lower pulsed
voltage and lower duty ratio are more suitable for enhancing the machining
accuracy while the grit size has no effect during machining [129].
gas bubbles gradually combine with each other and form a gas film which serves as
an insulating media and generate enough resistance creating higher potential dif-
ference between these two electrodes. When the voltage becomes high enough and
exceeds a critical value, electrical discharges occur between the tool electrode and
the upper layer of electrolyte. If the workpiece is placed in the discharge zone,
machining does take place in the form of melting, vaporization and thermal erosion
due to the heat generated by the discharges. The material is eroded by electro
chemical dissolution as well as electro-discharging between two electrodes [130].
The combined material removal mechanism facilitates higher material removal rate
in ECDM than ECM or EDM process. The schematic diagram of electrochemical
discharge machining is shown in Fig. 1.10. It is mostly used for micromachining
and scribing out hard and brittle materials, conductive, non conductive materials,
etc. This hybrid process is successfully used in non conductive materials such as
ceramics and glass for drilling of micro holes and slots by smaller electrodes
efficiently and economically. Machining of complex microfeatures is not possible
by ECDM process with better accuracy and surface finish on harder materials. So,
more systematic investigation is necessary for machining non conductive materials
because of their key applications in MEMS field. For example, semiconductor
materials can be bonded with quartz or glass because of their transparent property.
Also, the process is utilized for machining ceramic materials that are used in
high-tech apparatus [131]. ECDM is utilized to machine fine 3D micro-structures
on glass and to obtain good surface finish with better machining accuracy in drilling
and milling operations. In ECDM, micro structures with higher depth are
fabricated using high aspect ratio micro tool in lower electrolyte concentration.
biomedical filters, integrated circuit boards, pneumatic sensors, fluidic filters, grids,
fuel injection nozzles, high-pressure orifices, optical apertures and manipulators.
Ultrasonic assisted mechanical micromachining is an important hybrid
machining in which the material is removed by the simultaneous action of
mechanically rotating spindle and higher axial ultrasonic oscillation of workpiece or
tool [158]. One of the important ultrasonic assisted mechanical micromachining is
ultrasonic assisted grinding where the oscillation of the grinding tool by piezo-
electric oscillators is used for achieving better surface integrity of machined
products. In ultrasonic assisted EDM, the cavitation and acoustic wave enhance the
material removal and flushing condition for microgrooves, slots and micro drilling.
The better ejection of molten metal from craters increases due to the slurry circu-
lation. This fact increases the material removal rate as well as generates good
surface quality. Ultrasonic assisted abrasive slurry jet micromachining (UAASJM)
improves the machining efficiency and quality of the ductile and brittle materials
due to the assistance of ultrasonic vibration. Due to ultrasonic vibration the alu-
minum nitride is polished by the abrasive water jet to get the better polishing
efficiency and quality [159].
Abrasive flow finishing process is one of the super finishing processes in which
workpiece and tool moves relatively for accurate finishing of internal shapes of
components and complex geometries. The basic arrangements of AFF have been
shown in Fig. 1.11. In AFF, the surface is super-finished by the flow of abrasive
laden polymer media in single or two-way direction. The abrasive media is passed
in one way direction and it comes back from the other end. In two-way process, two
1 Non-traditional Micromachining Processes … 47
vertically opposite hydraulic cylinders push the abrasive media to and fro. The
process is used for complex cavities, edges, etc. At a given time, this process
finishes a number of parts or different areas of the same work piece. The atomized
AFM systems are capable for handling thousands of parts per day for finishing
operation reducing the labor costs and monotonous physical work. Through proper
control of the process parameters, this process can be used for variety of
super-finishing operations achieving very uniform and precise results.
The significance of all AFF parameters used in process i.e. media, tooling,
machine, etc. can be evaluated properly for wide range of applications in finishing
process [160]. For instance, the temperature effect on viscosity of AFF medium and
rheological properties of grit mixtures are two important factors for finishing of
mild steel dies [161]. AFF is also suitable for finishing of inner surface of spher-
oidal graphite cast iron [162]. The influence of various AFF process parameters i.e.,
number of AFF cycles, abrasive mesh size, extrusion pressure on the output
parameters i.e. surface finish and material removal rate can be controlled properly
during finishing of brass and aluminum workpieces [163]. However, the surface
finish depends upon the types of materials which should be taken care of before
operation [164].
slurry are combined with polishing pad where the ring diameter is greater than
wafer. The dynamic polishing head holds the pad and wafer and these combined
parts are kept on a plastic retaining ring. The dynamic polishing head forms the
smooth surface where wafer surface is also flat and smooth during operation.
Sometimes, this wafer is also used in additional circuit elements. In some cases,
CMP mechanisms are used for finishing operation using chemical and mechanical
based abrasion. For instance, CMP is able to remove the material from the selective
position for any photolithographic system. In some cases, machining by CMP can
achieve machining depths as low as few angstrom to 22 nm. CMP is widely used
for fine finishing of glass and ceramic surfaces and semiconductor wafers. This
process facilitates the control and optimization of the polishing operation for
microelectronic devices and can cope up with huge demands of global wise at
different levels. Evidently, the process has enough capability in micro and nano
ranges and can reduce the difficulties in polishing operation where improvement is
still going on in the field of etching and lithography after its introduction in early
80s.
surface roughness from few microns to nano levels in just few minutes [170, 171].
Moreover, various complex surfaces can easily be finished by this process [172–
175]. The schematic diagram of MAF is shown in Fig. 1.14. The process has
capability to produce smoother external surfaces on optics, turbine blades, cutting
tools, etc. and internal surfaces on capillary tubes, biopsy needles, curved pipes, etc.
Also the process can polish various magnetic materials like iron, cobalt, nickel, etc.
as well as non-magnetic materials like glass, ceramic, stainless steel, copper, etc.
with economically and effectively. This process is proper combination of homo-
geneous mixture of abrasive particles and magnetic particles in a magnetic field
with machining force for finishing operation. It has numerous advantages such as
controllability, self-adaptability, etc. Presently, magnetic field-assisted finishing
processes are becoming more attractive for its huge applications in the fields of
medical components and optical parts. However, MAF has still some problems in
fine finishing in nanometer level of flat and micro-complex surface of harder work
materials.
1.6 Conclusions
References
1. Liu X., DeVor R.E., Kapoor S.G., Ehmann K.F., The mechanics of machining at the
micro-scale: assessment of the current state of the science, J. Manuf. Sci. Eng. 126 (2004)
666–678.
2. Mecomber J. S., Hurd D., Limbach P.A., Enhanced machining of micron-scale features in
microchip molding masters by CNC milling, International Journal of Machine Tools &
Manufacture 45(2005) 1542–1550.
3. Chae J., Park S.S., Freiheit T., Investigation of micro-cutting operations, International
Journal of Machine Tools & Manufacture 46(2006) 313–332.
4. Filiz S., Conley C.M., Wasserman M.B., Burak Ozdoganlar N., An experimental
investigation of micromachinability of copper 101 using tungsten carbide micro-endmills,
International Journal of Machine Tools and Manufacture 47(2007)1088–1100.
5. Masuzawa T., State of the art of micromachining, Annals of the CIRP 49 (2000) 473–488.
6. Benedict G. F., Non-traditional Manufacturing Processes, Marcel Dekker Inc., New York,
1987.
7. Getu H., Ghobeity A., Spelt J.K., Papini M., Abrasive jet micromachining of polymethyl-
methacrylate, Wear 263(2007)1008–1015.
8. Getu H., Ghobeity A., Spelt J. K., Papini M., Abrasive jet micromachining of acrylic and
polycarbonate polymers at oblique angles of attack, Wear doi:10.1016/j.wear.2008.01.013.
9. Belloy E., Thurre S., Walckiers E., Sayah A., Gijs, M. A. M., The introduction of powder
blasting for sensor and microsystems applications, Sens. Actuators: A: Phys. 84 (2000)
330–337.
10. Pawlowski A., Belloy E., Sayah A., Gijs M. A. M., Powder blasting patterning technology
for microfabrication of complex suspended structures in glass, Microelectronic Engineering
67-68 (2003) 557–565.
11. Cooley W.E., Clipp L.L, High pressure water jets for undersea rock excavation, Journal of
Engineering for Industry, Trans. ASME, Series B 92(1970)281.
52 S. Debnath et al.
12. Sun X. Q., Masuzawa T., Fujino M., Micro ultrasonic machining and its applications in
MEMS, Sensors and Actuators, A 57(1996)159–164.
13. Egashira K., Masuzawa T., Fujino M., Sun, X. Q., Application of USM to micromachining
by on-the-machine tool fabrication, International Journal of Electrical Machining, IJEM, 2
(1997)31–36.
14. Tseng A. A., Topical review: Recent developments in micro milling using focused ion beam
technology, Journal of Micromechanics and Micro engineering 14(2004)R15-R34.
15. Vasile M. J. et al., Micro fabrication techniques using focused ion beam and emergent
applications, Micron 30(1999) 235–244.
16. Jain R.K., Jain V. K., Abrasive Fine Finishing Process-A Review, The Intl. J. Mfg. Sc. Prod.
2(1999)55–68.
17. Shinmura T., Takazawa K., Hatano E. Study on Magnetic Abrasive Finishing, Annals CIRP
39(1990)325–328.
18. Puranik M. S., Joshi S. S., Analysis of accuracy of high-speed aspect ratio holes generated
using micro-EDM drilling, Proceedings of Institution of Mechanical Engineering, Part B,
Journal of Engineering Manufacture 222 (2008)1453–1464.
19. Alemohammad H. Toyserkani E. Pinkerton A.J., Femtosecond laser micromachining of fiber
Bragg gratings for simultaneous measurement of temperature and concentration of liquids,
Journal of physics D: Applied Physics 41 (2008) 1–9.
20. Sugioka K. Cheng Y, Midorikawa K., Three-dimensional micromachining of glass using
femtosecond laser for lab-on-a-chip device manufacture, Applied Physics A 81(2005) 1–10.
21. Rathod V., Doloi B., Bhattacharyya B., Influence of electrochemical micromachining
parameters during generation of microgrooves, Int J Adv Manuf Technol. 76(2015)51–60.
22. Ghoshal B., Bhattacharyya B., Shape control in micro borehole generation by EMM with the
assistance of vibration of tool, Precision Engineering 38 (2014) 127–137.
23. McGeough J.A, (Ed.), Micromachining of Engineering Materials, Marcel Dekker Inc, NY
(USA) 2002.
24. Bhattacharyya B., Electrochemical Micromachining for Nanofabrication, MEMS and
Nanotechnology, William Andrew Applied Science Publishers, Imprint of Elsevier Inc.,
Massachusetts, pp. 270, 2015.
25. Egashira K., Masuzawa T., Microultrasonic machining by the application of workpiece
vibration, CIRP Annals—Manufacturing Technology 48(1999)131–134.
26. Egashira K., Mizutani K., Micro-drilling of Monocrystalline Silicon Using a Cutting Tool,
Precision Engineering 26(2002)263–268.
27. Egashira K., Masuzawa T., Fujino M., Sun X. Q., Application of USM to micromachining
by on-the-machine tool fabrication, International Journal of Electrical Machining 2(1997)
31–36.
28. Komaraiah M., Reddy P. N., A study on the influence of work piece properties in ultrasonic
machining, International Journal of Machine Tools and Manufacture 33(1993) 495–505.
29. Singh R., Khamba J. S., Ultrasonic machining of titanium and its alloys: a review, Journal of
Materials Processing Technology 173(2006)125–135.
30. Egashira K., Taniguchi T., Tsuchiya H., Miyazaki M., Microultrasonic machining using
multitools, in Proceedings of the 7th International Conference on Progress Machining
Technology (ICPMT ‘04), pp. 297–301, December 2004.
31. Sun X. Q., Masuzawa T., Fujino M., Micro ultrasonic machining and its applications in
MEMS, Sensors and Actuators A 57(1996)159–164.
32. Sun X. Q., Masuzawa T., Fujino M., Micro ultrasonic machining and self-aligned multilayer
machining/assembly technologies for 3D micromachines, in Proceedings of the IEEE Micro
Electro Mechanical Systems (MEMS’96), pp. 312–317, 1996.
33. Boy J. J., Andrey E., Boulouize A., Khan-Malek C., Developments in microultrasonic
machining (MUSM) at FEMTO-ST, International Journal of Advanced Manufacturing
Technology 47(2010)37–45.
34. Yu Z. Y., Rajurkar K. P., Tandon A., Study of 3D microultrasonic machining, Journal of
Manufacturing Science and Engineering, Transactions of the ASME 126(2004)727–732.
1 Non-traditional Micromachining Processes … 53
35. Zhang C., Rentsch R., Brinksmeier E., Advances in micro ultrasonic assisted lapping of
microstructures in hard-brittle materials: a brief review and outlook, International Journal of
Machine Tools and Manufacture 45(2005)881–890.
36. Curodeau A., Guay J., Rodrigue D., Brault L., Gagn´e D., Beaudoin L. P., Ultrasonic
abrasive l-machining with thermoplastic tooling, International Journal of Machine Tools
and Manufacture 48 (2008) 1553–1561.
37. Jameson E.C., Description and development of electrical discharge machining (EDM), in:
Electrical Discharge Machining, Society of Manufacturing Engineers, Dearbern, Michigan,
pp. 12, 2001.
38. Allen D.M., Lecheheb A., Micro electro-discharge machining of ink jet nozzles: optimum
selection of material and machining parameters, Journal of Materials Processing Technology
58 (1996) 53–66.
39. Newman S. T., Ho K. H., The state of art – Electrical discharge machining, International
Journal of machine Tools and Manufacture 43 (2003)1287–1300.
40. Koch O., Ehrfeld W., Michel F., Gruber H. P., Recent progress in micro-electro discharge
machining technology – Part 1, Proceedings of the 13th International Symposium for
Electromachining ISEM XIII, Bilbao, Spain, 2001.
41. Takezawa H., Hamamatsu H., Mohri N., Saito N., Development of micro-EDM with rapidly
sharpened electrode, Journal of Materials Processing Technology 149(2004)112–116.
42. Imai Y., Nakagawa T., Miyake H., Hidai H., Tokura H., Local actuator module for highly
accurate micro-EDM, Journal of Materials Processing Technology 149(2004) 328–333
43. Yan B. H., Wang A. C., Huang C.Y., Huang F.Y., Study of precision micro-holes in
borosilicate glass using micro-EDM combined with micro ultrasonic vibration machining,
International Journal of machine Tools and Manufacture 42(2002)1105–1112
44. Chern G., Wu Y. E., Liu S., Development of micro-punching machine and study on the
influence of vibration machining in micro-EDM, Journal of Materials Processing
Technology, 180(2006)102–109.
45. Hung J. C., Ling J. K., Yan B. H., Liu H. S., Ho P. H., Using a helical micro-tool in
micro-EDM combined with ultrasonic vibration for micro-hole machining, Journal of
Micromechanics and Microengineering 16(2006) 2705–2713.
46. Aspiwall D. K., Soo S. L., Berrisford A. E., Walder G., Workpiece Surface Roughness and
Integrity after WEDM of Ti-6Al-4 V and Inconel 718 Using Minimum Damage Generator
Technology, CIRP Annals - Manufacturing Technology 57(2008) 187–190.
47. Patel K.M., Pandey P.M., Rao P. V., Surface integrity and material removal mechanisms
associated with the EDM of Al2O3 ceramic composite, International Journal of Refractory
Metals and Hard Materials 27(2009) 892–899.
48. Jahan M.P., Rahman M., Wong Y.S., Fuhua L., On-machine fabrication of high- aspect-ratio
microelectrodes and application in vibration-assisted micro- EDM drilling of tungsten
carbide, Proceedings of the Institution of Mechanical Engineers, Part B: Journal of
Engineering Manufacture 224 (2010) 795–814.
49. Takahata K., Shibaike N., Guckel H., High-aspect-ratio WC–Co microstructure produced by
the combination of LIGA and micro-EDM, Microsystem Technologies 6 (2000) 175–178.
50. Liu K., Lauwers B., Reynaerts D., Process capabilities of Micro-EDM and its applications,
The International Journal of Advanced Manufacturing Technology 47(2010) 11–19.
51. Liao Y.S. et al., Fabrication of high aspect ratio microstructure arrays by micro reverse
wire-EDM, Journal of Micromechanics and Microengineering 15(2005) 1547.
52. Lin C.S. et al., Fabrication of micro ball joint by using micro- EDM and electroforming,
Microelectronic Engineering 87(2010) 1475–1478.
53. Gao G., Zhao W., Wang Z., Gou Y., Instantaneous fabrication of tungsten microelectrode
based on single electrical discharge, Journal of Materials Processing Technology 168(2005)
83–88.
54. Sen A., Doloi B., Bhattacharyya B., Experimental Studies on Fibre Laser Micromachining of
Ti-6Al-4V. 5th International & 26th All India Manufacturing Technology, Design and
Research Conference (AIMTDR 2014) December 14th, 2014.
54 S. Debnath et al.
55. Föehl C., Dausinger F., High precision deep drilling with ultra short pulses, Proceedings of
SPIE2003; 5063: 346–51.
56. Dausinger F., Hugel H., Konov VI., Micromachining with ultra short laser pulses: from basic
understanding to technical applications, Proceedings of SPIE 2003; 5147: 106–15.
57. Meijer J., Laser beam machining (LBM) state of the art and new opportunities, J Mater
Process Technol 149 (2004)2–17.
58. Breitling D., Ruf A., Dausinger F., Fundamental aspects in machining of metals with short
and ultra short laser pulses, Proceedings of SPIE 2004; 5339: 49–63.
59. Rizvi N.H., Femtosecond laser micromachining: current status and applications, Riken
Review 50(2003) 107–112.
60. Loeschner U., Mauersberger S., Ebert R. et al., Micromachining of glass with short ns-pulses
and highly repetitive fs-laser pulses, in Proceedings of the 27th International Congress on
Applications of Lasers and Electro-Optics (ICALEO ’08), pp. 193–201, October 2008.
61. Rizvi N., Femtosecond Laser Micromachining: Current Status and Applications. Riken Rev
50(2003) 77–82.
62. Gower M. C., Industrial application of laser micromachining, Opt Express 7(2000) 56–67.
63. Mishra S., Yadava V., Laser Beam Micro Machining (LBMM) – A review, Optics and
Lasers in Engineering 73(2015) 89–122
64. Ren J., Kelly M., Hesselink L., Laser ablation of silicon in water with nanosecond and
femtosecond pulses, Optics Letters 30(2005) 1740–1742.
65. Kruusing A., Underwater and water-assisted laser processing: part 2—etching, cutting and
rarely used methods, Optics and Lasers in Engineering 41(2004) 329–352.
66. Tao Y. L., Chen H., Zhang W., Time scale effects in laser material removal: a review, Int J
Adv Manuf Technol 26(2005) 598–608.
67. Hanemann T., Pfleging W., Haubelt J., Gahr K. H. Z., Laser micromachining and light
induced reaction injection molding as suitable process sequence for the rapid fabrication of
micro component, Microsyst Technol 7(2002) 209–14.
68. Bhavsar S.N., Aravindan S., Rao P.V., A Critical Review on Microtools Fabrication by
Focused Ion Beam (FIB) Technology, Proc. of the World Congress on Eng. (2009).
69. Raffa V., Castrataro P., Menciassi A., Dario P., Focused Ion Beam as a Scanning Probe:
Methods and Applications, Applied NanoScience and Technology (2006) 361–412.
70. Lucille A., Stevie G., Fred A., Introduction to focused ion beams, instrumentation, theory,
techniques and practice, Springer Inc, Boston, USA. 2005.
71. Sadoh T., Eguchi H., Kenjo A., Miyao M., Etching characteristics of SiO2 irradiated with
focused ion beam, Nucl Instrum Meth B 206 (2003) 478.
72. Kang H.J., Ahn S.H., Lee J.S., Lee J.H., Surface modification of aluminum by nitrogen-ion
implantation, Int J Precis Eng Man 7(2005) 1.
73. Villanueva G., Plaza J.A., Sanchez-Amores A., Bausells J., Martinez E., Samitier J., et al.
Deep reactive ion etching and focused ion beam combination for nanotip fabrication, Mater
Sci Eng C-Mater 26(2006) 164.
74. Venugopal G., Fabrication and Characteristics of Submicron Stacked-Junctions on Thin
Graphite Flakes, J. Nanosci. Nanotechnol 11(2011) 1405–1408.
75. Park C.M., Bain J.A., Focused ion beam induced grain growth in magnetic materials for
recording heads, J. Appl. Phys. 91(2002) 6380–6832.
76. Nastasi M., Mayer J.W., Hirvonen J.K., Ion- Solid Interactions: Fundamentals and
Applications (Cambridge University Press, Cambridge, UK, 1996).
77. Nellen P.M., Callegari V., Bronnimann R., FIB-milling photonic structures and sputtering
simulation, Microelectron Eng 83(2006)1805.
78. Miller M.K., Russell K.F., Atom probe specimen preparation with a dual beam SEM/FIB
miller, Ultramicroscopy 107(2007)761.
79. Ali M.Y., Ong A.S., Fabricating micromilling tool using wire electrodischarge grinding and
focused ion beam sputtering, Int J Precis Eng Man 31(2006)501.
1 Non-traditional Micromachining Processes … 55
80. Hopman W.C.L., Ay F., Hu W., Gadgil V.J, Kuipers L., Pollnau M., et al. Focused ion beam
scan routine, dwell time and dose optimizations for submicrometer period planar photonic
crystal components and stamps in silicon, Nanotechnology 18(2007)195305.
81. Li W., Minev R., Dimov S., Lalev G., Patterning of amorphous and polycrystalline
Ni78B14Si8 with a focused-ion-beam, Appl Surf Sci 253(2007)5404.
82. Malek C.K., Hartley F.T., Neogi J., Fast prototyping of high-aspect ratio, high resolution
X-ray masks by gas-assisted focused ion beam, Microsyst Technol 9(2003)409.
83. Hosokawa H., Shimojima K., Chino Y., Yamada Y., Wen C.E., Mabuchi M., Fabrication of
nanoscale Ti honeycombs by focused ion beam, Mater Sci Eng A-Struct 344(2003)365.
84. Youn S.W., Okuyama C., Takahashi M., Maeda R., A study on fabrication of silicon mold
for polymer hot-embossing using focused ion beam milling, J Mater Process Tech 201(2008)
548.
85. Li H.W., Kang D.J., Blamire M.G., Huck W.T.S., Focused ion beam fabrication of silicon
print masters, Nanotechnology 14(2003)220.
86. Igaki J., Kometani R., Nakamatsu K., Kanda K., Haruyama Y., Ochiai Y., et al., Three
dimensional rotor fabrication by focused-ion-beam chemical-vapor deposition,
Microelectron Eng 83(2006)1221.
87. Kometani R., Funabiki R., Hoshino T., Kanda K., Haruyama Y., Kaito T., et al., Cell wall
cutting tool and nano-net fabrication by FIB-CVD for sub-cellular operations and analysis,
Microelectron Eng 83(2006)1642.
88. Reyntjens S., Puers R., A review of focused ion beam applications in microsystem
technology, Journal of micromechanics and microengineering 11 (2001) 287–300
89. Fujii T., Iwasaski M., Munekane M., Takeuchi T., Hasuda M., Asahata T., et al.,
A nanofactory by focused ion beam, J Micromech Microeng 11(2005)S286.
90. Ding X., Lim G.C., Cheng C.K., Butler D.L., Shaw K.C., Liu K., Fong W.S., Fabrication of
a micro-size diamond tool using a focused ion beam, J. Micromech. Microeng. 18 (2008).
91. Selada A., Manaia A., Vieira M.T., Pouzada A.S., Effect of LBM and large-area EBM
finishing on micro-injection moulding surfaces, Int J Adv Manuf Technol 52 (2011)
171–182.
92. Desilets B. H., Mechanism of cavity formation in unfired ceramic by electron beam
machining, Journal of vacuum science technology 15(1978)3.
93. Moarrefzadeh A., Finite-Element Simulation of Electron Beam Machining (EBM) Process,
International Journal of Multidisciplinary Sciences And Engineering 2(2011).
94. Chryssolouris G., Anifantis N., Karagiannis S., Electron Assisted Machining: an Overview,
ASME Journal of Manufacturing Science and Engineering 119 (1997) 766–769.
95. Biamino S., Penna A., Ackelid U., Sabbadini S., Tassa O., Fino P., Pavese M., Gennaro P.,
Badini C., Electron beam melting of Ti-48Al-2Cr-2Nb alloy: microstructure and mechanical
properties investigation, Intermetallics 19 (2010) 776–781.
96. Uno Y., Okada A., Uemura K., Raharjo P., Sano S., Yu Z., Mishima S, A new polishing
method of metal mold with large-area electron beam irradiation, J Mat Process Technol 187–
188(2007) 77–80.
97. Utke, Hoffmann, and Melngailis, Gas-assisted focused electron beam and ion beam
processing, J. Vac. Sci. Technol. 26(2008).
98. Jain V. K., Advanced Machining Processes, Allied Publishers, Delhi, 2002.
99. Blak J.T., et. al., DeGarmo’s Materials and Processes in Manufacturing, John Wiley & Sons,
Inc, Tenth ed. 2007.
100. Drozda T.J., Tool and Manufacturing Engineers, Handbook (Chapter 14: Nontraditional
Machining), SME Publishing, 1989.
101. Fadaei T. A., A New Etchant For The Chemical Machining of St304, Journal of Materials
Processing Technology 149(2004) 404–408.
102. Al-Ethari A. H., Alsultani K. F., Dakhil N., Variables Affecting the Chemical Machining of
Stainless Steel 420, International Journal of Engineering and Innovative Technology (IJEIT)
3(2013).
56 S. Debnath et al.
103. Allen D.M., Talib T.N., Manufacture of stainless steel edge filters: an application of
electrolytic photopolishing, precision engineering (1983) 57–59.
104. Bhattacharyya B., Munda J., Malapati M., Advancement in electrochemical
micro-machining, International Journal of Machine Tools & Manufacture 44 (2004)
1577–1589.
105. Lohrengel M. M., Kluppel I., Rosenkranz C., Bettermann H., Schultze J. W., Microscopic
investigations of electrochemical machining of Fe in NaNO3, Electrochimia Acta 48 (2003)
3203–3211
106. Kozak J., Rajurkar K. P., Wei B., Modeling and analysis of pulse electrochemical
machining, Transactions of ASME, 116 (1994) 316–323.
107. Munda J., Malapati M., Bhattacharyya B., Control of micro-spark and stray –current effect
during EMM process, Journal of Materials Processing Technology 194(2007) 151–158.
108. Kock M., Kirchner V., Schuster R., Electrochemical micro machining with ultra short
voltage pulses-a versatile method with lithographic precision, Electrochimia Acta 48(2003)
3213–3219.
109. Rathod V., Doloi B., Bhattacharyya B., Parametric Investigation into the Fabrication of Disk
Microelectrodes by Electrochemical Micromachining, Journal of Micro- and
Nano-Manufacturing, Vol. 1/ 041005-1-041005-11, December 2013
110. Wang J.J.J., et al., Fabrication of wedge-shape tool via electrochemical micromachining with
diamond-like carbon coating, Journal of Materials Processing Technology 187–188[2007]
264–269.
111. Landolt D., Chauvy P. F., Zinger O., Electrochemical micro machining, polishing and
surface structuring of metals: fundamental aspects and new developments, Electrochimia
Acta 48(2003) 3185–3201.
112. Datta M., Landolt D., Fundamental aspects and applications of electrochemical micro
fabrication, Electrochimia Acta 45(2000) 2535–2558
113. Bassu M., Strambini L.M., Barillaro G., Advances in Electrochemical Micromachining of
Silicon: Towards MEMS Fabrication, Procedia Engineering 25(2011) 1653–1656.
114. Munda J., Malapati M., Bhattacharyya B., Control of microspark and stray-current effect
during EMM process, Journal of Materials Processing Technology 194(2007) 151–158.
115. Wang M., et al., Electrochemical machining of the spiral internal turbulator, International
Journal of Advanced Manufacturing Technology 49(2010) 969–973.
116. Jo C.H., Kim B.H., Chu C.N., Micro electrochemical machining for complex internal micro
features, CIRP Annals -Manufacturing Technology 58(2009) 181–184.
117. Bo Hyun K., Byung Jin P., Chong Nam C., Fabrication of multiple electrodes by reverse
EDM and their application in micro ECM, Journal of Micromechanics and Microengineering
16(2006) 843.
118. Nguyen M.D., Rahman M., Wong Y.S., Enhanced surface integrity and dimensional
accuracy by simultaneous micro- ED/EC milling, CIRP Annals - Manufacturing Technology
61(2012) 191–194.
119. Kunieda M., et al., Electrochemical micromachining using flat electrolyte jet, CIRP Annals -
Manufacturing Technology 60(2011) 251–254.
120. Hong Shik S., Hyun K. B., Chong Nam C., Analysis of the side gap resulting from micro
electrochemical machining with a tungsten wire and ultrashort voltage pulses, Journal of
Micromechanics and Microengineering 18(2008)075009.
121. Kunieda M., Mizugai K., Watanabe S., Shibuya N., Iwamoto N., Electrochemical
Micromachining using Flat Electrolyte Jet, CIRP Annals, Manufacturing Technology 60
(2011) 251–254.
122. Zinger O., Chauvy P.F., Landolt D., Scale-Resolved Electrochemical Surface Structuring of
Titanium for Biological Applications, J. Electrochem. Soc., 150(2003) B495.
123. Kock M., Kirchner V., Schuster R., Electrochemical Micromachining with Ultrashort
Voltage Pulses - a Versatile Method with Lithographical Precision, Electrochemical Acta 48
(2003) 3213–3219.
1 Non-traditional Micromachining Processes … 57
124. Trimmer A. L., Hudson J. L., Kock M., Schuster R., Single-step Electrochemical Machining
of Complex Nanostructures with Ultrashort Voltage Pulses, Applied Physics Letters 82
(2003) 3327–3329.
125. Karunakaran K., Pushpa V., Akula S., Suryakumar S., Techno-economic analysis of hybrid
layered manufacturing, International Journal of Intelligent Systems Technologies and
Applications 4(2008) 161–176.
126. Heisel U., Wallaschek J., Eisseler R., Potthast C., Ultrasonic deep hole drilling in electrolytic
copper ECu 57, CIRP Annals-Manufacturing Technology 57(2008) 53–56.
127. Lauwers B., Klocke F., Klink A., Hybrid processes in manufacturing, CIRP Ann-Manuf
Techn 63(2014) 561–583.
128. Curtis D.T., Soo S.L., Aspinwall D.K., Electrochemical superabrasive machining of a
nickel-based aeroengine alloy using mounted grinding points, CIRP Ann-Manuf Techn 58
(2009) 173–176.
129. Tehrani A.F., Atkinson J., Overcut in pulsed electrochemical grinding, P I Mech Eng B-J
Eng 214(2000) 259–269.
130. Bhattacharyya B., Doloi B., Sorkhel S.K, Experimental investigations into electrochemical
discharge machining (ECDM) of non-conductive ceramic material, Journal of Materials
Processing Technology 95(1999) 145–154.
131. Jain V.K., Adhikary S., On the mechanism of material removal in electrochemical spark
machining of quartz under different polarity conditions, Journal of Materials Processing
Technology 200(2008) 460–470.
132. Allesu K., Ghosh A., Muju M.K., Preliminary qualitative approach of a proposed
mechanism of material removal in electrical machining of glass, Eur. J. Mech. Eng.
36 (1992) 202–207.
133. Fascio V., Wüthrich R., Bleuler H., Spark assisted chemical engraving in the light of
electrochemistry, Electrochim. Acta 49 (2004) 3997–4003.
134. Tandon S., Jain V.K., Kumar P., Rajurkar K.P., Investigations into machining of composites,
Precis. Eng. 12 (1990) 227–238.
135. Langen H., Breguet J.M., Bleuler H., Renaud Ph, Masuzawa T., Micro electrochemical
discharge machining of glass, Int. J. Electr. Mach. 3 (1998) 65–69.
136. Crichton I.M., Mcgeough J.A., Studies of the discharge mechanisms in electrochemical arc
machining, J. Appl. Electrochem. 15 (1985) 113–119.
137. Cook N.H., Foote G.B., Jordan P., Kalyani B.N., Experimental studies in electro machining,
J. Eng. Ind. 95 (1973) 945–950.
138. Khairy A.B.E., Mcgeough J.A., Die-sinking by electro erosion-dissolution machining, CIRP
Ann. Manuf. Technol. 39 (1990) 191–195.
139. Didar T.F., Dolatabadi A., Wüthrich R., Characterization and modeling of 2D glass
micro-machining by spark-assisted chemical engraving (SACE) with constant velocity,
J. Micromech. Micro Eng. 18 (2008) 9.
140. Jain V.K., Chak S.K., Electrochemical spark trepanning of alumina and quartz, Mach. Sci.
Technol. 4 (2000) 277–290.
141. Furutani K., Maeda H., Machining a glass rod with a lathe-type electro-chemical discharge
machine, J. Micromech. Microeng. 18 (2008) 8.
142. Schöpf M., Beltram I., Boccadoro M., Kramer D., ECDM (Electrochemical discharge
machining) a new method for trueing and dressing of metal bonded diamond grinding tools,
CIRP Ann. Manuf. Technol. 50 (2001) 125–128.
143. Peng W.Y., Liao Y.S., Study of electrochemical discharge machining technology for slicing
non-conductive brittle materials, J. Mater. Process. Technol. 149 (2004) 363–369.
144. Solignac D., Sayah A., Constantin S., Freitag Rand M., Giijs M. A., Powder blasting for
realization of microchips for bio-analytic applications, Sensors Actuators A 92(2001)
388–93.
58 S. Debnath et al.
145. Liu C., Chen J., Engel J., Zou J., Wang X., Fan Z., Ryu K., Shaikh K., Bullen D., Polymer
micromachining and applications in sensors, microfluidics, and nanotechnology, 226th
National Meeting of the American Chemical Society (ACS) 2003 (NewYork, September
11–17).
146. Mills C. A., Martinez E., Bessueille F., Villanueva G., Bausells J., Samitier J., Errachid A.,
Production of structures for micro fluidic using polymer imprint techniques, Microelectron.
Eng. 78–9(2005) 695–700.
147. Holger B., Laurie E. L., Polymer micro fluidic devices, Talanta 56(2002) 267–87.
148. Lai S., Lee L. J., Yu L., Koelling K. W., Madou M. J. Micro-and nano-fabrication of
polymer based micro fluidic platforms for bioMEMS applications Proc. Materials Research
Society Symp. 729(2002) (U1.7.1-U1.7.11)
149. Getu H., Ghobeity A., Spelt J. K., Papini M. Abrasive jet micromachining of polymethyl-
methacrylate, Wear 263(2007) 1008–15.
150. Getu H., Ghobeity A., Spelt J. K., Papini M., Abrasive jet micromachining of acrylic and
polycarbonate polymers at oblique angles of attack, Wear doi:10.1016/j.wear.2008.01.013.
151. Singh R., Walia R. S., Study the effects of centrifugal force on abrasive flow machining
process. International Journal of Research in Mechanical Engineering and Technology 2
(2012) 34–39.
152. Singh R., Walia R. S., Suri N. M., Study of parametric effect on surface roughness
improvement for hybrid centrifugal force assisted abrasive flow machining process,
International Journal of Latest Research in Science and Technology 1(2012) 198–201.
153. Nouraei H., Kowsari K., Papini M., Spelt J.K., Operating parameters to minimize feature
size in abrasive slurry jet micro-machining, Precision Engineering 44 (2016) 109–123.
154. Liu Z., Nouraei H., Papini M., Spelt J.K., Abrasive enhanced electrochemical slurry jet
micro-machining: Comparative experiments and synergistic effects, Journal of Materials
Processing Technology 214 (2014) 1886–1894.
155. Shukla R., Singh D., Experimentation investigation of abrasive water jet machining
parameters using Taguchi and Evolutionary optimization techniques, Swarm and
Evolutionary Computation, doi:10.1016/j.swevo.2016.07.002.
156. Thoe T.B., Aspinwall D.K., Wise M. L.H., Review on Ultrasonic Machining, International
Journal of Machine Tools & Manufacture. 38(1998) 239–355.
157. Yu Z., Rajurkar K.P., Tandon A., Study of 3D Micro-Ultrasonic Machining, Journal of
Manufacturing Science and Engineering Vol. 126; 2004.
158. Markov A.I., Neppiras E., Ultrasonic machining of intractable materials, Iliffe, London,
1966.
159. Lv Z., Huang C.Z., Zhu H.T, Wang J., Wang Y., Yao P., A research on ultrasonic assisted
abrasive water jet polishing of hard-brittle materials, Int. J. Adv. Manuf. Technol. 78 (2015)
1361–1369.
160. Rhoades L., Abrasive flow machining: a case study, Journal of Material Processing
Technology 28 (1991) 107–116.
161. Davies P.J., Fletcher A.J., The assessment of the rheological characteristics of various
polyborosilixane/grit mixtures as utilized in the abrasive flow machining, Proceedings of
Institute of Mechanical Engineers 209 (1995) 409–418.
162. Raju H.P., Narayanasamy K., Srinivasa Y.G., Krishnamurthy R., Characteristics of extrude
honed SG iron internal primitives, Journal of Materials Processing Technology 166 (2005)
455–464.
163. Rajesha S., G Venkatesh., Sharma A.K., Kumar P., Performance study of a natural polymer
based media for abrasive flow machining, Indian Journal of Engineering & Materials
Sciences 17 (2010) 407–413.
164. Kumar R., Murtaza Q., Walia R.S., Three Start Helical Abrasive Flow Machining for Ductile
Materials, 3rd International Conference on Materials Processing and Characterization 6
(2014) 1884–1890.
165. Steigerwald J. M., Murarka S. P., Gutmann R. J., Chemical Mechanical Planarization of
Microelectronic Materials Wiley, New York, 1997, pp. 1–12.
1 Non-traditional Micromachining Processes … 59
166. Mori Y., Yamauchi K., Endo K., Mechanism of atomic removal in elastic emission
machining, Precision Engineering 10(1)(1988) 24–28
167. Hiraoka D., Hamazaki K., Matsumura K., Research on developing a prototype NC EEM
machine for machining high-power laser mirrors, Koyo Engineering Journal, 155E(1999)
42–47.
168. Mori Y., Ikawa N., Okuda T., Yamagata K., Numerically Controlled Elastic Emission
Machining; Technology reports of the Osaka University 26(1976) 283–294.
169. Endo K., Namba H., New machining method for making precise and very smooth mirror
surfaces made from Cu and Al alloys for synchrotron radiation optics, Rev Sci ln- strum 60
(1989)2.120-2.123.
170. Chang G.W., Yan B.H., Hsu R.T., Study on cylindrical magnetic abrasive finishing using
unbonded magnetic abrasives, Int. J. of Mach. Tool & Manuf 2002; 42: 575–583.
171. Yan B.H., Chang G.W., Cheng J.T., Hsu R.T., Electrolytic magnetic abrasive finishing, Int J
of Mach Tool & Manuf 43(2003) 1355–1365.
172. Yin S., Shinmura T., Vertical vibration-assisted magnetic abrasive finishing and deburring
for magnesium alloy, Int J of Mach Tool & Manuf 44(2004) 1297–1303.
173. Yamaguchi H., Shinmura T., Sekine M., Uniform Internal Finishing of SUS304 Stainless
Steel Bent Tube Using a Magnetic Abrasive Finishing Process, J of Manuf Sci & Eng. 127
(2005) 605–611.
174. Shinmura T., Takazawa K., Hatano E., Study on magnetic abrasive finishing – effects of
various types of magnetic abrasives on finishing characteristics, Bull Japan Soc of Prec Eng
21 (1987) 139–141.
175. Shinmura T., Takazawa K., Hatano E., Matsunaga M., Study on magnetic abrasive finishing,
Annals of the CIRP 39(1990) 325–328.
Chapter 2
Recent Advancement on Ultrasonic Micro
Machining (USMM) Process
Abstract There are a lot of developments in the micro manufacturing methods for
the production of the three-dimensional miniaturized products made up of different
advanced materials. Ultrasonic micro machining is an essential technique for the
fabrication of micro parts on the hard, brittle and non-conductive materials like
glass, ceramics and silicon with high aspect ratio. Ultrasonic micro machining is the
mechanical type non conventional micro machining process. Material removal
mechanism of USMM is similar to macro ultrasonic machining process. Adequate
surface finish with stiff tolerances and dimensions can be achieved by ultrasonic
micro machining (USMM) on hard and brittle materials. During the last decades, a
number of researchers have explored experimentally and theoretically this ultra-
sonic micro machining (USMM) process technique with different materials. Recent
development on ultrasonic micro machining (USMM) process has been highlighted
and discussed in details with different types of ultrasonic micro machining (USMM)
set up and material removal mechanism. Design and developments of micro-tools
for USMM process have also been discussed. Influences of different process
parameters on various responses of USMM have been discussed here.
2.1 Introduction
Fabrication of the miniaturized products with multi functions are the urgent need of
manufacturing industry. Micro-parts are required to meet the increasing demands in
various areas like electronics, aerospace, automotive, medical devices, etc. The
main advantage of those miniaturized products are small space requirement, less
energy and material consumption, easiness in delivery and less price of the product.
Now the products with the extraordinary characteristic of materials such as high
hardness, strength, corrosion resistant and heat resistant etc. are machined at the
micron range of dimensions. Production of complex 3D miniature components such
as fabrication of micro holes in thousand numbers on filters for processing food and
textile industries, which are not possible by any conventional machining methods.
Such features on those components can get only through the non-conventional
micro machining process.
The generation of micro machining features on ceramics, glass, carbides and
metallic alloys, etc. by traditional machining method is tremendously difficult and it
also takes more time. Adequate surface finish with stiff tolerances and dimensions
can be achieved by ultrasonic micro machining (USMM) on hard and brittle
materials. Other Non Traditional machining process like µEDM, µECM, and LBM
etc. can’t machine those materials in proper shape and size [1]. Using other
non-traditional machining process it is difficult to machine square, irregular and
complex shaped holes and surface impressions. Ultrasonic micro machining
(USMM) can be used for those purposes. Any hard and fragile material can be
machined using USMM. The main advantage of ultrasonic micro machining pro-
cess is that it can machine any electrical conductive and non-conductive materials
[2]. Micro tool development and fixing on the USMM system is the very much
problematic area. This problem can be eliminated by micro tool development with
the help of wire electro-discharged grinding (WEDG) method and the same tool can
be utilized to make micro-holes 5–20 µm in diameter on a silicon plate [3, 4].
A number of research works have been reported in micro-USM processes.
Recent advancement on ultrasonic micro machining (USMM) process has been
highlighted and discussed in details with different types of ultrasonic micro
machining (USMM) set up and material removal mechanism. Design and devel-
opments of micro-tools for USMM process have also been discussed. Influences of
different process parameters on various responses of USMM have been dis-
cussed in this chapter.
ceramics, inorganic glasses, and quartz etc. The ultrasonic frequency of the tool is
above 20 kHz with amplitude of 8–30 lm. Water based abrasive particles are
supplied through the machining zone by a recirculation pump. The tool is pressed
on the workpiece with fixed static load and the workpiece material is nonstop
hammered by numerous abrasive particles with high kinetic energy imparted by the
vibrated tool. Flushing of abrasive slurry refreshes the machining area and also
removes the debris from the machining zone.
In 1927, R.W. Wood and A.L Loomis observed the drilling and cutting action with
the help of ultrasonic vibration. After a long interval L. Balamuth proposed ultra-
sonic machining in 1942, while he was investigated the dispersion of solid in liquid
by means of a magnetostrictively vibrating nickel tube. Several types of ultrasonic
machine tool have been developed in recent year. The first communication on
equipment and techniques for ultrasonic cutting appeared in 1953–54 [5].
Originally USM used to be a finishing operation for the component processed by
the electro spark machines. However, this use becomes less important because of
the development in electric discharge machining. But then with the boom in solid
state electronics, the machining of electrically non-conducting, semi conductive,
and brittle material become more and more important. For this reason, ultrasonic
machining again gained importance and prominence. Through research and
development on ultrasonic machining technology, different types of ultrasonic
machining systems have been developed.
Fig. 2.1 Schematic diagram of ultrasonic machining set-up with process equipments
conjugate image of the tool form. Due to the fact USM is not restricted to the
manufacture of circular holes. The tool can be prepared to the required shape, and
therefore extremely complex shapes can be created on hard and brittle materials.
Any damaging or thermal effects on the metallic structure of the workpiece does not
found in this machining process.
grains are mixed with water is distributed across the tip of the tool. The
abrasive particles are mixed with water and are hammered by the tool into the
workpiece surface. Then the material is removed from the workpiece and the
conjugate images of the tool form are produced [6].
ii. Rotary ultrasonic machining (RUM) is a hybrid machining process that
combines the rotating diamond grinding tool with ultrasonic machining
(USM). Higher material removal rates (MRR) are found using rotary ultra-
sonic machining. In this machine set up, a rotary core drill with metal bonded
diamond abrasives tool is ultrasonically vibrated in the axial direction and the
tool is fed toward the workpiece at a constant pressure. Coolant is pumped
through the machining zone to prevent jamming of the tool and keeps it cool.
RUM provides a fast, high-quality material removal process for a variety of
glass and ceramic applications using abrasives bonded tools with combining
rotation and vibration [7].
iii. USM combined with electric discharge machining [8].
iv. Ultrasonic supported cutting or grinding. Ultrasonic assisted turning is the
most familiar process and is claimed to reduce machining time, residual
stresses of the working zone and improve surface quality and tool life com-
pared to conventional turning [9, 10].
The ultrasonic micro machining (USMM) process is copied from macro ultrasonic
machining (USM) for micro machining on any hard and fragile materials. The tool
frequency of USMM is above 20 kHz and lower amplitude of 0.5–5 µm. The
abrasive particles size of USMM is few microns of 0.5–15 lm. The material
removal mechanism is same as conventional USM.
Masuzawa of Tokyo University in the mid 1990s was first attempted of downsizing
macro-USM for micromachining [11]. The ultrasonic micro machining is used for
producing micro feature on any hard and brittle materials such as any bio ceramic
materials, glass and silicon etc. [12]. Ultrasonic micro machining has similar pro-
cess parameters as macro-USM. However, the micromachining process requires a
micro-sized tool with smaller amplitude, and micro-sized abrasive particles [13].
66 S. Das et al.
Table 2.1 Comparison of ultrasonic micro machining (USMM) and macro USM
Parameters Ultrasonic micro machining (USMM) MACRO-USM
Vibration frequency, kHz Usually >20 Usually >20
Vibrated component Tool or workpiece Tool
Amplitude, lm 0.5–5 lm 8–30 lm
Abrasive particle size, lm 0.5–15 lm 50–300 lm
Static load Gram force Kilogram force
Tool diameter <500 µm >500 µm
Thickness of workpiece maximum 3 mm Maximum 50 mm
Tool material Tungsten carbide (preferred) Stainless steel (preferred)
Ultrasonic Vibration can be provided either in tool or in workpiece. There are three
types of machining setup.
i. µ-USM setup with Tool vibration: Sun et al. developed µ-USM setup with
provision of tool making using Electric Discharge Machining (EDM) and
Wire electro Discharge Grinding (WEDG). In this µ-USM setup the tool is
vibrated with ultrasonic vibration. The WEDG unit is permanently fixed on the
machine body for grinding fine electrodes. Four axes X, Y, Z and C are
numerically controlled by the machine. The µ-USM unit consists of a high
frequency oscillation generator, transducer and horn-tool combination.
Computer control system is used to control the operation of µ-USM setup
[14]. Figure 2.2 shows the µ-USM setup with tool vibration.
ii. µ-USM setup with Workpiece vibration: The µ-USM setup with Workpiece
vibration as shown in Fig. 2.3. In this setup a micro tool is holed properly and
also rotated by a DC motor to move in X, Y and Z directions. Micro tools are
prepared by wire electrical discharge grinding (WEDG). Due to sensitiveness,
bending, vibration, and breakage of the micro tool, the controlled and limited
2 Recent Advancement on Ultrasonic Micro Machining (USMM) Process 67
1. Display unit
2. Computer
Control unit
3. Ultrasonic
generator
4. Data
Acquision
5. XYZ stage
6. Tool
7. Abrasive slurry
8. Workpiece
9. Ultrasonic
transducer
10. Load sensor
The basic component of the micro rotary ultrasonic machine system is ultrasonic
vibration system (transducer and generator), positioning system (XYZ-stages),
cutting force feedback sensor, system controller, machine spindle, tool holder and
work piece holder. The system is an assembly of a piezoelectric ultrasonic trans-
ducer. A spindle for rotating tool and position of tool is controlled in X, Y and Z
axis by a precision motion controller with 25 nm resolution. The work piece is
vibrated ultrasonically at 39.5 kHz by mounting it on the free end of the transducer.
The abrasive slurry mixed with water is injected into the machining gap between
the work piece and tool [16, 17].
Zarepour et al. investigated the mechanism of material removal and the relationship
between process parameters. They also investigated the analytical mode of material
removal mechanism in ultrasonic micro machining (USMM) process on silicon
material [19]. Yu et al. [20] studied the debris accumulation and reported an
explanation of the influences of abrasive particles on the surface roughness.
Guodong Lia et al. investigated the material removal mechanism on quartz crystals.
When the roughness value is very less, the machined surface by ultrasonic micro
machining (USMM) process is comparatively smooth. This was one of the proofs
of the existing of ductile machining [21]. Zarepour et al. [22] presented a new
method for the static force measuring and the workpiece clamping for the ultrasonic
micro machining (USMM) process. The proposed control system and force mea-
surement provide a compact arrangement and prevent the undesirable effects of
vibration of the horn.
In the ultrasonic micro machining (USMM) process, abrasive particles with
random shapes and sizes are supplied in the machining gap between the micro tool
and the workpiece. At each vibration cycle, each abrasive particle is interacted with
the workpiece in one of the following ways [23]:
i. Appling direct impact force on the workpiece surface by the abrasive particles:
this is common when the abrasive grain size is larger than the machining gap.
ii. Impact of free-moving abrasive particles on the workpiece surface: this is
common when the abrasive grain size is smaller than the machining gap.
iii. Cavitations effect erosion: the high frequency vibration power generates a high
frequency mechanical pressure in the slurry medium causing the abrasive
particles to impact the workpiece surface.
In USMM, the tool vibrates above 20 kHz, and water based abrasive slurry is
pumped to the small gap between the workpiece and the tool [2]. The removal of
material from the workpiece by USMM process is caused of micro-cracks by the
brittle fracturing of the workpiece. Understand crack generation in USMM in order
to improve machining efficiency and precision is investigated. The impact of a
single abrasive grain during USMM process can be very useful for understanding
crack generation of the workpiece. The main activities for removing material from
the workpiece have been described by some researchers as follows:
i. The hammering effect by abrasive particle is shown when the tool and
workpiece are in contact.
ii. The impact action is also shown by a free-moving abrasive particle in the
working gap.
iii. The cavitations erosion phenomenon is shown by abrasive particle in slurry
concentration [24–26].
70 S. Das et al.
Fig. 2.5 Schematic diagram of material removal in MUSM: a Hammering action, b Impacting
action
The material removes from the workpiece in the ultrasonic micro machining pro-
cess is very much depended by Initiation and propagation of median as well as
lateral cracks. Figure 2.6 shows that initiation of cracks and localized deformation
of a brittle material. This is generated by large or a small abrasive grain, which acts
as an indenter [28–30].
The abrasive particles act as indenter on the workpiece surface. The fracture is
started on the surface by impression of an indenter in the machining area. Many
authors have investigated in this area. It has been found that at first the sharp point
of the indenter produces an inelastic deformation zone during machining. Then
deformation is induced and suddenly develops into a small crack or median crack.
The median crack is increased progressively by increasing the load. The median
crack begins to close during unloading and inducing the formation of lateral vents.
The lateral vents are carried on their extension toward the workpiece surface upon
complete unloading and may lead to chipping. The sequence of crack procedures
that occur during the machining has been shown in Fig. 2.7.
+P means increasing load; −P means decreasing load. The sequence of vent
crack propagation is summarized as follows:
i. An inelastic deformation zone is produced by the sharp indenter.
ii. After that the deformation flow suddenly develops into a little crack. This is
known as median crack.
iii. Next the median cracks are developed gradually with increasing the load.
72 S. Das et al.
K4
Pc ¼ a ð2:1Þ
H3v
2 Recent Advancement on Ultrasonic Micro Machining (USMM) Process 73
where
a is a dimensionless feature which is related to the indenter geometry;
K is the fracture toughness of the workpiece; and
HV is the vickers diamond hardness of the workpiece.
For the size of the median or radial crack (CR) and lateral crack (CL), the
following equations have been derived [32]:
R ¼ n1 P
Cm ð2:2Þ
3=4
P
C L ¼ n2 ð2:3Þ
K
where, m = 1−1.5,
P is the applied load,
n1 and n2 are proportionality constants [33].
The depth of indentation is established by equating the mean static force. This
mean force comes from impacting the tool on the grains. Assume the number of
abrasive particles in the gap between tool and workpiece are inversely proportional
to the square of the diameter of each of the abrasive particles. The following
expression for machining depth h is described as follows [34]:
1=2
8FAd
h¼ ð2:4Þ
PK1 HV Cð1 þ qÞ
where
F is the applied static force,
A is the vibration amplitude of the tool,
HV is the hardness of the workpiece,
q is the hardness ratio of the workpiece to that of the tool,
d is average abrasive grain diameter,
C is the abrasive slurry concentration and
K1 is proportionality constant.
(continued)
Name of Mechanism of Assumptions
investigators material removal
Rajurkar et al. Combined effect i. Work-piece is considered as a semi-infinite solid.
[40] of impact ii. The movement of abrasive grit is perpendicular to the free
indentation and surface during machining.
fracture iii. Speed of abrasive is same as that of vibrating tool.
phenomenon.
Lee and Chan Brittle fracture. i. Pre-existing defect is considered in the workpiece material
[41] for the initiation of median or lateral cracks.
ii. Median or lateral crack size is related to pseudo pressure
between tool and work-piece.
Wiercigroch Micro-cracking i. MRR depends on the magnitude of impact force and its
et al. [42] due to impacts frequency.
of grains. ii. Diamond grain is equally distributed over the working part
of the tool with a uniform grain size.
iii. Ultrasonic amplitude of vibration, frequency and tool
geometry remain constant.
Nath et al. [43] The hole i. The effects of material removal phenomena from the
entrance workpiece on the hole integrity such as entrance chipping,
chipping, lateral wall roughness and subsurface damage are considered.
gap. ii. Material removal mechanism takes place in the gap between
the outer periphery of tool and the hole wall (called ‘lateral
gap’).
iii. The radial and the lateral cracks are founded due to
adjacent abrasives, which are under the tool face. It extends
towards radial direction of the hole resulting in entrance
chipping.
iv. The angle penetration and the rolling actions of the each
abrasive particle, which are at the edge of the cutting tool.
It contributes the entrance chipping. After that the lateral
gap of the sliding and the rolling mechanisms by the larger
abrasive particles take part of the material removal.
v. Unfavourably micro-cracks in the radial direction are
produced and cause subsurface damages, which are
ultimately responsible for rough surface.
vi. The size of micro-cracks in brittle materials is depended by
abrasive grain size.
vii. It is realized that such nature of the hole integrity during
USM can only be minimized by using smaller abrasive
grain size, but cannot fully be reduced.
Ichida et al. [44] liquid i. Non-contact ultrasonic abrasive machining (NUAM) method
cavitations, is introduced.
cavitations ii. Abrasive particles are excited by ultrasonic energy.
erosion. iii. Material is removed by the erosion due to liquid cavitations
collapse pressure or impact force.
iv. Material removal based on colliding or sliding of the
abrasive grains, which are accelerated by the impact force
due to cavitations collapse on the workpiece surface.
76 S. Das et al.
The essential part of ultrasonic micro machining set up consists of ultrasonic power
supply, oscillating system, horn, coupler, the mechanism of tool feeding, and the
abrasive slurry supply system unit. Figure 2.8 shows the schematic diagram of
ultrasonic micro machining set up.
The power supply for an ultrasonic machine tool is characterized as a sine wave
generator that supplies the frequency and power of the generated signal. The output
power supply with internal or external power control is variable. Low frequency
(50 Hz) electrical power is converted high frequency (greater than 20 kHz) by this.
The power supply is capable of automatic frequency control and automatic load
compensation at optimum efficiency. It also provides constant output amplitude at
required setting during the operating cycle for meeting the different energy
requirement. One overload monitor system is incorporated to the power supply for
defending the system from any failure conditions. If any overload condition takes
place, the overload indicator lamp is indicated on monitor and the ultrasonic fre-
quency is closed for balancing the cycle. After that the monitor is automatically
come to the reset position itself for stopping the operation until the fault condition is
Transducer
Vibrating Unit
Horn
Tool
eliminated. The monitor is reactivated on every operating cycle for avoiding the
damage to the transducer.
Ultrasonic transducer is the main part of this machining setup. It generates the
ultrasonic frequency of vibration above 20 kHz and range of the amplitude of
0.8–5 µm for USMM. The electrical supply voltage provides 50 Hz electrical
energy, which is also applied to the transducer element. The converter transforms
the high frequency electrical vibrations into high frequency mechanical vibrations.
Lead zirconate is the heart of the converter. This is actually titanate electrostrictive
element. When alternating voltage is applied, it expands and contracts at the fre-
quency of the voltage. This electrostrictive converter is highly efficient for saving
energy.
i. Magnetostrictive Transducer
Joule was first discovered the magnetostriction effect in 1874. According to this
effect, ferromagnetic metals and alloys is changed in their length in the presence
of an applied magnetic field. The ferromagnetic material is only responsible for
positive or negative deformation. One coil is wrapped around a stack made of
magnetostrive material (iron–nickel alloy) and electric signal of ultrasonic
frequency is fed into this coil. This stack is fully laminated for minimizing eddy
current and hysteresis losses; moreover, it must be cooled to dissipate the
generated heat. The stack expands and contracts at the same frequency with the
help of the alternating magnetic field produced by the AC generator. The
maximum magnetostriction effect is achieved using the high frequency AC
current, which must be superimposed on appropriate DC pre-magnetizing
current. That must be exactly adjusted for getting optimum or working point.
When this point is accurately adjusted, the maximum magnetostriction effect
(maximum oscillating amplitude) is provided and it also prevents the frequency
doubling phenomenon.
If the frequency of the ac signal in the magnetic field is tuned by same value of
the natural frequency of the transducer and the whole oscillating system, so it
acts at mechanical resonance. This time oscillation amplitude becomes mod-
erately large and the exciting power reaches its smallest value.
ii. Piezoelectric Transducer
Piezoelectric transducer works with piezoelectric effect. When an electric
current is passed through the piezoelectric material, then it expands. But when
the current is removed the piezoelectric material reaches its original size. This
phenomenon actually is called piezoelectric effect. The voltage measuring
instrument shows the electric voltage produced by piezoelectric transducer,
which can be used to measure forces. The main drawback of magnetostrictive
transducers is the high power loss (η = 55%). The power loss is converted into
78 S. Das et al.
heat. For this reason piezoelectric transducers are used and the efficiency is
greater than 90%, even at higher frequencies (f = 25–40 kHz). Piezoelectric
transducers use crystals like quartz that undergoes the dimensional changing
proportional to the applied voltage.
2.5.3 Horn
The horn is also called mechanical amplifiers or concentrators. The functions of the
horn describes as follows:
i. The mechanical energy is transmitted to the tool by the horn.
ii. The horn amplifies the amplitudes of vibration.
iii. The horn concentrates the all power on the small machining zone.
The main acoustic horn head is supplied by the company as an essential part
with the machine. The required tool is fixed by silver brazing to the free end of the
by threading. The difference of amplitude of vibration between the primary horn
and secondary acoustic horn is small enough.
2.5.4 Coupler
The coupler attaches between the converter or transducer and horn. This allows for
clamping of the converter, coupler, and horn assembly and provides amplitude
choices for various applications.
gauge indicates the static force. The tool displacement is indicated by the dial
gauge.
Several abrasives are available in various sizes for ultrasonic machining. The cri-
teria for selection of an abrasive for a particular application include hardness, size of
the abrasive particle, cost of the particle and working life. In order of hardness,
aluminium oxide (Al2O3), silicon carbide (SiC) and boron carbide (B4C) are the
most commonly used abrasives. The abrasive particles are mixed with water with
proper ratio to from the slurry. Average particle size of 3–10 lm is selected and the
abrasive slurry is supplied by a recirculating pump into the machining zone. The
abrasive used for an application should be harder than the material being machined
otherwise the usable life time of the abrasive will be substantially shortened. Boron
carbide is selected when machining the hardest work piece materials or when the
highest material removal rates are desired. Although the cost is five to ten times
greater than the next hardest abrasive, silicon carbide, the usable life of boron
carbide is 200 machine operating hours before cutting effectiveness is lost and
disposal is necessary. This compares with a usable life time of approximately 60 h
for silicon carbide. The combination of high removal rates and extended life time
justify the higher cost of boron carbide. The abrasive particles size influences the
material removal rate and surface finish. Abrasive for USM are generally available
in grit sizes ranging from 240 to 800 while the coarser grit exhibit the highest
removal rates, they also result in the roughest surface finish and are therefore, used
only for roughing operation, conversely, 800 grit abrasives will result in fine surface
finishes but at a drastic reduction in metal removal rate. The most popular general
purpose abrasive is used, based on the above considerations is 320 grit of boron
carbide. The common abrasive slurry concentration is 50% by weight; however, the
concentration can vary from 30 to 60%. The thinner mixtures are used to promote
efficient flow when drilling deep holes or when forming complex cavities. The
abrasive particles are stored in a reservoir at the USM machine and pumped to the
tool work piece interface by recirculation pumps at rates up to 26.5 lit/min. higher
power ultrasonic machine require the addition of a light-duty cooling system to
remove waste heat from the abrasive slurry.
In ultrasonic micro machining (USMM), the shape and dimension of the final
products depends on the developed tool. The fabrication of micro tool is a really big
challenge. It is extremely not easy to hold the micro tool properly with good
accuracy of the job due the application of vibrations at the tool end. One method
80 S. Das et al.
was introduced to overcome this problem. The tool is prepared on the machining
time in this method. At first the macro size tool was fixed to the tool head. Wire
electro discharge grinding (WEDG) method was applied to fabricate micro tool and
machining was done on the same machine tool. Using wire electro discharge
grinding (WEDG) method micro tool of less than 20 µm can be achieved [3].
Another method was introduced in 1999, in which workpiece was vibrated ultra-
sonically. In this method, the better tool holding is possible and high precision can
be achieved [4]. Figure 2.9 exhibits the micro tool developed by WEDG method.
Tool wear also occurs during USMM process. To reduce tool wear in USMM,
micro tool should be fabricated from stainless steel, brass and mild steel etc.
More tool wear was found using very hard tool material due to material removal
from tool by abrasive particle in the machining zone [45]. The tool material should
have superior elastic strength, high wear resistance most favorable values of
hardness and toughness, high fatigue strength properties for the application of any
hard and brittle material [46]. Tungsten carbide (WC) and sintered diamond (SD)
alloy tools were introduced and up to 5 µm micro hole was produced by this tool
with good accuracy. With the help of SD tool, micro tool of 21 µm diameter and
150 µm depth on soda glass was generated and the aspect ratio of 7 could be
achieved [4, 19]. Figure 2.10 shows micro tool for USMM.
Very few research works have focussed on the various responses of ultrasonic
micro machining such as material removal rate (MRR), tool wear rate, geometrical
accuracy and quality of the machined surface etc. The main objective of ultrasonic
micro machining (USMM) is to fabricate a micro feature with desired quality of the
surface, negligible surface damage, good geometrical accuracy, and satisfactory
material removal rate very economically. The possible process parameters in
ultrasonic micro machining (USMM) is illustrated by cause effect diagram as
shown in Fig. 2.11.
Fig. 2.11 Cause effect diagram for process parameter selection of USMM
82 S. Das et al.
The material removal rate significantly depends on the type and size of abrasive
particle in USMM. More material removal rate is found when the average grain
diameter of abrasives particle and hardness of the abrasive particles are increased
[3]. Extensively more materials are removed from the workpiece using coarser
abrasive particles. So that, material removal rate is increased [47]. The material
removal rate also depends on the average applied static load. However, MRR is
decreased beyond a certain value with increasing of the average static load. The
abrasive particles in the machining region are influenced by the static load. The
abrasive particles are striking and removing the more material from the workpiece
using high static load. As a result, MRR is increased [6, 48]. The vibration
amplitude is one of the major parameter. The material removal rate is increased with
increasing the amplitude of vibration [3].
The abrasive particles hit the workpiece and tool also into the machining zone
during machining. So that, the tool tendency to erode the materials due to abrasion
of those abrasive particles. Tool wear is an significant response of USMM process.
The more tool wear is found when coarser abrasive particles are used [3]. Tool wear
also depends on the vibration amplitude. Large amplitude of vibration provides
more kinetic energy of the abrasives particles under the bottom area of tool tip. At
this time the material from the tool tip also is removed and tool wear is shown [49].
Due to extreme tool wear, the stainless steel tool is not suitable in USMM process.
More tool wear is found, when the tool diameter is small [16]. The tool wear rate
depends on static load, amplitude of vibration also. The tool wear increases with
increasing the static load and amplitude of vibration. For achieving low tool wear
lower static load and lower amplitude of vibration are used [3].
Surface finish depends on the type and size of abrasive particle, concentration of
abrasive slurry. Good surface finished was achieved using fine and small abrasive
particles.
2 Recent Advancement on Ultrasonic Micro Machining (USMM) Process 83
Egashira et al. [3] has investigated that most unpleasant surface finish was found
using tungsten carbide (WC) tool as compared to titanium carbide (TiC) tool. Less
material is removed when fine abrasive particle size of less than 10 µm is used and
as a result the smooth surface is generated [6]. The static load and vibration
amplitude are the important process parameters. The Ra value of the surface
increases with increasing the static load and vibration amplitude due to more
material removal from the workpiece [48].
Ultrasonic micro machining has faced a problem which is proper fixing the micro
tools with high precision to the horn in this set up. One method was proposed for
USMM set up which was fabricating the micro tools by wire electro discharge
grinding (WEDG) procedure. Appling this method, micro holes on a silicon plate
and quartz of 20 lm in diameter and 50 lm in depth could be achieved [3, 4].
Figure 2.12 illustrates a micro-hole machining in Al2O3 ceramics, with an aspect
ratios of 10. Figures 2.13 and 2.14 shows the square, triangular, circular micro
holes on silicon and glass. Drilling multiple holes can be made by USMM process.
Figure 2.15 shows the array of microholes machined by USMM process.
Figure 2.16 shows micro cavity with 3D view, which was effectively fabricated
on silicon with a cylindrical-shaped micro tungsten tool [48]. Figure 2.17 shows
that machining of 48 holes with a single SD tool on Silicon, with 22 µm hole
diameter, and 20 µm tool diameter and 0.8 µm of amplitude [4].
84 S. Das et al.
Fig. 2.12 An example of micro-hole machining in Al2O3 ceramics, with an aspect ratios of 10
[47]
2 Recent Advancement on Ultrasonic Micro Machining (USMM) Process 85
iv. Drilling very fine holes can be possible on shafts and gears which are used in
helicopter power transmission.
v. It can be used for producing round, square, irregular shaped holes and sur-
face impressions.
vi. Round through holes with tight-tolerance for processing semiconductor’s
equipment can be possible.
vii. Micro machining of micro-structured glass wafers is fabricated by USMM
process for micro electromechanical systems (MEMS) applications.
viii. High-aspect ratio, 25:1 can be possible in glass and advanced material.
ix. USMM process can be applied in aerospace, tool/mold/machine construc-
tion, pump and valve industry, time piece industry/precision mechanics etc.
Process development for ultrasonic micro machining is one of the most significant
issues. In ultrasonic micro machining most difficult task is understanding of the
material removal mechanism. Few discussions are available till now but further
analysis of the material removal mechanism is necessary for this process. Micro
tool fabrication is one another aspect of this process. Preparation of micro tools,
handling of micro tools and fixing the micro tools with the tool holder are also the
challenging areas of research. The accuracy of micromachining processes depend
on these condition of the micro tools. In micromachining, there is reduction in size
of tool dimension, abrasive dimension and vibration amplitude etc.
Environmental aspects are one of the essential topics which have hardly been
reported. It is one of the important issues of modern manufacturing process.
The fabrication of components for micro fluidic application using USMM pro-
cess is one of the exploring areas. There is a scope of research in the area of
fabrication of micro channels on ceramics, silicon and glass for micro heat
exchanger and sensors applications by USMM process.
2.11 Summary
In this book chapter the important issues regarding different aspects of ultrasonic
micro machining (USMM) have been discussed. This chapter also focuses on the
process development of USMM, working principle and limitations of USMM.
Different types of USMM processes, micro tooling for USMM process, material
removal mechanism and influences of process parameters have been discussed.
Geometrical accuracy and capabilities of the USMM process have been reviewed.
Ultrasonic micromachining (USMM) is well-established process to machine
hard and brittle materials (like alumina, zirconia, silicon and glass etc.) The material
2 Recent Advancement on Ultrasonic Micro Machining (USMM) Process 89
References
1. S.G. Amin, M.H.M. Ahmed, H.A. Youssef, “Computer-aided design of acoustic horns for
ultrasonic machining using finite-element analysis”, Journal of Materials Processing
Technology 55 (1995) 254–260.
2. Thoe, T., D. Aspinwall, Wise M. Review on ultrasonic machining. International Journal of
Machine Tools and Manufacture, 1998. 38(4): p. 239–255.
3. Egashira K.; Masuzawa T.; Fujino M. and Sun X. Q. “Application of USM to microma-
chining by on-the-machine tool fabrication,” International Journal of Electrical Machining,
no. 2, pp. 31–36, 1997.
4. Egashira K. and Masuzawa T. “Microultrasonic machining by the application of workpiece
vibration,” CIRP Annals—Manufacturing Technology, vol. 48, no. 1, pp. 131–134, 1999.
5. Kremer D. Saleh S. M. Ghabrial S. R. and Moisan A. “The State of the Art of Ultrasonic
Machining,” CIRP Annals—Manufacturing Technology, vol. 30, no. 1, pp. 107–110, 1981.
6. Barash M.M. and Watanapongse D. (1970), “On the effect of ambient pressure on the rate of
material removal in ultrasonic machining”, International Journal of Mechanical Sciences, Vol.
12, pp. 775–779.
7. Li Z.C., Jiaoa Y., Deinesa T.W., Pei Z.J.(2005), “Rotary ultrasonic machining of ceramics
matrix composites: feasibility study and designed experiments”, International Journal of
Machine Tools and Manufacture, Vol. 45, No. 12–13, pp. 1402–1411.
8. Jianxin, D. and Taichiu, L (2000), “Surface integrity in electro-discharge machining,
ultrasonic machining and diamond saw cutting of ceramic composites”, Ceramic
International, Vol. 26, No. 8, pp. 825–830.
9. Balamuth L.A. (1966), “Ultrasonic assistance to conventional metal removal”, Ultrasonics,
Vol. 4, pp. 125–130.
10. Babitsky V.I., Mitrofanov A.V., Silverschmidt V.V. (2004), “Ultrasonically assisted turning
of aviation materials: simulations and experimental study”, Ultrasonics, Vol. 42, pp. 81–86.
11. X. Q. Sun, T. Masuzawa, and M. Fujino, “Micro ultrasonic machining and self-aligned
multilayer machining/assembly technologies for 3D micromachines,” in Proceedings of the
IEEE Micro Electro Mechanical Systems (MEMS ’96), pp. 312–317, 1996.
12. Ghahramani B. and Z. Y. Wang Z. Y., “Precision ultrasonic machining process: a case study
of stress analysis of ceramic (Al2O3),” International Journal of Machine Tools and
Manufacture, vol. 41, no. 8, pp. 1189–1208, 2001.
13. Masuzawa T. and Tönshoff H. K. “Three-dimensional micromachining by machine tools,”
CIRP Annals —Manufacturing Technology, vol. 46, no. 2, pp. 621–628, 1997.
14. Sun, X.Q., Masuzawa, T, Fujino, M., Micro ultrasonic machining and self-aligned multilayer
ma-chining/assembly technologies for 3D micromachines, Proc. IEEE, 1996, pp. 312–317.
15. Yu, Z.Y., Rajurkar, K.P., and Tandon, A. Study of 3D Micro-Ultrasonic Machining. Journal
of Manufacturing Science and Engineering, 2004, 126(4), 727–732.
16. Sarwade, A., Sundaram, M. M., & Rajurkar, K. P. (2010). Investigation of micro hole drilling
in bovine rib using micro rotary ultrasonic machining. In 16th International Symposium on
Electromachining, ISEM 2010. (pp. 411–416). Shanghai Jiaotong University Press.
90 S. Das et al.
17. Sarwade, A., Sundaram, M. M., & Rajurkar, K. P. (2010). Micro rotary ultrasonic machining:
Effect of machining parameters on material removal rate. In Transactions of the North
American Manufacturing Research Institution of SME. (Vol. 38, pp. 113–120).
18. Shimada, S., et al., Brittle-Ductile Transition Phenomena in Microindentation and
Micromachining. CIRP Annals—Manufacturing Technology, 1995. 44(1): p. 523–526.
19. Zarepour, H., Yeo. S.H. (2012) Predictive modeling of material removal modes in micro ultrasonic
machining. International Journal of Machine Tools and Manufacture, vol. 62, pp. 13–23.
20. Yu, Z., X. Hu, K.P. Rajurkar. Influence of Debris Accumulation on Material Removal and
Surface Roughness in Micro Ultrasonic Machining of Silicon. CIRP Annals—Manufacturing
Technology, 2006. 55(1): p. 201–204.
21. Lia G.; Yu Z.; Song J.; Li C., Li J. and Wataru Natsu W., “Material Removal Modes of Quartz
Crystals by Micro USM”, Procedia CIRP 42 (2016) 842–846.
22. H. Zarepour & S. H. Yeo & P. C. Tan, E. Aligiri, “A new approach for force measurement
and workpiece clamping in micro-ultrasonic machining”, Int J Adv Manuf Technol (2011)
53:517–522.
23. K. P. Rajurkar, and W. M. Wang, “Nontraditional Machining,” CRC Handbook of
Mechanical Engineering-Ch.13, 1997, pp. 29–34.
24. W. H. Fan, C. L. Chao, W. C. Chou, T. T. Chen, and C. W. Chao, “Study on the surface
integrity of micro-ultrasonic machined glass-ceramic material,” Key Engineering Materials,
Vol.407–408, pp. 731–734, 2009.
25. M. Komaraiah and P. Narasimha Reddy, “A study on the influence of workpiece properties in
ultrasonic machining,” Int. J. of Machine Tools and Manufacture, Vol.33, No.3, pp. 495–505,
1993.
26. Soundararajan V. and Radhakrishnan, V., “An experimental investigation on the basic
mechanisms involved in ultrasonic machining,” Int. J. of Machine Tool Design and Research,
Vol.26, No.3, pp. 307–321, 1986.
27. Y. Ichida, R. Sato, Y. Morimoto, and K. Kobayashi, “Material removal mechanisms in
non-contact ultrasonic abrasive machining,” Wear, Vol.258, No.1–4, pp. 107–114, 2005.
28. D. Kremer, S. M. Saleh, S. R. Ghabrial, and A. Moisan, “The state of the art of ultrasonic
machining,” CIRP Annals—Manufacturing Technology, Vol.30, No.1, pp. 107–110, 1981.
29. A.G. Evans, Fracture mechanics determinations, in: Fracture Mechanics of Ceramics, vol. 1,
Plenum, New York, 1974.
30. D. Charkaborty, J. Mukeryi, Indentation induced cracks in hot pressed Si3N4,
Indian J. Technol. 20 (1982) 361–365.
31. A.G. Evans, D.B. Marshall, in: D.A. Rigney (Ed.), Fundamentals of Friction and Wear of
Materials, ASME, 1981, pp. 439–440.
32. A.G. Evans, T.R. Wilshaw, Quasi-static solid particle damage in brittle solids—I.
Observations, analysis and implications, Acta Metallurgica, vol. 24, Pergamon Press, 1976,
pp. 939–956, printed in Great Britain.
33. M. Komaraiah, P.N. Reddy, A study on the influence of workpiece properties in ultrasonic
machining, Int. J. Mach. Tools Manuf. 33 (3) (1993) 495–505.
34. Shaw M.C. (1956), “Ultrasonic grinding”, Annals of CIRP, Vol. 5, pp. 25–53.
35. Miller G.E. (1957), “Special theory of ultrasonic machining”, Journal of Applied Physics,
Vol. 28, No. 2, pp. 149–156.
36. Rozenberg, L.D.; Kazantsev, V.F.; Makarov, L.O. and Yakhimovich D. F. (1964),
“Ultrasonic Cutting”, Consultant Bureau, New York, pp. 97–102.
37. Cook N.H. (1966), “Manufacturing analysis”, Addison-Wesley, New York, pp. 133–148.
38. Kainth G.S.; Nandy A. and Singh K. (1979), “On the mechanisms of material removal in
ultrasonic machining” International Journal of Machine Tool Design and Research, Vol. 19,
pp. 33–41.
39. Nair E.V. and Ghosh A. (1985), “A fundamental approach to the study of mechanics of
ultrasonic machining”, Int. Journal of Prod. Research, Vol. 23, pp. 731–753.
2 Recent Advancement on Ultrasonic Micro Machining (USMM) Process 91
40. Rajurkar K.P.; Wang Z.Y. and Kuppattan A. (1999), “Micro removal of ceramic material
(Al2O3) in the precision ultrasonic machining”, Precision Engineering, Vol. 23, No.2, pp 73–
78.
41. Lee T.C. and Chan C.W. (1997), “Mechanism of the ultrasonic machining of ceramic
composites”, Journal of Materials Processing Technology, Vol. 71, pp. 195–201.
42. Wiercigroch M., Neilson R.D., Player M.A. (1999), “Material removal rate prediction for
ultrasonic drilling of hard materials using an impact oscillator approach”, Physics Letters,
Vol. 259, pp. 91–96.
43. Nath C.; Lim G. C.; and Zheng H.Y. (2012) “Influence of the material removal mechanisms
on hole integrity in ultrasonic machining of structural ceramics”, Ultrasonics, Vol.52,
pp. 605–613.
44. Ichida, Y.; Sato, R.; Y. Morimoto, Y. and Kobayashi, K. (2005) “Material removal
mechanisms in non-contact ultrasonic abrasive machining”, Wear, Vol. 258, pp. 107–114.
45. Benedict G.F. (1987), Nontraditional Manufacturing Processes, new York, Marcel Decker
Inc. pp. 67–83.
46. Kennedy, D.K. and Grieve, R.J. (1975), “Ultrasonic machining—A review”, The Production
Engineering, Vol. 54, pp. 481.
47. Lee B.J., Kim K. E. (2009), “Characteristics of micro-hole machining of Al2O3 ceramics by
ultrasonic longitudinal vibration”, Journal of ceramics processing research, Vol. 10, No. 4,
pp. 482–490.
48. Yu Z. Y.; Rajurkar K.P.; and Tandon A. (2004), “Study of 3D micro-ultrasonic machining,”
Journal of Manufacturing Science and Engineering, Transactions of the ASME, vol. 126, no.
4, pp. 727–732.
49. Hocheng H.; Kuo K.L. and Lin J.T. (1999), Machineability of zirconia ceramics in ultrasonic
drilling. Mater. Manuf. Process. vol. 14, no. 5, pp. 713–724.
50. Egashira, K.; Taniguchi, T.; Tsuchiya, H. and Miyazaki, M. “Micro ultrasonic machining
using multi tools,” in Proceedings of the 7th International Conference on Progress Machining
Technology (ICPMT ’04), pp. 297–301, December 2004.
Chapter 3
Electrical Discharge Micro-hole
Machining Process of Ti–6Al–4V:
Improvement of Accuracy
and Performance
G. Kibria (&)
Mechanical Engineering Department, Aliah University, Kolkata 700156, India
e-mail: [email protected]
I. Shivakoti B.B. Pradhan
Mechanical Engineering Department, Sikkim Manipal Institute of Technology,
Sikkim 737132, India
e-mail: [email protected]
B.B. Pradhan
e-mail: [email protected]
B. Bhattacharyya
Production Engineering Department, Jadavpur University, Kolkata 700032, India
e-mail: [email protected]
3.1 Introduction
In the last several years, it has been seen that the demand of micromachining
technologies has increased in every shop floor and in wide range of industry seg-
ment from biomedical appliances to aerospace products or parts and automotive
world. Technocrats and manufacturing engineers are always seeking the challenges
to develop new micro manufacturing techniques to manufacture products from
hard-to-machine materials to meet the requirement of product miniaturization
considering numerous technical challenges. Therefore, to support the growth of
product miniaturization and to manufacture micro components effectively and
efficiently, it is the responsibility of manufacturing researchers to develop appro-
priate micro manufacturing processes which have the ability to meet the
above-mentioned challenges [1]. Micro-electrical discharge machining (µ-EDM) is
an cost-effective and widely utilized micromachining process for machining
materials which are difficult-to-machine in conventional methods. The inaccuracies
due to vibration of tool or workpiece can be eliminated in this process because the
machining method is non-contact and thermo-electric type [2]. Material erosion
using controlled spark discharges was first reported by B.R. and N.I. Lazarenko in
1940s in the Union Soviet Socialist Republics (USSR). After that, significant
progress and developments of EDM technologies has been carried out by
researchers worldwide to control the discharge phenomena, develop reliable
machine tools, implementing adaptive control mechanism, employ computer
numerical control (CNC), increase accuracy of geometrical features, high precision
micro-tool fabrication, tool wear compensations, etc.
Fig. 3.2 Representation of typical voltage and current trends with sequential phenomena
occurring due to single discharge
initiate to drift and they align at the strongest point of the field. These contaminants
along with other particles construct the conductive bridge across the IEG, typical
spark gap distance varies from 10 to 100 µm. As voltage between the electrode and
workpiece increases at the beginning of the pulse, the surface temperature of the
workpiece material increases. Some amount of the dielectric fluid and charged
particles of the conductive bridge vaporizes and ionizes thereby forming a plasma
channel. When the potential difference across the spark gap sharply falls, voltage
breakdown occurs. At this time, the plasma channel starts to conduct the applied
current whose magnitude rises instantaneously. The abrupt increase in current
creates instantaneous increase in localized temperature and pressure in the plasma
channel. During discharge between the tool and workpiece, when the local tem-
perature rises beyond the melting point of work material, material melted and
vaporized at the location of discharge and small tiny debri particles are ejected out
from material’s surface creating several number of craters [4]. The gaseous
bubbles in the plasma channel expand outward radially from the point of its origin.
96 G. Kibria et al.
At the end of the discharge, the supply of electrical pulse is terminated. This sudden
termination of the pulsed power results in collapse of plasma channel and conse-
quently the vapour bubble under the influence of pressure imposed by dielectric
fluid from surrounding. The violent in rush of relatively cool dielectric fluid creates
an explosive expulsion of molten materials both from the tool electrode. Due to
discharge, small amount of material from tool electrode is also removed creating
geometrical inaccuracies of shape and size of tool. The debri particles are removed
from the machining zone by fresh dielectric fluid supplied by the flushing jet.
The principle of material removal phenomena from workpiece in micro-EDM is
same as EDM process. However, the differences such as utilizing micro sized tool,
the amount of discharge energy and the X-Y-Z axes resolution make the
micro-EDM process more precise and reliable and capable of micro features gen-
eration [1, 5]. In micro-EDM, very high frequency pulses (>200 Hz), small dis-
charge energies (10−6–10−7 J) and applied potential difference (40–100 V) between
the electrodes are applied to achieve high accuracy features and surface finish
(roughness as much as 0.1 µm) [6]. Utilizing improved pulse generator and precise
servo feed system, the micro-tool electrode can be moved at micron rate to maintain
the required IEG and also to retract the micro tool if the servo feed senses any
short-circuit between the electrodes. In micro-EDM, the type of dielectric flushing
and the value of flushing pressure are important parameters as during machining,
micro-tool may vibrates at high dielectric pressure and deteriorate the accuracy of
micro features to be produced.
Micro-EDM is not only the scaled down version of EDM process, but also there
are significant differences of these two processes in terms of tool electrode type,
shape and dimensions, range of discharge energy, resolution of moving axis, inter
electrode gap control, type of dielectric flushing for debris removal, etc. The radius
of plasma channel in micro-EDM is comparable with tool dimension as
micro-EDM uses micro-tool electrode. However, in EDM, size of plasma channel is
much less compared to tool size [7]. As in micro-EDM, material removal per
discharge (unit removal, UR) should be less; therefore, the applied discharge energy
is limited. On the other hand, in EDM, unit removal is much higher. Further, to
avoid the micro-tool to be rupture or burnt due to excessive discharge energy, the
maximum applied energy in micro-EDM is limited. As in micro-EDM, small sized
(in micron dimensions) tool electrode is used and it has low electrode stiffness, thus,
during micro machining operation in micro-EDM, micro-tool may vibrate due to
flushing pressure and geometrical accuracy of micro features to be produced is
deteriorated. Therefore, the range of dielectric flushing pressure is kept in lower
settings. This problem is absent in EDM process. Further, in micro-EDM, the
amount of thermal load on micro-sized tool electrode is high and thus, the amount
of tool wear also high compared to conventional EDM. Thus, various tool wear
compensation strategies are considered for generating precise and accurate micro
features. Due to very low IEG in micro-EDM, short circuiting occurs frequently,
3 Electrical Discharge Micro-hole Machining Process … 97
which renders machined surface uneven. Moreover, when the debris are ejecting
out from work material, secondary sparking occurs and geometry of micro-tool get
degenerated. These drawbacks are very less in conventional EDM.
The micro EDM system typically consist of several sub-components such as servo
system, control unit, positioning system, dielectric circulating unit and the working
chamber. Figure 3.3 shows the schematic diagram of micro EDM system with
sub-systems. The servo system guides the micro electrode during the machining
and the feed movement of micro-electrode is controlled by the servo control unit.
The workpiece is firmly held in the working table and the positioning system
control the movement of work chamber in the X and Y axis. The constant feed of
the micro-tool is given by servo feed mechanism in Z axis direction. The dielectric
circulating system is another important component in micro-EDM in which con-
tinuous flow of fresh dielectric fluid is supplied to the machining chamber. The
servo control unit is one of the essential components of micro EDM as it controls
the movement of micro-tool and also it maintains the inter-electrode gap between
the micro-tool and the workpiece in micron range. In order to generate dimensional
accurate features, it is very important to keep constant inter electrode gap between
the electrodes [8]. The dielectric system serves an important role in micro-EDM as
the dielectric possesses a crucial role during machining. The dielectric tank contains
a dielectric which is pumped to the machining chamber. The pressure regulator
controls the flushing pressure of the dielectric jet onto the machining chamber. The
dielectric is continuously circulated for efficient machining and the used dielectric is
passed through the micro filters which captured the debris particle generated during
machining. The dielectric jet removes the debris from work material and also it
serves as insulation between the micro tool and the work material. Further, the
Fig. 3.3 Schematic diagram of a typical micro-EDM system showing different sub-systems
98 G. Kibria et al.
dielectric is required for the ionization and act as a medium to cool the micro-tool
and the workpiece.
The series of pulse has been generated for micro EDM with the help of pulse gen-
erator. The various type of pulse generator has been used for producing series of pulse
for micro-EDM process. In RC type capacitor, the charging time is more and due to
this, it cannot produce high frequency pulses and it also produces thermal damage of
the wok material. Sometimes, discharge current flows through the previous plasma
channel without recharging the series of capacitors [9]. Since the capacitor is absent in
the transistor type pulse generator as a result high discharge frequency pulses is
produced which enhances the material removal rate. Moreover, the transistor type
pulse generator is controlled easily as compared to RC type generator. The transistor
type pulse generator cannot be used when nanoseconds pulses are required for
machining as it is not capable of producing nanoseconds pulses. To reduce the delay
time of transistor-type pulse generator, the transistor-type isopulse generator was
developed and successfully employed for micro-EDM operation [10]. For rough and
semi finish machining, a field effect transistor is used to cut off the discharge current.
Instead of observing the gap voltage, the pulse current is observed for detecting the
discharge. As the current sensor provide an output less than 5 V and also it acts as
input to pulse control circuit, it eliminates the voltage attenuation circuit. In this way,
the delay time is shortened to significant amount and ultimately, about 80 ns pulse
duration was achieved. As in RC-type pulse generator, stray capacitance determines
the minimum discharge energy per pulse, therefore, it act as the limitation for gen-
erating micro-features on workpiece [11]. Due to difficulty in eliminating the stray
capacitance, crater diameter less than 2 µm cannot be achieved [12]. To avoid these
problems, a capacity coupling based pulse generator was developed. In this gener-
ator, the effect of the stray capacitance can be eliminated as electric feeding is done
without touching the micro-tool electrode. Thus, discharge crater dimension of
nanometer domain is realized.
The micro EDM process parameters have significant effect on various process
performances. The proper selection of control parameters results in better
machining performance. Figure 3.4 shows the fish-bone diagram showing all pro-
cess parameters related to machining parameters, work material, tool-electrode,
polarity, flushing pressure, etc. The micro EDM control parameters are categorized
as follows: (a) electrical (b) non-electrical and (c) gap and motion control param-
eters. Brief discussions on these process parameters are given hereunder.
3 Electrical Discharge Micro-hole Machining Process … 99
machining efficiency in terms of material removal rate. At the same time, the
surface finish is deteriorated and tool wear ratio increases.
(d) Duty factor: Duty factor is the ratio between the pulse duration to the total
cycle time. Mathematically, it is evaluated by using Eq. (3.1)
Pulse duration
Duty factor ðDF Þ% ¼ 100% ð3:1Þ
Cycle time
If the duty factor is high, the flushing time is very less and this might lead to the
short circuit condition and a small duty factor indicates a high pulse off time
and low machining rate.
(e) Pulse duration: Pulse duration or pulse-on-time is the time interval in which
the applied current is flowing through the IEG of two electrodes. In this time
period, breakdown of dielectric occurred and removal of material from work-
piece surface takes place. Large value of pulse duration means higher material
removal rate. Broader and deeper craters are achieved at longer the pulse
duration setting and consequently, rough machined surface is attained. On the
contrary, smaller craters which are obtained at low value of pulse duration
provides smoother surface finish.
(f) Polarity: Polarity refers to the electrical conditions determining the direction of
the current flow relative to the electrode. The polarity condition of electrodes is
of two type, (i) straight polarity and (ii) reverse polarity. Straight polarity is that
condition when the micro tool is connected to cathode (−), whereas, reverse
polarity is that condition in which tool electrode is connected to anode (+) and
workpiece to cathode (−). For achieving high material removal rate from
workpiece, tool electrode is used as cathode and workpiece as anode.
Depending on the application, some electrode/work material combinations
provide better results when the polarity is changed. Generally for graphite
electrode, a positive polarity gives better wear condition and negative polarity
gives better machining speed.
(g) Pulse frequency: It is the measure of number of cycle per second. Larger value
of pulse frequency decreases the pulse duration which results in minimum
thermal damage in the work piece during machining. However, at high value of
pulse frequency, the surface finish of the machined surface is improved.
process. Materials of higher melting, boiling points and heat conductivity are
used to fabricate the micro-tool for micro-EDM process [13]. There are several
criteria to choose proper tool electrode materials such as (i) machinability,
(ii) electrical and thermal conductivity, (iii) density, (iv) Hardness and tough-
ness, (v) cost and availability, (vi) material removal rate and wear ratio, etc.
(b) Work materials: The micro EDM can only machine electrically conductive
materials. Moreover, for efficient machining, the thermal properties of the
material such as thermal conductivity, specific heat, melting point are the
important aspects need to be considered while selecting the work piece material
[14].
(c) Dielectric fluids: The dielectric fluid has significant role during micro-EDM
possess as without it, it is no longer possible to generate efficient discharge
between the micro-tool tip and workpiece surface. The quality of surface finish
and geometrical accuracy of machined parts depend on several properties of
dielectric such as viscosity, dielectric strength, cooling capability, chemical
compositions, etc. For safe machining operation and stable sparking condition,
the dielectric strength and flash point temperature of the dielectric fluid should
be higher. Furthermore, low value of viscosity and specific gravity are another
two desirable properties of dielectric fluid. These properties significantly affect
the machining efficiency and consequently improves material removal rate,
lowers tool wear rate and enhances the surface finish of machined features.
Electrode rotation: The rotation of micro-tool about its axis during the
micro-EDM enhances the machining performance as the rotation of micro-tool
enhances the flushing action of the debris formed during micro-EDM at inter
electrode gap. Due to rotation of micro-tool, a tangential force is produced at small
IEG and this leads to effective and efficient discharge by smooth removal of debris
through small gap of micro-tool surface and micro-hole wall [15]. Moreover,
electrode wear ratio also reduces due to micro-tool rotation.
Tool geometry and shape: The micro-feature generated in the workpiece during
micro-EDM is the replication of the micro-tool geometry. Moreover, the geometry
of micro-tool has significant effect on tool wear ratio. Depending upon the
requirement, the shape of micro-electrode can be circular, rectangular, cylindrical
etc. Vibration assisted micro-EDM has significant effect on machining rate and
taper during micro-hole drilling [16].
Servo feed: For properly maintaining the discharge gap width and to avoid
arcing and short-circuiting between the micro-tool and the workpiece, the servo
feed control system play vital role during micro-EDM process. As soon as the value
102 G. Kibria et al.
of average gap voltage approach more than preset threshold voltage of pulse
generator, the feed rate of servo increases and compensating the discharge gap
between the electrodes and vice versa [3].
Tool and workpiece vibration: The performance of the micro-EDM has been
improved by incorporating the vibration of micro-tool or workpiece at certain
frequency and amplitude. During vibration of micro-tool or workpiece, the forward
and backward motion of tool or workpiece changes the discharge gap and conse-
quently, dielectric fluid pressure in the IEG also changes constantly. When the
micro-tool is advancing towards the workpiece, the dielectric fluid is forced out
from the machining zone. Then after, when the micro-tool move away from
machine zone, fresh dielectric is taken by discharge gap and thus, overall flushing
efficiency increases.
Flushing techniques: Dielectric flushing has important role for removing the
debris from machining zone and consequently, it enables stable discharge condition
by supplying fresh dielectric fluid in the gap. In general, there are mainly two types
of flushing, pressure flushing and suction flushing. Depending upon the type of
flushing, the amount of flushing pressure is provided. In micro-EDM operation, for
effective generation of high aspect ratio micro-features such as micro-holes, jet
flushing is more effectively used. In other cases, side flushing is commonly used. If
the jet flushing is provided from one direction, there may be chances to accumulate
the debris in the downstream, which creates irregular gap width and as a result,
accuracy of micro-feature is deteriorated [17]. To avoid this, jet flushing from both
side and sweeping type flushing also sometime recommended. In Fig. 3.5, different
types of flushing for micro-EDM are illustrated.
Flushing pressure: For quick removal of the debris from the IEG during
micro-EDM, it is more important to flush out debris particles from very narrow
discharge gap. Higher value of flushing pressure is preferable for effective debris
removal, stable machining and high aspect ratio micro-feature generation. However,
as stiffness of micro-tool is low, high flushing pressure may deteriorate dimensional
accuracy due to micro-tool vibration or deflection.
Fig. 3.5 Schematic of a jet, b flushing through tube electrode and c flushing through workpiece in
micro-EDM process
3 Electrical Discharge Micro-hole Machining Process … 103
Material removal rate: The amount of material removed from the workpiece per
unit time is known as material removal rate (MRR). It is evaluated in terms of
volume of material removed from the workpiece or can be evaluated by differen-
tiating the weight of the workpiece taken before and after machining. It is calculated
using Eq. (3.2)
The higher material removal depicts the increases the productivity and hence, the
material removal is always consider to be the higher the better type. Higher MRR
can be achieved at high discharge voltage, peak current, pulse duration and duty
cycle. However, other desirable process performances such as tool wear ratio,
surface finish and dimensional accuracy is also important aspects and taken into
account in micro-EDM.
Tool wear rate: The amount of material removed from the micro-tool during
machining is known as tool wear rate (TWR). The high electrode wear is not
desirable in micro-EDM as it changes the geometry of the tool which reduces
quality of the machined surface and inaccurate geometric features are achieved onto
the machined surface. The electrode wear is calculated by differentiating the weight
of the micro-tool before and after machining and is calculated by Eq. (3.3).
process in micro-EDM, overcut is calculated using Eq. (3.4). The overcut occurs
mainly due to secondary sparking during material removal from sidewall of the
micro-feature surface while the debris try to ejecting out by flushing pressure from
the machining zone.
Area of microhole
Circularity ¼ 4p ð3:5Þ
½Perimeter of microhole2
Machining time: The time during which the machining is performed in order to
produce micro-features on the workpiece. Due to inefficient discharge and various
unwanted phenomena, machining time increases for producing particular
micro-features on workpiece surface.
Depending upon the tool-work configuration and relative motion between the
micro-tool and workpiece to be machined, there are several varieties of micro-EDM
process. These machining varieties have been developed based upon the require-
ments of product intricacy and features.
The process in which deep micro-sized hole is generated by EDM process is termed
as micro-EDM drilling. In conventional EDM process, both tube and solid elec-
trodes can be used as tool material. However, for micro-EDM, as the geometrical
3 Electrical Discharge Micro-hole Machining Process … 105
dimensions of tool electrode is in micron range, therefore, only solid micro-rods can
be used. For efficient removal of eroded particles from the machining zone, it is
recommended to employ jet flushing in micro-EDM with low value of flushing
pressure to avoid vibration of micro-tool electrode. In Fig. 3.6, the schematic of
micro-EDM drilling process is depicted. When the debris particles try to eject out
from the IEG, due to secondary sparking between micro-tool and micro-hole walls,
material removal is more at entry side of hole and this result in taper in micro-hole
geometry. For high precision micro-hole drilling in EDM, sometimes, micro-tool
electrode is fabricated in the machine itself by wire-electrical discharge grinding
(wire-EDG) process to avoid tool deflection or breakage [19]. Different types of
micro-features (irregular, curved, inclined, tapered, etc) can be produced using
different alignment of micro-tool as well as tool feed mechanisms. Cooling holes in
turbine blades, nozzles for fuel injection system, parts for manufacturing of
micro-turbines and surgical instruments are the typical examples of micro-EDM
drilling.
Fig. 3.10 Schematic representation of planetary micro-EDM for generation of a circular hole and
b non-circular hole
The schematic view of block micro-EDG process is shown in Fig. 3.12. During
block micro-EDG process, cylindrical material is considered as workpiece and the
rectangular block is considered as electrode. During sparking between block surface
and rotating workpiece, it is very important factor to apply dielectric jet properly to
avoid deflection of material as well as uniformity of micro-tool geometry.
110 G. Kibria et al.
Fig. 3.13 Schematic illustration of moving block micro-EDG, a showing the movement of block
and macro-tool, b fabricated high aspect ratio micro-tool
Titanium alloy was developed in the early 1950s for defence and aeronautic
applications due to its very high strength-to-weight ratio. The unique combination
of high strength, low weight, and excellent corrosion resistant property of titanium
alloy has made it suitable for a wide variety of industrial applications. Its corrosion
resistant results from a very thin (−10 nm), stable, continuous oxide layer that
regenerates instantaneously if any oxygen or moisture is present. Commercially
Pure (CP) Titanium is used primarily for its corrosion resistance. Further titanium
alloy can withstand pitting, crevice and cavitations, corrosion, erosion, and stress
corrosion cracking in salt water, marine atmospheres, and a broad range of acids,
alkalis, and industrial chemicals. This alpha-beta alloy is the workhorse alloy of the
titanium industry. The alloy is fully heat-treatable in section sizes up to one inch
and is used up to approximately 400 °C. Since it is the most commonly used alloy,
over 70% of all alloy grades melted are sub- grade of Ti–6Al–4V. Its uses arc not
only confined and concentrated in aerospace engine and airframe components but it
is widely uses in major non-aerospace applications in the marine offshore, power
generation industries and biomedical applications also. Ti–6Al–4V is the most
widely used titanium alloy, accounting for more than half of all titanium tonnage
worldwide.
Various excellent properties possessed by titanium super alloys have led to a
wide and diversified range of successful applications in medical science as well as
in automotive, aerospace, chemical plants, and other precision engineering fields.
The wide variety of applications of this exotic material in almost all the precision
engineering fields demand the huge need of micro-machining of Ti–6Al–4V. Thus,
in order to meet up the huge market demand of micro-products manufactured from
Commercially Pure (CP) Titanium and its alloy necessitated the need of
micro-machining using micro-EDM technology utilizing different novel machining
strategies.
In last 15 years, a number of research and development activities have been carried
out around the globe for improving the machining performance as well as
dimensional accuracy of machined components in micro-EDM process. Moreover,
many researchers have utilized various statistical tools for finding out influencing
process parameters and optimization of the process for obtaining parametric con-
dition to achieve high performance machining and accurate geometrical features.
Micro-hole electro discharge machining has been carried out by Pradhan et al. on
Ti–6Al–4V alloy using 500 µm diameter brass micro-electrodes [24]. Four process
parameters such as peak current, pulse-on time, flushing pressure and duty ratio
112 G. Kibria et al.
of the helical micro-tool on process performances have also been studied. Blind and
through micro-holes and micro-slots were machined on brass and Ti–6Al–4V
materials by Moses and Jahan [32]. Dimensional accuracy, surface finish, and
profile accuracy of holes and slots were measured for analysis. Single through
micro-hole, single blind hole, letter H blind, three blind slots and three through slots
were machined also. The influence of various process parameters such as
pulse-on-time, peak current, gap voltage and flushing pressure on MRR, TWR,
overcut and taper of micro-hole during machining of Ti–6Al–4V were studied by
Tiwary et al. and empirical models were developed for to correlate the process
parameters and machining performances [33]. Multi performance optimization was
achieved as MRR of 0.0777 mg/min, TWR of 0.0088 mg/min, OC of 0.0765 mm
and taper of 0.0013 at parametric setting of pulse-on-time of 1 ls, peak current of
2.5 A, gap voltage of 50 V, and flushing pressure of 0.20 kgf/cm2.
Kuriachen and Mathew carried out investigation to machine Ti–6Al–4V with
tungsten carbide electrode employing SiC micro particle suspended dielectric
during micro-EDM milling operation [34]. The effects of various process param-
eters such as voltage, capacitance and powder concentration on MRR and TWR
was studied. The recommended process parametric setting was powder concen-
tration of 5 g/L, capacitance of 0.1 lF and voltage of 115 V for achieving high
material removal and low tool wear rate. Predictive thermal model was developed
by B. Kuriachen et al. for simulation of single-spark micro electric discharge
machining [35]. The crater geometry and temperature distribution in the workpiece
at various process parametric setting were predicted using Gaussian distribution of
heat flux, percentage distribution of energy among the workpiece, tool electrode
and dielectric. Mathematical model which predicts the radius of the single-spark
during micro-EDM process of Ti–6Al–4V was developed by Kuriachen and
Mathew [36]. The authors concluded that the spark radius increases proportionally
with in capacitance except in the higher energy levels where double sparking
phenomenon was observed.
It is observed from the literature review that most of the research investigation
and analysis is on investigating the effects of process parameters on machining
performances such as MRR, TWR, overcut, surface roughness, etc. Furthermore,
optimal parametric combination was also found utilizing several statistical tech-
niques as well as combined approach of different predictive tools for achieving high
machining rate, less tool wear rate and good geometrical micro-structures.
However, there are many issues which remained unsolved in micro-EDM. Such
issues are improving material removal rate, methodology for compensating the
micro-tool wear, improving the stability of discharge, improving the accuracy of
micro-feature implementing innovative ideas, etc. To solve these important issues
and to improve overall micro-EDM efficiency, several new micro-EDM machining
strategies have been developed and researchers already started to utilize these
innovative strategies during micro-EDM of Ti–6Al–4V material. In the following
sections, experimental investigation and analysis of micro-EDM process of Ti–
6Al–4V have been carried out extensively utilizing some innovative machining
strategies such as ultrasonic vibration assisted micro-ED machining, utilization of
114 G. Kibria et al.
Fig. 3.15 Schematic of ultrasonic vibration assisted micro-EDM process with amplitude of
vibration
micro-EDM, the adhesion of powder or abrasives in the narrow gap between the
micro tool and the work material occurs. Therefore, implementing ultrasonic
vibration during powder mixed micro-EDM, MRR increases significantly as it
enhances the dielectric circulation in the machining zone [42]. The drawbacks due
to arcing and short circuits in micro-EDM can be reduced substantially when
assisted with ultrasonic vibration as the number of normal pulses and the average
pulse energy increases [43, 44]. The machining time of micro-EDM can be reduced
significantly with increase in vibration frequency at constant amplitude which
significantly reduces the start-up process. The vibration between the micro-tool and
the work material obstructs the arc which ends the arcing state [45]. Thus, the total
duration of arcing event reduces and decreases with increase in vibration frequency.
Figure 3.16 shows the comparison of quality of blind micro holes produced with
and without ultrasonic vibration (frequency of 6 kHz and amplitude of 3 µm) [46].
The comparison shows the improvement in the dimensional accuracy by 10.5 µm.
Furthermore, the micro-hole produced without vibration is larger (diameter is
201.5 µm) than micro-hole generated with ultrasonic vibration (diameter is
191 µm) and this result indicates that the electrode wear is less in ultrasonic assisted
micro-EDM process. The recast layer formation has been always a drawback during
micro-EDM process. Due to better dielectric circulation in the machining zone, the
debris removal from narrow gap due to ultrasonic vibration is improved and results
in less re-solidification or recast layer [37]. Moreover, this leads to thinner
heat-affected zone produced around the machined cavities. The ultrasonic vibration
assisted micro-EDM machining not only shows the improvement in the process
performance when used with conventional and powder mixed dielectric, but it also
shows the tremendous contribution during dry EDM/micro-EDM. The improve-
ment in MRR has been reported when compared to gas based EDM and liquid
116 G. Kibria et al.
Fig. 3.16 SEM images of blind holes generated a without ultrasonic vibration and b with
vibration [46]
Fig. 3.17 SEM images of micro-hole of a entrance and b exit side machined with ultrasonic
vibration micro-EDM [48]
based EDM without vibration [47]. The reduction in taperness has been achieved
when micro-hole is machined with the aid of ultrasonic vibration. Figure 3.17
shows SEM images of micro-hole of entrance (diameter of 122 µm) and exit (di-
ameter of 106 µm) side when machined with ultrasonic assisted micro-EDM [48].
The difference in the diameter (16 µm) is due to secondary discharge and wear of
micro-tool.
Fig. 3.18 Photographic views of a and b EMS-5535-R50, ZNC EDM machine c external
dielectric supply system for circulating de-ionized water
in entry and exit (DVEE) were considered as the machining characteristics. Material
removal rate was calculated using Eq. (3.2). Similarly, tool wear rate is calculated
using Eq. (3.3). A high precision weighing machine (Manufacturer: Mettler Toledo,
Switzerland, Least measurable weight = 0.01 mg) is used to measure various
weights of workpiece and micro-tools. The overcut of micro-hole machined is
measured using Eq. (3.4). A high precision measuring microscope (Manufacturer:
OLYMPUS, Japan, Model: STM6, minimum measurable dimension = 0.5 lm) is
used to measure all the dimensions of micro-hole diameters as well as of micro-tool.
Experimentation were conducted at various micro-EDM parametric combinations,
measured and calculated the performance criteria. The discussion and analysis of
various test results are described in the following sections.
(b) Results and discussion
In this section, a detailed comparison of various machining performance charac-
teristics has been performed for the investigation of influence of dielectric liquid
with kerosene and de-ionized water in micro-EDM for micro machining of titanium
alloy (Ti–6Al–4V). Figure 3.19 depict the comparison of the material removal rate
(MRR) using two different dielectrics such as kerosene and de-ionized water
varying peak current (Ip) and pulse-on-time (Ton). The material removal rate
(MRR) is much more using de-ionized water than the kerosene throughout the
considered range of pulse duration and increase of peak current. When machining is
done with kerosene, as the dielectric fluid is kerosene which is a chemical com-
pound of carbon and hydrogen, decomposes and produces a layer of titanium
120 G. Kibria et al.
Table 3.3 Experimental condition for through micro-hole machining on Ti–6Al–4V alloy
Condition Description
Workpiece material (anode) Ti–6Al–4V plate of size 13 mm 15 mm and
thickness of 1 mm
Tool electrode (cathode) Solid tungsten micro-tool, diameter of 300 µm
Dielectric fluids Kerosene, de-ionized water
Peak current (A) 0.5, 1, 1.5, 2
Pulse-on-time (µs) 1, 2, 5, 10, 20
Duty factor (%) 95
Flushing pressure (kgf/cm2) 0.5
Resistivity of pure de-ionized water 4.2
(megohm-cm)
Fig. 3.19 Influence of different dielectrics on the material removal rate (MRR) with varying
pulse-on-time (Ton)
carbide (TiC) on the workpiece surface. But, when using de-ionized water, the
water decomposes and a layer of titanium oxide (TiO2) is produced on the
machined surface. Since, TiC has a higher melting temperature (3150 °C) than that
of TiO2 (1750 °C), a large discharge energy is required for improving the material
removal rate using kerosene. Also, the size of debris formed during machining with
kerosene is less compared to machining with de-ionized water, thus improving the
material removal rate.
3 Electrical Discharge Micro-hole Machining Process … 121
Fig. 3.20 Influence of different dielectrics on the tool wear rate (TWR) with varying
pulse-on-time (Ton)
Figure 3.20 shows the comparison of the tool wear rate (TWR) using two dif-
ferent dielectrics such as kerosene and de-ionized water varying peak current
(Ip) and pulse-on-time (Ton). It is seen from the figure that the tool wear rate
(TWR) is high using de-ionized water compared to machining with kerosene. When
using kerosene as the dielectric, it decomposes in the high discharge energy and
produces carbon particles that stuck or adhere to the surface of the electrode. These
carbon particles restrict the rapid wear of the tool. So, the tool wear rate (TWR) is
less while using kerosene as dielectric. On the other hand, when using deionized
water, no carbon adhere to the tool electrode surface, thus TWR is higher enough
with de-ionized water.
Figure 3.21 shows the comparative study of the overcut (OC) using two different
dielectrics i.e. kerosene and de-ionized water with varying peak current (Ip) and
pulse-on-time (Ton). From the figures, it is clear that the overcut of the machined
micro-holes is larger when using de-ionized water for the pulse duration of 1 and
2 µs when machining is done by varying peak current. But at higher pulse duration
the overcut of the micro-holes is larger when using kerosene as the dielectric. When
deionized water is used, it releases oxygen decomposed from water. This oxygen
influences the machining stability and helps to form more debris. These debris
particles ejected through the short gap of tool surface and micro-hole walls. Thus
increasing secondary sparking, resulting in higher overcut compared to kerosene.
But at higher pulse duration, the machining stability and efficiency increases due to
more pulses per cycle, resulting higher overcut with kerosene compared to
122 G. Kibria et al.
Fig. 3.21 Influence of different dielectrics on the overcut (OC) with varying pulse-on-time (Ton)
de-ionized water. When the overcut is analyzed with the increase of peak current it
is found that a high peak current results higher overcut with de-ionized water
compared to kerosene.
Figure 3.22 shows the comparison of the diameteral variance in entry and exit
(DVEE) using two different dielectrics i.e. kerosene and de-ionized water with
varying peak current (Ip) and pulse-on-time (Ton), respectively. It can be observed
from the figures that DVEE of the micro-holes increases at low discharge duration
when varying peak current was employed using de-ionized water as dielectric fluid.
But further increase of pulse duration results the decrease of DVEE of the holes
with de-ionized water. A straight through micro-hole can be generated at pulse
duration of 5 µs and peak current of 1.5 A. On the other hand, DVEE is lower at
peak current 0.5 and 1 A employing deionized water compared to kerosene. But, as
the peak current increases, the diameter variance increases with de-ionized water.
Thus, a straight through micro-hole is not achieved.
After machining of micro-holes utilizing various type of dielectric fluids, the
workpiece were carefully polished, cleaned, and etched with a solution of 2.5 ml of
HF acid (40%), 5 ml concentration of HNO3 and 42.5 ml of de-ionized water for
examining the surface topography of micro-holes as well as the recast layer formed
on the machined micro-hole surfaces with the aid of optical and SEM micrographs.
Figure 3.23 shows some optical micrographs of machined micro-holes that were
taken using a 10X zoom lens in a precision optical microscope for both pure
dielectrics i.e. kerosene and de-ionized water at the machining condition of 1 A
3 Electrical Discharge Micro-hole Machining Process … 123
Fig. 3.22 Influence of different dielectrics on the diameter variance between entry and exit
(DVEE) with varying pulse-on-time (Ton)
Fig. 3.23 Optical photographs of machined micro-holes with different dielectrics at 1 A/2 ls [51]
124 G. Kibria et al.
Fig. 3.24 SEM micrographs of white layer formed on micro-hole edge a and b machined at 0.5
A/1 ls and c, d machined at 1.5 A/10 ls [51]
peak current and 2 ls pulse duration. It is clear from these figures that kerosene
dielectric result in improved quality micro-hole than de-ionized water. In Fig. 3.24,
SEM micrographs of the micro-hole’s edges are shown to examine the white/recast
layer formation using kerosene and de-ionized water. The thickness of the white
layer is much lower using de-ionized water compared to kerosene. Moreover, with
increase of the pulse-on-time, the thickness of the white layer increases. As pulse
duration increases, the effective machining time also increases. Therefore, more
debris is generated and this debris adheres to the micro-hole surface and resolidified
as deionized water has high cooling rate than kerosene.
In micro-EDM, debris in the inter electrode gap facilitates the ignition process and
further increases the gap size and overall flushing conditions [52]. Absence of
debris particles in the gap can results arcing between the electrodes and it further
results in lack of precise feeding mechanism. However, excess debris leads to
uneven discharge and short-circuiting. Some debris particles in the machining gap
3 Electrical Discharge Micro-hole Machining Process … 125
provide better discharge transitivity, gap size, breakdown strength, and deionization
[53]. From the past research, it is revealed that most of the research has been
performed on EDM employing powder mixed dielectrics. However, no research
was reported to use powder mixed dielectric during micro-EDM of Ti–6Al–4V.
Thus, in the present experimental study, detailed analysis has been carried out to
investigate comparatively the influence of mixing boron carbide powder in kero-
sene and de-ionized water during micro-hole machining in micro-EDM on Ti–6Al–
4V material. This B4C powder has some excellent physical and chemical properties
such as high chemical resistance and hardness, excellent wear and abrasion resistant
etc. These exceptional characteristics of boron carbide may provide effective and
efficient discharge conditions at the machining zone and also enhancement in
above-mentioned machining performances. Electrical resistivity of boron carbide is
in the range of 0.1–10 X cm. As B4C abrasive lie in a transition zone between good
conductors and isolators, the potential difference as well as the plasma channel
produced in the micron sized inter electrode gap can make the abrasive to conduct
thermoelectric power in the machining zone [54, 55]. Boron carbide is characterized
by a relatively wide gap in its forbidden band, a low thermal conductivity, and a
high thermoelectric power. These properties make it a potentially useful material for
high-temperature thermoelectric energy conversion compared to silicon carbide as
well as tungsten carbide abrasives.
(a) Experimental details and machining conditions
As micro-EDM process uses discharge energy in the range of 5–150 µJ, so there is
a little chance to melt and evaporate the B4C particles due to discharge in the inter
electrode gap. It was observed in the optical measuring microscope that the powder
particles comprise of mixture of different shapes and sizes ranging from 8 to 20 µm.
When, Boron carbide (B4C) powder-mixed de-ionized water was applied in the
machining zone, most of the particles, which are more than 10 µm in size, get
accumulated at the base of machining zone because of self-weight of particles even
though a motor driven stirrer was applied to provide turbulence in powder mixed
dielectrics in the machining tank. Hence, the effective average particle size that may
involve in the machining phenomena at the micro-machining zone ranges from 8 to
10 µm during micro-EDM. Therefore, the average size of B4C particles which
actively take part in machining is in the range of 8–10 µm. The thermo-physical
properties of boron carbide powder are enlisted in Table 3.4. B4C powder additive
of size 8–10 lm and of concentration 4 g/l was added to pure kerosene and
deionized water when experimentations were performed with powder-mixed
dielectrics. This particular concentration of additive in dielectrics has been selected
based on past research studies on powder mixed dielectrics in EDM [56, 57]. The
same micro-EDM machine was utilized for this experimental investigation. When
experiments are done with powder mixed kerosene and powder mixed de-ionized
water, a separate dielectric chamber with separate pump, and pressure-regulating
valve and filter were used to circulate the dielectrics without affecting dielectric
supply system of the main machine. When machining was done with powder-mixed
dielectric, the external filter unit was removed, and a magnetic field was employed
to remove the machining debris from the dielectrics. In this research study,
micro-EDM characteristics such as material removal rate (MRR), tool wear rate
(TWR), overcut (OC), diameteral variance in entry and exit (DVEE) were con-
sidered as the machining characteristics. The discussion and analysis of various test
results are described in the following sections.
(b) Results and discussion
Figure 3.25 shows the comparative plots of the material removal rate (MRR) using
different dielectrics such as pure kerosene, pure de-ionized water and Boron
Carbide (B4C) mixed dielectrics powder for varying pulse-on-time (Ton) at dif-
ferent peak currents (Ip). This figure reveals that MRR is high with de-ionized water
Fig. 3.25 Variation of material removal rate (MRR) with pulse duration (Ton) at various fixed
peak current (Ip) for different dielectrics [51]
3 Electrical Discharge Micro-hole Machining Process … 127
than kerosene for all considered settings of pulse duration and peak current during
experimentation. Additionally, when machining is done by mixing B4C powder
additives in kerosene dielectric it is clearly seen that MRR increases with the
increase of pulse duration at constant peak current of 1.5 and 2 A. Also the MRR
with powder mixed dielectrics is larger compared to machining with pure kerosene
and de-ionized water at higher pulse duration discharge settings. The increase of
MRR with the increase of pulse duration using B4C mixed kerosene is due to
increase of spark discharge time i.e. longer effective machining time per pulse. The
presence of boron carbide additive in kerosene further helps in uniform distribution
of discharge energy and better conduction of discharge current thereby enabling
better machining condition. When B4C powder was applied to de-ionized water, it
is seen that MRR is more using additive compared to pure deionized water at peak
current 1.5 and 2 A. The same reason is applicable here also for the increase of
MRR as of additive mixed kerosene. So, it is concluded that the addition of carbide
powder particles in dielectrics prevails better machining efficiency than the pure
dielectrics due to uniform distribution of discharge energy in the machining zone.
In Fig. 3.26 comparative results of tool wear rate (TWR) with pulse duration at
different pulse discharge with various constant peak current are shown employing
kerosene, de-ionized water and B4C powder mixed dielectrics. This figure reveals
that TWR is high using de-ionized water compared to machining with kerosene
dielectric. Furthermore, it is revealed from the same figure that tool wear rate
Fig. 3.26 Variation of tool wear rate (TWR) with pulse duration (Ton) at various fixed peak
current (Ip) for different dielectrics [51]
128 G. Kibria et al.
associated with B4C mixed kerosene is less compared to machining with pure
kerosene at peak current of 0.5 and 1 A. When machining is done with boron
carbide abrasive mixed kerosene dielectric, the tool wear is less due to the presence
of more number of carbon particles evolving from the decomposition of kerosene
dielectric as well as boron carbide abrasive in the machining zone. From the same
figure it is observed that at fixed 1 A peak current tool wear rate is lesser than at
fixed 0.5 A current setting using additive mixed kerosene. This is due to the fact
that the higher discharge energy results in more decomposition of kerosene and it
further generates more carbon which in turn adheres onto the tool surface pre-
venting secondary sparking. Although higher peak current i.e. 2 A produces more
discharge energy, but that results in more current density and subjects the tool
electrode under large thermal stresses. The powder mixed de-ionized water results
in less tool wear rate at 2 A compared to 1.5 A due to more deposition of carbon
particles from B4C additives. It is also found that machining combined with boron
carbide powder mixed deionized water results in less tool wear compared to pure
de-ionized water due to adhesion of carbon particles from boron carbide powder on
the tool surface, which restrict tool wear to certain extent.
The comparative plots of overcut (OC) of micro-holes on Ti–6Al–4V employing
kerosene, deionized water and B4C abrasive mixed with these dielectrics are shown
in Fig. 3.27 when pulse duration was varied for fixed different peak current. It is
observed from these figures that the overcut of the machined micro-holes is less
Fig. 3.27 Variation of overcut (OC) with pulse duration (Ton) at various fixed peak current
(Ip) for different dielectrics [51]
3 Electrical Discharge Micro-hole Machining Process … 129
when dielectric was de-ionized water for peak current setting of 0.5 and 1 A.
However, at higher peak current i.e. 1.5 and 2 A, overcut is more in case of
de-ionized water compared to pure kerosene dielectric. In addition, when B4C
additive was used in dielectrics, it is found that OC is larger with both powder
mixed dielectrics compared to pure dielectrics. It is so because the suspended
additive particles remove the molten layer from the machining zone and further
reduce the formation of thick white layer, resulting larger OC. It is also revealed
that OC decreases with increase in pulse duration while using B4C suspended
kerosene as dielectric. It is due to decrease of overall machining time i.e. faster
machining. However, larger OC is found in case of B4C mixed deionized water as
dielectric because of secondary sparking.
Figure 3.28 shows the comparative outcomes of diameteral variance at entry and
exit (DVEE) using kerosene, de-ionized water and boron carbide powder mixed
with these dielectrics. It is found from this figure that DVEE of the micro-holes is
lower employing de-ionized water compared to kerosene as dielectric fluid at lower
peak current i.e. 0.5 and 1 A. However, at higher peak current i.e. 1.5 and 2 A,
DVEE is larger using de-ionized water. It is also found that boron carbide powder
mixed kerosene results in large DVEE compared to pure kerosene at low peak
current of 0.5 and 1 A. As the machining progresses, the additive boron carbide
particles creates more carbon adhesion on the work surface, that further results in
Fig. 3.28 Variation of diameteral variance at entry and exit (DVEE) with pulse duration (Ton) at
various fixed peak current (Ip) for different dielectrics [51]
130 G. Kibria et al.
Fig. 3.29 SEM micrographs of machined micro-holes using powder mixed dielectrics [51]
Fig. 3.30 SEM micrographs of white layer of machined micro-hole’s edges using powder mixed
dielectrics [51]
lower material removal at exit side of micro-hole and greater variance in entry and
exit diameters. But, when B4C additive mixed de-ionized water is used at higher
peak current of 1.5 and 2 A, the powder particles help in uniform distribution of
discharge energy which in turn leads to better dimensional accuracy micro-holes
compared to pure de-ionized water.
Figure 3.29 shows SEM micrographs of the inner surface of machined
micro-hole using powder mixed kerosene and de-ionized water at parametric
combinations of 1 A/5 ls and 2 A/10 ls of peak current and pulse-on-time. It is
revealed from these micrographs that with more discharge energy, inaccurate
micro-hole is generated using powder mixed de-ionized water due to more sec-
ondary sparking phenomena. However, smooth inner surface is produced using
powder mixed de-ionized water than powder mixed kerosene. In Fig. 3.30, SEM
micrographs of micro-hole’s edge are viewed for examining the recast/white layer
formation during micro-hole machining. It is revealed from these figures that the
3 Electrical Discharge Micro-hole Machining Process … 131
recast layer formed on the edges is very less than using pure dielectrics. It is due to
the fact that the additive particles help to remove the molten debris and restrict to
form thick white layer on machined micro-hole edges.
Fig. 3.31 Variation of MRR with a peak current and b pulse-on-time [58]
Fig. 3.32 Variation of TWR with a peak current and b pulse-on-time [58]
(Ton) with stationary and rotating electrode are shown in Fig. 3.31a, b, respec-
tively. It is observed from the graph that MRR increases with increase in peak
current as was expected for both stationary and rotating electrodes. Since higher
peak current leads to higher discharge energy, so it results in increase of MRR. It is
also observed from the same figure that with rotating electrode higher MRR is
achieved. The higher MRR with rotating electrode may be attributed to better
removal of sludge and carbonized particles from the machining zone due to cen-
trifugal force of rotation. This improved sludge removal due to rotating effect of
electrode helps in exposing the actual machining surface, which in turn improves
the overall machining condition leading to higher MRR. Thus, for maximum MRR
from within the considered range of parametric setting, the best parametric com-
bination in the present case study is 2 A/10 ls/0.5 kgf cm−2/95%/150 rpm.
Figure 3.32a, b respectively show the variations of TWR with peak current
(Ip) and pulse-on-time (Ton) with stationary and rotating electrode. It can be
observed from the graph that TWR increases as the peak current increases from 0.5
to 1.5 A. However, TWR is observed to decrease from 1.5 to 2 A. The increase in
TWR with the increase in peak current can be attributed to the increase in discharge
3 Electrical Discharge Micro-hole Machining Process … 133
energy and the rotational effect of the electrode. Further increase in peak current,
increases machining efficiency and decreases the tool wear because the tool elec-
trode is subjected to high-energy electric field for shorter duration. Thus, this figure
clearly indicates that for micro-hole machining with low TWR, smaller peak current
is suitable. Owing to rotational effect, the magnitude of TWR further decreases
which is evident from the figure under consideration. This may be attributed to
better removal of debris due to the tangential force of rotation. Thus, for least TWR,
the best parametric combination within the considered range of parametric settings
is 1 A/10 ls/0.5 kgf cm−2/95%/150 rpm.
Figure 3.33a, b respectively show the variations of OC with peak current
(Ip) and pulse-on-time (Ton) with stationary and rotating electrode. It is observed
from the figure that overcut decreases with the increase in peak current in the range
0.5–1 A which may be attributed to increase in discharge energy with the increase
in peak current and enabling faster machining and thereby reducing effective
machining time. The reduction in machining time means less exposure of tool
electrode to discharge energy which is responsible for tool wear. However, peak
current beyond 1 A, overcut has found to increase monotonically. Increase in peak
current above 1 A results in larger discharge energy which causes larger MRR
resulting in larger overcut. Thus the most suitable parametric combination for least
overcut from within the considered range of parametric settings is 1 A/10 ls/95%
duty factor/0.5 kgf cm−2/150 rpm.
The variations of DVEE with peak current (Ip) and pulse-on-time (Ton) with
stationary and rotating electrode are shown in Fig. 3.34a, b, respectively. It is
observed from the same graph that with the increase in peak current, the DVEE
decreases. Furthermore, the magnitude of DVEE with rotating electrode is less than
that of stationary electrode throughout the considered range of peak current. As the
depth of the micro-hole increases, the sparking point shifts radially inward. When
the peak current is increased, the thermal energy density increases at the pointed tip
of the micro-tools. This high density discharge energy rapidly melts and vapourizes
the sharp micro-tool tips and subsequently making the micro-tool end broader
134 G. Kibria et al.
Fig. 3.35 Optical micrographs of micro-holes with a stationary and b rotating tool electrode
machined at 1 A/5 ls/95% duty factor/0.5 kgf/cm2
micro-hole. In constant polarity machining condition, the job was positive and tool
electrode was negative i.e. normal polarity. But, in changing polarity machining
condition, the polarity of the job and the tool electrode has been changed in
exponential time domain.
(a) Experimental method and machining conditions
The machining begins with normal polarity for the first 10 min, then the polarity is
changed for next 3 s and again the polarity is switched over to normal polarity and
the machining continues for another 9 min before the second change. The time
duration of machining with normal polarity reduces after every change and this
continues till the through micro-hole is produced on the workpiece. However, the
machining with reverse polarity is kept constant at 3 s in each change. The time
chart has been prepared after conducting several trail experiments to find out the
time required to machine the through micro-hole in 1 mm thick Ti–6Al–4V alloy
sheet with 300 µm diameter brass tube electrode. The dielectric fluid used is ker-
osene. It is learnt from past literatures and experimental investigations in
micro-EDM that peak current and pulse-on-time are the most influential parameters.
Therefore, these dominating parameters have been selected as process parameters in
the present micro-EDM experimentation. To study the effects of pulse-on-time
136 G. Kibria et al.
(Ton) and peak current (Ip), the experimental planning has been carried out firstly
by only varying the peak current from 0.5 to 2 A keeping pulse-on-time (Ton), duty
factor (t) and flushing pressure (Pr) constant at 10 ls, 95% and 0.5 kgf/cm2
respectively and secondly by only varying the pulse-on-time (Ton) from 1 to 20 ls
keeping peak current (Ip), duty factor (t) and flushing pressure (Pr) constant at 1 A,
95% and 0.5 kgf/cm2 respectively. The experiments were conducted on the same
ZNC R50 EDM machine. Experiment at each parametric setting was conducted
three times and the average of the three were considered for calculating material
removal rate (MRR), tool wear rate (TWR), overcut (OC) and diameteral variation
at entry and exit (DVEE) of the micro-hole.
(b) Results and discussion
The variations of MRR with peak current and pulse-on-time with constant and
changing polarity, keeping all other process parameters constant i.e. pulse-on-time
at 10 ls in case of varying peak current and peak current at 1 A in case of varying
pulse-on-time, duty factor at 95%, and flushing pressure at 0.5 kgf/cm2, shown in
Fig. 3.36a, b, respectively. It is noticed from Fig. 3.36a that MRR increases
monotonically in both cases with the increase in peak current from 0.5 to 1.5 A but
for changing polarity it decreases as peak current increases from 1.5 to 2 A. The
magnitude of MRR in both cases is almost equal in the considered peak current
range. The low MRR at smaller peak current could be due to lower discharge
energy when machining in both constant and changing polarity. However, MRR at
changing polarity is low compared with constant polarity as shown Fig. 3.36a due
to the change in the position of maximum liberation of heat energy due to sparking.
The increase in MRR with increasing peak current is attributed to larger discharge
energy. Figure 3.36b shows the variation of MRR with pulse-on-time. It is
observed from this figure that the MRR variation is almost opposite in nature for
changing and constant polarity at lower pulse-on-time values between 1 and 5 ls.
MRR decreases from 1 to 2 ls for constant polarity but in the same pulse-on-time
range it increases for changing polarity. In the range from 2 to 5 ls, MRR increases
and decreases sharply for constant and changing polarity respectively. However,
Fig. 3.36 Variation of MRR with a peak current and b pulse-on-time [59]
3 Electrical Discharge Micro-hole Machining Process … 137
Fig. 3.37 Variation of TWR with a peak current and b pulse-on-time [59]
with increasing peak current in both machining conditions. This clearly indicates
that the optimum peak current setting is 1 A at the present level of process
parameters range. If peak current is low, the discharge energy is also low, which
means a longer machining time exposing the sidewall of the hole to secondary
sparking resulting in larger OC. However, the increase in OC at higher peak current
is due to higher discharge energy and larger debris concentration in the gap because
of higher MRR. Also, it can be observed from Fig. 3.38b that OC increases steeply
from 1 to 5 ls, decreases sharply from 5 to 10 ls, and again increases at 10–20 ls
for constant polarity. Thus the OC fluctuates with the change in pulse-on-time for
constant polarity. However, for changing polarity, OC is found to decrease grad-
ually for pulse-on-time from 1 to 20 ls, thereby suggesting the benefit of using the
changing polarity technique for achieving lower overcut in the machining of
micro-holes, hence increasing the geometrical accuracy of the machined micro-hole
in Ti–6Al–4V material. Further, it is observed throughout the range of
pulse-on-time from 1 to 20 ls that the magnitude of OC is far lower with changing
polarity than with constant polarity, which is an indicator in itself that changing
polarity yields low OC and results in improvement of micro-hole geometry. This is
due to the fact that the carbon particles, which are the by-product of the micro-EDM
process, are deposited on the surface of the tool electrode and this helps in pre-
venting secondary sparking. Thus only the end face or bottom face is exposed for
sparking, thereby reducing OC and resulting in straight-through micro-hole gen-
eration, thus improving the accuracy of micro-hole machining.
It is observed from Fig. 3.39a, b that DVEE decreases sharply with the increase
in peak current and pulse-on-time. The lowest DVEE is found at 1 A and 10 ls,
which can be seen in the figures for both constant and changing polarity machining
conditions. Also it is observed that DVEE is less with changing polarity than with
constant polarity throughout the peak current and pulse-on-time ranges considered
in the experiments. It can be concluded that with the novel polarity changing
technique, a straight micro-hole is possible. As the depth of the micro-hole
increases, the sparking points shift radially inward. When the polarity is changed
the pointed tip of the micro-tool wears off uniformly, making the tool end broader
and helping in machining a straight micro-hole, resulting in the decrease in DVEE.
3 Electrical Discharge Micro-hole Machining Process … 139
Optical micrographs of the micro-holes (entry and exit diameter) machined with
constant and changing polarity at 1 A/20 ls/95% duty factor/0.5 kgf/cm2 are
shown in Fig. 3.40a, b, respectively. The DVEE at parametric combination of
1 A/10 ls/95% duty factor/0.5 kg cm−2 for the constant polarity machining
condition is 0.0270 mm, and for changing polarity the value is 0.0173 mm.
Fig. 3.39 Variation of DVEE with a peak current and b pulse-on-time [59]
Fig. 3.40 Optical micrographs of micro-holes with a constant and b changing polarity machined
at 1 A/20 ls/95% duty factor/0.5 kgf/cm2
140 G. Kibria et al.
Fig. 3.41 SEM micrographs of micro-holes with a constant and b changing polarity machined at
1 A/20 ls/95% duty factor/0.5 kgf/cm2
The comparison of these data and the micrographs clearly indicate that DVEE and
geometrical shape are better when using the changing polarity condition for the
micromachining of micro-holes by the micro-EDM. The SEM micrographs of
machined micro-holes at parametric settings of 1 A/20 ls/95% duty
factor/0.5 kg cm−2 with constant and changing polarity techniques are shown in
Fig. 3.41a, b, respectively. It can be observed from these figures that the thickness
of recast layer formed on micro-hole surface with polarity changing technique
machining condition is less as compared to constant polarity machining condition
corroborating the fact that the surface quality of the machined micro-hole has
improved with this new machining technique. This observation clearly indicates
that with changing polarity technique, a better machining condition is achieved
during micro-hole machining by micro-EDM process.
3.11 Conclusions
micro-EDM were described with brief details of sub-systems and significant pro-
cess parameters with performance measures. Detailed research and investigation
was performed during micro-EDM of Ti–6Al–4V alloy implementing various
machining strategies such as ultrasonic vibration assisted micro-EDM, parametric
influence and comparative study of process criteria employing two different
dielectrics i.e. kerosene and de-ionized water, use of boron carbide mixed kerosene
and de-ionized water as dielectrics, providing rotation of micro-tool electrode
during micro-hole generation and reversing the polarity of electrodes. The exper-
imental results show that these innovative machining strategies have great influ-
ences for improving the machining rate and geometrical accuracy in terms of
material removal rate, tool wear rate, overcut and diameteral variance of entry and
exit of micro-hole. Furthermore, the process performances also greatly depend on
significant process parameters such as peak current, pulse-on-time and flushing
pressure. As micro-EDM process is slow process, therefore, novel machining
strategies mentioned above must be implemented to improve the process perfor-
mances to improve the accuracy of micro-structure, surface finish and efficiency.
Furthermore, innovative hybrid micro-machining processes can also be developed
for micro-EDM to machine hard-to-machine materials like Ti–6Al–4V alloy for
increasing the yield of micro-manufacturing.
Acknowledgements The authors acknowledge the financial support and assistance provided by
CAS Ph-IV programme of Production Engineering Department of Jadavpur University under
University Grants Commission (UGC), New Delhi, India.
References
1. Masuzawa T (2000) State of the Art of Micromachining. Annals of the CIRP 49(2):473-488
2. Ho KH, Newman ST (2003) State of the art electrical discharge machining (EDM).
International Journal of Machine Tools & Manufacture 43(13):1287-1300
3. Kunieda M, Lauwers B, Rajurkar KP, Schumacher BM (2005) Advancing EDM through
Fundamental Insight into the Process. CIRP Annals - Manufacturing Technology 54(2):64–87
4. König W, Klocke F (1997) Fertigungsverfahren - 3: Abtragen Und Generieren, Vol.3.
Springer, Berlin
5. Pham DT, Dimov S, Bigot S, Ivanov A, Popov KB (2004) Micro-EDM—recent
developments and research issues. Journal of Materials Processing Technology 149(1–3):
50–57
6. Gentili E, Tabaglio L, Aggogeri F (2005), Review on micromachining techniques. Courses
Lectures, CISM International Centre for Mechanical Science 486:387-396
7. Katz Z, Tibbles CJ (2005) Analysis of Micro-scale EDM process. International Journal of
Advanced Manufacturing Technology 25(9):923-928
8. Rajurkar KP, Levy G, Malshe A, Sundaram MM, McGeough J, Hu X, Resnick R, DeSilva A
(2006) Micro and nano machining by electro-physical and chemical processes. Annals of the
CIRP 55(2):643–666
9. Masuzawa T, Sata T, Kinoshita N (1971) The occurring mechanism of the continuous arc in
micro-energy EDM by RC circuit. Journal of Japan Society of Electrical-Machining
Engineers 5(9):35–52
142 G. Kibria et al.
30. Kuriachen B, Mathew J (2014) Modeling of material removal mechanism in micro electric
discharge milling of Ti-6Al-4V. Applied Mechanics and Materials 592–594:516–520
31. Plazaa S, Sancheza JA, Pereza E, Gila R, Izquierdob B, Ortegaa N, Pombob I (2014)
Experimental study on micro EDM-drilling of Ti6Al4V using helical electrode. Precision
Engineering 38(4):821–827
32. Moses MD, Jahan MP (2015) Micro-EDM machinability of difficult-to-cut Ti-6Al-4V against
soft brass. International Journal of Advanced Manufacturing Technology 81(5):1345-1361
33. Tiwary AP, Pradhan BB, Bhattacharyya B (2015) Study on the influence of micro-EDM
process parameters during machining of Ti–6Al–4V superalloy. International Journal of
Advanced Manufacturing Technology 76(1–4):151–160
34. Kuriachen B, Mathew J (2016) Effect of powder mixed dielectric on material removal and
surface modification in micro electric discharge machining of Ti-6Al-4V. Materials and
Manufacturing Processes 31(4):439-446
35. Kuriachen B, Varghese A, Somashekhar KP, Panda S, Mathew J (2015) Three-dimensional
numerical simulation of microelectric discharge machining of Ti-6Al-4V. International
Journal of Advanced Manufacturing Technology 79(1):147-160
36. Kuriachen B, Mathew J (2016) Spark radius modeling of resistance-capacitance pulse
discharge in micro-electric discharge machining of Ti-6Al-4V: an experimental study.
International Journal of Advanced Manufacturing Technology 85(9):1983-1993
37. Kremer D, Lebrun JL, Hosari B, Moisan A (1989) Effects of ultrasonic vibrations on the
performance in EDM. Annals of the CIRP 38(1):199–202
38. Ichikawa T, Natsu W (2013) Realization of micro-EDM under ultra-small discharge energy
by applying ultrasonic vibration to machining fluid. The Seventeenth CIRP Conference on
Electro Physical and Chemical Machining (ISEM) 6:326-331
39. Liew PJ, Yan J, Kuriyagawa T (2014) Fabrication of deep micro-holes in reaction-bonded SiC
by ultrasonic cavitation assisted micro- EDM. International Journal of Machine Tools &
Manufacture 76:13-20
40. Jahan MP, Rahman M, Wong YS, Fuhua L (2010) On-machine fabrication of
high-aspect-ratio micro-electrodes and application in vibration-assisted micro-electro dis-
charge drilling of tungsten carbide. Proceedings of the Institution of Mechanical Engineers
Part B: Journal of Engineering Manufacture 224(5):795-814
41. Changshui G, Zhengxun L (2003) A study of ultrasonically aided micro-electrical-discharge
machining by the application of work piece vibration. Journal of Materials Processing
Technology 139(1-3):226-228
42. Prihandana GS, Mahardika M, Hamdi M, Wong YS, Mitsui K (2009) Effect of micro-powder
suspension and ultrasonic vibration of dielectric fluid in micro-EDM processes-Taguchi
approach. International Journal of Machine Tools & Manufacture 49(12-13):1035-1041
43. Ghoreishi M, Atkinson J (2002) A comparative experimental study of machining
characterstics in vibratory, rotary and vibro-rotary electro- discharge machining. Journal of
Materials Processing Technology 120(1-3):374-384
44. Shabgard MR, Sadizadeh B, Kakoulvand H (2009) The Effect of Ultrasonic Vibration of
Workpiece in Electrical Discharge Machining of AISIH13 Tool Steel. International Journal of
Mechanical, Aerospace, Industrial, Mechatronic and Manufacturing Engineering 3
(4):404-408
45. Garn R, Schubert A, Zeidler H (2011) Analysis of the effect of vibrations on the micro-EDM
process at the workpiece surface. Journal of Precision Engineering 35(2):364-368
46. Tong H, Li Y, Wang Y (2008) Experimental research on vibration assisted EDM of
micro-structures with non-circular cross-section. Journal of Materials Processing Technology
208(1-3):289–298
47. Zhang QH, Zhang JH, Deng JX (2002) Ultrasonic vibration electrical discharge machining in
gas. Journal of Materials Processing Technology 129(1-3):135–138
48. Kim DJ, Yi SM, Lee YS, Chu CN (2006) Straight hole micro EDM with a cylindrical tool
using a variable capacitance method accompanied by ultrasonic vibration. Journal of
Micromechanics and Microengineering 16(5):1092–1097
144 G. Kibria et al.
4.1 Introduction
A WEDM process may be called as a Micro WEDM process only when it is used
for manufacturing micro parts, the rest underlying theory remaining same as of
WEDM. A scheme of the MWEDM setup is shown in Fig. 4.1. In WEDM, the
electrode is a continuously moving electrically conductive wire. The mechanism of
material removal in WEDM and MWEDM involves complex erosion effect by
rapid, repetitive and discrete spark discharges between the wire tool and the job
immersed in a liquid dielectric medium. A DC power supply is used to generate a
very high frequency pulses. The wire is unwounded from the feeding spool by a
drive unit moving at constant speed to pass through a tension mechanism and then
through the workpiece. The expended wire is either rewound on a take-up spool or
chopped off in small pieces to be collected in a bin. However, a fresh electrode wire
is continuously presented to the machining zone. The work is connected to the
positive terminal and the wire-tool is connected to the negative terminal of the
4 Advancements in Micro Wire-cut Electrical Discharge Machining 147
wire break
switch tension
+ clutch
wire electrode + Feeding
Current spool
pick up +
+
Upper
flushing
valve V-axis motor MONITOR
(-)
U-axis
Y-axis
nozzle motor
motor
upper
wire
Dielectric guide
flow line
Control
Panel
X-axis motor
(+)
workpiece
Wire feed motor
Lower wire
guide
Lower
flushing + Wire cutting
valve + + & collection
Current
pick up
Cut wire
in the discharge. This results in the formation of a tiny crater at the point of
discharge in the workpiece. In MWEDM, the diameter of the crater may range from
submicron level to a few micron. Furthermore, the particles removed from the
electrodes due to the discharge fall in the liquid and cool down to form a colloidal
suspension of metal. The dielectric, thus, becomes contaminated.
The mechanism of sparking and material removal in WEDM and MWEDM are
same. The spark gap between the electrodes at various points would vary due to the
asperities present at the surfaces of tool and work as well as due to wire-tool
vibration. When a suitable voltage is built up across the electrodes, a strong elec-
trostatic field is established causing cold emission of electrons from cathode to
anode at a point where least resistance is offered by the dielectric medium. These
electrons start accelerating to gain sufficient velocity with which they collide with
dielectric fluid molecules breaking them into electrons and positive ions. Electrons
so produced also accelerate and collide with dielectric molecules to dislodge more
and more electrons. Ultimately, an ionized column is established in the dielectric
across the gap. The conductivity of this ionized column is very high, so it connects
the tool and work, and an avalanche of electrons flow from cathode to anode. This
is seen as spark. As soon as this happens, the gap between the electrodes increases
at that spot and the next spark occurs at somewhere else where the spark gap is
minimum. Thus, the sparks move all over the electrode surface. As a consequence
of spark, the temperature generated is of the order of 8000–10,000 °C which melts
and evaporates the metal in the sparking zone, i.e., both in the surfaces of tool and
work. Also the dielectric fluid adjacent to the sparking zone evaporates and other
gaseous products may form. The products try to expand against the inertia of the
adjacent dielectric creating high compressive pressure wave. Shortly after, the
discharge column collapses and gaseous products cool down. Pressure starts falling
leading to cavitation (when pressure falls below its vapour pressure). So the sur-
rounding fluid rushes towards the sparking zone and occupies the space resulting in
a mechanical blast. This blast removes the molten metal from anode and cathode in
the shape of metallic globules. Thus, major portion of the molten metal is dispersed
into the dielectric fluid medium and forms a colloidal suspension. A small fraction
of molten metal adheres to the crater surface and resolidifies upon cooling to form
a thin white layer.
Any electrically conductive material can be used as work material with a minimum
electrical conductivity of j = 0.01 S/cm (siemens/cm). Electrical conductivity (j)
4 Advancements in Micro Wire-cut Electrical Discharge Machining 149
The most important requirements of a dielectric fluid are: (a) it should have high
dielectric strength, i.e. it should remain non-conductive until the breakdown voltage
is reached, (b) it should have high cooling ability, (c) it should deionise the spark
gap quickly and completely after the discharge takes place and (d) it should possess
low viscosity to assure good flow characteristics at room temperature. All these
qualities are generally found in hydrocarbon oils having a viscosity of 3–6 cSt at
20–22 °C. This is the reason why kerosene is most widely used dielectric medium
in die-sinking EDM process. However, a dielectric, usually, de-ionized water
(jw * 1 lS/cm), is continuously forced fed to the machining zone to flush away
the eroded particles from the machining zone in WEDM. De-ionized water is used
as the dielectric medium because it not only affords better flushing and cooling but
also creates an environment of low conductivity dielectric medium to provide a
larger spark gap compared to oil dielectric. The wire electrode under tension is
subjected to vibrations due to various forces (like, electrostatic, electrodynamic,
hydraulic etc.) during spark discharges. That is why a larger spark gap is required to
be maintained than that of traditional EDM process. It is worthy to mention that
water is not at all a suitable dielectric for traditional EDM as it causes rapid
electrode wear.
Although deionized water is normally used as the dielectric liquid in conventional
WEDM, dielectric oil (jw < 0.1 lS/cm) is more preferable than water as the
dielectric in micro-WEDM for several reasons. They are: (a) electrolysis corrosion of
workpiece does not occur in oil dielectric, (b) the discharge craters generated in oil
dielectric are smaller than those in water even under the same pulse conditions, and
(c) the permittivity of water is about 36 times higher than that of oil, i.e., the
capacitance of the working gap in water is about 36 times larger than that in oil [1].
This is one way of obtaining very low pulse energy content in the order of 0.1–10 lJ
for MWEDM. However, in addition to the above, the tool wear is less and deioni-
sation unit is not necessary when oil is used as dielectric.
In general, copper and brass are normally preferred as wire electrode material in
WEDM with diameters of the wire ranging from 100–300 lm. In MWEDM,
tungsten and molybdenum wire in the range of 20–100 lm are used as extremely
sharp corners and high precision are the major requirements of machining. Brass
150 A.B. Puri
wire and zinc coated brass wire are also used. The resistance to erosion and tensile
strength of tungsten and molybdenum are much higher than that of copper or brass
wire. Hence, a very high precision machining is achieved with the least possibility
of wire rupture. At the same time, tungsten and molybdenum wires are too costly.
A brief comparison of the properties of tungsten and molybdenum is given in
Table 4.1 [2]. It may be seen that tungsten is a few steps ahead of molybdenum so
far as wire material is concerned. That is why tungsten wire is used almost uni-
versally. However, for high precision machining a very low flushing pressure is
used as the wire vibrates during machining. Very often, the working gap is simply
kept immersed in dielectric medium (no flushing condition).
Among other problems, wire rupture is perhaps the most serious problem in the
application of MWEDM. The wire EDM machine is used to run continuously
without operator. If the electrode wire breaks during the process, rethreading of the
wire is done causing the downtime of the machine. It has two drawbacks as follows:
(i) it increases the overall machining time of a part or product, and (ii) the
machining accuracy of the profile decreases, since a stripe (tool mark) is left on the
work surface very often. This is due to the fact that it is very difficult to reset the
wire at the same position where it ruptured. To make the matter worse, the wire
rupture phenomenon has a more or less stochastic behaviour. However, the causes
of wire rupture during machining may be listed as follows:
(a) Contact resistance (between the wire and the current pick-up): Current pick-up
is a conductive ceramic object through which the electrical power is supplied
into the wire. In this case, localized joule heating depending on the contact
resistance between the wire and the current pick-up(s), becomes intense upon
4 Advancements in Micro Wire-cut Electrical Discharge Machining 151
increasing working current or effective pulse frequency. Thus the surface of the
wire is soiled.
(b) Improper winding system of the wire.
(c) Improper wire feed.
(d) Improper wire tension adjustment.
(e) Short circuiting: When the work-table feed rate (feeding of workpiece) is more
than the cutting speed, the wire electrode may get physical contact with the
workpiece. A short circuit is said to occur in this case. A high current passes
through a very small segment of wire producing joule heating followed by wire
rupture.
(f) Improper pulse types and frequency: The basic reason of wire rupture under
this category may be called as thermal failure due to time and space concen-
tration of spark discharges. This renders the local heating of the wire more
severe and wire rupture becomes inevitable. The increase in pulse frequency
leads to the same phenomenon to occur. Occurrence of arc pulses is another
reason of wire rupture. Thus, the remedies to this type of wire rupture are:
(i) avoiding a high pulse frequency; and (ii) avoiding occurrence of increased
arc and other abnormal pulses. Wire rupture of the first type may be avoided by
increasing pulse off time and to achieve a fairly stable process. The wire rupture
of the second type may also be avoided by increasing pulse off time, and
employing a specially designed pulse discriminator system which eliminates or
suppresses the arc and other abnormal pulses by maintaining a suitable ignition
delay period (tl).
In micro-WEDM, the key is to limit the energy in the discharge. Lower energy
results in low MRR, high accuracy and better surface finish. To generate small
energy pulses of the order of 0.1–10 lJ, a DC power supply system should be
properly designed as micro energy pulse generator. For better MRR discharge
frequency should be increased. This is ensured with the use of MOSFET.
A MOSFET (metal oxide semiconductor field effect transistor) is a device used for
amplifying or switching electronic signals. But, the biggest problem is posed by
‘stray capacitance’ prevailing in an R–C circuit. Any two adjacent conductors can
be considered as a capacitor. If the conductors are not close together for long, they
may also form a capacitor although the capacitance will be small. This (often
unwanted) effect is termed ‘stray capacitance’. Stray capacitance can allow signals
to leak between two isolated circuits (an effect called crosstalk), and it can be a
limiting factor for proper functioning of circuits at high frequency. The problem of
stray capacitance is tackled with the use of granite basement, piezo-electric
ceramics and other electrically nonconductive strong materials. Granite is quite
suitable for micro-WEDM machine equipment because it has good insulating
152 A.B. Puri
characteristics and has no inductance. Hence, it can be used for basement and work
table for its lower heat transmission coefficient. It is insensitive to temperature, and
good at absorbing vibration. Piezo-electric ceramics are good for making driving
parts. It has very high displacement sensitivity and high frequency response.
However, because of its limited stroke, researchers often make special mechanism
to increase its force and enlarge its stroke. Apart from the above, a good MWEDM
machine tool should have, (i) iso-energy and iso-frequency micro pulse generators
fitted with a suitable pulse discriminating system, (ii) a wire transport system
supplemented with a closed loop feedback control of precision wire tension
mechanism. However, designing and developing the micro pulse generator is the
task of an electrical engineer.
While cutting a straight job, the upper guide remains stationary in u-v plane at u = 0
and v = 0 with respect to lower guide (Fig. 4.1). Actually, instead of movement of
both the upper and lower guides, the worktable carrying the job blank is moved
along the programmed path while the lower guide remains permanently stationary.
Thus, during straight cutting of jobs, the wire tool is kept exactly vertical to x-y and
u-v plane. In case of taper cutting, the upper wire guide is not kept stationary but
moves along u and v axes with respect to the lower guide at a predetermined pace
with the worktable movement. The lower guide is kept stationary as stated earlier.
Thus, the wire does not remain vertical, embracing the generation of motion of the
top slide in u and v axes. The angle so produced with the vertical axis, can be varied
at various points which can be controlled by the path programming. A desired taper
angle can be achieved by simultaneous control of the movement of the x-y table and
the u-v auxiliary table along their respective predetermined path as designed and
stored in the controller. However, taper cutting in WEDM system is performed very
cautiously and at a considerably low cutting speed as compared to straight cutting
due to following difficulties encountered: (i) achieving proper flushing is difficult as
the wire remains tilted and flushing direction is vertical (this renders the heating of
wire more severe causing the wire rupture due to the thermal load), and (ii) wide
fluctuation in wire tension.
The trim cut (also called skim cut) is an operation where the wire electrode traces
back the same path after the first cut is over (Fig. 4.2). Obviously, this is used for
machining of job profile in multi-pass cuts. Multi-pass cutting of jobs is usually
done in two or three cuts depending on the specific requirement. While trim cutting,
very low energy pulses are applied to obtain a very less amount of material
4 Advancements in Micro Wire-cut Electrical Discharge Machining 153
removal. Generally, high pressure flushing is avoided in case of trim cut to obtain
better accuracy. However, the objective of using trim cuts may be listed as follows:
(i) to achieve better job accuracy; (ii) to achieve improved surface finish; (iii) to
reduce inaccuracies produced by minor job deformations after the first cut due to
residual stresses in the job material; (iv) to reduce the bow effect (or cambering
effect) on the cut job surface produced in the first cut due to wire vibration or
adverse flushing conditions; (v) to improve the life of the job by reducing thermally
affected layer formed on the machined surface in the first cut or previous cut.
In the MWEDM process, electrical energy in the form of short duration impulses is
required to be supplied in the machining gap. For this purpose several electrical
circuits or even specially designed generators are employed. The circuits are
154 A.B. Puri
distinguished according the way in which the voltage is built up and the pulse is
controlled and also the characteristics of discharge. However, in almost all such
circuits a capacitor is used for storing the electric charge before the discharge takes
place across the gap. Different circuits are used for different machining conditions
and requirements. The commonly used systems are:
i. R–C relaxation circuit with a constant D.C. source or Relaxation generator.
ii. High frequency electronic circuit.
However, irrespective of the circuits, the pulse energy may be determined as,
Zt2
Wp ðor EP Þ ¼ I(t)V(t)dt
t1
However, R–C relaxation circuit is the simplest type and it can produce sparks over
a wide range of frequency (although not in higher range). It is shown in Fig. 4.3.
When the circuit is switched on, there will be a current in the charging loop while
there is no current in the discharge loop and the capacitor charges itself through the
resistance Rc. The voltage across the capacitor goes on increasing. At a voltage
V = Vb, the spark occurs discharging the capacitor completely (theoretically). After
the spark, the dielectric deionises, the capacitor starts itself recharging and the cycle
repeats. The time taken to recharge the capacitor to the breakdown voltage (Vb)
must be sufficient to allow the dielectric to deionise completely.
Let, in the charging loop, the current at any instant is Ic (i.e., instantaneous
current), V0 is the supply voltage, Vc is the voltage across the capacitor at any
instant, Rc is resistance, C is the capacitance of the capacitor and t = time elapsed
after switching on the circuit. The instantaneous current in the charging loop will
be,
V0 Vc d(V0 Vc ) dVc
Ic = = C =C
Rc dt dt
ð4:1Þ
dVc 1
) = dt
V0 Vc Rc C
Thus, Ic ¼ V0RVc ¼ V0 Re c ; 0 t tc
R C
c c
Therefore, the charging voltage across capacitor increases exponentially while
the charging current decreases exponentially.
156 A.B. Puri
Let, in the discharge loop, Id is the current at any instant (i.e., instantaneous cur-
rent), Vd is instantaneous voltage, R is the resistance. The total resistance in the
discharge circuit R may be considered to be comprised of the line resistance (RL)
and the spark resistance or machine resistance (RS). As, RS RL, R RS. Thus,
Vd dVd Vd
Id ¼ ¼ C ¼
R dt Rs
ð4:2Þ
dVd 1
) ¼ dt
Vd RS C
t
Thus, Id ¼ V V b e RS C
Rs ¼ Rs ; 0 t td
d
Therefore, in the discharging circuit, the voltage will fall exponentially while the
capacitor discharges itself and the discharging current will also exponentially decay,
i.e., theoretically, the time taken for the current to be zero is very large. The
theoretical voltage and current waveforms are shown in Fig. 4.4. However, the
actual voltage and current waveforms reveal that there exists a negative voltage
during the later part of the discharge. Also, the profile of the discharge voltage
indicates definite existence of an inductive load in the discharging circuit. Hence,
neither purely resistive nor purely inductive is the discharging circuit, it behaves as
an R-L-C circuit.
Actually, Id ¼ VR d e
¼ C dVdt
d
Where, ‘e’ is the back emf generated in the discharging circuit due to inductance
and R = RL + RS. Importantly, when, e > Vd at the later part of the discharge (tail
end), Id becomes negative.
However, e ¼ L dI d
¼ LC d2 V d
dt dt2
Thus,
dVd
Vd e ¼ RC ;
dt
dV2 dVd
) LC 2d þ RC þ Vd ¼ 0 ð4:3Þ
dt dt
dV2 R dVd 1
) 2d þ þ Vd ¼ 0
dt L dt LC
The discharge voltage will be governed by the Eq. (4.3), which is a case of
damped oscillation. For purely inductive circuit (i.e., R = 0), the governing equation
2
for ‘Vd’ becomes, d V2 d þ LC 1
Vd ¼ 0. This is a case of simple harmonic fluctuation
dt pffiffiffiffiffiffiffiffiffiffiffi
of voltage with a time period 1=LC . Naturally, there will be more number of
reversal of sparks leading to high tool wear. Hence, this oscillation has to be damped
effectively by introducing a suitable R. The total resistance in the discharge circuit R
may be considered to be comprised of the line resistance (RL) and the spark resis-
tance (RS). RS is very large, almost constant and uncontrollable [3]. Hence, RL has to
be adjusted suitably.
The pulse energy in an R-C relaxation circuit may be obtained as, Wp = ½ CV2b J,
C = capacitance, F; V
b = breakdown
voltage, V.
V
Thus, tc ¼ Rc C ln V V ; and, td ¼ Rs C ln V
0 b
0 b Ve
The frequency of operation, m ¼ T1 ¼ tc þ1 td .
So, MRR ¼ K m Wp ¼ 1=2 Km CVb 2 ; K is a constant of proportionality
which depends grossly upon dielectric, type of flushing, work material properties. It
may be calibrated for a certain experimental condition.
158 A.B. Puri
A pulse generator for micro WEDM provides iso-energy and iso-frequency pulses
with low discharge energy and may be considered as ‘heart’ of the system. The
ideal voltage and current waveforms have been shown in Fig. 4.5, where VP is
pulse peak voltage or open circuit voltage, Vm is average working voltage, Vd is
discharge voltage, tl is ignition delay time, IP is pulse peak current, td is pulse
discharge time, TON is pulse on time; TOFF is pulse off time. Yan and Chien [4]
have developed a transistor-controlled elementary power supply which minimizes
the single discharge energy and also provides high frequency pulses (Fig. 4.6). The
circuit is composed of a discharge circuit and a snubber circuit driven by MOSFET
M1 and control MOSFET M2, respectively. Figure 4.7 illustrates the timing chart of
the pulse control signals and associated pulse trains of MWEDM pulse generator.
P1 and P2 are the pulse control signals of the MOSFET M1 and M2, respectively.
When the MOSFET M1 is turned on, the discharge circuit leads the gap to discharge
by supplying a DC voltage of 110 V. After each discharge, the excessive discharge
energy, if any, stored into the inductive part of the discharging path is directed to
the resistor R2 through the control MOSFET M2. If the excessive energy remains in
the discharging circuit and is not drained out in due time, it would result in
instability of the discharging process.
Like EDM, in Micro WEDM also, pulses are classified into four major types,
namely: open, normal, arc and short pulses (Fig. 4.8). The basis of this classifi-
cation is the time evolution of the gap voltage and gap current. In open pulses (also
called open circuit pulses), the discharge between the wire-tool and the work piece
does not take place. Hence, the energy is continuously accumulated in the elec-
trodes for a discharge to take place. A normal pulse is an effective and the most
desirable when it has a suitable ignition delay time (tl). Ignition delay-free dis-
charges are called arc pulses and in ‘off’ pulses, neither gap voltage nor gap current
is detected. A short circuit occurs when metal contact between the work piece and
the wire electrode takes place. The occurrence of arc discharges is due to poor
flushing, gap contamination and short ionization, which depend on the instanta-
neous concentration of the slag in the spark gap. Also, when the pulse interval of
each spark is not sufficient to flush away the spark debris and allow re-ionization of
the dielectric, the arc discharges and short circuits occur.
The time between the application of the voltage between electrode and work-
piece, and the start of ignition is termed as ignition delay time (tl). It is a parameter
of the WEDM process having correlation with the physical circumstances in the
gap. It is inversely proportional with the electrical field strength at the spot of spark
discharge. This is the reason why the average delay time is considered as an
evaluation parameter for on-line process information required for adaptive control
160 A.B. Puri
system in WEDM. The breakdown field strength as material constant, influences the
delay time and a lower value of the breakdown field strength of the dielectric fluid
causes a decrease of the delay time. Also, an increase in the contamination of the
dielectric with the uncharged gap width results in a lower value of the delay time. It
is worth mentioning here that none of these circumstances are constant not even for
a stable process and a great variation of the delay time occurs for every individual
pulses. However, results of various investigators have shown that generally a
decreasing average ignition delay time is attended by an increased relative electrode
wear and a decreased average MRR. This phenomenon had led to the idea that
pulses preceded by a very short ignition delay time are not good and ineffective.
But, at the same time it has also been experimentally verified that the elimination of
pulses with very short ignition delay does not yield any improvement in machining
performances as expected in connection with the above mention ideas [5].
However, a micro pulse generator in MWEDM should be able to generate
iso-frequency and iso-energy pulses and must have a suitable pulse discriminating
system incorporating the control strategy for regulating the pulse interval in
real-time according to the identified gap states to avoid the occurrence of arc
discharges and short circuits.
where, F is wire tension (N), y is wire deflection (m), t is time (s), q0 is q.s (kg/m),
q = wire mass density, kg/m3, s = wire cross section (m2), b = specific damping
co-efficient (N-s/m2), E = young’s modulus, N/m2, I = area moment of inertia,
(pd4/64), d = wire diameter (m), q (z, t) = specific external load or body force per
unit length of the wire, N/m. The term F @@z2y indicates the force due to bending
2
deformation because of the applied axial tension F. The term EI @@z4y represents the
4
force required for transverse bending against flexural rigidity of the string. As the
wire is perfectly flexible, as has been assumed, this term is negligibly small.
The terms q0 @@t2y and b @y
2
wire deviates through a distance a0 from its ideal initial stretched condition over the
workpiece height theoretically and the same is released at t = 0.
From the geometry of the wire shape, the displacement function y (z, t) may be
determined by the following initial conditions (IC):
2a0 z L H
IC: y(z,0) ¼ f(z) ¼ ; when, 0 z
LH 2
LH LþH
¼ a0 ; when, z
2 2
2a0 ðL z) LþH
¼ ; when, zL
LH 2
@2y 2@ y
2
@y
¼ c K Q ð4:5Þ
@t2 @z2 @t
@2y @2y @y
¼ c2 2 K ay ð4:6Þ
@t 2 @z @t
The above equation is solved by the method of separation of variables with the
following initial and boundary conditions (IC and BC):
@y
IC : y ðz; 0Þ ¼ f ðzÞ; and; ðz; 0Þ ¼ 0
@t
BC : yð0; tÞ ¼ 0; and; yðL; tÞ ¼ 0
X
1 np
2qbt
yðz; tÞ ¼ e 0 fAn cosðxn tÞ þ Bn sinðxn tÞg sin z ð4:7Þ
n¼1
L
np np
With: An ¼ n2 p8a 0L
2 ðLHÞ sin 2 cos 2 HL , Bn ¼ An 2qb x1n , and
0
164 A.B. Puri
sffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffi
2 2
1 4n p F b2
xn ¼ 2 þ 4a
2 q0 L2 q0
The static deflection of a stretched wire supported by the two wire guides at
opposite ends, is defined as wire lag in WEDM and is shown in Fig. 4.12. Thus, the
wire bending or the static deflection (y) of the stretched wire of length ‘l’ in a plane
(along z-axis) may be expressed as [12]:
@2y
F ¼ q0 ð4:8Þ
@z2
where, F = wire tension (N), y = y(z) = wire deflection (m), q0 = specific external
load or body force per unit length of the wire (N/m),
The solution of the Eq. (4.8) will appear as follows:
q0
y¼ zðl zÞ
2F
This is an equation of a parabola which indicates that the shape of the wire
within the work piece will be parabolic during machining operation.
2
Also, ymax ¼ 2F
q0
Hðh þ HÞ q8F
0h
¼ y1 þ y2
2
where, y1 ¼ 2F
q0
Hðh þ HÞ, and y2 ¼ q8F
0h
On the other hand, the solution of equation F @@z2y ¼ q0 outside the work piece and
2
within the wire span between the guides (q0 = 0) will appear as,
q0
y¼ ðh þ HÞ z
2F
This equation describes a straight line, i.e., the wire outside the work piece will
be straight up to the guide during machining. However, as the ‘y’ appears to be
negative, it ascertains that the static deflection or wire lagging occurs in the opposite
166 A.B. Puri
direction of cutting. The geometrical error resulting out of this wire lag should affect
any contour cutting as depicted in Fig. 4.13, which clarifies that the magnitude of
wire lag (y) is equal to the maximum deviation of the traced path from the defined
path of the wire-tool in WEDM. However, as the pulse energy is very less in
MWEDM, the lag effect is less pronounced with appropriate machining conditions
and magnitude of wire lag may be made significantly less as would be seen later in
Sect. 4.8.
4 Advancements in Micro Wire-cut Electrical Discharge Machining 167
The lag effect in a WEDM rough cutting process affects the generation of contour of
a product or part directly. This has been further illustrated in Fig. 4.14 where
generation of a 90° corner is exhibited. The programmed path is A-o-A2. The guide
position would be at ‘o’ at the extreme corner and the ideal position of the wire
along with the surrounding spark gap would be the dotted circle with its center at
‘o’. But, due to the wire lag, the actual position of the wire will be the circle C with
center at c where oc is the wire lag (=y). Thus, while the guides trace the path o-A2,
the center of the wire traces the path c-c1-c2-cn-A2. This phenomenon directly
affects the generation of the job profile. In Fig. 4.14, the dotted circles (O and On,
O1 and O2 are not shown in the figure to avoid clumsiness) are the ideal positions of
the wire in the programmed path and circles C, C1, C2 and Cn (with their centres at
c, c1, c2 and cn respectively) are actual positions of the wire on the traced path. It is
assumed that the constant body force acts on the wire always in the reverse
direction of cutting, then the distances oc, o1c1, o2c2, and oncn are equal and
constant. Further, if a circle is imagined with radius oc with its center at ‘o’, which
moves along a path oA2 and the circle rolls over the line cA3 (Fig. 4.15), befitting to
the exact situation described above, then the path c-c1-c2-cn will be a cycloid. The
situation may be compared with a heavy ball tied up with a rope. The free end of the
rope is at ‘o’ and is moving on the line oA2 while the center of the ball is at ‘c’. Let,
the point C is the origin (0, 0) and the straight line CFD is X-axis as shown in
_
Fig. 4.16. While rolling at an instant, say, CD ¼ C1 D ¼ rh, where, r = radius of the
circle, and h = \C1 O1 D.
Let, the coordinate of C1 is (x, y). C1E is perpendicular on O1D and C1F is
perpendicular on CD. Hence,
Thus, if the circle starts to roll from the origin on X-axis (base line), then the
parametric equation of the locus of its center may be described as above. The
greatest distance from the base (vertex) will be obtained for h = p/2. Thus, for the
vertex;
It is worth to mention here that when the corner angle will be lesser or higher
than 90°, the wire will trace only a part of a full cycloid whose vertex will depend
on the corner angle.
A micro part can be machined with good dimensional accuracy and surface finish
only when the kerf (slot) width and corner radius become considerably smaller
compared to that obtainable in conventional WEDM. Truly speaking, the cutting
tool in WEDM/MWEDM is not the wire, but it is the pulse (electrical discharge).
In MWEDM, both the workpiece and the wire are eroded although the erosion of
4 Advancements in Micro Wire-cut Electrical Discharge Machining 169
the wire does not affect the accuracy as the wire passes through the work only once.
The size of the kerf is always more than the diameter of the wire used. This is due to
the presence of side sparks as shown in Fig. 4.17. The width of the cut (b) depends
on the wire diameter (d), the spark gap (g) and the amplitude of vibration (a). Thus,
The spark gap is controlled by setting servo reference voltage while the
amplitude of vibration mainly depends on pulse energy, pulse on time, pulse fre-
quency, type of pulse, wire tension and distance between the wire guides. Naturally,
a low pulse energy, normal pulse with suitable ignition delay time, minimum
distance between wire guides and a very low flushing pressure are absolutely
necessary for obtaining a minimum kerf width in a particular micromachining
setup. Di et al. [11] have obtained a kerf width as low as 30.8 lm and a corner
radius 15.8 lm using a 30 lm wire tool diameter in their self-developed MWEDM
system. This is shown in Fig. 4.18. Figure 4.19 shows the variation of kerf width
with discharge energy obtained by varying the capacitances as obtained with
experimental condition (II) shown in Table 4.3.
Wire tension plays the major role in minimising process inaccuracy. The minimum
kerf width and corner radius are governed by two process phenomena, namely
wire-tool vibration and the wire lag. Both the amplitude of vibration and the
(magnitude of) wire lag vary inversely with the wire tension. Thus, the tension in
the wire should be as maximum as it could bear. On the other hand, the wire tension
is set during machining depending on the feed velocity of the wire and the thermal
170 A.B. Puri
Fig. 4.18 A minimum kerf width and corner radius with 30 lm diameter tungsten wire [11]
load on the wire which is basically governed by pulse on time, pulse types and
pulse frequency. Thus, the tension of the micro wire may require to be changed
during machining as and when necessary. Hence, the wire transportation system in
WEDM/MWEDM should be a precise closed loop controlled system necessarily.
The wire transportation system in micro WEDM has the general layout as shown
in Fig. 4.20, which is widely used for keeping the wire tension at a constant level
[13, 14]. It consists of a wire electrode supply spool, a wire feed control apparatus
and a wire tension control apparatus. The feeding wire is directly coupled to a pair
of feeding rollers, which determine the feeding velocity of the wire electrode. While
the wire electrode is pulled out from the wire spool, it passes through another pair
of tension control rollers driven by an electromagnetic brake gear causing a braking
force on the wire.
4 Advancements in Micro Wire-cut Electrical Discharge Machining 171
Fig. 4.21 Corner cutting error a corner shape at end surface (re) and b corner shape at middle
surface (rm) [14]
Fig. 4.22 A fuzzy logic controller for the wire transport system [15]
A multi-layered heat affected zone is formed at the machined surface of the work-
piece while machining it with WEDM. The upper recast layer of this zone is called
‘white layer’. The workpiece material which gets melted is not completely expelled
during the process. The residual material resolidifies on the machined surface to
form a hard skin on the workpiece. In MWEDM, the formation of white layer can not
be eliminated but can be minimised. The sub-surface characteristics occur in various
layers or zones, which are usually termed as altered material zones (AMZ).
4 Advancements in Micro Wire-cut Electrical Discharge Machining 173
These alterations caused by the thermal energy of spark discharges are generally in
the forms of micro-cracks, spalling, increase in hardness, residual stresses, metal-
lurgical transformations and, of course, heat affected zone (HAZ). Thermal spalling
is a mechanical failure of the material by overcoming the bond strength of the
material due to the generated internal stresses without being melted. The thickness of
white layer depends on pulse on time, frequency, pulse energy and the properties of
work material. The scanning electron microscope (SEM) photograph in Fig. 4.23
shows the white layer has been reduced to as less as 2 lm for a 1 mm thick stainless
steel sheet [16]. The micro hardness of the surface white layer (recast layer) is three
to four times higher than the base material in Micro-WEDM. This is basically due to
an increase in amount of cementite dendrites that result from absorption of carbon
originating from the pyrolysis of the hydrocarbon oil dielectric. This energy dis-
persive spectroscopy (EDS) study of the white layer suggests that some amount
(*2.28%) of wire material (i.e., tungsten) get deposited on the workpiece surface.
However, instead of having detrimental effect, the existence of W element in micro
die surface improves quality of the micro part by increasing wear and corrosion
resistance.
174 A.B. Puri
It is a well known fact that the surface finish obtainable is not good for a spark
eroded surface in EDM. For EDM process the CLA values (Ra) of surface
roughness varies between 1 and 3.5 lm whereas in conventinal WEDM it varies
between 0.8 and 2 lm. However, in a carefully cut specimen, the same may be
obtained as minimum as 0.1 lm in MWEDM [5]. Hence, micro parts with such an
excellent finish may quite suit for fabrication of miniature products and devices.
The machining accuracy (tolerance) of micro WEDM can be limited in a
range ±0.2 lm with a worktable’s position accuracy ±0.1 lm. Figure 4.24 shows
an AFM image (atomic force microscopy) of topography of a surface obtained in
micro WEDM [16]. The surface roughness (Ra) obtained by AFM is *0.1 lm
for a 1 mm thick stainless steel sheet machined appropriately by Micro WEDM.
One effective way of improving the flushing condition in EDM has been using
vibration-assisted tool, which is called vibration-assisted EDM. Applications of
ultrasonic vibration to WEDM had been studied by many researchers [17–19]. With
ultrasonic vibration applied to the wire, the MRR is found to increase by 30%. The
surface roughness and the surface residual stress are also improved. By studying the
mechanism of the system, it is proved that the improvement of surface finish and
material removal rate attribute to the formation of multi-channel discharges and the
increased energy utilization ratio [17, 18]. Hoang and Yang [20] developed a
vibration assisted method for micro-WEDM systems wherein vibration of both the
wire and workpiece were considered. Effects of imparted vibration on machining
4 Advancements in Micro Wire-cut Electrical Discharge Machining 175
Fig. 4.26 SEM photographs of various micro parts machined by MWEDM and used in micro
fabrication [16]
Apart from making micro grooves, micro channels and micro beams, micro
WEDM is successfully used to manufacture shaped micro holes, micro bearing
brackets, micro gears and micro-gear dies with improved software technology
supplemented with suitable NC interpolation functions and programming.
The SEM photographs of a few machine components are shown in Fig. 4.26 [16].
The shaped holes are made on stainless steel sheet with thickness 1 mm. These
holes are widely used for spinneret orifice in textile industries and in fabrication of
micro dies. The micro bearing bracket is made on SS sheet of thickness 2.5 mm.
These brackets are used in MEMS (micro electro mechanical system) for housing
bearings. The micro gears are machined in stainless SS sheet of thickness 1 mm
4 Advancements in Micro Wire-cut Electrical Discharge Machining 177
Fig. 4.27 a Micro slit (groove) and b micro beam machined by MWEDM with electrostatic
induction feeding method [1]
with a module as less as 40 lm. Figure 4.26f shows an aluminum alloy micro gear
fabricated from micro-gear die as shown in Fig. 4.26e, by micro-forming process.
Yang et al. [1] used electrostatic induction feeding method to develop an
MWEDM setup. The construction and working principle of the pulse generator
using electrostatic induction feeding method is completely different in regard to the
conventional ones. The electrostatic induction feeding method essentially requires
the use of oil dielectric (sometimes air), because the open voltage of the working
gap decreases the discharge delay time, since the leak current flows into the water
dielectric, if used. However, using this method and experimental condition as stated
in Table 4.4, micro groove of a minimum width 32.4 lm and straight micro-beam
of a minimum thickness 3.8 lm with 100 lm length were obtained (Fig. 4.27).
However, further research is required to apply electrostatic induction feeding
method to develop a micro pulse generator for MWEDM setup.
178 A.B. Puri
References
Abstract One of the newly developed laser micromachining processes for gen-
erating micro-turn surface on cylindrical work sample is laser micro-turning pro-
cess. To explore the capability of this laser micromachining process for achieving
particular surface profile and dimensional accuracy of machined parts, authors
considered a number of experimental investigation to find the effect of process
parameters. During investigation and analysis, a number of experimental designs
are applied to in-depth analyse the effect of process parameters on surface rough-
ness (Ra and Rz) and depth deviation. The governing equations of spot and cir-
cumferential overlap were developed for investigating the effect of these overlaps
on surface criteria. By adopting statistical design of experiments approaches such as
Response Surface Methodology, the influence of process parameters on process
performance were studied. Moreover, novel machining strategy of laser defocusing
condition was also implemented for improving the micro-turning surface features.
For qualitative assessment of important process parameters, scanning electron
microscopic images of machined surface were analysed for better understanding the
process.
G. Kibria (&)
Mechanical Engineering Department, Aliah University, Kolkata 700156, India
e-mail: [email protected]
B. Doloi B. Bhattacharyya
Production Engineering Department, Jadavpur University, Kolkata 700032, India
e-mail: [email protected]
B. Bhattacharyya
e-mail: [email protected]
5.1 Introduction
To fulfil the demand of high-end products with specific features in terms of high
precision, accuracy and surface topography, researchers and technocrats are always
engaged with micromanufacturing of macro as well as micro-components with which
continuous miniaturization is developing day-by-day. It is also a challenging job for
the manufacturing engineers and researchers to develop suitable micromachining
process which can be applied to machine hard-to-cut materials such as alloys, com-
posites etc. effectively with unique accuracy and productivity. For achieving effective
machining accuracies and desired surface finish, a number of traditional and advanced
micro-manufacturing processes have been developed for applying these machining
techniques for product manufacturing of wide varieties. Moreover, various micro-
devices and miniature MEMS need specific functional characterization which
necessitate the incorporation of micro-features in diverse range of products. Therefore,
at this stage, it is urgently needed to implement novel machining techniques, besides
traditional processes, which can fulfil these demands. As most of the non-traditional
micromachining techniques utilize different kind of energy for material removal, the
material removal processes are irrespective of material’s mechanical and physical
properties. Amongst various non-traditional processes, laser beam machining
(LBM) is a widely applied and successful material removal process for fabrication of
different geometries with close tolerances at high production rates.
Based on laser types, type of operations and different wavelength, LBM is clas-
sified at various types. Pulsed and continuous wave Nd:YAG laser, Fiber laser and
Excimer laser are widely applied laser sources for manufacturing of different features
in components. In the pulsed mode laser operation, the material instantly melts as well
as vaporises with very short intervals. Therefore, the conduction of heat into the bulk
material does not occur. The compilation of Nd:YAG laser with Q-switch mode offers
exceptional machining geometries during micro-machining processes such as
micro-milling, micro-turning, micro-drilling and micro-cutting. One of the newly
developed Nd:YAG laser micro-machining processes is laser micro-turning operation
in which the cylindrical samples can be machined successfully to micro-turn the
material at small depth with specific surface quality and accuracy. As pulsed mode of
Nd:YAG laser has several advantages during processing of materials that include
instant material melting and vaporization, small resolidified layer and less damage of
machined surface due to micro-cracks formation. In laser micro-turning process, very
thin depth from material’s upper surface is removed due to laser irradiation while
rotating the cylindrical workpiece. Thus, the process can efficiently be applied for
micro-turning of several exotic materials such as ceramics and composites. The length
of micro-turn surface is controlled by axial feed of workpiece. The micro-turning
surface with specific surface properties has huge high precision applications such as
self assemblies, ceramic spikes, ceramic bearing ring etc. Furthermore, due to long
time operation of grinding wheel, the cutting ability of micro-abrasives reduces. The
generation of cutting surface by laser irradiation on blunt grinding wheel surface can
be carried out by laser micro-turning process.
5 Laser Micro-turning Process of Aluminium Oxide … 181
Laser grooving process is carried out by scanning the irradiated laser beam over
path of surface where the micro-groove is to be generated. There are two methods
of laser micro-grooving process, (i) using a single laser beam and (ii) using two
laser beams. In case of single laser beam, the desired width of groove is machined
by producing multiple micro-grooves side-by-side causing overlap between two
adjacent groove widths. This process produces trapezoidal or rectangular shaped
184 G. Kibria et al.
However, WEDT can only be applied for conductive materials. Thus, it is challenging
task for the manufacturer engineers and scientist to find out novel material processing
technique which can be utilized for micro-turning of ceramics.
Amongst various ceramics used for manufacturing small parts for micro-systems
as well as for biomedical implants, Aluminium Oxide (Al2O3) is most important
and widely used ceramics materials due to its several extraordinary thermal,
physical and mechanical properties such as stability at high temperature, high
degree of corrosion and wear resistance, extreme hardness, high stiffness, etc. [16].
Micromachining of ceramic materials using laser beam is complex and dynamic in
nature and the large number of process parameters such as beam power, pulse
repetition rate, pulse duration, beam scanning speed etc. have non-linear behaviours
during fabrication of complex geometries and surface features [17]. Moreover, the
optical and physical properties of the workpiece materials to be machined provide
significant variations of the output characteristics during laser micro-machining of
engineering ceramic materials [17, 18]. Therefore, at this stage, it is urgently need
to develop a novel non contact type micro manufacturing process which can effi-
ciently and effectively micro-turn ceramics as well as difficult-to-machine super-
alloy. Past research revealed that research in the direction of numerical model
development and experimentation have been carried out by number of researchers
across the globe in several laser micro machining processes such as micro-drilling,
micro-cutting, micro-grooving, surface modification etc. [19, 20]. Thus, to machine
or micro-turn cylindrical shaped aluminium oxide ceramic utilizing laser beam,
laser micro-turning process has been developed.
In 1988, Chrysolouris et al. [21] first demonstrated the capability of laser beam for
three dimensional machining employing two intersecting beams. However, two
such intersecting laser beams can remove material from work sample in bulk form.
To simplify the laser micro-turning process, single laser can effectively be utilized
where material is removed from the rotating cylindrical work sample in
layer-by-layer form. Basically, laser micro-turning process is generation of spiral
micro-grooves over a defined length of sample where the each groove has some
overlap onto the previous groove [22]. Thus, planar surface of thickness in micron
range is removed from the top cylindrical surface. The quantity of overlap between
two consecutive micro grooves are controlled by mainly two factors, axial feed rate
and rotating speed of workpiece. For obtaining desired depth of micro-turning,
continuous scanning of laser beam is carried out while rotating of work sample. The
surface characteristics i.e. quality of surface profile of laser micro-turning is gov-
erned by two overlap factors, spot overlap (SOp) and circumferential overlap
(COp). To achieve quality surface features during laser micro-turning process, the
values of these overlap factors must be high as possible. Thawari et al. [23]
5 Laser Micro-turning Process of Aluminium Oxide … 187
formulated the relationship between spot overlap, pulse frequency, spot diameter
and scanning speed of laser beam as depicted in Eq. (5.1).
Thus
v
Spot overlap ðSOp Þ ¼ ð1 Þ 100% ð5:2Þ
D Fp
In the above equation, D is the spot diameter (in mm), Fp is the pulse frequency
(in Hz) and v is the linear scanning speed of laser beam (in mm/s). The relationship
of linear scanning speed with workpiece rotating speed is
p Ds N
v¼ ð5:3Þ
60
In this equation, Ds is the diameter of workpiece (in mm) and N is the workpiece
rotating speed (in rpm).
p Ds N
Spot overlap ðSOp Þ ¼ ð1 Þ 100% ð5:4Þ
60 D Fp
overlap length xc lc 60 f
COp ¼ ¼ ¼ ð1 Þ ¼ ð1 Þ 100% ð5:5Þ
laser spot diameter D D DN
In this equation, xc is the overlap length (in mm) between two laser spots
produced in two consecutive rotations of workpiece. Figure 5.5 shows the
188 G. Kibria et al.
Fig. 5.4 Schematic view of overlap between two consecutive spots produced by laser scanning
onto the workpiece showing Gaussian energy distribution and crater depth
Maintaining the standard and performing high quality micro machining operations
on advanced engineering material, a high power pulsed Nd:YAG laser set-up
(Make: M/s Sahajanand Laser technology, Model no: SLT-SP-2000) with some
modifications has been utilized for carrying out various experimentation in laser
micro-turning operation. The detailed specifications of this pulsed Nd:YAG laser
5 Laser Micro-turning Process of Aluminium Oxide … 189
Fig. 5.5 Schematic view of overlap between two spots produced by two consecutive rotations of
workpiece showing Gaussian energy distribution and crater depth
set-up are listed in the Table 5.1. The beam operates in Gaussian mode (TEM00).
The wavelength of Nd:YAG laser beam is 1064 nm. The focusing lens has focal
length of 50 mm. To carryout different set of experimentations utilizing various
laser machining strategies on flat and cylindrical shaped work samples using the
existing laser machining set-up, various fixtures have been developed indigenously.
The pulsed Nd:YAG laser beam machining system includes the various subsystems
that include laser beam generation unit, cooling system (internal and external),
power supply system, CCD camera, CCTV, X-Y-Z controller, assist air/gas supply
system and developed fixtures etc. The photographic view of these subsystems of
laser beam machining set-up is shown in Fig. 5.6.
To conduct experimentation on laser micro-turning process on different work-
piece materials utilizing pulsed Nd:YAG laser micromachining system, workpiece
rotating system is developed separately. The rotating system is made of three sub
components, (i) servomotor with workpiece holding collet system, (ii) servo
amplifier, and (iii) power supply unit. The schematic representation of the work-
piece rotating system is shown in Fig. 5.7. In Table 5.2, the details of the servo-
motor and servo controller, which are utilized for developing the rotating system,
are enlisted. The workpiece holding collet can hold workpiece in the range of
2–16 mm diameter sample. The collet was fixed to the axis of motor precisely to
190 G. Kibria et al.
Fig. 5.6 Photographic view of the pulsed Nd:YAG laser machining system indicating various
sub-systems [24]
reduce the eccentricity error. The eccentricity of rotation was found as 3 lm, which
is acceptable. The whole rotating system is placed on X-Y worktable of the laser
machine as shown in Fig. 5.7.
To rotate the workpiece at desired rotational speed, all the sub systems are inter
connected. The power supply system has several switches and knobs to change the
rotating speed of servomotor as well as to change the rotational direction of ser-
vomotor. After placing the rotating system underneath the laser beam, the axial feed
of workpiece is given using the software installed in the personal computer attached
to the laser beam machining system. Multi pass micro-turning is carried out by
scanning the desired length of rotating workpiece surface and also by focusing the
laser beam onto the new surface generated by previous laser beam scan. Therefore,
laser micro-turning process of desired axial length and micro-turn depth is achieved
on cylindrical workpiece.
5 Laser Micro-turning Process of Aluminium Oxide … 191
Fig. 5.7 Schematic diagram of the developed workpiece rotating system with connections
between sub-components [25]
Fig. 5.8 Methodology of micro-turn depth measurement utilizing optical measuring microscope
Y feed rate, defocusing positions and number of passes. Performance criteria were
measured at all machining parametric settings and the test results were analysed
through various plots and analytical tools. The results of validation experiments
show good sign of validity of empirical models and optimizations. Optical and
194 G. Kibria et al.
Table 5.4 Process parameters and various levels for RSM based experimentation [25]
Parameters Unit Symbol Levels
L1 L2 L3 L4 L5
Average power W X1 6 7 8 9 10
Pulse frequency Hz X2 3000 4000 5000 6000 7000
Rotational speed rpm X3 200 300 400 500 600
Air pressure kgf/cm2 X4 0.3 0.8 1.3 1.8 2.3
Y feed rate mm/s X5 0.1 0.2 0.3 0.4 0.5
Coded value −2 −1 0 +1 +2
Here, X1, X2, X3, X4 and X5 are the uncoded values of input process parameters
i.e. average power, pulse frequency, workpiece rotational speed, assist air pressure
and Y feed rate, respectively. The ranges of these process parameters are as
6 X1 10 (W), 3000 X2 7000 (Hz), 200 X3 600 (rpm), 0:3 X4 2:3
(kgf/cm2) and 0:1 X5 0:5 (mm/s). The analysis of variance (ANOVA) results
for micro-turning depth deviation and surface roughness (Ra) models are shown in
Tables 5.6 and 5.7. The standard F-value for lack-of-fit is 4.06 for 95% confidence
level. However, the calculated F-values for depth deviation and surface roughness
(Ra) are 3.11 and 1.18, which are lower than the standard F-value. These imply that
the developed mathematical models are adequate at 95% confidence level. The
values of adjusted R2 are 87.07 and 86.90% and these values indicate the degree of
accuracy of the developed models. The p-values for lack-of-fit are 0.117 and 0.436,
indicating that the models adequately fit the data and ensuring that these models can
well correlate the responses.
In Table 5.8, the results depth deviation and surface roughness of eight verifi-
cation experiments obtained from experimentation are enlisted. The parametric
combinations were chosen in the considered range of each process parameters. In
Table 5.7 Analysis of variance test for surface roughness (Ra) [25]
Source DF Seq SS Adj SS Adj MS F p
Regression 20 18.7631 18.7631 0.93816 11.28 0.000
Linear 5 14.7690 0.5454 0.10908 1.31 0.328
Square 5 2.6320 2.6320 0.52641 6.33 0.005
Interaction 10 1.3620 1.3620 0.13620 1.64 0.215
Residual error 11 0.9148 0.9148 0.08316
Lack-of-fit 6 0.5367 0.5367 0.08945 1.18 0.436
Pure error 5 0.3781 0.3781 0.07561
Total 31 19.6779
Table 5.9, the comparative results of prediction errors of responses for experimental
and RSM predicted results are shown for eight verification experiments. The pre-
diction errors for depth deviation and surface roughness are 3.12 and 3.19%,
respectively. The overall prediction error is 3.16%. These percentage errors of
prediction are within acceptable limit and it is concluded that the developed models
are valid within the parametric ranges.
Utilizing various surface plots which represent the variation of response during
simultaneous increasing of two process parameters, the responses were analysed. In
Fig. 5.10, the influence of variation of laser average power and laser pulse fre-
quency on depth deviation is shown. The figure shows that the depth deviation is
increasing with laser beam average power. Due to high intense energy in the laser
198 G. Kibria et al.
Table 5.9 Comparison between experimental and RSM predicted results of test data
Expt. Experimental results RSM predicted results % of prediction error
no. Micro-turning Surface Micro-turning Surface Micro-turning Surface
depth roughness, depth roughness, depth roughness
deviation Ra (lm) deviation Ra (lm) deviation (Ra)
mm) (mm)
1 0.0314 7.51 0.0303 7.28 3.66 2.95
2 0.0352 6.16 0.0341 5.96 3.25 3.19
3 0.0094 7.00 0.0091 6.74 3.14 3.64
4 0.0480 6.26 0.0468 6.09 2.48 2.70
5 0.0517 7.23 0.0504 6.96 2.39 3.83
6 0.0253 6.74 0.0243 6.56 4.17 2.66
7 0.0002 6.09 0.0002 5.84 3.89 4.03
8 0.0017 6.89 0.0016 6.72 2.01 2.53
Average percentage of prediction error 3.12 3.19
Overall percentage of prediction error 3.16
Fig. 5.10 Response surface plot of depth deviation for varying average power and pulse
frequency [25]
beam at high average power, the amount of material evaporation is increasing and
this result in more depth deviation. It is also observed that at low value of average
power, the depth deviation is not so high and it is due to the fact that pulse off
duration decreases with increase of pulse frequency and due to this, number of
pulses reaching the workpiece surface increases. These huge numbers of pulses
cause more material to remove from workpiece surface. However, at higher setting
of laser average power, the increase of pulse frequency results in more depth
deviation. With increase of pulse frequency, according to Eq. (5.9), peak power of
5 Laser Micro-turning Process of Aluminium Oxide … 199
Fig. 5.11 Response surface plot of depth deviation for varying average power and workpiece
rotational speed [25]
laser beam decreases. But, at the same time, the duration of successive pulses
decreases and large amount of material is removed from workpiece surface.
In Fig. 5.11, the effect of average power and rotational speed of workpiece on
depth deviation is shown. The surface plot shows that with the increase of laser
average power, the depth deviation increases. As per Eq. (5.9), the peak power of
laser beam increases with the increase in average power and thus, the amount of
material melted and evaporated is more. It is observed that increase in workpiece
rotating speed results in increase in depth deviation. At high average power,
increase in workpiece rotational speed results in reduction in depth deviation. Due
to increase in rotating speed, the amount of absorbed energy by cylindrical material
is low and consequently, the amount of material removal is high enough and more
depth deviation.
In Fig. 5.12, the influence of air pressure and Y feed rate on depth deviation is
shown. By closely observing the surface plot, it is obvious that the parameter assist
air pressure has less effect on variation of depth deviation. Moreover, it is also
observed that with the increase in Y feed rate, the depth deviation decreases. It is
due to the fact that due to higher feed rate value, the time duration of material
melting and evaporation is less per laser scan area and thus, material removal is
moderate.
In Fig. 5.13, the surface plot shows the effect of variation of laser average power
and pulse frequency on roughness of machined surface. It is seen that surface
roughness first increases and after that, it decreases due to varying the laser average
power. As per Eq. (5.9), with increase in laser average power, the peak power also
200 G. Kibria et al.
Fig. 5.12 Response surface plot of depth deviation for varying air pressure and Y feed rate [25]
Fig. 5.13 Response surface plot of surface roughness (Ra) for varying average power and pulse
frequency [25]
increases and therefore, the amount of material melted and vaporized is more due to
more incident energy and ultimately, the roughness of machined surface increases.
At high setting of average power, due to removal of more material and wider crater
formation on the workpiece surface, the surface roughness decreases. From the
same surface plot, it is also seen that with increase in pulse frequency, the
roughness of machined surface increases. Although, the value of peak power of
laser beam decreases with pulse frequency according to Eq. (5.9), the duration of
consecutive laser pulses is small and the upper surface of material melts and
5 Laser Micro-turning Process of Aluminium Oxide … 201
Fig. 5.14 Response surface plot of surface roughness (Ra) for varying average power and
workpiece rotational speed [25]
vaporizes instantly. Due to this, more peaks and valleys are generated on the
machined surface and cause more roughness.
The surface plot of variation of laser average power and rotating speed of
workpiece on surface roughness is shown in Fig. 5.14. The minimum value of
surface roughness is obtained at high setting of average power and moderate value
of rotational speed of workpiece. It is obvious from this surface plot that the
increase in workpiece speed causes the absorbed amount of laser energy per unit
scan area is less and it further reduces the amount of material removal from
workpiece. This causes fewer irregularities on the machined surface. The surface
plot also depicts that when the workpiece rotating speed is high, the surface
roughness is less for varying laser average power. According to Eq. (5.4), it is
obvious that spot overlap decreases with increasing value of workpiece rotational
speed. This causes more waviness in circumferential direction of work sample.
Moreover, according to Eq. (5.5), the circumferential overlap increases with
workpiece rotational speed and therefore, the value of surface roughness decreases.
In Fig. 5.15, the surface plot shows the effect of assist air pressure and Y feed
rate on roughness criterion. The minimum value of surface roughness is achieved at
low value of assist air pressure and large setting of Y feed rate. At low value of Y
feed rate, as the time duration of laser beam material interaction is high, therefore,
the absorbed energy per laser scan area is high. Due to this, more material is
removed from the laser irradiated zone creating large micro-peaks, which ultimately
causes high value of roughness. From the same plot, it is also observed that the
variation in assist air pressure has very less effect on surface roughness criterion.
However, it is seen that with increase in air pressure, surface roughness value at first
increases; however, at high air pressure, it decreases the roughness value of
machined surface. At high air pressure, the melted and vaporized material can be
202 G. Kibria et al.
Fig. 5.15 Response surface plot of surface roughness (Ra) for varying air pressure and Y feed rate
[25]
Fig. 5.16 Results of multi objective optimization for minimum depth deviation and surface
roughness (Ra) [25]
removed uniformly and completely from machining zone; therefore, the irregular-
ities on the surface are quite less.
For obtaining the accurate geometrical dimensions of machined parts as well as
for achieving quality machined surface, multi performance optimization was carried
out using MINITAB software. The results of multi objective optimization for
achieving the minimum value of depth deviation and surface roughness are shown
in Fig. 5.16. The parametric setting at which the target machined depth and min-
imum surface roughness was achieved as average power at 7.81 W, pulse frequency
at 5601.59 Hz, rotating speed at 435.60 rpm, assist air pressure at 0.30 kgf/cm2 and
5 Laser Micro-turning Process of Aluminium Oxide … 203
Y feed rate at 0.443 mm/s. Verification experiments were performed to confirm the
multi-objective optimized results at parametric combination that can be set to the
nearer feasible setting achieved in RSM based optimization. Table 5.10 shows the
results of verification experiment and calculated error percentage for both respon-
ses. It is observed from the results of percentage of prediction error calculation that
the prediction errors were 4.76 and 4.78% for surface roughness and depth devi-
ation. These errors are within acceptable limit and it can be concluded that the multi
objective optimization is valid within the parametric range of consideration.
It has been found in the previous section that there are huge influences of various
process parameters on surface roughness (Ra) and depth deviation for obtaining
desired surface features and dimensional geometries during laser micro-turning
process of alumina ceramic. However, for achieving better surface characteristics, it
is urgently to know the basic understanding of surface roughness variation as the
surface quality and irregularity is governed by two overlap factors i.e. spot overlap
and circumferential overlap. As the values of these overlap factors depend on range
and value of various process parameters, therefore, in this section, attempts have
been made to carry out in-depth studies of overlap factors on surface features during
machining.
For experimentation, same pulsed Nd:YAG laser micromachining system and
workpiece rotating fixture is utilized. The ranges of various process parameters
considered are enlisted in Table 5.11. For each of the experiments, the number of
laser scan passes was 100. In this experimental investigation, the values of work-
piece rotating speed and pulse frequency were selected cautiously so that the per-
centage values of spot overlap (SOp) lay as some distinct and positive value. In
204 G. Kibria et al.
Fig. 5.17 Influence of rotational speed of workpiece and pulse frequency on spot overlap
Fig. 5.17, the graph represents the variation of spot overlap (%) at various pulse
frequency and rotational speed of workpiece. During trial runs, the parametric range
of Y feed rate was chosen very cautiously so as to keep the circumferential overlap
within acceptable limit. In Fig. 5.18, the influence of rotational speed of workpiece
and Y feed rate on circumferential overlap (%) is depicted. By observing these two
plots, it is concluded that the variation of significant process parameters have huge
influence on these overlaps. In these graphs, some data points were taken in which
there are no overlaps to analyse its effect on response criteria.
The graphical plots shown in Fig. 5.19 and 5.20 represent the effect of spot
overlap on surface roughness criterion due to variation in pulse frequency and
rotational speed of workpiece, correspondingly. As per Eq. (5.4), the spot overlap
can be varied using two schemes, one by varying rotational speed of workpiece
while pulse frequency kept at particular value, and second by varying pulse fre-
quency while rotational speed kept at particular value. For the Fig. 5.19, the con-
stant parameters were average power at 7 W and Y feed rate at 0.3 mm/s. From this
5 Laser Micro-turning Process of Aluminium Oxide … 205
Fig. 5.18 Influence of rotational speed of workpiece and Y feed rate on circumferential overlap
Fig. 5.19 Effect of spot overlap on surface roughness (Ra) at various pulse frequencies [26]
Fig. 5.20 Effect of spot overlap on surface roughness (Ra) at various rotational speed of
workpiece [26]
frequency setting, the time interval between two consecutive pulses is low. The
laser irradiated material get evaporation energy instantly and ultimately, the total
energy absorbed by the material surface is high. Consequently, depth of craters
obtained is high and ultimately increases surface roughness values. The graph
shown in Fig. 5.20 was drawn by keeping the average power at 8 W and Y feed rate
at 0.3 mm/s. From this figure, it is clear that the value of surface roughness is
decreasing with increase in spot overlap at all values of rotational speed of work-
piece. As more material is removed from the laser irradiated zone due to high
amount of spot overlap, therefore, uniform machined surface is achieved. For any
particular spot overlap value, the roughness of machined surface is high at higher
value setting of workpiece rotational speed. The value of spot overlap is less at high
rotating speed and thus, the uneven machined surface is obtained. Figures 5.21 and
5.22 represent the variation of surface roughness values due to varying the cir-
cumferential overlap (%) drawn at different values of Y feed rate and rotational
speed of workpiece, consecutively. Figure 5.21 is drawn by keeping parameters at
constant as average power at 8 W and pulse frequency at 5000 Hz. It is clear from
Eq. (5.5) that circumferential overlap is governed by two significant process
parameters i.e. workpiece rotational speed and Y feed rate. The increasing value of
rotating speed of workpiece at constant Y feed rate setting results in increase in
circumferential overlap and surface roughness value decreases. As per Eq. (5.5),
with decreasing value of workpiece rotational speed, the value of circumferential
overlap increases and this result in reduce in roughness value of machined surface
due to uniform material removal. It is also obvious from Fig. 5.21 that for any
particular setting of circumferential overlap, higher value of surface roughness is
5 Laser Micro-turning Process of Aluminium Oxide … 207
Fig. 5.21 Effect of circumferential overlap on surface roughness (Ra) at various Y feed rate [26]
Fig. 5.22 Effect of circumferential overlap on surface roughness (Ra) at various rotational speed
of workpiece [26]
obtained for increasing the Y feed rate. It is due to the fact that lot of null spacing is
generated for successive laser scanning and uneven machined surface is generated.
The graphical plot shown in Fig. 5.22 depicts the variation in surface roughness
due to increase in circumferential overlap. The constant process parameters were
average power at 8 W and pulse frequency at 5000 Hz, correspondingly. From this
plot, it is obvious that roughness of micro-turn surface reduces due to increase in
circumferential overlap for all values of rotational speed of workpiece. At higher
208 G. Kibria et al.
In previous sections, laser micro-turning process has been carried out based on
response surface methodology (RSM) approach to explore the effect of process
parameters on machining criteria and also to achieve the optimum machining
parametric combination to obtain minimum value of micro-turning depth deviation
and surface roughness simultaneously. Moreover, in-depth investigation and studies
of spot and circumferential overlaps have also been done. The values of surface
roughness (Ra) show that the laser micro-turning surface has lot of irregular
micro-peaks, which have been generated due to variation in spot as well as cir-
cumferential overlaps and also due to sudden solidification of melted material.
However, manufactured products must be geometrically and dimensionally accu-
rate with high quality machined surface. Therefore, at this stage, further experi-
ments must be conducted taking novel machining strategies considering defocusing
conditions to remove the irregular micro-peaks from laser micro-turn surface
without much impeding the geometrical dimensions of machined parts. At defo-
cusing condition, due to enlargement of laser beam spot, the energy density of the
laser beam is reduced and the micro-peaks get sufficient energy to melt and
evaporate from the upper surface without affecting the base material. As it is not
possible to completely remove the micron-sized peaks from the surface in one pass,
therefore, multi pass laser micro-turning operation at various defocusing conditions
has been carried out and the test results were analyzed through graphical plots.
Figure 5.23 shows the schematic representation of scheme laser micro-turning
process for removing micro-peaks from laser micro-turn rough surface. The sche-
matic view of defocusing conditions of laser beam for machining micro-peaks from
rough surface is shown in Fig. 5.24. The defocus position is termed as upward
when the laser focus plane is above the workpiece surface, whereas defocus
position is termed as downward when the laser focus plane is inside the workpiece
or below the workpiece surface. As the present experimentation is dealing with
surface features, therefore, surface roughness (Ra and Rt) have been taken into
consideration as responses for the analysis. All the experiments have been carried
out at nearer feasible process parametric setting of RSM based multi-objective
optimization. Eight number of job surfaces were prepared at parametric combina-
tion of average power, pulse frequency, workpiece rotating speed, assist air pressure
and Y feed rate at 7.81 W/5600 Hz/436 rpm/0.30 kgf-cm−2/0.443 mm/s. The
5 Laser Micro-turning Process of Aluminium Oxide … 209
values of surface roughness (Ra and Rt) measured for these eight experiments are
listed in Table 5.12. These eight machined work samples were used for carrying out
experimentation by varying the two process parameters i.e. defocus positions and
number of passes. The values of these two process parameters are enlisted in
Table 5.13. For each focusing position, each experiment is carried out by increasing
the number of laser scan passes (up to 10). After conducting each experiment by
increasing the number of laser scan pass, the values of surface roughness (Ra and
Rt) were measured by the same surface roughness measuring instrument. The
variation of surface roughness values was graphically plotted and analysed.
The variation of surface roughness (Ra) with number of laser passes for upward
laser defocusing positions is shown in Fig. 5.25. From this figure, it is obvious that
210 G. Kibria et al.
Table 5.12 Results of surface roughness (Ra and Rt) machined at RSM based optimal parametric
combination during preparation of surface
Expt. Process parametric combination Experimental results
No Surface roughness
Ra (lm) Rt (lm)
1 Average power = 7.81 W 5.94 45.38
2 Pulse frequency = 5600 Hz 5.87 46.21
Workpiece rotating speed = 436 rpm
3 5.84 46.02
Air pressure = 0.30 kgf/cm2
4 Y feed rate = 0.443 mm/s 5.89 45.68
5 5.98 45.69
6 6.00 45.88
7 5.88 46.39
8 5.81 46.01
Table 5.13 List of parameters and different levels for defocusing experiments [24]
Process parameters Unit Values
Defocus conditions mm −0.2, −0.4, −0.6, −0.8, +0.2, +0.4, +0.6, +0.8
Number of passes – 1, 2, 3, 4, 5, 6, 7, 8, 9, 10
Fig. 5.25 Influence of number of laser scan passes on surface roughness (Ra) at various upward
defocus conditions [24]
surface roughness is decreasing with scan passes for all downward defocusing
conditions. With number of laser scan passes, the height of micron sized peaks
decreases due to removal of materials from the peaks. From this figure, it is also
5 Laser Micro-turning Process of Aluminium Oxide … 211
Fig. 5.26 Influence of number of laser scan passes on surface roughness (Ra) at various
downward defocus conditions [24]
revealed that for any value of laser scan pass, the surface roughness obtained are
different for various defocusing conditions. With higher value of defocusing,
roughness of machined surface is low due to finishing of irregular micro-peaks for
delivering adequate beam energy of laser. It is also obvious from the same figure
that at higher setting defocus, the surface roughness is high due to inadequate
energy density of laser beam that cannot reduce the height of micro-peaks.
In Fig. 5.26, the variation of surface roughness (Ra) with laser scan passes with
downward defocus conditions is shown in Fig. 5.26. From this graph, it is obvious
that with increase in scan passes, the value of surface roughness is decreasing due to
removal of micro-peaks from the surface. It is seen from the plot that surface
roughness again increases after certain number of laser scan passes. It is due to the
fact that the removal of irregular peaks from machined surface is reducing. At high
value of defocusing, the spot diameter of laser beam on the material is high and due
to this, the laser energy density is less. Due to this fact, the laser beam has incapable
for removal of micro-peaks from machined surface and consequently, the surface
roughness is high.
In Fig. 5.27, the variation in surface roughness (Rt) with laser scan passes is
shown for different values of upward defocus conditions. From this plot, it is
obvious that surface roughness (Rt) is decreasing for increasing value of scan
passes. As the laser scan pass is increasing, the total height of micro-peaks are
decreasing and this phenomena has direct effect on surface roughness (Rt) values.
For any particular value of laser scan pass, low value of defocus results in rough
machined surface and this is due to variation in energy densities of laser beam at
different defocus conditions. At high value of defocus i.e. at 0.8 mm, Rt is high
compared to other defocus conditions and this is due to less energy density at high
setting of defocus.
212 G. Kibria et al.
Fig. 5.27 Influence of number of laser scan passes on surface roughness (Rt) at various upward
defocus conditions [24]
Fig. 5.28 Influence of number of laser scan passes on surface roughness (Rt) at various
downward defocus conditions [24]
In Fig. 5.28, the variation in surface roughness (Rt) is shown with number of
laser scan pass at different downward defocus conditions. The graph shows that the
roughness of machined surface decreases up to definite value of scan passes. This is
due to decrease in overall height of micro-sized peaks on the machined surface. It is
seen from the plot that after few number of laser scan passes, there is no such
5 Laser Micro-turning Process of Aluminium Oxide … 213
Table 5.14 Results of parameter settings to obtain least surface roughness (Ra and Rt) values
Responses Parameter settings of average Parametric setting of Minimum value of
power, pulse frequency, additional parameters responses
workpiece rotating speed, air Number Defocus Surface Surface
pressure and Y feed rate of position roughness, roughness,
passes Ra Rt
Surface 7.81 W/5600 Hz/436 rpm/0.30 9 0.6 mm 5.07 lm 35.08 lm
roughness, kgf-cm-2/0.443 mm/s (upward)
Ra
Surface 8 0.4 mm 5.28 lm 34.65 lm
roughness, (downward)
Rt
improvement in surface roughness. At defocus positions of 0.4 and 0.8 mm, the
value of surface roughness slightly increases afterward 7th laser scan pass. It is also
obvious from the plot that the values of surface roughness obtained are random and
least value of Rt is achieved at 8th number of laser scan pass and at defocus
condition of 0.4 mm.
By analyzing various plots of Ra and Rt, it can be concluded that the values of
surface roughness (Ra and Rt) are decreasing with number of laser scan pass for all
values of upward defocus conditions. Moreover, it is also observed that with same
value of defocus condition, Ra values are decreasing, while the values of Rt are
moderately changing. In Table 5.14, the least values of surface roughness (Ra and
Rt) obtained at different parametric settings are enlisted. The minimum value of Ra
is obtained as 5.07 lm (corresponding Rt is 35.08 lm) for upward defocus whereas
the least value of Rt is obtained as 34.65 lm (corresponding Ra is 5.28 lm) for
downward defocus.
In the previous section, it has been found that the laser micro-turning process at
defocused positions have great influence for removing the micro-peaks from the
rough machined surface. In this section, an attempt has been made to comparative
study and analysis of laser micro-turning process at focused and defocused con-
ditions considering four process parameters such as laser beam average power,
pulse frequency, workpiece rotating speed and Y feed rate. In Table 5.15, the
details of constant and varying process parameters are shown. The target
micro-turning depth is same as 100 µm. All the experiments were carried out using
one factor at a time methodology. It is revealed from the previous section that
minimum surface roughness (Ra) is achieved at upward defocusing position.
Therefore, the present experimentation is carried out at focused as well as upward
214 G. Kibria et al.
Fig. 5.29 Effect of variation of average power on surface roughness (Ra) at focused and different
upward defocus positions
defocusing conditions. Surface roughness (Ra and Rt) were measured after con-
ducting each experiment and the test results were analyzed through various
graphical plots.
The variation of surface roughness (Ra) with laser beam average power for
focused and defocused (upward) positions is shown in Fig. 5.29. The constant
process parameters were pulse frequency at 5000 Hz, rotational speed of workpiece
at 400 rpm and Y feed rate at 0.4 mm/s. It is seen from this plot that the quality
surface is achieved at lower setting of average power. This is due to less amount of
material ablated from workpiece surface. However, with laser beam average power,
the roughness of machined surface increases. From this comparative graph, it is also
observed that the values of surface roughness are low for the machined surface
generated during laser defocused positions than focused condition. It is due to the
laser beam energy density to be low and consequently, adequate laser energy for
melting and evaporation is received by material surface which efficiently remove
5 Laser Micro-turning Process of Aluminium Oxide … 215
Fig. 5.30 Effect of variation of pulse frequency on surface roughness (Ra) at focused and various
upward defocus positions
micro-peaks generated on the surface. For a particular value of average power, the
values of surface roughness decreases with increasing value of defocusing and it is
only due to efficient removal of micro-peaks from the machined surface.
The variation in surface roughness (Ra) with laser pulse frequency at focusing
and defocusing positions is shown in Fig. 5.30. The average power, rotational
speed of worpiece and Y feed rate were kept at 8 W, 400 rpm and 0.4 mm/s,
correspondingly. The values of surface roughness (Ra) are found to increase
slightly at focused and defocused machining conditions. With increase in pulse
frequency, peak power is decreasing. However, the time duration between two
pulses is very short and the material from top surface gets adequate thermal energy
to remove the material rapidly creating higher peaks and valleys. From the same
plot, it is observed that the roughness values are less at same parameters setting
when machining is done at defocus positions when compared to focus position and
this is due to adequate thermal energy which is received on the material surface and
consequently, the height differences of peaks and valleys are less. When applying
higher setting of defocus during machining keeping other factors constant, it is
observed to obtain less value for surface roughness.
The variation of surface roughness (Ra) with increasing value of rotational speed
of workpiece at different upward defocus positions and focused condition is
observed in Fig. 5.31. The values of other process parameters were constant as
average power of laser beam at 8 W, laser pulse frequency at 5000 Hz and Y feed
rate at 0.4 mm/s. The plot shows that the roughness of micro-turning surface is less
at defocus conditions when compared with roughness value for focus condition
machining. As it is a known phenomenon that at defocus condition, the laser energy
density is reduced and therefore, the height differences of generated peaks and
valleys are less. With increase in rotating speed, it is seen that the roughness of
216 G. Kibria et al.
Fig. 5.31 Effect of variation of rotational speed of workpiece on surface roughness (Ra) at
focused and various upward defocus positions
Fig. 5.32 Effect of variation of Y feed rate on surface roughness (Ra) at focused and various
upward defocus positions
Fig. 5.33 Effect of variation of average power on surface roughness (Rt) at focused and various
upward defocus positions
at 400 rpm. The plot shows that the roughness of machined surface increases with
Y feed rate and this is due to decrease in circumferential overlap values for higher
values of Y feed rate. Due to this, the machined surface obtained as uneven and
irregular. Here also, it is seen that at focused condition machining, the surface
roughness value is high when compared to defocused conditions.
The variation of surface roughness (Rt) with laser beam average power at
defocus conditions and focused machining condition is depicted in Fig. 5.33. The
pulse frequency, rotational speed of workpiece and Y feed rate were kept constant
at 5000 Hz, 400 rpm and 0.4 mm/s, respectively. The plot shows that the roughness
of machined surface increases with average power due to generation of micro-peaks
on the material surface. At defocused position of laser beam, with constant value of
average power, surface roughness achieved as low compared to focus machining
condition. Moreover, for higher defocus values, there is no such effect of average
power on Rt values.
In Fig. 5.34, the graph shows the variation in surface roughness (Rt) with pulse
frequency at focused and defocused conditions while keeping the other process
parameters as constant at average power at 8 W, rotational speed of workpiece at
400 rpm and Y feed rate at 0.4 mm/s. From the plot, it is obvious that Rt has no
such variation with pulse frequency at defocused positions. However, at focused
condition, Rt is slightly increasing. The values of Rt is higher at all defocus con-
ditions compared to focused positional micro-turning.
The variation in Rt with respect to rotational speed of workpiece is depicted in
Fig. 5.35 at focused and different defocus positions. The constant parameters were
average power at 8 W, pulse frequency at 5000 Hz and Y feed rate at 0.4 mm/s.
The figure shows that the roughness of machined surface decreases with rotating
speed of work sample and it is due to increase in circumferential overlap with
218 G. Kibria et al.
Fig. 5.34 Effect of variation of pulse frequency on surface roughness (Rt) at focused and various
upward defocus positions
Fig. 5.35 Effect of variation of rotational speed of workpiece on surface roughness (Rt) at
focused and various upward defocus positions
rotating speed. The plot also shows that there is no such variation in Rt at defocus
conditions. The Rt values obtained is higher in focus positional micro-turning than
roughness at defocus positions.
The variation in surface roughness (Rt) with Y feed rate at various defocus
conditions and focused position is graphically shown in Fig. 5.36. The pulse fre-
quency was 5000 Hz, average power was 8 W and rotational speed of work sample
was 400 rpm. The graph shows that the Rt values are increasing with Y feed rate
5 Laser Micro-turning Process of Aluminium Oxide … 219
Fig. 5.36 Effect of variation of Y feed rate on surface roughness (Rt) at focused and various
upward defocus positions
(a) (b)
(c) (d)
(e) (f)
comparatively low. Moreover, the SEM micrograph shown in Fig. 5.37d shows low
degree of peaks and valleys on the machined surface compared to micrograph
shown in Fig. 5.37b. Comparing the SEM micrograph shown in Fig. 5.37b, d, f, it
is observed that the there are small amount of irregularities with some peaks and
5 Laser Micro-turning Process of Aluminium Oxide … 221
(a) (b)
(c) (d)
Fig. 5.38 Micrographs of the surfaces machined at average power, pulse frequency, workpiece
rotating speed and Y feed rate of a 7 W/4000 Hz/600 rpm/0.3 mm/s (Ra is 6.72 µm),
b 7 W/6000 Hz/300 rpm/0.3 mm/s (Ra is 6.18 µm), c 8 W/5000 Hz/400 rpm/0.5 mm/s (Ra is
7.77 µm) and d 8 W/5000 Hz/600 rpm/0.1 mm/s (Ra is 6.02 µm) [26]
(a) (b)
(c) (d)
(e) (f)
Fig. 5.39 Surface conditions of alumina machined at a, b defocus of 0.2 mm (downward) and
10th laser scan pass (Ra = 5.50 lm and Rt = 38.96 lm); c, d defocus of 0.8 mm (upward) and
10th laser scan pass (Ra = 5.26 lm and Rt = 36.34 lm) and e, f defocus of 0.6 mm (upward)
and 10th laser scan pass (Ra = 5.10 lm and Rt = 34.91 lm)
(a) (b)
resolidified material
micro-peaks
(c)
Fig. 5.40 Magnified SEM graphs of surface machined at a defocus of 0.2 mm (downward) and
10th laser scan pass, b defocus of 0.8 mm (upward) and 10th laser scan pass and c defocus of
0.6 mm (upward) and 10th laser scan pass
(a) (b)
Fig. 5.41 Quality of machined surfaces at average power at 8 W, rotational speed of workpiece at
400 rpm, pulse frequency at 5000 Hz and Y feed rate at 0.4 mm/s at a focused condition
(Ra = 5.46 lm and Rt = 33.6 lm) and b defocused position (Ra = 5.1 lm and Rt = 31.4 lm)
The exhibited SEM images shown in Fig. 5.41a, b represent the machined
surface obtained at focused condition (Ra and Rt were obtained as 5.46 and
33.6 µm) and 0.6 mm defocused position (Ra and Rt were obtained as 5.1 and
31.4 µm) at parametric combination of laser average power at 8 W, pulse frequency
at 5000 Hz, rotational speed of work sample at 400 rpm and Y feed rate at
0.4 mm/s. By comparing these values of surface roughness as well as observing the
SEM images, it is concluded that the machined surface obtained at defocus con-
dition is much better in quality than machined at focused conditional machining.
Furthermore, there are lot of micro-peaks found on the machined surface generated
at focused condition than obtained in defocused positions.
5.10 Conclusions
In the present chapter, the capability of pulsed Nd:YAG laser for carrying out laser
micro-turning operation on difficult-to-machine 99% pure aluminum oxide (Al2O3)
ceramic has been investigated in-depth through various machining strategies and
experimental schemes. Through various experimental schemes and novel machin-
ing strategies, it is found that pulsed Nd:YAG laser has the potential to achieve
desired micro-turn depth and surface finish of the cylindrical aluminum oxide
(Al2O3) workpiece by proper controlling the process parameters. Moreover, for-
mulations of spot and circumferential overlaps have been done and effect of overlap
factors on machined surface criteria were studied to achieve accurate geometrical
dimensional parts with desired surface features. The outcomes of the present
research based on various experimental schemes in the area of the pulsed Nd:YAG
laser micro-machining of advanced ceramic material will be effectively utilized to
predict the surface conditions and dimensional features to fulfill the urgent
requirement for high precision micro-machining and micro-fabrication of ceramic
materials. Furthermore, author trusts that the research findings will definitely
5 Laser Micro-turning Process of Aluminium Oxide … 225
Acknowledgements The authors acknowledge the financial support and assistance provided by
CAS Ph-IV programme of Production Engineering Department of Jadavpur University under
University Grants Commission (UGC), New Delhi, India.
References
18. Chryssolouris G (1991) Laser machining: theory and practice. Springer-Verlag, New York
19. Dubey AK, Yadava V (2008) Experimental study of Nd:YAG laser beam machining—an
overview. Journal of Materials Processing Technology 195:15–26
20. Dahotre NB, Harimkar SP (2008) Laser machining and fabrication of materials. Springer
Science, New York
21. Chrysolouris G, Bredt J, Kordas S, Wilson E (1988) Theoretical aspects of a laser machine
tool. Journal of Engineering for Industry 110(1):65–70
22. Kruth JP, Yasa E, Vanparys M, Vaerenbergh JV (2007) The enhancement of
micro-machining ability of selective laser melting by selective laser erosion. International
Conference on Polymers and Moulds Innovations, PMI Gent, Belgium
23. Thawari G, Sundar JKS, Sundararajan G, Joshi SV (2005) Influences of process parameters
during pulsed Nd:YAG laser cutting of nickel-base superalloys. Journal of Materials
Processing Technology 170(1–2):229–239
24. Kibria G, Doloi B, Bhattacharyya B (2015) Investigation and analysis on pulsed Nd:YAG
laser micro-turning process of aluminium oxide (Al2O3) ceramic at various laser defocusing
conditions. The International Journal of Advanced Manufacturing Technology 76(1–4):17–27
25. Kibria G, Doloi B, Bhattacharyya B (2013) Predictive Model and Process Parameters
Optimization of Nd:YAG Laser Micro-turning of Ceramics. International Journal of
Advanced Manufacturing Technology 65(1–4):213–229
26. Kibria G, Doloi B, Bhattacharyya B (2014) Investigation into the effect of overlap factors and
process parameters on surface roughness and machined depth during micro-turning process
with Nd:YAG laser. Journal of Optics and Laser Technology 60:90–98
Chapter 6
Fiber Laser Micro-machining
of Engineering Materials
Abstract In the present era, fiber lasers have been successfully replacing Nd-YAG
and CO2 lasers along with other conventional laser systems for various
micro-machining applications such as micro-cutting of stents, thin sheet of ferrous
and non-metals in terms of cutting speed, cut edge quality and the length of micro
cracks. The usage of fiber laser can also be observed in field of micro-machining of
various engineering materials owing to the characteristics of short pulse lengths
which range from millisecond to picosecond or even femtosecond. The present
chapter aims to carry out an in depth study of the fiber laser micro-machining, i.e.,
micro-cutting, micro-drilling, engraving, marking, etc., of engineering materials
ranging from polymer to ceramics. The aim of the chapter is also to include an
overall concept of fiber laser micro-machining system in the present scenario and its
applications along with the occurring physical phenomena and influence of various
process parameters on the fiber laser generated micro-features.
6.1 Introduction
Fiber laser, since its inception in 1961, moved along the path of technological
advancement from the developments of high power diode lasers, low loss doped
glass fiber, diode-fiber coupling devices, Bragg gratings, etc. [3]. A simple fiber
laser can be constructed by placing a fiber amplifier inside a cavity designed to
provide optical feedback. Laser is generated by pumping the diodes to excite lower
energy molecules to the excited states. Fibers, having one core and one cladding
along with the protective coating, are usually made of silica glasses for the purity.
The propagation of the lasing mode is in the core, whereas, the propagation of the
pump beam is by the outer layer cladding. The primary function of the outer layer
cladding is to confine the pump light, which allows the pumping of the core with a
high power beam. Fiber glass usually has a higher refractive index core which is
followed by a low refractive index of the cladding. Further, this particular property
of the outer layer cladding converts pump light of relatively low brightness to a
6 Fiber Laser Micro-machining of Engineering Materials 229
aperture-higher the broad light of acceptance. The light propagation into the fiber
itself is dependent on five characteristics; (a) fiber type, (b) fiber size, (c) numerical
aperture, (d) refractive index and (e) doping of the fiber. Fiber Bragg gratings act as
mirrors which also control the amount of reflections for a particular wavelength.
The combination of fiber with Nd3+, Yb3+ etc., along with the fiber Bragg gratings
form the base of a fiber laser. The wavelength of the reflected light is determined by
the longitudinal period of the grating and the percentage of the reflected radiation is
controlled by the magnitude of the refractive index [3]. Fiber lasers reflect the light
through the optical cavity so that the string of photons stimulates the atoms to store
and release the light energy by means of useful wavelengths. The photons absorbed
by ytterbium ions, may disappear. The electrons moving around the atomic nucleus
move to the higher orbit by absorbing energy. Pumping is a process by virtue of
which the energy is injected and stored by the fiber. Within a millisecond, the
stimulated electrons drop to ground states (for example, drops to 1064 nm in the
case of infrared laser system). In order to maximize the coordination of pumping
and emission, the fiber cavity resonator is formed [3]. At the pump end of the
cavity, a high reflector fiber Bragg grating is sliced to the fiber doped with the
ytterbium atoms. However, at the output end, a similar kind of Bragg grating with a
modest reflectivity is installed. A schematic representation of the fiber laser
structure is represented in the Fig. 6.2.
As a result of the above mentioned phenomenon, the light which propagates
along the fiber, stays with the fiber. Such a design of the fiber laser is termed as a
monolithic device. The length of the doped fiber is important as it determines the
amount of light that can be absorbed within the fiber. The long length of the fiber
results in a high surface to volume ratio, which aids in removing the excessive
amount of heat from the fiber. Usually, fiber laser has an absorption length, which is
95% of the pump energy [5].
The number of diodes for pumping is dependent on the output power of the fiber
laser. Large numerical aperture diodes with high power along with the larger
diameter output fiber are the most preferable for the construction of the high power
fiber laser. In the recent years, invention of double clad fiber lasers leads to fiber
lasers with high power, greater electrical efficiency and astoundingly high bright-
ness. Double clad fiber lasers have higher numerical aperture and larger in diameter
as compared to the single mode fiber lasers. When the laser is assembled and
pumped power to the diode, much of pump light passes down the cladding without
intersecting the dopant ions in the core of the fiber. Without the intersection and
Fig. 6.2 Schematic representation of fiber laser structure inside the laser head
6 Fiber Laser Micro-machining of Engineering Materials 231
Fiber laser power output up to 1 kW range are most desirable for material pro-
cessing applications, such as metal cutting, welding, brazing and marking [7]. In the
present era, ultrafast fiber lasers, based on passive mode-locked fiber oscillators,
have been dominating both the industrial and scientific realms. The amplification
during the several stages of ultrafast fiber laser generation and beam deliver system
have allowed them to reach at the desired output pulse energies. A large variety of
fiber components rely on all-fiber systems to be constructed rather being utilized
only for the beam delivery system. Core diameters of a conventional rare earth
doped fiber amplifiers are typically in the range of 5–10 lm. Chirped pulse
amplification (CPA) technique for ultrafast fiber laser systems, is a new design
concept designed for preventing nonlinear processes in the fiber amplifiers for better
utilization in various micro-machining applications [8, 9]. Over the years, the fiber
mode area has undergone several modifications to achieve a continuous increase in
achievable pulse energies.
In general, fiber laser can be broadly classified into two types: (a) continuous
fiber laser and (b) pulse fiber laser. Fiber laser can be further classified into single
frequency fiber laser, Q-switched fiber laser and mode locked fiber laser.
A continuous fiber laser consists of high reflector (HR) and output coupler
(OC) along with fiber Bragg gratings [10].
Usually, a single-frequency fiber laser is pumped by a single-mode pump diode
in order to obtain an output power, ranging from a few tens up to hundreds of
milliwatts. In Q-switched fiber lasers, longer pulses are obtained in longer fibers.
However, if the pulse duration becomes longer than round-trip cavity time, pulse
breakup may occur. On the flip side, optimal utilization of the intrinsic cavity mode
structure in an optical fiber oscillator is utilized by the mode locked fiber laser, in
order to produce short pulse, as depicted in the Fig. 6.3. In the recent years,
232 A. Sen et al.
Fig. 6.3 Schematic representation of a mode locked fiber laser with acousto optic modulator
The importance of fiber laser system for the micro-machining domain is inevitable.
Fiber lasers are ideally suited for the generation of micro-features required for the
bio-medical applications, electronics industries, automotive and aerospace indus-
tries. The importance of fiber laser for the fabrication of micro-features on a wide
range of engineering materials lies in its characteristic features. The astounding
features of fiber laser such as compactness, elimination of complex cooling systems,
excellent constant beam properties, long focal lengths, and rapid warm-up make it
ideal for the applications in the aforesaid manufacturing industries. Fabrication of
stents and seam welding pacemakers and implantable batteries for medical appli-
cations are fewer possibilities of the fiber laser [11].
The laser beam quality is determined by the wavelength, beam waist radius along
with far-field divergence and further, it is defined by M2 value. Further, the highest
beam quality lasers will be defined as M2 close to 1. The high quality laser beams
are formed due to the long and thin gain medium. Fiber lasers which are com-
mercially available are high quality beams ranging up to a few kW.
6 Fiber Laser Micro-machining of Engineering Materials 233
The primary characteristics of the high quality beams are that, it can be focused
on a small spot on the workpiece, providing high power density thereby leading to
faster processing time. Compared to the other laser technologies, fiber laser beams
have a longer focal length (working distance) along with greater depth of focus
(workpiece positioning tolerance) [11]. Further, the beam diameter can be smaller if
there is a fixed focal length and focus spot size. Therefore, a larger area of
parameter space is achieved because of the high beam quality and hence, the optical
parameters for a process are easily optimized.
The wall plug efficiency of a laser is defined by the ratio of the electrical power
efficiency to optical power efficiency. High wall plug efficiency around 25–30% can
be achieved for the fiber lasers due to the high efficiency of the pump source and the
extraction from the gain medium. Therefore, this not only involves lower operating
cost but also requires reduced electrical supply along with reduced cooling
requirements which is up to 300 W, compact laser head design.
Further, fewer mechanical components are required in the construction of the
laser as compared to the other solid state lasers. This invariably helps the fiber laser
to be cost competitive compared to the other kW class, such as CO2 lasers, as used
in several flat-bed cutting applications.
Fiber Laser products in the present market are offering 100,000 h MTBF (mean
time before failures) for their pump sources which is equivalent to over 11 years of
operation in total [11]. At present, the fiber laser products have demonstrated over
40,000 h of operation already and they are still being used today, owing to its high
reliability. Therefore, it will be difficult for any industrial technology to currently
replace any laser diodes primarily due to the cost and time effectiveness of the
system. Another interesting feature that adds a feather in the cap of the diode
pumped fiber laser system is the low routine maintenance. This feature is primarily
because of its all fiber construction, which means that no beam delivery optics or
alignment of the resonator is required. In addition to this, minimum or almost no
cooling system is required for the running of the fiber laser system as compared to
Nd-YAG laser system.
Apart from being highly reliable and cost effective, fiber lasers possess easy
operating features that are the light that generates inside the fiber, delivers to the
234 A. Sen et al.
work material within the fiber. This particular phenomenon enables a stable setup
and eradicates any issue relating to the number of beam delivery mirrors or prob-
lems arising out of coupling laser beam into a beam delivery fiber.
The working range of the fiber laser is either in the near infrared (NIR) or infrared
region (IR). Fiber laser micro-machining process is based on the interaction of the
laser light with the top surface of the working material in order to remove a small
amount of material from the surface. It is a well known fact that the photon energy
is inversely proportional to the laser working wavelength, i.e., shorter the
wavelength-higher the photon energy. When the working wavelength (1064 nm) of
the fiber laser is shortened either to the first order harmonic wavelength (532 nm) or
second order harmonic wavelength (264 nm), the thermal process changes into a
chemical process, which eventually break the bonds of the workpiece material [12].
As a result of this, fiber laser micro-machining process can be classified into two
distinct features, i.e., photo-thermal process and photo-chemical process.
Photo-thermal processes are identified mostly in metals, ceramics, alloys, etc.
Photo-thermal processes are characterized by a rapid thermal cycle, heating, melting
and partly evaporation of the heated volume [13]. Whereas in photo-chemical
process, the photon energy is sufficient enough to break the chemical bonds, which
is mostly suitable for polymers and plastics.
Fiber laser micro-machining process for various engineering materials ranges
from nanosecond regime to femtosecond regime. Depending on the laser-material
interaction time, the micro-machining quality is varied. Based on the laser-material
interaction time regime, three processes can be distinguished. In all the three pro-
cesses, first, absorption of the photon by an electron occurs and then the rest of the
set of other physical steps are varied depending on the time regime. In nanosecond
ablation of the materials (for metals), the absorbed laser energy first, heats the
workpiece to its melting point and further to the vaporization temperature. During
the interaction time, the loss of energy is associated with the heat conduction into
the solid material. Nanosecond pulse ablation is associated with the detrimental heat
affected zone (HAZ) which can be partially overcome by picosecond ablation. In
picosecond ablation, the pulse length is in the same order during the time of
transferring the energy from the electrons to the lattice. However, the picosecond
ablation also suffers from a considerable amount of evaporation and the formation
of the melted zone inside the material [13]. This pertinent problem can be com-
pletely eliminated by femtosecond ablation as no time is available for the heat
transfer to the lattice during this series of processes in femtosecond ablation. This
results in no heat affected zone and precise micro-machining characteristics.
6 Fiber Laser Micro-machining of Engineering Materials 235
In the field of medical sciences, fiber laser micro-cutting process has been widely
accepted process instead of lamp pumped pulsed Nd-YAG lasers. Manufacturing of
medical devices is a daunting task because of their relatively small size, use of
expensive materials and ability to fit into small areas. In this scenario, fiber lasers
can operate in the areas which can tolerate the power of only a few microns for
being an effective solution for costly and smaller devices.
Fiber laser micro-machining has emerged through the micro-cutting of cardio-
vascular stents over the years. Fiber lasers have obtained a decent market share in
the present era, in the field of fine and precise micro-cutting which combines both
continuous mode as well as pulse mode, aided by fusion cutting (inert gas to
sublimation cutting) [14]. Fiber lasers are commonly employed in thin material
cutting, whereas the other solid state lasers and gas lasers such as Nd-YAG and
CO2 lasers are mostly utilized for the thick material cutting. Although, experimental
studies carried out by Olsen et al. [15] demonstrated that the fiber laser cutting
efficiency for thick materials is better than that of a CO2 laser. Comparative
experiments were conducted by Kleine et al. [16] and Meng et al. [17] in order to
analyze the quality of cutting between the fiber lasers and the Nd-YAG lasers. The
result of the analysis was that, with the fiber laser cutting, cut quality was com-
paratively better than the Nd-YAG lasers, i.e., in terms of roughness, heat affected
zone (HAZ) and kerf width. The number of research works employing fiber laser in
order to micro-machining of difficult to machine materials with the aid of fiber laser
systems, is increasing rapidly in the recent years. Fiber laser ablated micro-holes in
various super alloys such as Ti-6Al-4V, nickel super alloys are utilized for various
automotive and aerospace applications.
Fiber laser marking process is one of the key areas that have emerged through
the marking of electronic goods to the daily household products. Hard coated
plastic cases have been adopted by several manufacturers in order to provide
scratch resistance. However, laser marking over such surfaces without damaging it
is typically daunting task because in this case, a précised balance between the peak
power, average power as well as the pulse energy has to be maintained. As a result
of this, fiber lasers are replacing green [18] and other ultrashort lasers which are not
cost effective compared to the fiber lasers.
An increase in the touch screen usage has created a more functional thin-film
processing application for fiber laser systems. Multi-pass processing enables this
application, where the initial pass removes the bulk of the film and the secondary
passes cleanses the residues by using a combination of different process parameters,
short pulses, high pulse frequency and high speed. Fiber lasers have the ability to
change the parameters such as pulse energy, pulse duration within few microsec-
onds. Controlled heating characteristics that provide better and faster marking can
be obtained by the use of long duration pulses and high repetition rates. These long
duration pulses and high repetition rates strongly resemble gated continuous wave
236 A. Sen et al.
pulse fiber laser than the high peak power nanosecond pulses. Fiber laser engraving
is another emerging area of fiber laser in the field of micro-machining. Other key
features of fiber lasers are hallmarking, texturing, and personalized marking on a
wide range of precious materials.
The power supply unit consists of a 1.5 kVa of isolation transformer and 1 kVa of
uninterruptible power source (UPS). The isolation transformer is connected with the
main power supply unit and the UPS is connected to the isolation transformer. The
pumping of laser diodes inside the laser head is achieved via the power supply unit.
The diode pumped fiber laser system is comprised of a fiber itself doped with Yb3+,
fiber Bragg grating and number of diodes. The number of laser diodes is dependent
on the total output power of the system. A total number of 8 diodes are utilized in
the present system for pumping. Fiber Bragg gratings are sliced into two ends of the
fiber optics so that the laser can be generated. The total length of the fiber can be up
to 3 mm depending upon the output power generated by the fiber laser.
6 Fiber Laser Micro-machining of Engineering Materials 237
6.2.3 Collimator
After the generation of the laser within the optical fiber, the laser is transferred into
a collimator. In the collimator, two prisms are fitted at the two ends of it. This
collimator acts as a beam expander, i.e., the laser can propagate to the required
distance. The diameter of the laser beam is 9 mm at the end of the collimator.
After the collimator, a beam bender with 100% reflectivity is placed at an angle of
45º with the horizontal plane so that the laser can be perpendicular to the focus lens.
At the top of the beam bender, a charge couple device camera (CCD) is placed
which is further connected to a CCTV.
238 A. Sen et al.
The laser finally propagates through a f-h lens of 71 mm of diameter (focus lens)
which is protected by a nozzle for preventing against dust and other contaminations.
The spot diameter of the fiber laser beam is 21 µm. The laser beam falling on the
surface from the focusing lens has to be précised and appropriately aligned. If the
center of the lens does not coincide with the beam center, then the beam that will
pass through the lens will not be linear, resulting in low energy of the laser beam
and less micro-machining efficiency. CCTV and CCD camera are the two units
used for focusing. At the top of the laser head, the CCD camera is placed in order to
capture the image during the operation of the laser micro-machining. Further, the
beam should also be focused on the surface so as to receive optimum
micro-machining operations.
The function of the CCTV is to adjust the position of the focused beam on the
workpiece. This device is connected to the CCD camera so as to obtain précised
laser beam focusing condition. After the laser beam is appropriately focused, the
material melts at a faster rate and thereby evaporates. This is the reason why the
focal point position of the laser beam should be properly adjusted. A CNC con-
trolled arrangement is provided in the experimental setup, in order to effectively
adjust the focal point of controlling the lens movement position along the Z axis.
Inert gases such as nitrogen, argon, helium, etc., along with compressed air can be
supplied through a co-axial nozzle attached to the beam delivery system depending
upon the selection of micro-machining process and materials. The jet flow of
assisting gas assists in removing the molten material from the ablated surface to
partially overcome re-solidification of the molten material from the
micro-machining zone. If any compressed air flow is required, then the supply line
must pass through a moisture separator and should be connected further to a
pressure regulating valve. It results in the jet flow of dry pressurized air to the laser
micro-machining zone. The laboratory setup has a vacuum job fixture which can
hold a workpiece up to 1 mm of thickness when the compressed gas pressure is
4 kgf/cm2.
A CNC controller unit not only controls the movement of the worktable along the
X-Y axis, but also controls the movement of the laser nozzle along the z axis. Servo
motors are attached to each of the axis and are also connected to the servo
6 Fiber Laser Micro-machining of Engineering Materials 239
interfacing unit. This servo controller is connected to the computer system (inter-
face software-I mark plus) from where the axis movements of the X–Y worktable
are controlled. If any movement of the X, Y or Z axis is required, then the computer
system sends a command to the servo interfacing unit which is followed by
receiving a command for the respective servo motor movement in the specific
directions.
The axis of the fiber laser system can be governed by either CNC based motor
system or galvanometer type motor system, depending upon the applications of the
fiber laser systems. For marking and scribing applications, a galvanometer type
system is most preferable. In contrast to the aforesaid system, CNC based system is
well recognized for cutting, drilling and various micro-machining applications.
Generally, in CNC based fiber laser systems, the table can only move in the X–Y
direction, whereas the laser head can only travel in Z direction. In a sharp contrast,
galvanometer type laser systems rely only on the movement of the laser head in
X-Y-Z direction. As a result of this, scanning speed can be very high, sometimes
even up to 3000 mm/s. In the aforesaid fiber laser micro-machining system, a CNC
type system is utilized where the maximum cutting speed ranges up to 70 mm/s.
Although, for the optimum results of the system, maximum cutting speed of
40 mm/s can only be utilized.
6.3.1 Micro-cutting
Okamoto et al. [20] partially tried to overcome dross free fiber laser micro-cutting
of a copper plate of 100 µm of thickness in the presence of nitrogen assists gas with
the aid different set of nozzles. It can be summarized from the experimental results
that not only the maximum cutting speed varied with the different set of nozzles, but
also straight cut profiles were achieved with minimum HAZ. Another investigation
on laser cutting of various micro-patterns on carbon fiber reinforced polymer
(CFRP) with a continuous wave fiber near-IR laser (k = 1090 nm) to achieve
précised cutting of CFRP, devoid of debris and thermal damages around the
grooves was conducted by Niino et al. [21]. A fast beam galvanometer scanning
process with the multiple-scan-pass method was conducted along with the fiber
laser irradiation on CFRP. The observations that were made out of the experiment
was that, fine cutting of 3 mm CFRP sample at fiber laser irradiation with a 15
multiple-scan-pass (scanning speed: 0.8 m/s) was free of debris and other thermal
damages around the periphery of the micro-machining zone. Further, around
600 µm of the kerf width of the groove on the laser beam incident surface was
observed. Thin film solar cell micro-machining with the aid of high power ultra-
short fiber laser was carried out by Lecourt et al. [22], where the pulse repetition
rate was varied from 100 to 1 MHz. Another set of comparative study [23]
showcased the advantages of using bursts of picosecond pulse for micro-machining
of materials compared to the nanosecond source, having the same pulse energy
along with pulse width and pulse shape. The result of the experiment was satis-
factory when bursts of picosecond pulses were used, as the material removal along
with the surface quality was as high as 25% and more in comparison to the
nanosecond pulses having the same pulse energy along with the combination of
pulse width and pulse shape.
In a set of comparative study, femtosecond pulsed micro-machining with
1.56 µm erbium-doped fiber-laser oscillator-amplifier system along with direct
amplification and pulse extraction was carried out by Mizunami et al. [24]. For the
pulse extraction and amplification, a peak power, as high as 25 kW was obtained.
Further, with the process of pulse extraction and amplification, a 6 µm trace of
ablation was observed on an amorphous carbon film. The experimental result was
narrower than that of 16 µm of direct amplification. On the flip side, when
6 Fiber Laser Micro-machining of Engineering Materials 241
polyvinyl chloride film underwent micro-machining with the aid of a fiber laser, it
was observed that direct amplification was more suitable and a cutting width as low
as of 4 µm was obtained from the experiment. Further, for an increased repetition
rate of 100 kHz, optical damage was observed to be less, owing to the lower peak
power of the fiber laser. However, the same phenomenon was not observed in the
case of direct amplification. Another study of precise laser micro-machining on
multiple layers of ceramic/metal (thermal barrier coated super alloy) was conducted
by Qi et al. [25]. In this experiment, an industrial-grade economic nanosecond
pulsed fiber laser was utilized in order to study the relationship between the process
parameters and machining geometric features of stainless steel (SS) 304, copper,
Inconel 718 and TBC coating samples. It was found that the depth of the trench was
dependent on the laser peak fluence in a logarithmic relation. When the beam waist
was 50 µm for SS304 and 30 µm for copper, the volume removal rate was high. It
was also observed that a similar trend was followed by the finite element model
(FEM) model predicted volume removal rate along with the beam waist variation.
Finally, for TBC coating, fiber laser micro-machined surface roughness using laser
scanning was measured 5.96 µm (Ra), whereas for Inconel 718, surface roughness
turned out to be 7.32 µm (Ra).
The most promising possibility of fiber laser in the field of bio-medical lies in
profile cutting for cardiovascular stent, which is a lattice-shaped metal tube which is
utilized for the implantation into arteries [26]. Cardiovascular stents can be made of
various materials such as nickel titanium (NiTi) alloy, stainless steel. Liu et al. [27]
analyzed the effect of fiber laser process parameters such as surface roughness, kerf
width, heat-affected zone (HAZ) and formation of dross for the fabrication of
vascular stent on NiTi alloy tube of outer diameter of 1.8 mm and wall thickness of
240 µm. The experiments were performed with the continuous water flowing
through the inside walls of the tube in the presence of argon as an inert gas
(constant pressure of 0.45 bar). It was observed that due to the wet cutting con-
ditions, pure striation topography was not formed. The optimum choice was the
mixed topography striation ratio for the micro-cuts having lower surface roughness,
low kerf width and corresponding small recast layer than the micro-cuts bearing
other topographies. Kerf width geometry was influenced by the power density. An
increment in the power density causes an increase in pulse energy. This in turn
resulted in the increment of the kerf width dimensions. The entry cut width was
found to be wider than 30 µm or even 35 µm, when the power density varied from
2900 to 8000 J/nm. Further, at an intermediate power density along with the low
cutting speed, smallest entry width of 25.53 µm could be achieved. On the other
hand, at high power density followed by fast cutting speed, entry kerf width was
obtained which was 38.59 µm (maximum dimensions for the kerf width). With the
increase in the power density, it was also observed that the surface roughness along
with the kerf width had the tendency to increase. However, with the settings of
242 A. Sen et al.
different combinations of the aforesaid parameters, the results varied. Further, it was
observed that the cutting speed was the most critical parameter for obtaining good
surface finish compared to the other process parameters. In addition to this, surface
topographies also varied with the cutting speed, while keeping the power density as
constant. Spot overlapping factor determines the uniformity and smoothness of the
micro-machined profiles, i.e., higher the spot overlapping factor-higher the uni-
formity and smoothness of the profiles. Cutting speed is also associated with the
spot overlapping factor [14]. When the cutting speed is high, the spot overlapping
factor is low. The phenomenon reverses back with the increment in the cutting
speed. Meng et al. [17] utilized a 50 W fiber laser system for the micro-cutting of
316L stainless steel tube (thickness 110 mm, diameter 2 mm) cardiovascular stents
in order to observe the effects of various micro-cutting parameters including laser
output power, pulse length, repeat frequency, cutting speed and assisting gas
pressure on the kerf width profiles. The kerf width was the primary function of the
cutting speed in order to obtain different laser power outputs. The repeat frequency
was observed to be 1500 Hz, followed by 0.15 ms of pulse lengths along with
0.3 MPa of assisting oxygen gas pressure. The kerf width dimensions increased
with the increment of laser output powers owing to high power density. The
phenomenon reversed back when the cutting speed increased, because of the low
power density. The kerf width size also increased when both the pulse length and
repeat frequency were increased. It was observed that the kerf width was less than
20 µm along with low roughness and HAZ when the fiber laser process parameters
were, laser output power of 7 W, pulse length of 0.15 ms, the repeat frequency of
1500 Hz, cutting speed of 8 mm/s and assisting oxygen pressure 0.3 MPa. Another
experiment carried out by Muhammed et al. [28], showed the effect of both wet and
dry 316L stainless steel with the aid of fiber laser system. It was concluded from the
experiment that in the case of wet stainless steel cutting, the results were com-
paratively better in terms of narrower kerf width along with low surface roughness,
less dross, no back wall damages and smaller HAZ. All these positive features
would lead to lower cost of post-processing of the material. In order to control the
micro-cutting quality, low average power with the combination of low pulse width,
play a significant role. To achieve high aspect ratio profiles, pulse width should be
lower in order to increase the laser beam penetration rate. However, this in turn will
lower the pulse energy irradiated on the workpiece. The controlling of all the
process parameters is critical and can be achieved by the extensive research works.
6.3.2 Micro-grooving
Laser grooving process can be characterized by the jet flow of gas in order to
remove excessive amount of molten material from the micro-grooved zone. The
characteristics of three-dimensional heat transfer, moving boundary, a multi-phase
and spatially distributed heat source are associated with the fiber laser
micro-grooving process [29]. Sen et al. [14] carried out a total of 49 experiments of
6 Fiber Laser Micro-machining of Engineering Materials 243
Fig. 6.5 Microscopic view of the micro-groove width at different number of passes [14]
6.3.3 Micro-channeling
Laser ablated micro-channels are growing field of interest for the fabrication of
micro-fluidic channels not only in the bio-medical applications, but also in micro
electrical mechanical systems (MEMS). Fiber laser technology has moved away
beyond the growing interest for the fabrication of micro-fluidic channels using
nanosecond pulse or picosecond pulse fiber laser systems. Sen et al. [31]
244 A. Sen et al.
Fig. 6.6 Microscopic view showing the widths of the micro-channel profile at 50 mm/s of scan
speed, 15 W of average power, 50 kHz frequency and number of pass of 1 [31]
successfully facilitated a multi diode pumped infrared fiber laser system to fabricate
micro-fluidic channels on polymethyl methacrylate (PMMA). Scan speed of
10–300 mm/s, pulse frequency of 50–90 kHz, average power of 5–15 W and
number of passes of 1–5; were considered for the utilization of fiber laser in this
domain. The author found some of the micro-channel profiles having high aspect
ratios such as 2.34, 2.06 and 0.87. In addition to this, the waviness of the
micro-channel profiles along with HAZ width was found to be less for some of the
micro-channeling conditions. However, some of the micro-channel profiles suffered
from the uniformity and re-solidification along the micro-channel profiles which is
shown in the Fig. 6.6. Sen et al. [32] also carried out sensitivity analysis of the
process variables (scan speed, pulse frequency, number of passes and average
power) considered for the fiber laser ablated micro-channel profiles on PMMA. The
sensitivity analysis revealed that pulse frequency was the most critical parameter for
obtaining desired width and depth dimensions on PMMA. The sensitivity of the
other three process parameters, i.e., scan speed, laser average power and number of
passes on the depth dimensions were found out to be negative. The author suc-
cessfully facilitated infrared fiber laser micro-machining system for the fabrication
of micro-features on polymer materials.
6.3.4 Micro-drilling
Pulsed mode of fiber laser system is quite suitable for micro-drilling of high ductile
and brittle materials also. Many research works are being carried out in this area and
the results are being discussed as follows.
From the past research works, it is evident that sputtering along with other
metallurgical defects such as cracks, morphological irregularities are always asso-
ciated with the laser micro-drilling process owing to the rapid solidification of the
molten materials [33]. In this regard, Biffi et al. [33] carried out percussion
micro-drilling of commercially pure titanium sheets having 0.5 mm of thickness
6 Fiber Laser Micro-machining of Engineering Materials 245
Fig. 6.7 SEM views of drilled holes according to the two boundary process conditions: a entrance
at pulse frequency of 20 kHz and pulse energy of 0.5 mJ; b exit hole at pulse frequency of 20 kHz
and pulse energy of 0.5 mJ; c entrance at pulse frequency of 50 kHz and pulse energy of 1.2 mJ;
d exit hole at pulse frequency of 50 kHz, and pulse energy of 1.2 mJ [33]
with the aid of nanosecond pulsed fiber laser system. Figure 6.7 depicts the
obtained entrance and the exit holes at the two limit process conditions along with a
maximum average power (pulse frequency of 20 kHz, pulse energy of 0.5 mJ) and
a minimum average power (pulse frequency of 50 kHz, pulse energy of 1.2 mJ). An
annular corona of melted material was observed at both the entrance holes, but on
the other hand, the exit holes were almost devoid of drops and sputter (Fig. 6.7b, d).
They successfully demonstrated high aspect ratio sputter free holes on the exit side,
although the entry side holes suffered from a considerable amount sputter.
When ultrafast fiber laser percussion micro-drilling of high purity copper
(99.9%), stainless steel (Fe/Cr18Ni10) and high-carbon steel (C 1095) sheets with
0.25-mm thickness each [34] were utilized, the results were satisfactory compared
to Q-switched nanosecond laser. However, the overall accuracy of the ablated
structures was not as good as compared to the femtosecond laser micro-drilling of
aforesaid materials. Ghosal et al. [35] identified that wait time and modulation
frequency were the most important parameters for the material removal rate
(MRR) during the micro-drilling of Al/Al2O3-MMC by a ytterbium doped fiber
laser system. The authors concluded that the material removal rate increased with
an increase of N2 gas pressure and maximum material removal rate observed within
246 A. Sen et al.
6.3.5 Engraving
The number of research works on engraving process with the aid of fiber laser, is an
emerging field of interest. An engraving operation was carried out on C45 carbon
steel by Genna et al. [38], where, a Q-Switched 20 W Yb: YAG fiber laser with the
fundamental wavelength of k = 1070 nm was utilized, in order to study the
influence of process parameters on surface roughness along with the material
removal rate (MRR). The engraved depth was found out to be highly dependent on
the scan speed, pulse frequency along with the scan number. It was also observed
that the line spacing, pulse frequency along with the scan speed governed the
surface roughness of the engraved profiles. However, after around 10 scans, the
surface roughness remained unaltered with the combination of aforesaid parame-
ters. It was summarized that the selection of appropriate and accurate process
conditions would lead to higher values of MRR and better surface roughness.
Finally, when the combination of scan speed of 20 mm/s, pulse frequency ranges of
30–40 kHz along with line spacing of 0.04 mm were utilized, better MRR and
surface roughness (Ra) were observed. In comparison with the other process
parameters, the effect of the scan speed was found to be negligible. Further,
experimental tests were carried out on Ti-6A1-4V alloy sheet having a thickness of
4 mm, using Q-Switched 30 W Yb: YAG fiber laser by Tagliaferri et al. [39].
6 Fiber Laser Micro-machining of Engineering Materials 247
The aim of the experiment was to identify the effect of the process parameters over
the depth of the machined volume along with the quality of the roughness of the
machined surface. After the first phase of the experimentation, the effect of the
process parameters over the machined volume along with the quality of the
roughness of the engraved surface was identified. The results of the experiment
revealed that the machined volume was linearly dependent on the total amount of
released energy, for each of the pulse frequency.
6.3.6 Micro-turning
6.3.7 Marking
Fiber laser marking is the key area that has emerged in the recent times. The
utilization of fiber laser for marking applications produces clean and high end
finishing of a wide variety of materials. Astarita et al. [41], carried out fiber laser
marking of titanium cold sprayed coatings on aluminium substrates. The authors
observed that the heat input rules the fiber laser marking process in particular three
different conditions. Firstly, irregular groove was observed due to a too high energy
released for unit length, whereas regular mark with hidden damages along with
regular and effective mark was also observed. It was concluded by the authors that
regular mark with inadequate groove was observed due to a low heat input during
the process. The homogeneity of the cold spray coating played a crucial role in
obtaining high end finishing of marking. The discontinuous nature of coating
affected the nature of the marking process. Penetration depth more than 0.4 and
248 A. Sen et al.
0.2 mm were observed on titanium sheet (without coating) and cold sprayed
coating, respectively. A microscopic view of markings on the titanium cold sprayed
layer performed at output power of 20 kW is shown in the Fig. 6.8.
In order to exceed the limited peak power (*10 GW) of fiber systems, fiber-laser
pumped parametric amplifiers are being developed by the researchers in the present
era. These solutions necessarily engage a range of complexities to the systemic
architecture. Further, in order to eradicate any group delay between the individual
amplifier sections, these amplifiers need to be appropriately designed. Along with
the aforementioned tasks, the optical path delay between the individual amplifiers
must be controlled by using proper feedback electronics to reach to a fraction of a
wavelength. Pulse energies in the micro-joule to millijoule range are required for
the micro-machining of dielectrics and metals. Superior hole quality in
micro-drilling is the driving force for the usage of femtosecond pulses in
micro-machining applications as compared to the nanosecond or picosecond pulses
along with the faster ablation speed, when it is combined with the use of pulse
burst. With the introduction of large-mode-area fibers, fiber lasers capable of
generating femtosecond pulses with millijoule pulse energies became possible.
These fiber lasers have allowed the construction of micro-joule level fiber
6 Fiber Laser Micro-machining of Engineering Materials 249
picoseconds pulse sources that does not utilize the CPA [9]. By the usage of
nonlinear spectral compression, high spectral quality can be obtained. In order to
expand the mode area of optical fibers, the most suitable method is to increase the
core diameter. This phenomenon is effective for the core diameters in the range of
25–50 lm. The fundamental mode can be excited if appropriate mode matching at
the input, higher order mode filtering via bending and/or the insertion of satellite
cores, which channel out higher-order modes from the central core structure, is
carried out; although resulting fibers are multimedia in nature. New applications are
invented with the utilization of nonlinear effects in gas-filled fibers. Another
interesting area that is still under progress is the combination of coherent beam with
the fiber laser system, in order to expand its capabilities in the ultrafast region. Two
different forms of multimedia fibers have become widely accepted in the recent
years, which are, large-path fibers and leakage channel fibers. The characteristics of
both the fibers are, firstly, they are derived from photonic crystal fiber designs,
bearing a core which is encompassed by air holes in a cladding to make sure that
there is countless single-mode propagation.
In the previous years, research works on the fiber laser systems were primarily
based on generating micro-features mainly for biomedical industries and thin
material cutting. Although, few researchers have showcased the utility of fiber laser
for thick material cutting, but the number of research works in this field are not
satisfactory. In the present day scenario, researchers are trying to utilize the fiber
laser in various hybrid machining approaches, i.e., laser assisted micro-machining,
laser assisted micro-turning, etc. along with the conventional micro-machining
approaches for the newly developed materials. Utilization of infrared fiber laser for
generating micro-fluidic channels on polymer materials such polymethyl
methacrylate, is a new dimension in the domain of fiber laser micro-machining [31].
Research works are also being conducted on fiber laser micro-machining of various
engineering materials with the aid of developed set ups for assisting the fiber laser
micro-machining process. However, further research works on hybrid fiber laser
micro-machining processes need be carried out.
6.5 Summary
Fiber laser has emerged as one of the strong force in the solid state laser systems in
the recent years. The utilization of the fiber laser is not only confined to the
fabrication of micro-features on a few selected fields, but also successfully managed
to diversify its applications in the realm of thick material cutting also. The number
of research works is escalating for the developers of fiber laser systems, such as
amplifiers, high diode lasers, along with the generation of burr, dross free
micro-cuts on a wide spread of materials. The potential of fiber laser system in the
micro-machining area is still not completely utilized as a consequence of which the
market share of fiber laser is still lagging behind the conventional solid state laser
systems such as Nd-YAG laser systems. In the present chapter, a vivid discussion
250 A. Sen et al.
has been conducted with the concept of the fiber laser generation along its diversity
of applications in the various micro-machining arenas. Fiber laser diversified from
the conventional laser systems only from the fact that the laser is generated within
the fiber itself while the other laser systems only utilize fiber as a beam delivery
system. The past research studies show that most of the research works with the aid
of fiber laser micro-machining are confined only to micro-cutting, micro-drilling
and engraving. Only a hand full of work has been conceptualized for hybrid laser
machining with the aid of fiber laser systems. Although, the experimental results
turn out to be satisfactory compared to CO2 and Nd-YAG lasers, but even then, heat
affected zone, dross formation etc., are inevitable for ultrafast fiber laser systems.
The problem can be partially or fully overcome by introducing pico and fem-
tosecond fiber laser systems. However, the aforesaid lasers are not at all cost
effective. Efforts are being made by engineers and researchers to not only reduce the
overall costs, but also to establish outstanding industrial applications which will be
critical factors to converge both the academic and the industrial arenas.
Acknowledgments The authors acknowledge the financial support and assistance provided by
CAS Ph-IV program of Production Engineering Department of Jadavpur University under
University Grants Commission, New Delhi and TEQIP phase II program of Jadavpur University.
References
11. M. Naeem, Choice of laser sources for micro-machining applications, SPI Lasers, http://www.
spilasers.com/whitepapers/choice-of-laser-sources-for-micromachining applications/.
12. D. Teixidor, F. Orozco, T. Thepsonthi (2013), Effect of process parameters in nanosecond
pulsed laser micromachining of PMMA-based microchannels at near-infrared and ultraviolet
wavelengths, The International Journal of Advanced Manufacturing Technology, 67
(5), 1651–1664.
13. J. Meijer (2002), Laser micromachining, Micromachining of engineering materials. USA:
Marcel Dekker, 203–238.
14. A. Sen, B. Doloi and B. Bhattacharyya (2015), Fiber laser micro-machining of Ti-6Al-4 V,
Lasers Based Manufacturing: 5th International and 26th All India Manufacturing Technology,
Design and Research Conference, AIMTDR 2014, Springer India, 255–281.
15. F. O. Olsen, K. S. Hansen, and J. S. Nielsen (2009), Multibeam fiber laser cutting. Journal of
Laser Applications, 21, 133.
16. K.F. Kleine and K.G. Watkins (2003), Fiber laser for micro cutting of metals. Proc. SPIE
4974, 185.
17. H. Meng, J. Liao and Y. Zhou (2009), Laser micro-processing of cardiovascular stent with
fiber laser cutting system. Optics of Laser Technology, 41(3), 300–302.
18. W.P. Risk, T. R. Gosnell and A. V. Nurmikko (2003), Compact blue-green lasers, Cambridge
University Press, Cambridge, 1–19.
19. C.H. Fu, J.F. Liu and A. Guo (2015), Statistical characteristics of surface integrity by fiber
laser cutting of Nitinol vascular stents. Applied Surface Science. 353, 291–299.
20. Y. Okamoto, N. Kataoka, H. Tahara, K. Shiwayama and Y. Uno (2006), Micro cutting of thin
copper plate by fiber laser with laval nozzle, Journal of Laser Micro/Nanoengineering, 1, 3.
21. H. Niino, Y. Kawaguchi, T. Sato, A. Narazaki, R. Kurosaki, M. Muramatsu, Y. Harada, K.
Wakabayashi, T. Nagashima, Z. Kase, M. Matsushita, K. Furukawa and M. Nishino (2013),
Laser Cutting of Carbon Fiber Reinforced Plastics (CFRP) by Fiber Laser Irradiation,
Conference on Lasers and Electro-Optics/Pacific Rim, ISBN: 978-1-4673-6475-1.
22. J.B. Lecourt, C. Duterte, F. Liegeois, D. Lekime and Y. Hernandez (2012), High-power
ultrashort fiber laser for solar cells micromachining, Proc. SPIE8237, Fiber Lasers IX:
Technology, Systems, and Applications, 823738, DOI:10.1117/12.907951.
23. P. Deladurantaye, A. Cournoyer, M. Drolet, L. Desbiens and D. Lemieux (2011), Material
micromachining using bursts of high repetition rate picosecond pulses from a fiber laser
source, Proc. SPIE 7914, Fiber Lasers VIII: Technology, Systems, and Applications, 791404,
DOI:10.1117/12.875265.
24. Toru Mizunami and and A. Ehara (2011), Femtosecond-pulsed laser micromachining and
optical damage by an erbium-doped fiber-laser system, Proceedings of the 36th International
Conference on Micro- and Nano-Engineering (MNE), 36th International Conference on
Micro- and Nano-Engineering (MNE), Microelectronic Engineering, 88(8), 2334–2337.
25. H. Qi and H. Lai (2012), Micromachining of metals and thermal barrier coatings using a
532 nm nanosecond fiber laser, Physics Procedia, Laser Assisted Net shape Engineering 7,
39, 603–612.
26. YP. Kathuria (2003), Biocompatible metallic stent for medical therapy. SPIE, 5287:52–61.
27. L. Liu, D. B. Li, Y. F.Tong and Y.F.Zh (2016), Applied Physics A, 122:638,
DOI 10.1007/s00339-016-0170-0.
28. N. Muhammad, D. Whitehead, A. Boor and L. Li (2010), Comparison of dry and wet fibre
laser profile cutting of thin 316L stainless steel tubes for medical device applications, Journal
of Materials Processing Technology, 210, 15, 2261–2267.
29. W.C. Choi and G. Chryssolouris (1995), Analysis of the laser grooving and cutting processes,
J. Phys., Appl. Phys, 28, 873–878.
30. C.A. Biffi and A. Tuissi (2016), Micro-processing of NiMnGa shape memory alloy by using a
nanosecond fiber laser, Optics &LaserTechnology, 78, 42–49.
31. A. Sen, B. Doloi and B. Bhattacharyya (2016), Fibre laser micro-channeling of PMMA,
Lasers in Engineering, 35, 1–4, 123–138.
252 A. Sen et al.
32. A. Sen, B. Doloi and B. Bhattacharyya (2015), Effect of process parameters on IR fiber laser
micro-machining of PMMA, International Conference on Precision, Meso, Micro and
Nano Engineering, IIT Bombay, India, 10–12 December 2015, 1–6.
33. C.A. Biffi, N. Lecis, B. Previtali, M. Vedani and G. M. Vimercati (2011), Fiber laser
microdrilling of titanium and its effect on material microstructure; International journal of
Advanced Manufacturing Technology, 54:149–160, DOI 10.1007/s00170-010-2918-6.
34. A. Ancona, D. Nodop, J. Limpert, S. Nolte and A. Tünnermann (2009), Microdrilling of
metals with an inexpensive and compact ultra-short-pulse fiber amplified microchip laser,
Applied Physics A, 94: 19–24, DOI 10.1007/s00339-008-4906-3.
35. A. Ghosal and A. Manna (2013), Response surface method based optimization of ytterbium
fiber laser parameter during machining of Al/Al2O3-MMC, Optics and Laser Technology, 46,
67–76.
36. H. Huang, L-M. Yang and J. Liu (2014), Micro-hole drilling and cutting using femtosecond
fiber laser, Optical Engineering, 53 (5), 051513.
37. B. Adelmann and R. Hellmann (2015), Rapid micro hole laser drilling in ceramic substrates
using singlemode fiber laser, Journal of Materials Processing Technology, 221, 80–86.
38. S. Genna, C. Leone, V. Lopresto, L. Santo and F. Trovalusci (2010), Study of fibre laser
machining of C45 steel: influence of process parameters on material removal rate and
roughness, International Journal of Material Forming, 1, 1115–1118.
39. F. Tagliaferria, N. Paganob, C. Leoneb, B. Palumbo, Statistical analysis of fiber laser
machining of titanium alloy, https://www.researchgate.net/publication/267411159.
40. O. F. Biswas, A. Sen, G. Kibria, B. Doloi and B. Bhattacharyya (2016), Experimental
investigation into spiral micro-grooving on aluminium using fiber laser, Proceedings of 6th
International & 27th All India Manufacturing Technology, Design and Research
Conference (AIMTDR-2016), College of Engineering, India, 16–18 December, 411–415.
41. A. Astarita, S. Genna, C. Leone, F.M.C. Minutolo, A. Squillace and C. Velotti (2016), Study
of the laser marking process of cold sprayed titanium coatings on aluminium substrates,
Optics & Laser Technology, 83, 168–176.
Chapter 7
Laser Beam Micro-cutting
Abstract This chapter gives a brief overview of laser beam cutting. An illustration
of basic fundamentals of laser material interaction and material removal is given
here which considers generation of photon and interaction with electron to generate
heat, absorption of heat, phase transformation, plasma generation, ablation and
removal mechanism of cut material from the irradiate region at dry condition. An
experimental study of laser beam cutting of Inconel 625 superalloy at dry condition
is given at the end of this chapter. During this experimental study effect of different
process parameters on machining characteristics also discussed in details.
7.1 Introduction
Fig. 7.2 Various governing physical phenomena of material removal mechanism [2]
v
F ¼ eE þ e H
c
IðZÞ ¼ I0 elz
where, I0 is the incident intensity, I(z) is the intensity at depth z, and l is the
absorption coefficient.
Conversion of absorbed energy into heat is happened in very short time period
(<pulse width) by degradation of the ordered and localized primary excitation
energy. The temperature distribution on laser irradiate zone not only depends on
absorbed laser energy but also on thermal diffusivity (D). Thermal diffusivity [4]
can be expressed in terms of specific heat (Cp) and thermal conductivity (k),
D ¼ k=qCp
z ¼ ð2Dtp Þ1=2
m_ ¼ Vs q
where m_ the mass of material removed per unit time, Vs is the velocity of the
liquid–vapour interface and q is the density.
d ¼ Vs tp
Based on the role of assist gas and interaction between laser beam and workpiece
substrate laser beam cutting operation can be classified into four groups, i.e. laser
sublimation cutting, controlled fracture technique, fusion cutting and reactive fusion
cutting.
V ¼ F0 =q½L þ Cp ðTV T0 Þ
where,
F0 = absorbed power density (W/m2); q = density of solid (kg/m3); L = latent heat of
vaporization (J/kg); Cp = heat capacity of solid (J/kg °C); Tv = vaporization tem-
perature (°C); T0 = temperature of the material at start (°C).
During laser sublimation cutting, no additional evaporation occurs after cut
width reaches its maximum value due to insufficient laser energy at machining zone
by conduction and convection loss of thermal energy [9].
In laser induced stress cutting, irradiate laser energy generates mechanical stress on
the machining zone, which causes crack propagation with controllable fracture
growth, results in material separation on the direction of laser beam movement. In
this process, a laser beam moves over the work substrate only to heat up (>melting
temperature) the irradiate region. During the cooling period, the thermo-mechanical
stress is induced on the irradiate region which produced the crack. A high plastic
compressive stress is generated around the laser spot diameter which relaxed with
the movement of laser beam, results in generation of residual tensile stress on the
upper surface of the irradiate region. This artificial crack then propagates along the
path of laser movement for precision separation of materials in a controlled manner.
Due to asymmetry of thermo-mechanical stress along with crack generation, the
crack trajectory does not follow the laser movement path precisely [10]. Controlled
fracture technique requires very less energy due to the absence of melting or
vaporization processes. Thus, this technique is very useful to process brittle
materials with clean cut with higher cutting speed than other laser cutting
techniques.
Fig. 7.4 Schematic diagram of the inert-gas laser beam fusion cutting process
In some of the laser cutting processes, co axially flown high pressure reactive gas
not only assists in removal of molten material from the machining zone, but also
adds some energy on the machining process in terms of exothermic reaction to
enhance the process. This aforesaid laser cutting process is a variation of laser
fusion cutting and known as laser reactive cutting technique. During laser beam
cutting, thermal energy source is added by the exothermic reaction at the erosion
front when the impinged high pressure oxygen gas reacts with the molten material.
Oxide of the base material is also formed on the top surface of the melt pool.
Generation of enormous exothermic heat energy not only nullifies the conductive
thermal loss to the parent work substrate, but also helps to enhance the cutting
speed as a combine effect of higher fluidity and absorptivity of hot molten layer of
oxide slag on the erosion front [12]. This increased cutting speed results in better
cut quality due to less thermal diffusion to the adjacent base work substrate. The
extra thermal energy added by the exothermic reaction at the irradiate region helps
the rise of temperature of the melt pool up to evaporation temperature very rapidly
results in ease of material removal by vaporization. Erosion front propagates
through the melt pool-parent material interface in the direction of laser cutting by
further melting into the unmachined region and material removal due to friction
force works between impinged assist gas and melt pool to accomplish the cutting
process. Heat balance at the machining zone is described by the heat gain at the
melt pool by laser irradiation and exothermic reaction due to oxidization and heat
losses due to conduction, vaporization and ejection of melt pool [13]. Generally,
oxygen or oxygen enriched gas mixture is used as an assist gas for reactive fusion
7 Laser Beam Micro-cutting 261
cutting. Thin layer of oxide above the melt pool have some good as well as adverse
affect on quality of laser reactive fusion cutting. Sometimes oxide adherent on the
kerf edges as dross which affects the cut quality adversely in terms of micro crack
formation. Striation on the side wall of the kerf may be reduced sometimes due to
blanket effect of the thin oxide film on melt pool. This process mainly used to cut
thick section of hard to machine metals, i.e. stainless steel, aluminium alloys,
titanium superalloy etc.
Absence of thermal effects make this laser cutting technique known as laser cold
cutting. In this technique, ultra-short pulsed laser, in the range of picosecond to
femtosecond interact with the work substrate with a very high fluence, results
material removal by molecular fragmentation due to direct bond breaking by multi
photon absorption mechanism. Photon energy of 4.9 eV is very much sufficient to
break the chemical bond directly [14]. To get debris free cutting of various material
along with surface modification of biodegradable materials, this cutting process is
used in industries i.e. medical industries, electronics manufacturing industries.
Laser beam cutting is one of the most widely used laser material processing
technique in industries. It is a complicated process dominant by various process
parameters, i.e., laser beam properties, beam delivery system, assist gas properties,
to get desired quality aspects in terms of narrow cut width, smoother inner kerf,
striation and dross free cut along with less heat affected zone. The term laser beam
properties indicate at laser fluence, wavelength, mode of operation (continuous or
pulse), pulse frequency which have great impact on laser cutting as well as on
physical, thermal and metallurgical properties of kerf generated.
Laser fluence or energy density determines the energy input at the irradiate region
which is the most significant factor to effect the performance and quality of the
machining. Laser fluence also the deciding factor to determine minimum cutting
speed required for a through cut [17].
7.3.2.3 Wavelength
Beam delivery or optical system determines the spot diameter, relative focal dis-
tance and beam energy distribution on the workpiece. Spot diameter is determined
by measuring the area of single pulse laser irradiate zone. The laser power intensity
on the irradiate zone is determined by laser spot diameter. Deep cut cannot be
achieved by focusing the laser beam just on the top surface of the work substrate
due to multiple reflections on the kerf wall. To get the optimum cut quality gen-
erally, laser beam is focused just beneath the top surface. Mainly, Gaussian energy
distribution with the combination of very low spot diameter and very high energy
density laser beam, is preferred in the industries. Similar interaction with work
substrate in all direction due axial symmetry of the Gaussian beam, results in low
roughness in and outside of the kerf.
Polarization is defined by the way of oscillation of electric and magnetic field
vector respect to each other. In laser beam cutting operations, generally electric and
magnetic vectors are oscillating in a same plane and perpendicular to each other.
The angle between plane of incidence and electric field vector defined different
types of polarization, such that S type or P type. Beam polarization is a control
factor for absorption of incident laser beam energy by work substrate [18].
Assist gas velocity not only act as an coolant but also helps to enhance the ejection
of molten material from the erosion front to accelerate the cutting process. From the
past research works, it has been found that velocity of assist gas enhance the cutting
process up to a certain point, then the efficiency of the cutting process is degraded
due to nonlinear effect of cooling by the assist gas velocity [19]. Generation of
density gradient fields by non uniform assist gas velocity leads to change in
refractive index which affects the performance characteristics [20]. The alignment
of nozzle where gas jet is used co-axially has a great impact on surface roughness
264 N. Roy et al.
Quality characteristics of laser beam cutting are a great concern with increased
application in biomedical industries, aerospace industries and automobile indus-
tries. Geometric qualities like corner accuracy, kerf with good aspect ratio, smooth
inner surface and surface roughness in the range of nanometer along with great
metallurgical quality, i.e. less heat affected zone (HAZ) and thermal stress induced
micro crack free cut is required to get during laser beam cutting.
7.3.3.1 Dross
Incomplete expulsion of molten material from the bottom side of the kerf during
through cut is known as dross. It is required to understand mechanism of dross to
get nonadherent dross by controlling the process variables. Arata et al. first explain
the mechanism of dross during laser beam cutting of stainless steel. A small portion
of molten material is ejected as droplet form whereas the other portion subsequently
flows in reverse direction and solidified at the bottom corner edge of the kerf to
form dross. This phenomenon is happened when the cutting operation takes place at
lower cutting speed [23]. Dross free cut can be achieved when the maximum exit
momentum thrust is equal to ambient gas pressure. This aforesaid condition con-
trols the nature of the geometrical shape of ejected molten material from the bottom
of the kerf [24]. Surface tension force dependent ejection speed of melt and
insufficient melt expulsion due to blockage by excess molten material is the two
mechanism of dross formation [25].
7.3.3.2 Striation
Formation of periodic patterns along the kerf inner edge. Frequency and amplitude
of striation are the characteristics of striation on the inner edge which are mainly
affects by cutting speed. Side wall burning and oscillation of melt pool phenomenon
may be the most accepted mechanism of striation formation by the researchers [27].
Burning front is established by extra energy gain by the exothermic oxidation
reaction apart from the laser irradiation. Burning fronts propagate faster than laser
7 Laser Beam Micro-cutting 265
beam in radial direction from the centre of laser beam, end at the edge of the beam.
Thus, single striation is created. Further movement of laser beam at the erosion
front, reinitiate burning front to generate a striation pattern along the kerf edge.
Temperature fluctuation on the melt pool due to sudden temperature drop by
resistance to oxygen diffusion by oxide layer and subsequently temperature rise by
sudden increase in reaction energy by extra oxide slag result in periodic striation
[28]. Figure 7.5 illustrate different patterns of striation.
Laser beam cutting process is on of the fastest, clean and green manufacturing
technique applied in manufacturing industries with a precision and cost effective
way. Laser cutting technique is first applied in industry to cut Die board [29]. This
technique I used in job shop to produce complex profile like valve plates, gaskets,
complex shape medical parts, i.e. coronary/pulmonary stent. In aerospace industry it
is used to make titanium ducting, fuselage skin stiffeners an jet engine component
with the dimensional profile. This process is utilized to produce micro electronics
parts like circuit boards. For dismantling or repair nuclear power station, this
technique is obvious choice. Fabrication of micro fluidic device is done by laser
cutting process.
Fig. 7.6 Photographic view of the CNC-pulsed Nd:YAG Laser machining system [31]
X
k X
k XX
k
yu ¼ b0 þ bj xj þ bjj x2j þ bij xi xj ð7:1Þ
j¼1 j¼1 i\j j¼2
where yu is the corresponding response, e.g., kerf width. xi is the coded value of the
i-th machining parameter, k is the number of machining parameters and bi, bii, bij
are the second order regression coefficients.
Olympus optical measuring microscope has been used to capture the image of
cut region at 20 magnification from where kerf width is calculated by image
268 N. Roy et al.
analysis software. Measured value of kerf width is listed in Table 7.3. Minitab 17
Software is used for analysis of the measured responses and determining the
mathematical models with best fits. The adequacy of the model is tested using the
sequential f-test, lack-of-fit test and the analysis-of-variance (ANOVA) technique
by the same software to obtain the best fit model.
ANOVA analysis of the quadratic model with other adequacy measures R2,
adjusted R2 and predicted R2 are given in Table 7.4.
The associated p-value of less than 0.05 indicates that the model term can be
considered as statistically significant at 95% confidence level. Value of lack of fit of
the model is more than 0.05 which indicates at non significant as desired. From the
table it is found that lamp current is the most dominating factor followed by pulse
frequency, assist gas pressure, cutting speed and pulse width. It can be concluded
7 Laser Beam Micro-cutting 269
that the data for each response are well fitted in the developed model from the
values of S, R-sq, R-sq(adj) and R-sq(pred) given in Table 7.4.
Parametric analysis:
From Fig. 7.7 it is observed that kerf width first increase with increase in lamp
current but it marginally decreases with lamp current after 26 A. Firstly increase in
lamp current generates more laser power for which amount molten material
increases, results in increase in kerf width. But when lamp current exceeds 26 A
value, excess amount of molten material is formed in machining zone which cannot
properly removed by assist gas from the machining zone and results in decrease in
kerf width. Kerf width marginally increases with increases in pulse frequency up to
4 kHz then gradually decreases. At low pulse frequency comparatively high energy
beam is generated which removes more material from the top surface of the
270 N. Roy et al.
workpiece and vice versa. From Fig. 7.7 it can be concluded that low kerf width
can be achieved at lowest lamp current with highest value of pulse frequency.
From Fig. 7.8 it is observed that kerf width first increases with increase in lamp
current but it marginally decreases with increase in lamp current after 26 A whereas
incase of cutting speed kerf width gradually increases up to mid value of cutting speed
then decreases. In beginning due to increase in lamp current along with low cutting
speed at that very point of operation, more laser power is transferred to machining
zone results in increase in kerf width but further increase in cutting speed results in
decrease in interaction time between laser beam and workpiece results in decrease in
kerf width inspite of higher laser power at higher lamp current.
From Fig. 7.9 it is observed that lowest kerf width can be achieved at highest
cutting speed along with highest value of pulse frequency. At highest value of pulse
frequency comparatively low beam power generates which incorporates with less
interact time at high cutting speed transferred lower amount of energy to the
machining zone results lesser value of melt pool. For that lower kerf width may be
achieved.
From Fig. 7.10 it is observed that, lowest kerf width is achieved at highest value
of cutting speed and lowest value of assist air pressure. During aforesaid parametric
condition interaction time between laser beam and work piece is very small but due
7 Laser Beam Micro-cutting 271
to moderate value (hold value) of lamp current some adequate amount of melt pool
may be formed which may not be properly removed by assist gas at that lowest
value. That result in resolidification of the molten material along kerf edges and
inner wall of the cut profile, make the kerf width narrow.
Figure 7.11 shows the optimization results for the minimum kerf width based on the
mathematical model developed using Eq. (7.2). To get ideal machining response, the
value of the weight for linear desirability function (D) is considered as 1.
It is found from the figure that minimum kerf width of 0.0486 mm dimension
can be achieved at process parameter settings of 20 A lamp current, 7 kHz pulse
frequency, 5% pulse width, 1 mm/sec cutting speed and 1 kg/cm2 of assist gas
pressure (Fig. 7.12).
272 N. Roy et al.
Experimental study of pulsed Nd:YAG laser beam cutting is carried out success-
fully on Inconel 625 superalloy. From ANOVA analysis it is found that lamp
current is the most dominating process parameter whereas pulse width is the least
effecting process parameter. Optimal parameter setting is determined by RSM CCD
technique at highest level of pulse frequency and pulse width with lowest level of
lamp current and moderate level of cutting speed and assist gas pressure to get
minimum kerf width.
7.6 Summary
Acknowledgements The authors acknowledge the financial support from UGC, New Delhi under
the scheme of Rajiv Gandhi national Fellowship scheme and technical equipment support from
UGC, New Delhi under the CAS Ph-IV program of Production Engineering Dept. of Jadavpur
University.
7 Laser Beam Micro-cutting 273
References
25. Tani G, Tomesani L, Campana G (2003) Prediction of melt geometry in laser cutting. Applied
Surface Science 208–209:142–147.
26. Dong-Gyn AHN, Kyun-Won BYUN (2009), Influence on cutting parameters on surface
characteristics of cut section in cutting of Inconel 718 sheet using CW Nd:YAG laser,
Transactions of nonferrous metals society of China, vol.19, S32–S39.
27. Powell, J. (1993). CO2 laser cutting. Springer, London.
28. Chen SL (1999) The effects of high-pressure assistant-gas flow on high-power CO2 laser
cutting. Journal of Materials Processing Technology 88:57–66.
29. Dawson P (1996) The use of lasers in the die board industry. Industrial Laser User (3):21–22.
30. Dinda G.P., Dasgupta A.K., Mazumder J., Laser aided direct metal deposition of Inconel 625
superalloy: Microstructural evolution and thermal stability, Materials Science and
Engineering A 509 (2009) 98–104.
31. Biswas R., Kuar A.S., Sarkar S., Mitra S. (2010),A parametric study of pulsed Nd:YAG laser
micro-drilling of gamma-titanium aluminide, journal of Optics & Laser Technology, 42 23–31.
Chapter 8
Electrochemical Micromachining (EMM):
Fundamentals and Applications
Abstract Product miniaturization is the principal driving force for 21st century’s
industries because of the escalating demands for compact, intelligent, robust,
multi-functional, and low cost products in all fields. As demand of miniaturized
products is exponentially increasing, the need to manufacture such products from
advanced engineering materials becomes more apparent. Micromachining plays
significant role in miniaturization, and consist of machining different microfeatures
on products. Design of microtools, tool wear, surface quality, burr and heat removal
are the main challenges in various micromachining methods. Electrochemical
micromachining is one of the important techniques because of its special material
removal mechanism, better precision and control, environmentally acceptable, and
mainly it permits machining of any metallic materials irrespective of its hardness.
For better understanding of EMM process, the basic concepts such as electro-
chemistry, Faraday’s laws of electrolysis, electrical double layer, equivalent elec-
trical circuit, and material removal mechanism have been discussed. Significant
process parameters which affect the process performance, need of EMM setup
development, various subsystems, along with the challenges in setup developments,
and important techniques for improving the machining accuracy have been high-
lighted. Machining, finishing, and surface engineering applications of EMM, as
well as recent advancement in EMM for micro and nanofabrication have also been
discussed.
V. Rathod (&)
Department of Mechanical Engineering, Government Polytechnic Ratnagiri,
Maharashtra, India
e-mail: [email protected]
B. Doloi B. Bhattacharyya
Production Engineering Department, Jadavpur University,
Kolkata 700032, India
e-mail: [email protected]
B. Bhattacharyya
e-mail: [email protected]
8.1 Introduction
Material removal as a means of making things dates back to prehistoric times, when
ancient man started to carve wood and chip stones to make the hunting and farming
tools. Human beings shaped copper by casting for metal and jewelry work before
5000 BC. Invention of copper, bronze and then iron age revolutionized the ancient
civilizations. Development of modern machine tools is closely related to the
Industrial revolution. Introduction of hard, temperature resistant materials in various
fields of application led to the development of various non-conventional machining
processes. The non-traditional processes have been developed since World War II,
in response to new and unusual manufacturing requirements such as machining of
complex part geometries with close tolerances, without any surface damage that
could not be realized by conventional methods. There are various non-traditional
machining processes, most of which are unique in their range of applications.
Electrochemical machining (ECM) is one of the important non-conventional
machining processes used for machining of extremely hard alloys, which cannot be
machined satisfactorily by conventional methods. The metal removal phenomenon
of controlled anodic dissolution was known early in 20th century, but it was until
the 1960s that ECM came into use as a practical machining method. In last decades,
ECM has been developed, and anodic dissolution can be effectively utilized for
high-precision ultrafine machining to generate macro-as well as micro features on
work pieces, due to its advantages like no tool wear, ability to machine any metallic
surfaces irrespective of its hardness, stress/burr free surfaces, high MRR and
accuracy, and capability to machine irregular 3D shapes.
Miniaturization is the principal driving force for 21st century’s developments
because of the escalating demands for compact, intelligent, robust, multi-functional,
and low cost industrial products. As the demand of micro and nano products is
exponentially increasing, the need to manufacture micro and nano products from
advanced engineering materials becomes more apparent. Advanced micro
machining may consist of machining different micro features on micro or macro
work pieces. Micro features such as micro holes, micro slots, microgrooves, thin
walls etc. are to be machined on different surfaces of a product to fulfill its func-
tional requirements. Design of microtools and micro fixtures, tool wear, lack of tool
rigidity, poor surface finish, scrap and heat removal etc. are the main challenges,
when these micro features are machined with traditional machining techniques.
The principle of ECM was discovered long back in the nineteenth century by
Michael Faraday (1791–1867). Faraday established the laws of electrolysis in 1833,
which is the foundation of both the better-known electro deposition and electro
dissolution techniques. In 1929, the Russian researcher W. Gussef first developed a
8 Electrochemical Micromachining (EMM): Fundamentals and Applications 277
gap between the electrodes should be maintained uniform by advancing the cathode
toward the anode at the same rate at which the metal is being dissolved. As the
cathode tool advances during machining operations the anode workpiece gradually
attains a shape that is almost a replica of the cathode tool.
Controlled metallic dissolution with high accuracy is required to put the ECM
technique in industry for practical applications. For this purpose the ECM setup
needs electrical power source to supply the machining current to the electrodes,
arrangement to circulate an electrolyte in the machining gap, and mechanical
structure for regulating the tool movement towards the workpiece. In ECM, dis-
solution rate of anodic surface depends upon the machining current, machining
time, atomic weight of the workpiece metal, and valency of the ion produced,
whereas it does not depends on the hardness of material. Various process param-
eters such as applied voltage, machining current, electrolyte type, concentration,
flow rate, and inter electrode gap (IEG) influences the major ECM machining
criteria like metal removal rate, surface finish, and accuracy. The shape of the tool
remains unchanged during machining, since only hydrogen gas is evolved at the
cathode surface [1]. Significant technological development such as tool vibration,
pulsed machining current, electrolyte microfiltration, CNC controller and applica-
tion of computer aided design to predict cathode tool profiles, for improving
machining accuracy and waste disposal make today’s ECM technique a better
choice than many other conventional as well as non-conventional machining
techniques.
based on the number of criteria’s such as required machining accuracy, surface finish,
type of workpiece material, production rate, and cost of production [2].
The EMM process has numerous advantages and some limitations which can be
categorized by product, material and machine advantages.
(a) Product Advantages
The EMM has the following advantages on the final product:
(i) Initial investment on process design and micro tool fabrication is low. Also
the, running cost and tooling costs are low.
(ii) The shape of the microtool remains unchanged during machining, since only
the hydrogen gas is evolved at cathode microtool surface during electrolysis.
Hence microtools of complicated shapes can be reused multiple times.
(iii) EMM is a process with high machining speed and relatively low cost.
8 Electrochemical Micromachining (EMM): Fundamentals and Applications 281
(i) ECM was previously known as process that harms environment. After
thorough developments in the treatment of electrolytes, the process has
become less harmful to the environment. However, EMM also needs very
less volume of electrolyte.
(ii) Each micro product and material requires new research. So, higher produc-
tion numbers are essential for the cost effectiveness of the process.
(iii) Needs careful handling of micro tools with in situ fabrication.
(iv) EMM requires a relatively high knowledge base for operation.
inter-electrode gap, and low voltage pulsed direct current is applied in between the
electrodes. The workpiece material dissolves into metallic ions by the electro-
chemical reactions according to Faraday’s law of electrolysis. The dissolved
material and other process by-products such as precipitates, sludge, hydrogen gas
etc. are carried away from narrow machining zone by the electrolyte. The final
shape, and size of the machined micro feature is approximately negative mirror
image of the microtool electrode. Machining accuracy depends on different
machining conditions in the narrow machining zone. Machining criteria like
material removal rate, machined surface characteristics, and machining accuracy are
influenced by the process parameters such as pulse amplitude i.e. applied voltage,
pulse frequency, duty ratio, machining current, electrolyte type and its concentra-
tion, inter-electrode gap and tool feed rate etc. [6].
The chemical process which occurs when an electric current is passed between the
two conductors immersed into electrolytic liquid solution is known as
‘Electrolysis’. The metallic conductors immersed in liquid solution are termed as
‘electrodes’. The electrode with positive polarity is called as ‘anode’ and the
electrode with negative polarity is called as ‘cathode’. Electrodes conduct electrical
current by the movement of electrons. The liquid solution in which electrodes are
immersed, and also conducts electricity through it is known as ‘electrolyte’. The
system of electrodes and electrolytes is called as ‘electrochemical cell’. The reac-
tions which occur at anode and cathode are called as ‘anodic reaction’ and ‘cathodic
reaction’ respectively. Electrolytes carry electrical current by the movement of
atoms or group of atoms, which have either lost or gained electrons, thus acquiring
either positive or negative charge. Such atoms are called as ‘ions’. Ions which carry
positive charges and moves through an electrolyte towards cathode are known as
‘cations’. Similarly, the negatively charged ions which move towards the anode are
known as ‘anions’ [7].
When small electric current (DC) is applied across the workpiece as anode and
the microtool as cathode, submerged in an electrolyte with very small
inter-electrode gap, the transfer of electrons between ions and electrodes completes
the electric circuit. Since the electrons cannot flow through the electrolyte, the
electric current is maintained by the removal of electrons from the atomic structure
of the workpiece, i.e. the current is carried by the ions. The metal material dissolves
atom by atom from anodic surface and enters into the electrolyte as positive ions.
The positively charged ions move through the electrolyte towards the cathode and
the negatively charged ions travel towards the anode as shown in Fig. 8.2. The
movement of ions is accompanied by the flow of electrons in the opposite sense
outside cell and both the actions are a consequence of the applied potential dif-
ference. The least strongly bounded electrons are found at the surface of the
8 Electrochemical Micromachining (EMM): Fundamentals and Applications 283
workpiece and flow into the electrolyte circuit. These electrons dissociate them-
selves from the workpiece and flow into the electric circuit.
In electrochemical machining, dissolved metal appears as precipitated solid of
metal hydroxides. Chemical reactions occur at the cathode, and anode in the
electrolyte. At cathode i.e. microtool, the reaction having the smallest oxidation
potential takes place, and at anode i.e. the workpiece, the reaction having the largest
oxidation potential occurs first. Hence, the factors such as (i) nature of metal being
machined, (ii) type of electrolyte, (iii) current density and, (iv) temperature of
electrolyte influences the oxidation potential and thus determine the kind of reaction
that will occur. Different variables as shown in Fig. 8.2, also affects the rate of
electrochemical reaction. The material removal in electrochemical reactions are
governed by (i) electrical variables such as an applied potential, and quantity of
electricity passed i.e. machining current passed for machining time, (ii) electrolyte
variables like type of electrolyte, its concentration, pH, and temperature of elec-
trolyte, (iii) mass transfer variables i.e. different modes of mass transfer such as
diffusion, convection, surface concentrations and adsorption, (iv) electrode vari-
ables namely electrode material, surface area, surface conditions and geometry of
electrode, (v) External variables such as room temp., pressure and machining time.
The electrochemical reactions taking place at cathode and anode during
machining are as follows [8].
The reactions causing the evolution of hydrogen gas at the cathode are:
M þ þ e ! M ðMetalÞ ð8:3Þ
For example, when the workpiece is iron, the cathode reactions are:
Fe 2e ! 2Fe2 þ ð8:4Þ
Metal ions form the metal hydroxides when neutral electrolytes are used. They
appear as solid precipitates since these are insoluble in water. These precipitates do
not affect the electrochemical reaction.
Ferrous oxide may further react with water and oxygen to form ferric hydroxide
such as:
M ! M þ þ e ð8:10Þ
8 Electrochemical Micromachining (EMM): Fundamentals and Applications 285
The overall reactions occurring during ECM of iron can be given as:
It has been observed that, the metal dissolution is the main or the only reaction that
occurs at the anode, and the electrolyte acts as carrier of current only. The current
efficiency, which is the ratio of the amount of dissolved metal to the amount that should
be dissolved according to Faraday’s law for the known current and time, is often lower
than 100%. This is because apart from the dissolution of the metal, other anode reactions
can occur, such as the oxidation of water, with the release of oxygen gas:
The extent to which this reaction lowers the current efficiency depends greatly on
the material of the workpiece, the electrolyte and the current density. Besides the
oxidation of water further oxidation of metal ions can also occur at the anode.
where, ‘Q’ is the total electric charge passed through the metallic material, ‘F’ is
Faraday’s constant (96.485 C/mol), ‘M’ is the atomic weight of the substance, ‘z’
is the valancy number of the substance (electrons transferred per ion), and (M/z) is
286 V. Rathod et al.
the chemical equivalent weight of the substance altered. As per Faraday’s first and
second law, Q, M, F, and z are the constants hence larger value of Q, as well as
chemical equivalent weight of metal implies higher mass of material removal.
For constant current electrolysis, total electric charge passed through the metallic
material can be given as:
Q ¼ I:t ð8:16Þ
where, ‘I’ is the current passed through the electrodes for time ‘t’Therefore, amount
mass removed (m) can be given as
I:t M
m¼ ð8:17Þ
F z
When the product (I.t) is unity i.e. one coulomb charge is passed through the
electrodes, the mass of material removed (M/z.F) is known as ‘electrochemical
equivalent of the metal’. From above equations, it can be concluded that rate of
anodic dissolution depends upon atomic weight, valency of the ions produced, the
current, and the time for which the current is passed. The metallic dissolution rate is
not influenced by the hardness or any other mechanical properties of metal. During
the electrochemical reaction only hydrogen gas is evolved at the cathode surface,
hence the shape of cathode tool remains unchanged i.e. no tool wear takes place.
This feature is very much useful during machining of complex micro features with
micron sized tools in EMM applications.
involves only electro-static force and independent of the chemical properties of the
ions. These ions are called as non-specifically adsorbed ions. These ions are dis-
tributed in three dimensional region called as diffusion layer or Gouy-Chapman
layer and its thickness depends on ionic concentration in the electrolyte. The bulk
electrolyte with its usual properties is located outside the Gouy-Chapman layer. The
structure of the double layer affects the rate of electrode reactions. The transfer of
ions will cease, when the energy required for an ion to dissolve is less than the work
necessary to pass it across the double layer. The excess charge stored on both sides
of the double layer depends on the electrode potential and acts like the charged
plates of capacitor separated by very small distance. Therefore, double layers at the
electrode-electrolyte interface can be represented by a capacitor in equivalent cir-
cuits and the interfacial capacity can be described as two capacitors in series. The
resulting potential drop across the interface due to this capacitance is termed as
‘double-layer potential’.
current, and the double layers which form at electrode-electrolyte interfaces which
act as capacitors.
Hence the electrodes i.e. anode and cathode, immersed in the electrolyte can be
represented by the basic analogous equivalent R-C circuit as shown in Fig. 8.4,
which consist of two capacitors (Cdl) representing double layers at both the
electrode-electrolyte interfaces and resistance of the electrolyte (Re) in between two
electrodes.
At metal-electrolyte interface, the metal molecule dissolves into the elecrolyte.
In the forward reaction, electrons enter the metal and metal ions diffuse into the
electrolyte, called as ‘charge transfer’. Whereas in backward reaction, metal ions
are discharged to metal, and thus equilibrium condition is reached. For the disso-
lution of anodic metal, the reaction must be in the forward direction only i.e.
irreversible. The resistance involved in irreversible reaction is called ‘charge
transfer resistance’. The electrolyte flow velocity is negligible or stagnant elec-
trolyte is preferable in the case of EMM. So there is not sufficient transfer of mass
from one electrode to the other electrode due to convection. This gives rise to
another diffusion component called Warburg Impedance (Rw). Faradic reaction
consists of an active charge transfer resistance (Rct) and Warburg resistance.
In EMM, the equivalent electrolyte resistance can be represented by considering the
effect of flow of current from the lateral and longitudinal surfaces of the microtool
to the workpiece. The inter-electrode gap in case of EMM is very small, hence
current flow path is small across the front end of the microtool, and this electrolyte
resistance is represented by Rbottom. Path of current flow from longitudinal surface
of the microtool to the workpiece surface is much longer and this electrolyte
resistance is represented by Rside. Therefore by considering the flow of a current
along lateral and longitudinal surfaces of the microtool, their respective electrolyte
8 Electrochemical Micromachining (EMM): Fundamentals and Applications 289
resistances, and polarized resistance (Rp), the equivalent circuit of EMM can be
modified as shown in Fig. 8.5 [10].
In EMM, ultra short pulses of very low voltage amplitude are applied between the
electrodes which are separated by very narrow machining gap. At narrow
machining zone, in addition to the electrolyte resistance, other resistances which are
not so prominent in conventional ECM have much more influence in EMM. Hence,
all of these resistances at machining zone need to be considered in electrical circuit
model of EMM. The inter-electrode gap electrolyte resistance in EMM is given as:
qs :h
R ¼ ð8:18Þ
A
g:M:I:t
Vm ¼ ð8:19Þ
z:F:qw
where, ‘M’ is the atomic weight of the material dissolved, ‘I’ is the amount of current
passed through the electrode, for machining time ‘t’, ‘qw’ is the density of workpiece
material, and ‘η’ is the dissolution efficiency or current efficiency. The current
efficiency is defined as the ratio of the actual amount of metal dissolved to the
theoretical amount as predicted by Faraday’s laws. The material removal rate or unit
removal in electrochemical reaction basically depends on the following factors [11]:
(i) Anodic reaction and current efficiency,
(ii) Mass transport and controlled anodic dissolution, and
(iii) Current distribution and shape evolution.
(i) Anodic reaction and current efficiency
Based upon the various machining conditions and electrode-electrolyte combina-
tions, different anodic reactions take place. Rate of these reactions depends upon the
ability of the electrochemical cell to remove the reaction products as soon as they
are formed, and supply of fresh electrolyte at machining zone. All of these factors
influence the machining performance namely dissolution rate, shape control and
surface finish of the workpiece. The current efficiency (η) of the metal dissolution is
related to the weight loss (∇w), which is given as:
rw:z:F
g¼ ð8:20Þ
I:t:M
where, ‘z’ is the valency of metal dissolved, ‘F’ is Faraday’s constant, ‘I’ is
machining current, ‘t’ is machining time, and ‘M’ is atomic weight of the metal.
Current efficiency for metal dissolution is the function of current density and
local flow conditions, and varies as a function of distance from the tool. Though
current efficiency is a commonly used factor in ECM, a more accurate evaluation of
the process requires an estimate of electrical power efficiency. Power efficiency is
the ratio between output power and input power of a device. Conductivity of
electrolyte increases with the increase of temperature. Hence, for the same operating
condition power requirements decreases and power efficiency increases.
(ii) Mass transport and controlled anodic dissolution
Electrolyte with negligible flow velocity or almost stagnant electrolyte is utilized in
the case of EMM. Therefore, mass transport plays significant role in shaping and
surface finishing of anode in dissolution process. Rate of electrochemical reactions
at electrode surfaces are mainly influenced by the current passing through the
electrodes, and also depends on mass transport, various surface effects, and kinetic
variables. Current distribution and machining accuracy may get affected by mass
transport conditions. The simplest electrode reactions are those in which the rates of
8 Electrochemical Micromachining (EMM): Fundamentals and Applications 291
v:F:D:Csat
J¼ ð8:21Þ
d
where, ‘D’ is the effective diffusion coefficient that takes into account the contri-
bution from transfer by migration, ‘Csat’ is surface concentration, and ‘d’ is dif-
fusion layer thickness.
(iii) Current distribution and shape evolution
The nature of current distribution pattern also influences the shape generation and
degree of leveling in EMM. In through mask EMM, three different scales must be
considered with respect to current distribution, i.e. workpiece scale or cell scale,
pattern scale and feature scale. At the workpiece/cell scale, geometry of the
workpiece and tool can be controlled by the current distribution. On the pattern
scale, current distribution is achieved by carrying out dissolution under mass
transport control. Current distribution also depends on the spacing of the features
and on their geometry. On the feature scale, shape is evaluated through the current
distribution. The current distribution at the anode depends on the geometry, anode
reaction kinetics, electrolyte conductivity and hydrodynamic conditions.
292 V. Rathod et al.
Material removal from the workpiece surface is not limited by photoresist masking
but is controlled by localized material dissolution mechanism. Highly localized
selective metal dissolution from workpiece surface can generate the desired pattern
or shape in 2D or 3D scale [15]. Anodic dissolution in maskless EMM is controlled
by the current density, which depends on various predominant machining param-
eters. Inter electrode gap between the workpiece surface and tool is maintained at a
very low value such that stray current effect is minimized. Passivating electrolyte is
suitable for maskless EMM due to its ability to form transpassive oxide films and
evolve oxygen in the stray current zone. To achieve highly localized anodic dis-
solutions, maskless EMM requires machining setup for precise movement of the
tool as well as workpiece. During micromachining, to maintain and monitor the
narrow IEG, the EMM setup needs highly sensitive sensing and controlling devices
that should work on close loop control strategies. Circulation of fresh electrolyte at
narrow machining zone is one of the important challenges in maskless EMM.
Selection of a suitable electrolyte during micromachining of different materials is
another essential task that influences the controlled metal removal process at dif-
ferent metal–electrolyte combinations. Another significant problem is the removal
of machining by-products such as sludge, gas bubbles, and heat generated at fine
IEG. For effective localization of metal removal, maskless EMM demands a higher
frequency pulsed power supply.
Maskless EMM is competent to machine a high aspect ratio micro feature, which
is one of the main limitations of through-mask EMM process. One of the main
advantages of maskless EMM is the machining of 3D micro features. Different
types of micro features can be fabricated by maskless EMM by exploiting its
flexibility of material removal mechanism. It can be utilized to generate
microstructures starting from a very low depth to very high aspect ratio, including
surface structuring, micro patterns, deep micro holes, as well as 3D micro features.
Depending on the depth of machining and geometrical complexity of the micro
features, different techniques of maskless EMM may be selected. Maskless EMM
can be classified into three categories, for example, Jet EMM, micro drilling, and
8 Electrochemical Micromachining (EMM): Fundamentals and Applications 295
Fig. 8.9 Microholes and micro patterns machined by a jet EMM [15], b micro drilling, and 3D
EMM [16]
3D EMM. Figure 8.9a shows micro hole array and micro pattern machined by jet
EMM on stainless steel foil of 250 µm thickness with a nozzle diameter of 100 µm,
voltage 56 V, 5 M NaNO3 as an electrolyte, with at a feed speed of 300 µm/s. The
cavity has a geometries consisting of lines having length of 1500 µm and semi-
circles with a radius of 250 µm, depth of about 180 µm and width of approximately
190 µm. Figure 8.9b shows the micro hole and micro patterns machined on nickel
at 1 MHz pulse frequency, 5% NaCl + 0.3 M HCl electrolyte concentration, 3 V
applied voltage, 30 ns pulse duration, 50 lm tool diameter [16].
predominant process parameters, which have major influences on EMM criteria are
identified as follows:
(i) Nature of power supply i.e. DC or pulsed DC, its amplitude, and pulse
frequency etc.
(ii) Microtool parameters like shape, size, surface quality, IEG, tool feed rate.
(iii) Electrolyte parameters such as type of electrolyte, its concentration, tem-
perature, flow rate, and density.
(iv) Mechanical capabilities of machining setup such as resolution, rigidity, damp
proof structure etc.
Electrical power is the driving force for the flow of charged particles inside the
electrolyte, which is essential for continuation of electrochemical reaction. The
applied power supply may be direct current or pulse direct current. With direct
current supply workpiece material dissolves continuously. It may give very high
concentration of reaction products, which can only be partly removed by the elec-
trolyte, especially if the inter-electrode gap is very narrow. The increasing contam-
ination can cause a deposit to form on the microtool surface, so that the workpiece
material no longer dissolves uniformly. Furthermore, changes in the electrolyte
composition rise in electrolyte temperature, and increase in electrical resistivity can
8 Electrochemical Micromachining (EMM): Fundamentals and Applications 297
also affect the machining accuracy. These problems can be largely minimized by
applying the pulsed direct current instead of continuous one [20]. Pulse duration and
the intervals between the pulses are properly matched to the current density, so that
the machining gap can be completely swept clean during machining resulting in a
continuous EMM process. The pulse off-time should be long enough to ensure a
complete flushing of the electrolyte in narrow machining gap. The current efficiency
is much more dependent on the current density when pulsed current is used than the
use of continuous current. With continuous supply, the efficiency decreases gradually
when the current density is reduced, where as with pulsed supply the decrease is
much more rapid. A steep fall in efficiency with decreasing current density improves
the machining accuracy. This improvement depends upon the pulse duration and to
somewhat lesser extent on the interval. By using pulsating current one can apply
extremely high instantaneous current densities to the workpiece without the need for
an elaborate electrolyte pumping system and rigid machine frame. This is possible
since each current pulse is followed by a relaxation time of zero current, which allows
removal of reaction by-products and heat from the inter electrode gap. Compared to
direct current dissolution where only average current can be chosen, pulsating current
has three parameters, i.e. pulse on-time, pulse off-time, and peak current density
which can be varied independently in order to achieve a desired machining rate. By
proper selection of these parameters, it is possible to minimize variations of elec-
trolyte conductivity in the machining region and to achieve high instantaneous mass
transport even at low electrolyte flow rates. On the other hand, the average current
density in pulse EMM is lower than the direct ECM. Pulsating current is therefore,
particularly suitable for high precision micromachining of delicate micro features
where high electrolyte flow velocity cannot be tolerated. Shorter pulse period is
preferable for achieving higher accuracy. Anodic dissolution becomes more local-
ized, the throwing power is more restricted and the machining accuracy is improved
with the application of shorter pulses.
machining method for actual micro machining applications. Some of the important
issues related to the micro tool are as discussed below:
(a) Microtool material
EMM demands micron sized tools to be used in working conditions like extremely
corrosive environment, at elevated temperature due to Joules effect. Hence,
microtool materials should have properties like high electrical and thermal con-
ductivity, good wear and corrosion resistance, mechanical strength i.e. stiffness to
withstand the pressure of electrolyte, and be easily machinable. Considering these
requirements of the microtool materials, the microtools are generally made of
chemically inert materials. The best choice of the materials limits to tungsten,
platinum, titanium, and some super alloys. Other metals, such as gold, nickel,
copper, silver, molybdenum, and steel are also used as electrode materials in
connection with specific applications. Among a wide choice of metals available,
tungsten and its alloy, platinum and its alloy, and titanium are most widely used as
metallic electrodes. Such electrodes offer a very favorable electron-transfer kinetics,
large anodic potential range and low hydrogen overvoltage. Platinum wire is a soft
metal but alloying with iridium and rhodium increase its hardness. Tungsten is
widely used as tool material because of its important properties like high rigidity,
toughness and resistance to chemicals [21].
Tungsten carbide (WC) with cobalt binder is also used as tool material. Titanium
and its alloys have also been used in electrochemical micromachining due to the
high strength, high melting point and has proven suitable for harsh environment
where the corrosion resistance plays a major role. Tungsten wires are commercially
available in a long pieces and cutting-off the tungsten wire with wire cutter or micro
grinder may leave burrs or micro-cracks. Therefore, the cut ends should be grind
and clean in order to get a good microtool tip shape. No single material has been
proven to be superior over all others, no single material can satisfy all the microtool
design purposes, since each material has its benefits and limitations.
(b) Microtool shape, size, and surface finish
In EMM, geometry i.e. shape of the microtool plays an important role in machining
accuracy, as well as machining performance. Microtool size is also an important
parameter to be considered in EMM, which helps to improve the machining
accuracy, as well as machining performance [22]. Microtools of higher diameter
increases the effective surface area of microtool, increasing machining current and
tool polarization area, and finally generates micro features of higher overcuts. Use
of micron sized tool, not only generates accurate micro features but also takes less
time to machine the micro features [23]. Microtools with different end shapes have
already proven their effectiveness in micromachining applications. Cylindrical
microtools with flat end, conical end, reverse conical end, spherical end, and disc
shaped microtools, can be developed by different methods and utilized in EMM
[24]. Use of disc shaped microtool generates straight walled micro features of
higher depths, with minimum stray current effects. Surface quality of the microtool
also plays an important role during machining of micro features by EMM.
8 Electrochemical Micromachining (EMM): Fundamentals and Applications 299
The minor defects on the surface of microtool, directly affects the surface quality of
machined micro features [25]. This can be observed on features machined with a
microtool having a surface not finished to a high degree of surface smoothness. The
presence of nicks, notches, scratches, lines, burrs, or other similar type of surface
defects will be reproduced as the mirror image on the work surface. Therefore,
special care must be taken to maintain the surface of the microtool very smooth.
(c) Microtool insulation
While machining micro features of high aspect ratio by EMM, workpiece material
dissolves from the front end, as well as the lateral surface of the microtool. This
results a micro features whose entry side is wider than exit side i.e. taper along the
depth and also poor surface quality due to stray current effects [26]. Therefore
sidewalls of the microtools are insulated to minimize the stray current effects and
taper formation along the walls of the micro features.
(d) Microtool feed rate
In EMM, material dissolution depends upon machining time also. Tool feed rate
regulates the time for which microtool is available at particular position during
machining of micro features, hence microtool feed rate is one of the important
process parameter in EMM. The micro tool feed rate should be always less than
material removal rate to avoid short circuit during machining, since short circuit can
seriously damage both the microtool and delicate surface of workpiece. The
maximum value for the microtool feed rate for a particular machining condition can
be determined depending on the occurrence of sparks or short-circuits between
microtool and the workpiece during machining operation.
The aforesaid changes mean that the electrolyte has got finite life and in practice
the life may be limited because of the following reasons:
(i) The need to maintain a reasonably constant electrical conductivity so as to
facilitate the control over the process and to ensure the machining accuracy.
(ii) The need to prevent plating out of dissolved material on the microtool sur-
face to ensure the machining accuracy.
(iii) The need to avoid formation and accumulation of excessive quantities of
precipitate and sludge at narrow machining zone.
The first of the aforesaid consideration applies to all type of electrolytes, the
second consideration applies mainly to acidic electrolytes and the third one applies
mainly to neutral type of electrolytes.
(d) Electrolyte concentration, temperature and flow
(i) Electrolyte concentration
The electrolytes in electrochemical cell carry electrical current by the movement of
ions and the number of ions available for electrochemical reaction increases with
increases in concentration. Therefore increased concentration of an electrolyte offers
low resistance to flow of current resulting increased electrical conductivity. The
magnitude of conductivity is determined by the type and number of ions present in
the electrolyte. Hence, to compare the conductivities of the different electrolytes, the
term electrolyte concentration is generally used, which can be applied to all elec-
trolytes. Electrolyte concentrations are measured as weight of the solute per unit
(w/w) or weight per unit volume (w/v) of solution, or the volume of the solute per unit
volume (v/v) of the solution. Molecular weight in grams i.e. gram-molecules, or
moles of solute per liter of solution (M), is generally used to measure the concen-
tration of the electrolytes. Electrical current is carried out by the movement of ions in
electrochemical cell. The rate of ionic movement is termed as the ionic mobility.
Increase in electrolyte concentration increases machining current due to reduced
electrolyte resistance, however further increase in electrolyte concentration reduces
the electrical conductivity due to reduced ion mobility. Also increased density of
electrolyte at very high electrolyte concentration makes it difficult to remove the
process by-products from narrow machining zone. Therefore dilute electrolytes are
preferred in electrochemical micromachining of micro features [28].
(ii) Electrolyte temperature
During electrochemical micromachining of micro features, electrolyte concentration
and temperatures are expected to be constant throughout the process for machining
the micro structures with uniform features. Temperature of electrolyte at narrow
inter-electrode gap increases due to Joule’s heating effect. Electrical conductivity of
an electrolyte increases with increase in temperature because of increase in mobility
of ions at increased temperature. Finally, increase in machining current because of
reduced electrolyte resistance may result micro features with varied characteristics
like increased surface roughness, reduced machining accuracy, and higher MRR.
8 Electrochemical Micromachining (EMM): Fundamentals and Applications 303
Fig. 8.12 Different types of Mechanical Machine units a column and Knee type, b gantry type,
and c structure with rotational axis
comprises of the various machine elements like main machine structure, machine
controller unit, and desktop computer with graphics user interface software.
(a) Main machine structure
Main machine structure provides rigid support to various components during
machining, and space to mount the different components such as base plate, linear
stages, tool holder at required positions. The main structure comprises of platform
with support, vertical or horizontal supports, Stepper motor or servomotor operated
long travel linear stages with precise movements to represent X, Y, Z axis.
Figure 8.12 shows the different combinations of linear stages to fabricate
mechanical machine unit.
8 Electrochemical Micromachining (EMM): Fundamentals and Applications 307
Power supply unit is very important unit in EMM system setup, since the nature of
pulse and pulse parameters directly affect the machining accuracy. Machining takes
place during pulse ‘on’ time only, and sludge removal from narrow machining zone
mainly takes place during pulse ‘off’ time, therefore pulsed DC supply with short
pulse period is preferred to machine the micro features by EMM. Better control over
process needs pulse monitoring and control of the pulse parameters during machining
operation. Main components of the power supply unit can be elaborated as:
(a) Pulse generator
Pulse generator generates DC pulses of required parameters and is the heart of
power supply system. Continuous supply of the stable pulse patterns during
machining is the prime function of a pulse generator. Various pulse parameters such
as pulse period, pulse amplitude, pulse ‘on-time’ and ‘off-time’ i.e. duty ratio, pulse
rise/fall times, positive or negative bias, as shown in Fig. 8.13 can be adjustable
from a minimum to maximum value, resulting in different outputs for the same
frequency.
(b) Digital storage oscilloscope
Digital storage oscilloscope provides the online image of the supplied pulse along
with the detail information during machining. Digital storage oscilloscope can also
be used during initial IEG setting and to monitor the machining conditions at
narrow machining zone to detect the occurrence of short circuit if any between
electrodes. As soon as the short circuit is detected, microtool feed and power supply
is turned off, and microtool is retracted back by few microns to clear the IEG, and
machining is continued again with required parameter settings. Digital storage
oscilloscope can also be interfaced to the desktop computer for online monitoring,
and pulse parameters can be directly stored using external storage devices for
further analysis.
308 V. Rathod et al.
It is the space where electrochemical reaction takes place in between anode and
cathode that are submerged in an electrolyte with very small IEG. It consists of an
electrolyte tank and workpiece holding fixture. Material used to fabricate the
electrolyte tank must be non-conductive, non-corrosive, light in weight, transparent,
machinable into the required size. Perspex is one of the most suitable materials to
satisfy all of these requirements [35].
8 Electrochemical Micromachining (EMM): Fundamentals and Applications 309
To exploit full potential of EMM, research is still needed to improve the machining
accuracy by controlling different factors such as the effect of overcut and taper
formation during the machining of various micro features. Geometrical shape, size
and surface quality of the microholes, microslots and grooves affect the perfor-
mance and service life of the various micro components. Hence, fabrication of
micro features consisting of various types of microholes; microgrooves and slots
with good shape accuracy and surface quality are the focused areas of research in
EMM. To improve the machining accuracy of EMM, the control of stray current
phenomenon is one of the major challenges. The proper removal of sludge, pre-
cipitates and gas bubbles from the very narrow machining gap in EMM is another
major challenge to the researchers. Because of the improper flushing of machining
310 V. Rathod et al.
Geometry of microtools i.e. shape and size plays an important role during con-
trolled anodic dissolutions to achieve the desired shape, size, and surface finish of
the micro-features. In many application microfeatures like straight cylindrical
microhole, taper free microgrooves and vertical walled 3D microstructures are
essential, whereas during machining of such microfeatures of higher depths using
straight cylindrical microtools, taper is formed on the sidewalls of the structure
because of the machining time difference between top face and bottom face of the
microfeature. Microtools of different shapes or end shapes such as reverse conical,
spherical based, disc shape microtools as shown in Fig. 8.18 can be successfully
used to improve the machining accuracy.
Cylindrical microtools with a flat end are suitable for machining of microholes,
microgrooves, and microcavities by controlling the movement of the tool. For
machining straight cylindrical microholes, cylindrical microtools with a flat end and
cut edge electrode can be effectively used with a rotary arrangement. Cut edge
microtools enhance the supply of fresh electrolyte flow and improve the machining
accuracy as compared to microtools with flat ends. Conical microtools are suitable
for machining of conical microholes to fabricate micronozzles required for the
applications in inkjet printers, etc. Reverse microtool electrodes are suitable for
taper reduction of microfeatures, Disk shape, and spherical end-shaped microtools
are suitable for reducing the taper formation on vertical walls of the microfeatures
with straight edges as shown in Fig. 8.19. Use of disc shape microtool restricts the
dissolution of the workpiece along the disc height only which minimizes the taper
along the vertical wall of the microfeature.
312 V. Rathod et al.
High aspect ratio micro features are commonly used in many applications. For the
fabrication of these micro features, cylindrical microtools of a few microns in
diameter are used in EMM, and scanning type machining strategies are followed for
the microtool movement. The microstructures fabricated by un-insulated microtool
are not capable of producing higher aspect ratio micro features, because of the
8 Electrochemical Micromachining (EMM): Fundamentals and Applications 313
Fig. 8.18 Microtools of different end shapes a cylindrical b cut edge c conical d reverse conical
e spherical and f disc shape
Fig. 8.19 Effect of microtool shape on wall profile of microhole machined by a cylindrical b disc
microtool
Fig. 8.20 Effect on wall profile of microhole machined a without b with, sidewall insulation
machined at 3 V, 8 MHz, 35% duty ratio and 0.2 M H2SO4. with scanning speed
93.75 lm/s and microtool feed of 0.3125 lm at the end of each scan, with and
without sidewall insulations of the microtool are shown in Fig. 8.22 [41].
In EMM, presence of fresh electrolyte at narrow machining zone is essential for the
continuation of the process. Practically, IEG between tool and workpiece is very
small i.e. of few microns and the circulation of electrolyte through machining gap is
difficult task. Fresh electrolytes cannot be circulated with high velocity through
8 Electrochemical Micromachining (EMM): Fundamentals and Applications 315
Fig. 8.21 Micro holes machined a without, b with sidewall insulations [41] and c variation in
microhole diameter
Fig. 8.22 Microgrooves and its depth profiles machined a without and b with sidewall insulations
[41]
machining zone, since it may vibrate the microtool and delicate workpiece which
will affect the stability of dissolution process and may deter the machining accu-
racy. However, it is essential to remove process by-products, heat, precipitates as
well as gas bubbles from the narrow machining gap to achieve higher machining
accuracy. There are various techniques by which electrolyte circulation in the
machining zone can be improved. Electrolyte circulation can be improved by
hybridized EMM with low-frequency tool vibration. The microtool vibrates
316 V. Rathod et al.
Micro sparks in the narrow machining zone cannot be eliminated completely, which
deteriorates the machining accuracy of EMM. The micro sparks are occurring in
narrow machining zone due to the variation in machining parameters apart from
tool feed rate, heat generation across IEG accumulation of sludge and gas bubbles
8 Electrochemical Micromachining (EMM): Fundamentals and Applications 317
in the very small IEG. The increase in gap resistance due to various reasons such as
generation of gas bubbles, sludge formation etc. leads to the occurrence of micro
sparks, causing higher overcut as well as micro spark affected zone that results in
the poor quality of final products.
8.11.1.1 Micronozzles
Micronozzles with high surface quality can be fabricated on advanced high strength
temperature resistance (HSTR) materials such as titanium, nickel alloys, and
stainless steel utilizing the EMM technique. These micronozzles can be success-
fully utilized in various applications such as injectors for automobile and aerospace
applications, microfluidic applications for heat transfer devices, as well as for
various biomedical applications. Figure 8.23 shows a magnified view of a
micronozzle fabricated by EMM utilizing a conical microtool [43].
318 V. Rathod et al.
Fig. 8.23 a Micronozzle fabricated by EMM. b Surface quality of internal wall [43]
Fig. 8.24 Microscopic image of a microhole [50], b micro slots [45] and c microgrooves by
EMM
Microholes, slots, and channels can be fabricated successfully by EMM with high
precision and quality. Figure 8.24 shows the microhole of average entry diameter
24 µm and exit diameter 22.5 µm drilled on an SS-304 plate. Conical microtool can
be used for the generation of taperless micro channel. Initial drilling followed by
milling, i.e., sinking and milling method, is used for the generation of micro channel.
Microchannels separated by very thin fins can also be fabricated by EMM [44].
8 Electrochemical Micromachining (EMM): Fundamentals and Applications 319
Fig. 8.26 Complex 3D microstructures a micro hemisphere [46] b micro cube [58]
320 V. Rathod et al.
Fig. 8.27 Microrods fabricated by EMM a microelectrode of 5.8 µm length with diff. diameters
[47] b WC micro-shaft of / 5 lm diameter and 3 mm length [48] c micro electrode of / 50 lm
[49] d sharp conical microtool [50]
Micropins or microrods of different shape and size are used for different applica-
tions, such as ultra high aspect ratio penetrating metal microelectrodes can be used
in biomedical applications for painless surgery [47]. Microrods can also be used as
microtools in EMM for machining of various micro features. These types of
micropins or microrods of different features can be easily fabricated by reverse
EMM by regulating various process parameters [48, 49]. Figure 8.27 shows the
various microtools fabricated by EMM.
Disc shape microtools have already proven their effectiveness in EMM for
machining of taper free micro features. Disc shape microtools of different features
namely disc height, disc diameter, shank diameter, and shank height can also be
fabricated by EMM. Figure 8.28 shows the microscopic image of precise disc shape
microtool fabricated by EMM from microrod of 300 µm diameter, under the
machining conditions of applied voltage 1 V, 1 MHz, 80% DR, and 1 M NaOH
8 Electrochemical Micromachining (EMM): Fundamentals and Applications 321
electrolyte [51]. For achieving strength and rigidity to the microtool, disc microtool
has been fabricated in multiple steps of diameter reduction.
Micro components fabricated by different methods may consist of uneven and sharp
edges, microburrs, and rough surfaces, which needs further finishing operations to
make them suitable for various applications. Finishing of such micro components is
a challenging task due to the size limitations. EMM can be effectively utilized for
finishing of different micro components. Some of the finishing applications using
EMM are specified as:
322 V. Rathod et al.
The print bands used in high-speed impact printers are fabricated from stainless
steel. The print band system consists of group of formed characters. Precise location
of all the characters on a band is achieved through timing marks. The characters and
timing marks on the print bands must have special characteristics to meet the
desired trade-off between ribbon life and print quality. Bands with round-edge
characters increase the ribbon life. To provide a high degree of character rounding,
the EMM should involve a high rate of dissolution. Surface finishing of print bands
is most important in print band manufacturing process. An electropolishing process
has been developed that gives microsmooth surfaces of print bands. Figure 8.29
shows a print band (a) before finishing and (b) after electropolishing and character
rounding [52].
Titanium and its alloy have very good mechanical and chemical properties, because
of which they are in high demand for various engineering applications. Surface
structuring of titanium is a main requirement in micro engineering and biomedical
applications. EMM is one of the important process for surface structuring of tita-
nium, whereas micro structuring of titanium surface is a challenging task due to the
rapid formation of passive oxide layer, which obstructs the smooth anodic disso-
lution of titanium. Figure 8.32 shows SEM micrograph of a regular pattern
machined on a titanium surface by 20 V, 200 ns pulse length and 20% duty cycle,
using ethylene glycol as an electrolyte.
Microscopic features on surfaces are critical factors that affect successful applica-
tion of titanium as a load-bearing implant in orthopedic surgery. EMM offers a
means to produce patterns on titanium surfaces. Figure 8.33 shows the microscopic
image of microhole patterns machined on Ti6Al4V for biomedical applications. Jet
electrochemical micromachining (jet-EMM) is used to machine microholes with a
high aspect ratio on titanium surfaces. The etching process was con-ducted with a
voltage of 200 V and average current of 45 mA.
8 Electrochemical Micromachining (EMM): Fundamentals and Applications 325
Anodic dissolution in EMM can be utilized for metal removal in micro as well as
nanoscopic level, because of which EMM has emerged as one of the best alter-
natives for fabrication of micro components with high quality and precision eco-
nomically. In recent years EMM technology has been introduced to meet the
increasing demands of advanced micro as well as nanoscale applications in various
fields of applications. Over the years through research and development in this area,
EMM has diversified its operational capabilities by the introduction of different
features to exploit its potential in the area of submicron and nanorange fabrication.
Different variants of EMM such as wire EMM, solid-state EMM, surface struc-
turing by EMM, micropatterning and stamping by EMM, and nanofabrication by
applying EMM have been established. Recent advancements in the area of EMM
demonstrating the potential of EMM as a solution to the various challenging
problems especially those that arise in the micro and nanofabrication areas have
been presented as:
Basic properties and characteristics of the materials are to be retained after fabri-
cation of microdevices for MEMS. Advanced engineering such as copper, alu-
minum, steel, nickel, titanium, and their alloys, are some of the most suitable
materials for the fabrications of mechanical microdevices. Machining of these
materials is a difficult task, when features as well as components are in the
microscale size. EMM can be successfully utilized for micromachining of various
microfeatures made of different metals without altering the basic material charac-
teristics and properties because of the unique mechanism of material removal by
anodic dissolution at atomic level. Therefore the process can be precisely controlled
326 V. Rathod et al.
Fig. 8.34 a Channel-net of symmetrical micro cantilevers [45], b magnetically driven micro
turbine of nickel [11], c two-level structure machined in titanium [57], d freestanding micro
cantilever [58], e high-aspect-ratio micro column [46]
Fig. 8.36 a Micro hole with array of internal microgrooves [60], b microgrooves with internal
features, machined by EMM
contact areas, i.e., shape of the apex or other electrochemical machining parameters.
Figure 8.37a shows the basic arrangement of solid-state EMM cell silver with
pyramid like microelectrode as cathode and target metal substrate M: Ag or Zn as
anode in the system. SEM image of the Ag surface after micromachining under a
constant current of 100 µA for 7 min at 873 K, is as shown in Fig. 8.37b.
8.12.3 Wire-EMM
workpiece. The motion and path of the micro wire electrode is controlled by
computerized numerical control system, and complex shape parts of high aspect
ratio can be fabricated. Different process parameters of WECM such as feed rate,
pulse voltage, and pulse on time influence the size of the machining gap that affects
the machining accuracy. Very thin wires of diameter 5–10 µm are used in this
process [63]. Platinum, tungsten, and copper are some of the common types of
wires used in wire-EMM.
In WEMM microstructures with high aspect ratio up to 30 could be fabricated by
electrolyte flushing and wire traveling. However, with further increase in aspect
ratio, machining gap becomes extremely narrow and long, during which electrolyte
flushing is less effective. Mass transport inside the machining gap plays an
important role in WEMM. The machining stability, the material removal rate and
surface quality can be significantly improved by introducing microwire vibration
along with electrolyte flushing and wire traveling during machine [64].
330 V. Rathod et al.
Fig. 8.39 Micro structures by WEMM a complex micro structure [63], b micro square helix [64]
Figure 8.39a shows the SEM image of with the slit width of 20 lm machined using
micro tungsten wire with the diameter of 5 lm, wire feed rate 0.125 lm/s., slight
vibration of workpiece with the frequency of 5 Hz, nanosecond pulses with pulse
amplitude of 4.2 V, on-time of 50 ns and off-time of 1 ls [63]. Figure 8.39b shows
the SEM image of micro square helix fabricated with 10 lm tungsten wire and
2 Hz wire vibration [64].
Anodic dissolutions can be controlled to atomic scale in EMM, which permits the
use of EMM for nanofabrication in many applications. Use of ultrashort voltage
pulses of nanosecond duration, material dissolution can be localized by spatial
confinement of electro-chemical reactions which leads to high precision machining
of metallic materials with nanometer accuracy. Use of few pulses of ultrashort
duration, complicated shapes in the nanoscale can be fabricated on the workpiece
by utilizing an appropriate shaped microtool containing nanofeatures, which allows
parallel nano-fabrication that is difficult to attain by traditional techniques.
Figure 8.40a demonstrates the improvement in machining resolution improves
with reduction in pulse duration, while machining troughs by EMM on nickel sheet
with different pulse durations, machining voltage 2.2 V, 10% duty ratio, 0.2 M HCl
and feed rate of 2 µm/min with tungsten tool tip of 2 µm diameter [65].
Figure 8.40b shows a spiral trench machined into Ni sheet with 3 ns pulses and
2 V. The depth of the spiral trench is about 5 µm and surface roughness is less than
100 µm. It proves that application of ultrashort voltage pulse in EMM may improve
the precision up to the nanometer range. Figure 8.41 shows SEM images of high
aspect ratio nanometer features fabricated by EMM in nickel sheet with 2 ns pulse
duration, machining voltage of 2.2 V, 10% duty ratio, and 0.05 M HCl electrolyte
[66]. The width of parallel lines in the center of the fabricated structure is 90 nm.
The nanometer features are machined in very short period of time, hence the same
microtool or array of microtools can be repeatedly utilized for mass production.
8 Electrochemical Micromachining (EMM): Fundamentals and Applications 331
Fig. 8.40 a Influence of pulse duration b spiral trench on Ni sheet by EMM [65]
Fig. 8.41 a Tungsten microtool fabricated by FIB, b nano-features fabricated by EMM [66]
Application of ultrashort voltage pulses with very small IEG in EMM improves
the machining precision to nanoscale and provides an alternative to the existing
nanoscale fabrication techniques which are mostly limited to two-dimensional
structures. EMM can also be successfully utilized for nano-fabrication of
three-dimensional structures economically, and in shorter time which is still a
challenge to the researchers. However, the area of EMM requires in-depth research
to make it commercially successful in various nanotechnology applications.
332 V. Rathod et al.
References
7. V. S. Bagotsky, Fundamentals of Electrochemistry, John Wiley & Sons, Inc., Hoboken, New
Jersey, USA, 2006.
8. John F. Wilson, Practice and Theory of Electrochemical Machining, John Wiley and Sons
Inc., USA, 1971.
9. Allen J. Bard, Larry R. Faulkner, Electrochemical Methods – Fundamentals and Applications,
second ed., John Wiley & Sons, Inc, 2001.
10. Bijoy Bhattacharyya, Electrochemical Micromachining for Nanofabrication, MEMS and
Nanotechnology, Elsevier Publications, Waltham, MA 02451, USA, 2015
11. M. Datta, D. Landolt, Fundamental aspects and applications electrochemical micro
fabrication, Electrochimica Acta 45 (2000) 2535–2558.
12. G.J. Kwon, H.Y. Sun, H.J. Sohn, Wall profile developments in through mask electrochemical
micro machining of invar alloy films, J. Electrochem. Soc. 142 (9) (1995) 3016–3020.
13. R.V. Shenoy, M. Datta, Effect of mask wall angle on shape evolution during through mask
electrochemical micromachining, Journal of Electrochemical Society, 143 (2) (1996) 544–549.
14. M. Datta, Fabrication of an array of precision nozzles by through-mask electrochemical micro
machining, Journal of Electrochemical Society, 142 (11) (1995) 3801–3805.
15. Matthias Hackert-Oschätzchena, Gunnar Meichsner, Mike Zinecker, André Martina, Andreas
Schubert Micro machining with continuous electrolytic free jet, Precision Engineering 36
(2012) 612–619.
16. Zhi-Wen Fan, Lih-Wu Hourng, Ming-Yuan Lin, Experimental investigation on the influence
of electrochemical micro-drilling by short pulsed voltage, Int. J. Adv. Manuf. Technol., 61
(9) (2012), 957–966
17. B. Bhattacharyya, S.K. Sorkhel, Investigation for controlled electrochemical machining
through response surface methodology-based approach, Int. J. Mater. Process. Technol.
86 (1999) 200–207.
18. J. Kozak, K.P. Rajurkar, Y. Makkar, Selected problems of micro-electrochemical machining,
Int. J. Mater. Process. Technol. 149 (2004) 426–431.
19. J. Munda, B. Bhattacharyya, Investigation into electrochemical micromachining
(EMM) through response surface methodology based approach, Int. J. Adv. Manuf.
Technol. 35 (2008) 821–832.
20. J. Kozak, K.P. Rajurkar, B. Wei, Modeling and analysis of pulse electrochemical machining,
Trans. ASME 116 (1994) 316–323.
21. P.I. Ortiz, M.L. Teijelo, M.C. Giordano, Electrochemical behavior of tungsten in alkaline
media, J. Elec-troanal. Chem. 243 (1988) 379–391.
22. B.J. Park, B.H. Kim, C.N. Chu, The effects of tool electrode size on characteristics of micro
electrochemical machining, CIRP Ann. 55 (1) (2006) 197–200.
23. M. A. H. Mithu, G. Fantoni, J. Ciampi, How microtool dimension influences electrochemical
micromachining, Int J Adv Manuf Technol (2014) 70:1303–1312.
24. Yong Liu, Di Zhu, Yongbin Zeng, Hongbing Yu, Development of microelectrodes for
electrochemical micromachining, Int. J. Adv. Manuf. Technol. 55 (2011) 195–203.
25. V. Rathod, B. Doloi, B. Bhattacharyya, Influence of electrochemical micromachining
parameters during generation of microgrooves, Int. J. Adv. Manuf. Technol. 76 (2015) 51–60.
26. Malapati, M.; Bhattacharyya, B. Investigation into electrochemical micromachining process
during micro-channel generation. Materials and Manufacturing Processes 26 (8), (2011)
1019–1027
27. S. Anasene, B. Bhattacharyya, Experimental investigation on suitability of electrolytes for
electrochemical micromachining of titanium, Int. J. Adv. Manuf. Technol. 86 (5), (2016)
2147–2160.
28. B. Bhattacharyya, Electrochemical micromachining, in: V.K. Jain (Ed.), Introduction to
Micromachining, Narosa Publishing House, New Delhi, 2014.
29. B. Bhattacharyya, S. Mitra, A.K. Boro, Electrochemical machining: new possibilities for
micromachining, Robotics and Computer Integrated Manufacturing 18 (2002) 283–289.
30. Alexandre Spieser, Atanas Ivanov, Recent developments and research challenges in
electrochemical micromachining (µECM), Int. J. Adv. Manuf. Technol., 69 (2013) 563–581.
334 V. Rathod et al.
31. Zhaoyang Zhangz, Yaomin Wang, Fei Chen, and Weiping Mao, A micro machining
system based on electrochemical dissolution of material, Russian Journal of
Electrochemistry, 47 (7) (2011) 819–824.
32. B. Ghoshal, B. Bhattacharyya, Micro electrochemical sinking and milling method for
generation of micro features, IMechE, Part B: J. Eng. Manuf. 227 (11) (2013) 1651–1663.
33. Alexandre Spieser, Atanas Ivanov, Design of an electrochemical micromachining machine,
Int. J. Adv. Manuf. Technol., 78 (5) (2015) 737–752.
34. B. Bhattacharyya, M. Malapati, J. Munda, A. Sarkar, Influence of tool vibration on machining
performance in electrochemical micro-machining of copper, International Journal of Machine
Tools & Manufacture, 47 (2007) 335–342.
35. B. Bhattacharyya, B. Doloi, and P.S. Sridhar, Electrochemical micromachining: New
possibilities for micro manufacturing, Journal of Materials Processing Technology, 113
(2001) 301–305.
36. L. Yong, Z. Yunfei, Y. Guang, P. Liangqiang, Localized electrochemical micro machining
with gap control, Sens. Actuators-A Phys. A108 (2003) 144–148.
37. T. Kuritaa, K. Chikamorib, S. Kubotac, M. Hattoria, A study of three-dimensional shape
machining with an ECmM system, Int. J. Mach. Tools Manuf. 46 (2006) 1311–1318.
38. M.A.H. Mithu, G. Fantoni, J. Ciampi, M. Santochi, On how tool geometry, applied frequency
and machining parameters influence electrochemical microdrilling, CIRP Journal of
Manufacturing Science and Technology 5 (2012) 202–213.
39. B. Bhattacharyya, J. Munda, Experimental investigation on the influence of electrochemical
machining parameters on machining rate and accuracy in micromachining domain,
International Journal of Machine Tools & Manufacture, 43 (2003) 1301–1310.
40. Hu, M.; Li, Y.; Yue, Z.; Jian, W.; Xiaogu, Z. Experimental study of micro electro-chemical
milling with side insulated electrode. Applied Mechanics and Materials, 159, (2012) 127–131
41. V. Rathod, B. Doloi, B. Bhattacharyya, Sidewall insulation of microtool for electrochemical
micromachining to enhance the machining accuracy, Int. Journal of Materials and
Manufacturing Processes, 29 (3) (2014) 305–313.
42. Natsu Wataru, Nakayama Hisashi, and Yu Zuyuan, Improvement of ECM characteristics by
applying ultrasonic vibration, International Journal of Precision Engineering and
Manufacturing, 13 (7) (2012) 1131–1136.
43. B. Ghoshal, B. Bhattacharyya, Shape control in micro borehole generation by EMM with the
assistance of vibration of tool, Precis. Eng. 38 (2014) 127–137.
44. V. Rathod, B. Doloi, B. Bhattacharyya, Experimental investigations into machining accuracy
and surface roughness of microgrooves fabricated by electrochemical micromachining, Proc.
Inst. Mech. Eng. Part B: J. Eng. Manuf. (2014) 1–22.
45. B. Ghoshal, B. Bhattacharyya, Generation of microfeatures on stainless steel by electro-
chemical micromachining, Int J Adv Manuf. Technol. (2015) 76:39–50.
46. B.H. Kim, et al., Micro electrochemical machining of 3D micro structure using dilute
sulphuric acid, Ann. CIRP 54 (1) (2005) 191–194.
47. A.B. Kamaraj, M.M. Sundaram, and R. Mathew, Ultra high aspect ratio penetrating metal
microelectrodes for biomedical applications, Microsystem Technology, 19 (2013) 179–186.
48. S. H. Choi. S. H. Ryu. D. K. Choi. C. N. Chu, Fabrication of WC micro-shaft by using
electrochemical etching, Int J Adv Manuf Technol, 31, (2007) 682–687.
49. Young-Mo Lim, Hyung-Jun Lim, Jang Ryol Liu, Soo Hyun Kim, Fabrication of cylindrical
micropins with various diameters using DC current density control, Journal of Materials
Processing Technology 141 (2003) 251–255.
50. B. Ghoshal, B. Bhattacharyya, Influence of vibration on micro-tool fabrication by
electrochemical machining, International Journal of Machine Tools & Manufacture, 64
(2013) 49–59.
51. V. Rathod, B. Doloi, and B. Bhattacharyya, “Parametric investigation into the fabrication of
disk microelectrodes by electrochemical micromachining”, Journal of Micro and
Nano-Manufacturing-ASME Transactions, 1(041005) (2013) 1–11.
8 Electrochemical Micromachining (EMM): Fundamentals and Applications 335
52. M. Datta, J.C. Andreshak, L.T. Romankiw, L.F. Vega, Surface finishing of high speed print
bands: I. A prototype tool for electrochemical microfinishing and character rounding of print
bands, J. Electrochem. Soc. 145 (9) (1998) 3047–3051.
53. D. Berestovskyi, M.P. Soriaga, P. Lomeli, J. James, B. Sessions, H. Xiao, W.N.P. Hung,
Electrochemical Polishing of Microcomponents, Proceedings of the 8th International
Conference on Micro Manufacturing University of Victoria, Victoria, BC, Canada, March
25–28, 2013.
54. Jung Won Byun, Hong Shik Shin, Min Ho Kwon, Bo Hyun Kim, and Chong Nam Chu,
Surface Texturing by Micro ECM for Friction Reduction, International Journal of Precision
Engineering and Manufacturing, 11 (5), 747–753.
55. Terje Sjöström, BoSu, Micropatterning of titanium surfaces using electrochemical microma-
chining with an ethylene glycol electrolyte, Materials Letters 65 (2011) 3489–3492.
56. X. Lu, Y. Leng, Electrochemical micromachining of titanium surfaces for biomedical
applications, J. Mater. Process. Technol. 169 (2005) 173–178.
57. D. Landolt, P.-F. Chauvy, O. Zinger, Electrochemical micromachining, polishing and surface
structuring of metals: fundamental aspects and new developments Electrochimica Acta 48
(2003) 3185/3201.
58. V. Kirchner, L. Cagnon, R. Schuster, G. Ertl, Electrochemical machining of stainless steel
microelements with ultrashort voltage pulses, Appl. Phys. Lett. 79 (11) (2001) 1721–1723.
59. Yong Liu, Di Zhu, Linsen Zhu, Micro electrochemical milling of complex structures by using
in situ fabricated cylindrical electrode, Int J Adv Manuf Technol, 60 (9), (2012) 977-984.
60. C.H. Jo, B.H. Kim, C.N. Chu, Micro electrochemical machining for complex internal micro
features, CIRP Ann. – Manuf. Technol. 58 (2009) 181–184.
61. K. Kamada, K. Izawa, Y. Tsutsumi, S. Yamashita, N. Enomoto, J. Hojo, Y. Matsumoto,
Solid-state electrochemical micromachining, Chem. Mater. 17 (2005) 1930–1932.
62. K. Kamada, M. Tokutomi, N. Enomoto, J. Hojo, Electrochemical micromachining using a
solid electro-chemical reaction at the metal/b-Al2O3 microcontact, Electrochim. Acta 52
(2007) 3739–3745.
63. D. Zhu, K. Wang, N. S. Qu, Micro Wire Electrochemical Cutting by Using In Situ Fabricated
Wire Electrode, CIRP Annals - Manufacturing Technology, 56 (1) (2007), 241–244.
64. Yong-Bin Zeng, Qia Yu, Shao-Hua Wang, Di Zhu, Enhancement of mass transport in micro wire
electrochemical machining, CIRP Annals - Manufacturing Technology, 61 (2012) 195–198.
65. M. Kock, V. Kirchner, R. Schuster, Electrochemical micromachining with ultrashort voltage
pulses-a versatile method with lithographical precision, Electrochim. Acta 48 (2003) 3213–3219
66. A.L. Trimmer, J.L. Hudson, M. Kock, R. Schuster, Single-step electrochemical machining of
complex nanostructures with ultrashort voltage pulses, Appl. Phys. Lett. 82 (19) (2003) 3327–3329.
Chapter 9
Electrochemical Micromachining
of Titanium and Its Alloys
9.1 Introduction
alloys and stainless steel, which are widely used in biomedical, electronic and
MEMS applications. EMM can be advantageously employed in most applications
related to micromachining of metallic parts due to its cost effectiveness and
achievable high precision, which are previously fabricated by chemical
micromachining.
Neutral solution like aqueous solution of NaNO3, NaCl, NaBr etc. are mostly
used as electrolyte in electrochemical micromachining process and hence it does not
cause any harmful effect to the operators. Electrochemical micromachining process
generates sludge during electrochemical dissolution. Most of the cases the sludge is
formed during the process are neutral salts, which are not harmful to the human
beings as well as to the environment. But some time these sludge materials may
contains small amount of metal ions, acids, nitrates, oils and even traces of heavy
metal ions which may be harmful to the environment and finally to the human
beings. Electrolyte is filtered during the EMM operation, which reduces the amount
and frequency of electrolyte disposal. During electrochemical micromachining
material removed only from the specified area, which also reduces the material
removal rate as well as the generation of sludge. Furthermore, the harmful sludge is
treated before disposal to the atmosphere to make the process environmental
friendly. Since miniaturization will continue as long as people require effective
space utilization with more efficient and better accuracy products without intro-
ducing any harmful material to the environment, electrochemical micromachining
process will be more important in the future.
Furthermore, the use of EMM will widen the range of materials application for
electronic industries, MEMS etc. The role of convective mass transport and current
distribution on the surface finish and shape evolution is very important.
Effective EMM process can be achieved by optimal combination of the process
parametric conditions. In order to achieve the effective and highly precise material
machining in the order of microns, the predominant process variables of the EMM
system will have to be optimally controlled.
Titanium was first discovered in 1791 by William Gregor, who was the mineral-
ogist and chemist. William Gregor observed the magnetic sand from the local river,
Helford, in the Menachan Valley in Cornwall, England, and isolated “black sand”,
now known as “ilmenite”. By removing the iron with a magnet and treating the
sand with hydrochloric acid he produced the impure oxide of a new element, called
as “mechanite”. Subsequently, Martin Heinrich Klaproth, who is the Berlin che-
mist, isolated titanium oxide from a mineral, identified as “rutile”. Greek mythology
provided him a new name the Titanium from the children of Uranos and Gaia, the
titans. Matthew Albert Hunter from Rensselaer Polytechnic Institute in Troy, N.Y.,
was able to isolate the metal in 1910 by heating titanium tetrachloride (TiCl4) with
sodium in a steel bomb. Finally, Wilhelm Justin Kroll from Luxembourg is
9 Electrochemical Micromachining of Titanium and Its Alloys 341
for the choice of material for orthopedic devices such as various implants for hip,
knee, as well as it is used to make substitute parts of the shoulder, the spine, the
elbow, and the hand. Titanium has a relatively low modulus of elasticity, which
reduces the differences in stiffness between the human bone and the implant.
The introduction of a titanium implant into the jawbone favors osseointegration
before the superstructure is built onto the implant. Today, titanium is successfully
used in prosthetic dentistry for implant screws, crowns, bridges, dental posts, inlays,
and removable partial dentures.
Titanium possesses two electrons in the third shell and two electrons in the fourth
shell. Titanium has arrangement of electrons, in which outer shells are filled before
the inner shells are completely occupied, which makes titanium transition metal. This
arrangement of electrons is responsible for the unique physical properties of titanium.
Due to the versatile physical and mechanical properties such as high strength to
weight ratio, high compressive and tensile strength, low density, high fatigue
resistance in air and seawater, and exceptional corrosion resistance. Titanium,
machining is always a concern to the researchers. Owing to poor thermal properties
of the titanium as well as low modulus of elasticity with its ability to maintain high
strength at elevated temperature made machining of titanium an intricate task.
Titanium proved its wider range of applications in different domains due to its
excellent properties. However, machining of titanium is difficult either by con-
ventional or non-conventional machining methods. In conventional machining
process, where cutting tool removed material by shearing due to deformation
through physical contact, in this mode, Titanium and its alloys are considered as
difficult to cut materials due to the high cutting temperature and the high stresses at
and/or close to the cutting edge during machining. The poor thermal properties of
the materials forced the larger portion of heat generated in machining process which
will be absorbed by the tool thus causes the rapid wear of tools. Both the high
temperature and the high stresses developed at the cutting edge of the tool may
create plastic deformation and/or accelerate the wear of the tools [3].
Low modulus of elasticity of titanium can cause chatter, deflection, and rubbing
problems [4]. During conventional machining forces perpendicular to the work-
piece may increase three to four times as a result of a build up of titanium on the
wear land of the tool [5]. Because of this high thrust force and the low elastic
344 S.S. Anasane and B. Bhattacharyya
Material removal based on the principle of anodic dissolution was started in early
twentieth century. The Russian engineer V.N. Gusev was the first to develop
Electrochemical machining set up and patented all basic principles of ECM.
The ECM process is conducted in the working chamber (electrochemical cell) of
the machine, where a workpiece (Anode) and a tool electrode (Cathode) are
positioned. The anode is connected to the positive polarity of a power supply, and
the tool electrode to the negative polarity of the power supply. The electrolyte
(usually an aqueous solution of an inorganic salt is pumped through the inter-
electrode gap (IEG) in order to remove the electrode reaction products (gases,
hydroxides) and the heat generated by the current. Electric current is passed through
9 Electrochemical Micromachining of Titanium and Its Alloys 345
the electrodes by the movement of electrons. Flow of electric current in the elec-
trolyte is takes place by the movement of ions. As the electrons transferred between
the electrodes and the electrolyte, physical changes occur at the electrodes and
anodic dissolution begins. To continue the process of material removal by anodic
dissolution tool electrode is moved in the direction of the intended anodic disso-
lution (metal loss) in order to maintain a prescribed machining gap. As the anode
dissolves, the cathode shape is reproduced on the anode i.e. work piece.
Machining of titanium by anodic dissolution is different than anodic dissolution
of other metals such as Stainless steel, copper and mild steel etc. According to the
position of titanium in periodic table and its electrochemical behaviour the titanium
is metal, which always contain a natural oxide film, when it is exposed to air, water
or media containing oxygen. Thickness of this natural oxide film of titanium ranges
from 5 to 70 Å [9]. Titanium gains its excellent corrosion resistance due to the
existence of this persistent and passivating surface film of oxide. This corrosion
resistance property of stable oxide layer obstructs the electrochemical dissolution of
titanium. Hence, to achieve controlled anodic dissolution of titanium it is necessary
to dissolve protective oxide film of titanium.
The nature of this thin tenacious film of oxide is highly passive in nature, which
makes the anodic dissolution of titanium difficult compared to most of the other
metals.
The oxocation, TiO2+ is acidic in nature and subsequently reacts with OH− to
form stable TiO2 [11].
Following chemical reaction represents the formation of stable TiO2:
Throughout the anodic dissolution process, development of oxide layer with the
help of titanium and hydroxide ions has been accelerated by the application of
electric field. This thin oxide film is highly passive in nature, causes anodic dis-
solution of titanium difficult. The controlled anodic dissolution titanium contains
this oxide film is difficult by EMM process parameters generally utilized for
micromachining of other metals especially in terms of machining voltage and type
of electrolyte. Hence, in order to attain uniform transpassive dissolution of titanium,
the oxide film that obstructs the controlled dissolution of pure titanium in the
passive potential region must lose its passivation phenomenon. Removal of oxide
film is possible when the applied potential is adequately high [12]. The passive
oxide film develops linearly with potential until a significant value is attained and
the breakdown of the film takes place from random pitting at higher current
densities and then shape controlled dissolution begins [13]. An additional factor,
9 Electrochemical Micromachining of Titanium and Its Alloys 347
which plays vital role in rupturing this passive oxide film, is the electrolyte type.
EMM offers both the advantages i.e. to achieve higher localized current density as
well as possibility to utilize various non toxic eco-friendly aqueous as well as non
aqueous electrolytes. Hence, EMM can be a potential micromachining method to
achieve controlled anodic dissolution of pure titanium as well as titanium alloys.
When potential is applied between the electrodes, electrolyte plays crucial role in
flowing the electric current from electrode to electrolyte solution to achieve anodic
dissolution through electrochemical reactions by completing the electric circuit.
Selection of electrolyte is governed by material properties of workpiece and
micromachining criteria such as machining rate, accuracy, surface texture, and
surface integrity. Type and concentration of electrolyte proves crucial in anodic
dissolution of materials which posses passive oxide film such as titanium.
Electrolytes of different combination and concentrations have been employed by
various researchers during masked as well as maskless electrochemical microma-
chining of titanium. Regular pattern of up the depth of 30 µm on pure titanium by
electrochemical dissolution through the patterned photoresist using sodium bromide
and methanol solution containing sulfuric acid and the etching performance of these
two electrolytes has been tested [14]. With the aqueous solution of bromide
irregularly shaped cavities with a rough surface have been appeared. However,
348 S.S. Anasane and B. Bhattacharyya
Regular shape and smooth surface textures were obtained when titanium was dis-
solved in the methanol electrolyte. Solution of methanol sulfuric acid has also
effective in electro polishing of titanium. It has been reported that the electro
polishing of titanium in methanol sulfuric acid electrolytes is mass transport con-
trolled. The limiting current density vary with electrolyte composition. This con-
cluded that the dissolution of titanium tetravalent species from anode surface to the
bulk solution is rate limiting due to the presence of compact salt film at the anode
surface under limiting current conditions [15]. Crucial role of mass transport phe-
nomenon in anodic dissolution process and presence of thin salt film at the limiting
current has confirmed the linear growth of passive film with potential until a critical
value reached where the film breakdown occurs and initiates the transpassive dis-
solution [13]. The porous anodization of titanium to create nano-scale features on
titanium surfaces has been possible by utilizing sulfuric acid and H3PO4 electrolyte
with potential sweep [12]. Electrochemical anodization of titanium through pat-
terned photoresist mask using 0.5 M sulfuric acid and Phosphoric acid (H3PO4)
were also performed [16]. Electrolyte combination containing Sodium chlorate
(NaClO3), Sodium nitrite (NaNO2) and sodium fluoride (NaF) can be suitable for
the generation of etchants of Hydrofluoric acid (HF) and Nitric acid (HNO3) for
machining of Ti alloy (Ti6Al4V) with the help of confined etchant layer technique
(CELT). Its micromachining resolution depends mainly on the rate of the scav-
enging reaction. Sodium hydroxide (NaOH) is an effective scavenger to obtain
sub-micrometer resolution [17]. Use of high concentration of aqueous sodium
bromide with working voltage of as high as 200 V through jet electrochemical
micromachining (Jet-EMM) technique were also successful to create deep holes in
titanium alloy [18]. Anodic dissolution of titanium has been performed in NaCl
containing ethylene glycol solution. Anodic polarization of titanium electrode in
NaCl-containing ethylene glycol solutions involves dissolution of titanium as
tetravalent species with the gas being evolved initially [19]. The electrochemical
micromachining of pure Titanium with Ethylene glycol and Sodium Bromide of
higher molar concentration up to 5 M can deliver satisfactory results however,
machining time is very high due to the slower etch rate [20]. Aqueous solution of
sodium bromide has been suitable for carrying out anodic dissolution of titanium
with the help of conventional ECM in macroscopic domain [21].
Majority of electrolytes which can dissolve titanium in microscopic domain are
Sulphuric acid, Hydrofluoric acid (HF), Nitric acid (HNO3) and combination of
Methanol and Sulphuric acid. All these electrolytes are either hazardous as well as
toxic and may create problem to environmental issues. Aqueous solution of Sodium
Bromide (NaBr) and sodium perchlorate can be suitable for anodic dissolution of
titanium. These two electrolytes can be effectively utilize for controlled electro-
chemical micro machining of titanium by employing lower range of machining
voltage and duty ratio. However, formation of black oxide film is predominant in all
these aqueous base electrolytes. In order to overcome the effect of regeneration of
oxide film due to aqueous base electrolytes non-aqueous base electrolytes can be
effectively employed. Non-aqueous base electrolytes, which are non-toxic and
environment friendly are combination of ethylene glycol and sodium bromide
9 Electrochemical Micromachining of Titanium and Its Alloys 349
In order to dissolve the titanium anodically, passive oxide film must lose its pas-
sivity. To overcome this difficulty suitable composition and type of electrolyte plays
vital role to attack on the film and to break it through pitting. However, mere pitting
or breaking the passive film at random points is not adequate. Phenomenon of
pitting should be controlled to achieve uniform dissolution of base metal i.e. tita-
nium. Another factor which is crucial to attain controlled anodic dissolution of
titanium is applied voltage i.e. voltage between cathode and anode. To achieve
uniform transpassive dissolution of titanium, the anodic oxide film that usually
protects the titanium in the passive potential region must lose its protective prop-
erties. Rapid removal of oxide film is obtained when the applied potential is suf-
ficiently high. The passive oxide film develops linearly with potential until a critical
value is attained and after that the breakdown of the film takes place from local
pitting at higher current densities and then shape controlled dissolution begins.
Hence, to achieve proper current density with the application of appropriate
potential range is crucial to overcome passivity of the oxide film. In order to attain
shape controlled dissolution the desired current density in the appropriate potential
region should maintain until the controlled dissolution gains stability. To make the
process stable so as to attain desired accuracy of the machined product, influence of
applied machining voltage, play vital role.
Study based on the breakdown voltage in terms of a change in efficiency of film
growth the change in slope of the voltage/time relation at constant current density,
are deceptive in the case of Ti in that such changes are not always accompanied by
a change in columbic efficiency. This indicates that the higher voltage is necessary
to breakdown the oxide film because the film consists of amorphous oxide which
gives way to a new anodic behaviour low efficiency oxide growth and gas evolution
associated with crystalline oxide in the film [23]. Based on the changes in the slopes
of the voltage/time relations at constant current density occurred at *100% effi-
ciency for growth indicated that there is variable oxide field strength. During
through-mask electrochemical machining, regular shape and smooth surface tex-
tures were obtained when titanium was dissolved at 8 V with mass transport lim-
iting current density [14]. Micro-dimples with a diameter of 110 lm and depth of
20 lm could be generated with applied voltage of 24 V, pulse duty cycle of 10%
and frequency of 100 Hz [24]. In masked EMM of titanium feature aspect ratio is
350 S.S. Anasane and B. Bhattacharyya
limited as well as toxic and reactive electrolytes can be used hence, applied
potential can vary from 5–30 V. However, in maskless EMM machining voltage
can be limited to the range of 8–20 V, in few exceptional cases such as
jet-electrolyte titanium machining voltage can be elevated to 200 V [18].
Maskless EMM of titanium, machining voltage is the major parameter in breaking
down the passive oxide layer. Removal of passive oxide film under the influence of
increased machining voltage is governed by the induced current density, as the
current density increases passive layer breaks randomly at some weaker points and
exposes the base metal. Further, increase in machining current rupture the passive
oxide film and turns into transpassive leads to initiation of controlled anodic dis-
solution of titanium. Increase in machining voltage tends to rise in machining
current. According to Faraday’s law material removal rate increases with machining
current and hence, higher material removed at higher machining voltage. With the
increase in machining current in the narrow machining zone Joule heating effect
generated which leads to elevation in the temperature in the narrow machining
zone. This causes variation in electrolyte conductivity results in non-uniform cur-
rent distribution in the inter electrode gap. Hence, reduces localization of current
flux flow leads to random material removal with higher stray machining. Therefore,
higher stray current flows in the micromachining zone causes more material
removal from the larger area of workpiece, results in an increase in overcut.
Figure 9.2 shows typical behaviour of radial overcut and material removal rate of
micro holes machined on pure titanium sheet of 100 µm thickness, machining
voltage is varied in the range of 8–14 V, utilizing maskless EMM process.
The micro holes machined with machining voltage of Fig. 9.3 shows the SEM
micrographs of micro holes machined at 8 and 14 V machining voltage. From the
Fig. 9.2 Effect of machining voltage on radial overcut and MRR of micro hole
9 Electrochemical Micromachining of Titanium and Its Alloys 351
SEM micrograph it is also confirmed that the effect of stray machining is pre-
dominant in micro hole machined at 14 V.
Stray machining induced by higher machining voltage can also increase conicity
or tapering effect during microfeature fabrication on titanium. The effect of stray
machining is higher at higher machining voltage, majority of stray machining takes
place at the entry of the micro hole. When micro tool further advances into the
workpiece machining depth increases, circulation of fresh electrolyte becomes
crucial and accumulation of sludge in the narrow machining gap increases which in
turn lower down material removal rate result in generation of smaller diameter at
exit of micro hole compared to entry. Hence, tapering effect takes place and micro
hole becomes taper in shape. However, this tapering effect can be utilized for
fabrication of micro nozzles. To reduce the effect of stray machining during micro
hole generation lower machining voltage is preferred or suitable microtool insu-
lation has been applied.
Duty ratio represents the percentage of time for which pulse remains on i.e. per-
centage of time available for both faradic and non-faradic current. Increase in duty
ratio in turn increases time available for faradic current. Hence, the amount of
faradic effect and current density increases results in more material removal and
causes increase in overcuts and MRR. Micro holes machined with varied duty ratio
keeping other process parameters fixed at machining voltage 8 V, pulse frequency
200 kHz, tool feed rate 0.2 µm/s and keeping electrolyte concentration as 2 M/L.
the influence of duty ratio on overcut and MRR during micro holes generation on
titanium by EMM has been shown. From Fig. 9.4, it can be observed that radial
overcut of micro hole at entry and exit is increases as duty ratio increases.
Figure shows the influence of duty ratio on overcut and MRR during micro holes
352 S.S. Anasane and B. Bhattacharyya
Fig. 9.4 Influence of duty ratio on radial overcut and MRR of micro hole
generation by EMM. From Fig. 9.4 it can be observed that radial overcut of micro
hole at entry and exit is increases as duty ratio increases.
Increase in radial overcut at entry follows linear trend. The lowest radial overcut
at 30% duty ratio at entry and exit is found to be 41 and 26 µm respectively. The
highest radial overcut is found to be 124 and 36 µm at entry and exit at 45% duty
ratio. As the duty ratio increases pulse ON time increases and machining current
flows for higher time, which causes higher material removal as well as stray
machining effect is also increases at the entry. Hence, radial overcut at entry is
much larger than exit, which in turn increases taper of micro hole. The micro hole
with highest taper angle of 41° has been obtained at 45% duty ratio. The SEM
micrograph represented in Fig. 9.5 exhibits dominant effect of larger metal removal
right from the entry of micro hole, machined at higher duty ratio of 45%.
In EMM, pulse frequency directly governs pulse period. Total pulse period
decreases as the pulse frequency increases, results in proportionate reduction in
pulse ON time. Pulse ON time plays crucial role in charging and discharging of
double layer capacitance. In the EMM, during pulse ON time of pulse period, the
total current available consists of two components i.e. non faradic current and
faradic current. Charging and discharging of double layer capacitance has been
performed by Non faradic current and faradic current governs material dissolution
rate. Thus, material dissolution performed only during faradic time of every cycle.
Increase in pulse frequency results in lower faradic time tends to lesser material
9 Electrochemical Micromachining of Titanium and Its Alloys 353
Fig. 9.6 Influence of pulse frequency on radial overcut and MRR of micro hole
removal per cycle as a result amount of sludge and gas bubbles are also lesser
which will washed out completely from the narrow machining zone during pulse
OFF time. Hence, it facilitates completely clean machining zone to accomplish
more controlled dissolution. Therefore, controlled and localized material removal
takes place which in turn improves the geometric accuracy of the microfeature. This
is clearly observed from the experimental results of MRR as plotted against pulse
frequency as shown in Fig. 9.6.
Micro hole machined with lower range of pulse frequency i.e. at 140 kHz has
282 µm entry diameter and 226 µm exit diameter. Whereas, micro hole machined
with higher pulse frequency of 200 kHz has entry as well as exit diameter is
reduced to 196 and 167 µm respectively. Hence, remarkable improvement will
354 S.S. Anasane and B. Bhattacharyya
circulate the fresh electrolyte and hence increase the convective mass transport
which in-turn increase rate of diffusion as well as conductivity results in increase in
current density.
The current efficiency, which is the ratio of observed amount of metal dissolved
to the theoretical amount predicated from Faraday’s law has been influenced by
dissolution of titanium with the application of microtool vibration. Figure 9.8
shows the change in current efficiency with respect to voltage during micro hole
machining on pure titanium.
The major change in current efficiency proves that the application of microtool
vibration facilitates circulation of electrolyte, which causes increase in the utiliza-
tion of considerable portion of machining current for the metal dissolution and leads
to increase in current efficiency which further enhances mass of metal removal
results in increase in machining depth. Figure 9.9 shows the comparison of
machining depth achieved by two conditions of with microtool vibration and
without microtool vibration. It is clear that the microtool vibration significantly
improves the controlled anodic dissolution of titanium even at lower machining
voltage.
SEM micrograph shown in Fig. 9.10 exhibits the micro holes machined on
titanium with and without microtool vibrations with machining voltage of 8 V.
Fig. 9.10 SEM image of microhole machined at a with microtool vibration b without microtool
vibrations [32]
Uncovered or unmasked metal surface is removed by high rate anodic metal dis-
solution. In through-mask EMM, metal dissolution takes place at the workpiece
surface that lies at the bottom of the cavity created by the photoresist mask [26].
The metal removal in TMEMM can be possible by two ways i.e. on one side of
masked metal or from two sides of masked anode workpiece which is as shown in
Fig. 9.11.
Through mask electrochemical micromachining of titanium has been carried out
in solutions containing hydrofluoric acid. Figure 9.3 shows a SEM micrograph of
an individual cavity etched for 2 min in a solution containing aqueous hydrofluoric
acid. An irregular shape and a rough surface texture result from crystallographic
attack by the acid solution. Anodic dissolution of titanium through the patterned
photoresist was also accomplished with the NaBr electrolyte at applied potentials
9 Electrochemical Micromachining of Titanium and Its Alloys 357
Fig. 9.11 Through-mask EMM: a one sided and b two sided [29]
mask on the anode workpiece. However, in oxide film laser lithography oxide layer
on the surface of titanium is developed through anodic oxidation of the titanium in
an anodising electrolyte such as sulphuric acid, thereafter patterning of the oxide
layer has been carried out by excimer laser irradiation in air to form desired pattern
in such a way that the irradiated area of oxide layer is exposed for anodic disso-
lution. Electrochemical dissolution of the exposed titanium metal from the irradi-
ated areas has been performed with an electropolishing electrolyte such as H2SO4 in
methanol. After dissolution, protruded oxide film due to under-etching is removed
by ultrasonic cleaning [27]. The OFLL technique is better adapted for fabricating
multilevel structures since it does not require application of a photoresist.
Figure 9.15 shows microstructure fabrication by EMM utilizing OFLL. Various
microfeatures which will find potential applications in MEMS can be effectively
produced by this method.
Electrochemical bulk micromachining method named the confined etchant layer
technique (CELT) for micromachining of titanium and its alloys. In this process the
etchant is generated electrochemically on the surface of a machining tool or a mold
360 S.S. Anasane and B. Bhattacharyya
Fig. 9.16 Trapezoidal slot microstructure fabricated on Ti alloy surface in the solution composed
of 0.2 M NaF + 0.4 M NaClO3 + 0.6 M NaClO4 + 0.3 M NaNO2 + 0.1 M NaOH [17]
9 Electrochemical Micromachining of Titanium and Its Alloys 361
Titanium and titanium alloys gained popularity in aerospace, chemical process and
biomedical industry due to their biocompatibility, good mechanical properties and
excellent corrosion resistance. Titanium has also possesses plasticity-based failure
when subjected to external loading which makes titanium superior device safety
capability with increase safety and reliability. These properties qualifies the tita-
nium as potential material to MEMS and BioMEMS applications. Titanium has also
a established superior biocompatible metal with a proven applications in dental and
orthopaedic implants, which confirms its physiological compatibility for novel
biomedical microdevices. To state few examples of such devices are microneedles
for transdermal drug delivery [22], thin-foil devices for biomolecule separation and
characterization [23], large-area thermal ground planes for electronics cooling [24,
25], and rationally nanopatterned substrates for improved cellular response [26].
Titanium has also proved its compatibility for sophisticated area such as aerospace.
In many aerospace applications, array of micro holes, micro-nozzles in titanium
alloy plays vital role in critical aerospace applications. EMM can provide better and
reliable micromachining solution for titanium micromachining so as to meet these
emerging titanium microfeatures requirements.
9.9 Conclusions
References
1. Snoeys, R., Staelens, F., Dekeyser, W., 1986, Current trends in non-conventional material
removal processes, Annals of the CIRP, 35, 2, 467–480
2. M. Peters, J. Hemptenmacher, J. Kumpfert and C. Leyens, “Structure and Properties of
Titanium and Titanium Alloys,” In: Titanium and Titanium Alloys: Fundamentals and
Applications, C. Leyens and M. Peters (eds.), 2003 WILEY-VCH Verlag GmbH & Co.
KGaA, Weinheim. (2003)
3. W. Konig, “Applied Research on the Machinability of Titanium and Its Alloys,” Proceedings
of the Forty-seventh Meeting of AGARD, AGARD, CP256, 1.11.1 O(1979), AGARD
Structural and Material Panel
4. A. R. Machado and J. Wallbank, “Machining of Titanium and Its Alloys-A Review,”
Proceedings of Institution of Mech Engrs, Part B: Journal of Engineering Manufacture,204
(1990) 53–60
5. N. Zlatin and M. Field, “Procedures and Precautions in Machining Titanium Alloys,”
Titanium Science and Technology, 1(1973)489–504
6. Kumar Jatinder, Khamba J.S., Mohapatra S.K., An investigation into the machining
characteristics of titanium using ultrasonic machining, International Journal of Machining and
Machinability of Materials, Vol. 3, Nos. 1/2, 2008
7. Vinod Yadav, Vijay K. Jain, Prakash M. Dixit, Thermal stresses due to electrical discharge
machining, International Journal of Machine Tools & Manufacture 42 (2002) 877–888
8. Yan Cherng Lin, Biing Hwa Yan, Yong Song Chang, Machining characteristics of titanium
alloy (Ti6Al4 V) using a combination process of EDM with USM, Journal of Materials
Processing Technology 104 (2000) 171–177
9. Aladjem A., Anodic Oxidation of titanium and its alloys, J.O. Material Science 8 (1973) 688–704
10. Anasane S.S., Bhattacharyya B., Experimental investigation on suitability of electrolytes for
electrochemical micromachining of titanium, International Journal of Advanced
Manufacturing Technology, DOI 10.1007/s00170-015-8309-2
11. Cotton FA, Wilkinson G, Murillo CA, Bochmann M (1999) Advanced inorganic chemistry,
6th edn. Wiley, New York
9 Electrochemical Micromachining of Titanium and Its Alloys 365
12. Zinger O.,Chauvy P.-F, Landolt D., Scale-Resolved Electrochemical Surface Structuring of
Titanium for Biological Applications, Journal of The Electrochemical Society, 150 * 11
B495-B503 * 2003
13. Landolt D., Chauvy P-F.Zinger O., Electrochemical micromachining, polishing and surface
structuring of metals: fundamental aspects and new developments, Electrochemica Acta 48
(2003) 3185–3201
14. Madore C., Landolt D., Electrochemical micromachining of controlled topographies on
titanium for biological applications, J. Micromech. Microeng,7 (1997) 270–275
15. Piotrowski O., Madore C. and Landolt D., The mechanism of electropolishing of titanium in
Methanol-Sulfuric acid electrolytes, J. Electrochem. Soc., Vol. 145, No.7, July 1998 The
Electrochemical Society, Inc.
16. P. Kern, J. Vehand J. Michler, New developments in through-mask electrochemical
micromachining of titanium, J. Micromechanics and Microeng. 17 (2007) 1168–1177
17. L. M. Jiang, W. Li, A. Attia, Z. Y. Cheng, J. Tang, Z. Q. Tian, Z. W. Tian, “A potential
method for electrochemical micromachining of titanium alloy Ti6Al4 V”, J Appl
Electrochemistry (2008) 38:785–791
18. Xiong Lu, Yang Leng “Electrochemical micromachining of titanium surfaces for biomedical
applications”, J of Material processing technology 169 (2005) 173–178
19. Fushimi Koji, Habazaki Hiroki, Anodic dissolution of titanium in NaCl containing ethylene
glycol, Elechtrochimica Acta 53 (2008) 3371–3376
20. Terje Sjöström, Bo Su, Micropatterning of titanium surfaces using electrochemical
micromachining with an ethylene glycol electrolyte, Materials Letters 65 (2011) 3489–3492
21. Dhobe Shirish D., Doloi B., Bhattacharyya B., Surface characteristics of ECMed titanium
work samples for biomedical applications, Int J Adv. Manuf. Technol (2011) 55:177–188
22. Bannard J., On the electrochemical machining of some titanium alloys in bromide
electrolytes, J. Applied electrochemistry 6 (1976) 477–483
23. C. K. Dyer and J. S. L. Leach, Breakdown and Efficiency of Anodic Oxide Growth on
Titanium, J. Electrochem. Soe.:ELECTROCHEMICAL SCIENCE AND TECHNOLOGY
July 1978 pp-1032–1038
24. Xiaolei Chen & Ningsong Qu, &Zhibao Hou, International Journal of Advanced
Manufacturing Technology, DOI 10.1007/s00170-016-8807-x April 2016
25. Ghoshal B., Bhattacharyya B., Influence of vibration on micro-tool fabrication by
electrochemical machining, Int. J. Mach. Tool. Manuf. 64 (2013) 49–59
26. G.J. Kwon, H.Y. Sun, H.J. Sohn, Wall profile developments in through mask electrochemical
micro machining of invar alloy films, J. Electrochem. Soc. 142 (9) (1995) 3016–3020
27. P.F. Chauvy, P. Hoffmann, D. Landolt, Applications of laser lithography on oxide film to
titanium micromachining, Appl. Surf. Sci. 208–209 (2003) 165–170
28. M.F. Aimi, M.P. Rao, N.C. Macdonald, A.S. Zuruzi, D.P. Bothman, High- aspect-ratio bulk
micromachining of titanium, Nat. Mater. 3(2004) 103–105
29. Bhattacharyya B., “Electrochemical Micromachining for Nanofabrication, MEMS and
Nanotechnology”, William Andrew publications 2015
30. Qu Ningsong, Fang Xiaolong, Li Wei, ZengYongbin, Zhu Di, Wire electrochemical
machining with axial electrolyte flushing for titanium alloy, Chinese Journal of Aeronautics,
2013,26(1): 224–229
31. Anasane S.S., Bhattacharyya B, Investigation on micromilling of through microslots on titanium
by electrochemical micromachining, Int. J. Precision Technology, Vol. 6, Nos. 3/4, 2016
32. Anasane S.S., Bhattacharyya B, Experimental investigation into fabrication of microfeatures on
titanium by electrochemical micromachining, Advances in Manufacturing (2016) 4:167–177
Chapter 10
Electrochemical Discharge
Micro-machining of Engineering Materials
10.1 Introduction
In µ-ECDM the electrolyte cell as shown in Fig. 10.1 is similar to that used in
ECM. The workpiece is dipped in an appropriate electrolyte solution (typically
sodium hydroxide or potassium hydroxide) and the level of electrolyte is just 1 mm
above the tool tip and it is controlled by electrolyte supply unit. A constant D.C.
voltage is applied between the machining tool or tool-electrode and the auxiliary
electrode with proper polarity, generally positive terminal as anode (auxiliary
electrode) and negative terminal as cathode (tool). The auxiliary electrode is in
general a flat metal plate. The tool-electrode surface is always significantly smaller
than the auxiliary electrode surface (by a factor of 100). When tool touches the job,
there are micro-gaps present both in the surface of tool and job due to surface
irregularities. The electrolyte present in micro-gaps is responsible for the generation
of gas and vapour bubbles in the micro-gaps and surrounding tool surface. The
generation of the combined gas and vapour bubbles takes place due to electro-
chemical reactions in ECM and joule heating of electrolyte respectively. From the
analysis of the ECM, it has been found that there are two types of reactions usually
occur in the system: electrochemical reactions at the electrodes and chemical reac-
tions in the bulk of the electrolyte [3]. When the applied voltage is increased
hydrogen gas bubbles grow in size. Their nucleation site density increases, current
path gets restricted between cathode and electrolyte interface causing discharge to
occur at this interface instantly. Thus these bubbles ultimately form an insulating gas
film layer around the tool-electrode as shown in Fig. 10.2. When voltage gradient is
sufficient to breakdown this gas bubbles layer between the tool and workpiece i.e.
beyond a threshold value, a conductive path is developed for the spark discharge
owing to the ionisation of the gas bubbles, which thereby causes the flow of a large
amount of current. The electro-discharge action takes place between the tool (cath-
ode) and the electrolyte across the gas bubble layer. Each electric discharge causes a
focused stream of electrons to move with a very high velocity and acceleration from
the tool (or cathode) towards workpiece. Ultimately it creates the compressive shock
waves on the workpiece surface as depicted in Fig. 10.3. This discharge phenomenon
occurs within few micro-seconds and as a result temperature of the spot hit by
370 B.R. Sarkar et al.
the focused stream of electrons may rise to a very high value. When this temperature
is above the melting temperature of the workpiece, material is melted and finally
vapourised.
these materials. In Abrasive Water Jet Machining (AWJM) the cutting ability is
hazardous due to the traverse cutting speed and requires high investment as well as
maintenance cost. Also the quality of the product is not so good due to the
machined surface roughness. Ultrasonic Machining (USM) is generally used for
machining electrically non-conductive material but this process has some inherent
limitations such as tool wear, high capital cost and there is a chance of tool bending.
In case of Laser Beam Machining (LBM) a high intensity of monochromatic light is
used during machining operation. But this process requires very high investment
and the formation of very large undesirable heat affected zone degrades the quality
of the product. ECM requires high capital investment, skilled labour to operate and
large space for installation. Also the disposal of used electrolyte and effect of stray
current are the major drawbacks of ECM process. Electro-discharge machining
(EDM) has some drawbacks like difficult to fabricate various shapes, long
machining time required to produce micro-products and high cost of equipments.
Also, the process is useful mainly for electrically conductive materials.
Hence, there is a need of special machining process, which will be helpful for
fabricating products of electrically non-conductive materials and can cope up the
adverse effects of above machining processes. Electrochemical Discharge
micro-Machining (micro-ECDM) process has a great ability to machine electrically
non-conductive materials. It utilizes the electro-discharge phenomena to machine
advanced engineering materials such as ceramics, glass etc. In comparison to above
machining processes, thermal effects i.e. formation of heat affected zone is small.
The process is independent of physical and chemical properties of the material. The
investment cost is very low.
Sources Process
of Error Parameter
The accuracy in positioning of the machining zone with respect to the measuring
point should be high. Inaccurate positioning of the workpiece may damage the tool
electrode. Hence, workpiece and its holding device preparation have some effects
on machining accuracy. The electrode holder is manipulated by turning, conven-
tional drilling and milling etc. In micro-ECDM the material is removed from both
the tool and workpiece due to the thermal effect. This causes the errors in the
machining process. Also, plating and etching of workpiece take place due to
chemical reactions. When machining is done by micro-ECDM, side sparking lies
among the problematic areas observed during machining the workpiece materials.
Controlling this side sparking is not easy task. By using the heat absorbed material
or insulator the side sparking may be controlled to some extent. Again, the con-
trolling of feed rate in micro machining by electro-chemical discharge phenomenon
is a difficult task. Feed can be given by two ways: one is where workpiece is fed and
tool is kept stationary, another is where the tool is fed keeping the workpiece
stationary. To modify the feeding arrangement some researchers used various types
of special devices such as gravity and spring feeding mechanisms, encoder, dial
indicator and load cell.
One of the major problems in micro-ECDM process is to control the DC power
supply, which provides the breakdown voltage and essential current flow that
causes sparking. The ranges of voltage, frequency and duty ratio are provided from
the power supply unit. Selection of critical process parameters for micro-machining
is not also an easy task. Carefully selected machining parameters and lots of pilot
experiments with different electrolyte concentrations can give better result for
finding the range. From various research works, different process parameters and
their ranges have been investigated and with the help of experimental design the
combination of various process parameters are chosen to carry out various
machining operations. For example, the suitable concentration is not same for
NaOH and KOH electrolytes to perform the machining operation by using
micro-electrochemical discharge machining process. Also, mixing of these two
electrolytes may enhance the performance of the machining process though the
necessity of suitable concentration range is hard to find.
Micro-
ECDMing
Operation
Building
micro and
nano
systems
The micro-ECDM can be effectively used for high precision machining opera-
tions such as making grooves, micro-channels and 3D micro-machining etc. [12,
13]. Figures 10.7 and 10.8 exhibit some examples of micro-features generated by
micro-ECDM process on glass. Micro channel formation and surface treatment can
be done by micro-ECDM [14]. Glass-based micro-fluidic systems can be produced
by µ-ECDM [15].
376 B.R. Sarkar et al.
in one direction and the vice is placed on a rotating table for proper positioning of
the job with tool. Within the machining chamber, job-holding unit, tool holding
unit, inter-electrode gap controlled unit, auxiliary electrode device and feeding unit
have been attached. At the bottom of the chamber there is an exit passage for the
electrolyte to flow out.
The job, which will be machined, should be hold rigidly for getting better
micro-machining performance and the developed job holding unit fulfils this pur-
pose. In the system the job is placed on a supporting plate, which itself rests on a
support structure connected to the machining chamber of µ-ECDM system. The
supporting plate is also made of stainless steel. A rectangular shaped cover plate,
made of Perspex, is placed on the job in order to restrict the movement of work-
piece during machining operation. The cover plate is tightened at four corners with
the supporting plate by nuts. There is a slot on the cover plate for the easy
movement of tool towards the job during micro-machining. The displacement of the
job from the original job holding position may lead to the variation in the
dimensional accuracy of the job.
378 B.R. Sarkar et al.
Since the rigidity of micro-tool as well as its holding unit is one of the main factors
in micro-machining processes. Special attention has been given during the devel-
opment and fabrication of such tool-holding unit. In µ-ECDM system, tool holder
not only holds micro-tool during machining operation but also provides enough
rigidity to micro-tool as well its holding unit. The micro-tool holding unit is made
up of mild steel and consists of a small drill chuck having internal thread at one end.
Lower portion of the support column is made of insulator to insulate the remaining
part of the machine from tool holding arrangement. To generate micro-channel on
the workpiece a template with a curved profile on its outer edge is made and fitted
with the tool holding unit so that the tool can move along the same profile guided
by the template. The tool holder along with micro-tool can be rotated by a handle.
The tool holding unit is fitted with the cover plate by means of screw-nut mech-
anism so that the position of the tool can be adjusted according to the requirement.
There is also a provision for connecting the micro-tool holding unit to the negative
terminal of power supply unit. The diameter of micro-tools used for experiments is
ranging from 300 to 400 µm and the material is stainless steel or other. The
schematic diagram of the micro-ECDM set-up for micro-structuring is shown in the
Fig. 10.10.
The tool material is worn out due to thermal effect of the process and it influences
the process performances specially the accuracy and repeatability. So, the devel-
opment of micro-tool for micro-ECDM process is a hill task and depends on the
physical and chemical properties of micro-too material. There are several types of
micro-tool such as cylindrical shaped with flat end, conical end and spherical end
etc. are generally used in micro-ECDM process. The fabrication techniques of the
micro-tools and their materials in micro-ECDM are quite similar with the fabri-
cation techniques and materials of micro-tool used in micro-EDM process. The
micro-tool is developed by wire electro-discharge grinding (WEDG) technique,
block electro-discharge grinding (BDG) technique, electrical discharge grinding
using two block electrodes (EDG-TBE) and also by rotary disc with wire
electrode-discharge grinding technique etc.
Two electrodes are immersed into the electrolyte to complete the electrolytic cell.
Micro-tool is considered as one of the electrodes in micro-ECDM process.
µ-ECDM process machines electrically non-conducting materials. Workpiece
cannot be used as another electrode because it is electrically non-conducting.
Therefore, a special electrode known as auxiliary or counter electrode is necessary
to complete the electrolytic cell and highly electrically conductive material is used
to act as auxiliary electrode. In µ-ECDM system auxiliary electrode is a flat rect-
angular metal plate and placed parallel to the job holding plate. It is made of
stainless steel or graphite. Also, in order to fulfil the criteria of electrochemical
discharge (ECD) phenomenon the size of auxiliary electrode is generally hundred
times greater than the area of smaller electrode i.e. micro-tool. It is connected to
positive or negative terminal of the power supply unit.
As discussed in the previous section, the inter-electrode gap plays a vital role in
µ-ECDM process. Therefore, special attention is given during its development and
fabrication in such a way that inter-electrode gap can be varied during
micro-machining operation. The distance between the tip of tool (cathode) and top
surface of auxiliary electrode (anode) is known as inter-electrode gap (IEG). In
order to study the effect of the gap on different machining performance charac-
teristics, the inter-electrode gap should be adjusted with the help of inter-electrode
gap control mechanism. Two long vertical screws are joined to the auxiliary
380 B.R. Sarkar et al.
electrode holder block and screwed to the plates projected from the top of main
machining chamber. The movement of the screws in upward or downward direction
can be adjusted by rotating the nuts. Due to this, the auxiliary electrode unit moves
in the upward or downward direction and the desired inter-electrode gap can be set
during the µ-ECDM process.
supply of electrolyte in the machining chamber is needed. The outlet pipe is fitted
with control valve at the bottom level of the machining chamber for removing the
used electrolyte containing sludge and precipitates. This can also be used for
cleaning of the machining chamber.
Fig. 10.11 a Electrical circuitry of pulsed D.C. power supply unit; b Pulsed waveform
382 B.R. Sarkar et al.
is shown in Fig. 10.11. The arrangements for adequate protective circuit for the
transformer rectifier and machine have been provided to avoid the short-circuit and
over-load conditions. But, the common µ-ECDM system is not fully compatible to
control the sparking phenomenon when it is used for micro-machining operation,
although it has some provisions such as worktable movement, tool movement, etc.
Therefore, the modification in power circuit configuration of the µ-ECDM system is
essential in order to machine non-conductive engineering materials in the
micro-machining domain with high machining rate.
An inductor does the filtering of supply voltage/current and generates high
current spikes when it is connected to the positive terminal of the power supply.
Therefore, inductance (L) is used in the power circuit of micro-ECDM set-up to
achieve controlled discharge during micro machining operation. There is a provi-
sion to vary the values of inductor during experimentation. A resistance (R) is
added to the negative terminal of power supply in the ECDM system to decrease the
load at the inter-electrode gap between tool electrode and auxiliary electrode. As in
case of micro-machining a controlled sparking as well the less energy per sparking
is desirable. There is a provision in the power circuit configuration where the value
of the resistance can be varied. A filter for light loads is observed in the capacitor,
which is connected directly across the load. The capacitor charges up to the peak
value of the input voltage and tries to maintain this value so that D.C. power supply
behaves as a smooth D.C. power supply. The capacitance (C) is connected across
the two terminals of the power supply of µ-ECDM system during micro-machining
operations. The values of the capacitor can also be varied in the power circuit
configuration of the developed micro-ECDM system. The schematic diagrams of
these various power circuit connections have been exhibited in Fig. 10.12.
The detailed specifications for the various subsystems of the µ-ECDM system are as
follows:
(i) (ii)
10.3.1 Micro-drilling
Fig. 10.13 Effects of applied voltage and electrolyte concentration on MRR [7]
10 Electrochemical Discharge Micro-machining of Engineering Materials 385
Fig. 10.14 SEM images of micro-holes machined by different tool electrodes [26]
varies with the pulse frequency because the duration of the discharge increases as the
frequency decreases, even though the total time when voltage is applied remains the
same [23]. Also, MRR is increased significantly with the help of the vibration of
gravity feed tool [24] and due to increase in drilling speed [25]. But, it decreases as
the duty ratio decreases [22].
Overcut (OC) during micro-ECDM operations increases with an increase in
applied voltage because of the fact that at high voltage a large number of gas
bubbles are generated at the tool’s sidewall. Overcut is observed small under high
voltage and low inter-electrode gap compared to that under high applied voltage
and high inter-electrode gap [7, 8]. Resistance-capacitor circuit is found to be
suitable in micro-ECDM process for low overcut [22]. A tool electrode with
spherical tip exhibits higher machining rate and accuracy as compared to the
conventional cylindrical tool electrode [26] as shown in Fig. 10.14. The combi-
nation of pulse voltage and side insulation demonstrates a significant effect on the
reduction of overcut in the ECDM micro-drilling operation [27]. By utilizing a
side-insulated electrode the overcut and roundness error of the holes are signifi-
cantly reduced [28]. Tool wear behavior for different tool materials at various
voltage levels plays an important role to preserve the machining accuracy in
electrochemical discharge micro-drilling. It is observed that the steel and tungsten
carbide (WC) tools result in better performance over brass tool [27].
Large amount of heat is generated while machining the ceramic materials by
micro-ECDM process. Heat-affected zone (HAZ) is formed around the machined
zone due to the heat energy conducted to the workpiece during sparking and
micro-cracks are produced within this zone. These cracks degrade the quality of
products. HAZ increases with an increase in applied voltage due to a higher intensity
of sparking [7, 8]. HAZ also varies with electrolyte concentration as shown in
Fig. 10.15. HAZ decreases initially with increase in concentration, gets maximized
and then starts to increase with increase in concentration. HAZ (Fig. 10.16) is
reduced for tungsten carbide tool than tungsten and stainless steel tool [26].
386 B.R. Sarkar et al.
Fig. 10.15 Effects of applied voltage and electrolyte concentration on HAZ [7]
Fig. 10.16 Current responses at optimal voltage and SEM images of HAZ [26]
activities [17]. Figures 10.17 and 10.18 show the relationships between the
machining time and the entrance diameter, respectively, with machining depth
under different magnetic field configurations [30]. Further a tool-surface bonding
reduces the machining rate during micro-drilling in gravity-feed or
constant-velocity-feed mechanism [31].
10.3.2 Micro-cutting
10.5 Summary
Acknowledgements The authors acknowledge the financial support provided by UGC under
CAS-IV programme of Production Engineering Department, Jadavpur University, Kolkata-32,
India.
10 Electrochemical Discharge Micro-machining of Engineering Materials 391
References
19. C.P. Cheng, K.L. Wu, C.C. Mai, Y.S. Hsu, and B.H. Yan, Study of gas film quality in
electro-chemical discharge machining, International Journal of Machine Tools &
Manufacture, 50 (2010) 689–697.
20. M.S. Han, B.K. Min, and S.J. Lee, Geometric improvement of electrochemical discharge
micro-drilling using an ultrasonic vibrated electrolyte, Journal of Micromechanics &
Microengineering, 19 (2009) 8.
21. R. Wüthrich, L. A. Hof, H. Lal, K. Kujisaki, H. Bleuler, P. Mandin, and G. Picard, Physical
principle and minituarisation of spark assisted chemical engraving (SACE), Journal of
Micromechanics & Microengineering, 15 (2007) S286–S275.
22. B. R. Sarkar, B. Doloi, and B. Bhattacharyya, Investigation into the influences of the power
circuit on the micro-electrochemical discharge machining process, Proceedings of the
Institution of Mechanical Engineers, Part B: Journal of Engineering Manufacture, 223
(2) (2009), 133–144.
23. D. J. Kim, Y. Ahn, S. H. Lee, and Y. K. Kim, Voltage pulse frequency and duty ratio effects
in an electro-chemical discharge micro-drilling process of Pyrex glass, International Journal of
Machine Tools & Manufacture, 46 (2006) 1064–1067.
24. R. Wuthrich, B. Despont, P. Maillard, and H. Bleuler, Improving the material removal rate in
spark-assisted chemical engraving (SACE) gravity-feed microhole drilling by tool vibration,
Journal of Micromechanics & Microengineering, 16 (2006) N28–N31.
25. M. Jalali, P. Maillard, and R. Wuthrich, Toward abetter understanding of glass gravity-feed
micro-hole drilling with electrochemical discharges, Journal of Micromechanics &
Microengineering, 19 (2009) 045001 (7 pp).
26. C. K. Yang, K. L. Wu, J. C. Hung, S. M. Lee, J. C. Lin, and B. H. Yan, Enhancement of
ECDM efficiency and accuracy by spherical tool electrode, International Journal of Machine
Tools & Manufacture, 51 (2011) 528–535.
27. C. K. Yang, C. P. Cheng, C. C. Mai, A. C. Wang, J. C. Hung, and B. H. Yan, Effect of surface
roughness of tool electrode materials in ECDM performance, International Journal of
Machine Tools & Manufacture, 50 (2010) 1088–1096.
28. P. Maillard, B. Despont, H. Bleuler, and R. Wüthrich, Geometrical characterization of
micro-holes drilled in glass by gravity-feed with spark assisted chemical engraving (SACE),
Journal of Micromechanics & Microengineering, 17 (2007) 1343–9.
29. C. T. Yang, S. L. Song, B. H. Yan, and F. Y. Huang, Improving machining performance of
wire electro-chemical discharge machining by adding SiC abrasive to electrolyte,
International Journal of Machine Tools & Manufacture, 46 (2006) 2044–2050.
30. C.P. Cheng, K.L. Wu, C.C. Mai, Y.S. Hsu, and B.H. Yan, Magnetic field-assisted electrochem-
ical discharge machining, Journal of Micromechanics & Microengineering, 20 (2010) 7.
31. T.F. Didar, A. Dolatabadi, and R. Wüthrich, Characterization and modelling of 2D- glass
micro-machining by spark-assisted chemical engraving (SACE) with constant velocity,
Journal of Micromechanics & Microengineering, 18 (2008) 9.
32. B.K. Bhuiyan, and V. Yadava, Experimental study of traveling wire electrochemical spark
machining of borosilicate glass, Materials and Manufacturing Processes, 29 (2014) 298–304.
33. K.Y. Kuo, K.L. Wu, C.K. Yang, and B.H. Yan, Wire electrochemical discharge machining
(WECDM) of quartz glass with titrated electrolyte flow, International Journal of Machine
Tools & Manufacture, 72 (2013) 50–57.
34. D. Jana, A. Ziki, T.F. Didar, and R. Wüthrich, Micro-texturing channel surfaces on glass with
spark assisted chemical engraving, International Journal of Machine Tools & Manufacture, 57
(2012) 66–72.
35. L. Paul, and S.S. Hiremath, Characterisation of micro-channels in electrochemical discharge
machining process, Applied Mechanics and Materials, 490–491 (2014) 238–242.
36. T. Singh, and A. Dvivedi, Developments in electrochemical discharge machining: A review
on electrochemical discharge machining, process variants and their hybrid methods,
International Journal of Machine Tools & Manufacture, 105 (2016) 1–13.
Chapter 11
Travelling Wire Electrochemical Spark
Machining: An Overview
11.1 Introduction
in industries. Again, these materials become more difficult to machine once they are
highly sintered. Therefore, it is crucial to develop an accurate and efficient
machining method for machining of advanced ceramic and composite materials.
Non-conductive materials e.g. glass fibres, ceramic, composites etc. can be
machined by utilizing the hybrid machining technique i.e. Travelling Wire Electro
Chemical Spark Machining (TWECSM) process. Advanced Ceramics and glass
fibre composites is having good strength, low weight, flexibility in shape and sizes,
good corrosion, high thermal shock resistance and good creep resistance than that
of monolithic metals. Advanced glass fibre reinforced composite materials can be
used in place of aluminium, steel, their alloys and other monolithic materials.
Advanced ceramics and glass fibre composites materials have extensive range of
applications in industries due to their high performance properties particularly in the
water and wastewater processing or storage, corrosive areas such as chemical
processing and storage, aeronautical and defence, automotive industry, building
construction, electrical utility, marine industry etc. Keeping in view, the hybrid
machining methods can be successfully utilized for machining of non-conductive
materials i.e. ceramics and composites. A TWECSM was designed, developed and
utilized for effective machining of e-glass fibre epoxy composite materials [1].
Authors explained the effect of various parameters of the developed TWECSM on
the machining performance characteristics. In this hybrid machining process,
removal of material takes place because of combined actions of electro chemical
reaction and electrical spark discharge action. TWECSM process has two electrodes
immersed in an electrolytic solution which may be acidic or alkaline in nature. The
workpiece material required to be machined is immersed in the electrolyte and
placed adjacent to the cathode (tool). A constant direct current voltage supply is
applied between the auxiliary electrode (anode) and the electrode (cathode). The
auxiliary electrode used usually is a flat plate has larger surface as compared to wire
surface i.e. about 100 times larger. When voltage applied is below 25 V (i.e. critical
voltage) then electrolysis occurs. H2 gas bubbles are formed at cathode (tool
electrode) and O2 gas bubbles at anode (counter electrode). It has been witnessed
that if the two electrodes (cathode and anode) both are of different sizes then after
certain applied voltage, electric sparks appear on the smaller electrode at the
electrode-electrolyte interface and the cell current drops. As voltage increases,
current density also rapidly increases. The mean radius and number of the bubbles
increases, and finally bubbles are merging in form of a gas film around the
tool-electrode.
However, the main principle of material removal in TWECSM process is electro
chemical dissolution of the workpiece and it is due to the collective effects of
electro chemical reaction and electrical spark discharge action. This collective
action takes place when applying enough direct current (DC) supply voltage to the
electrolytic cell in appropriate polarity; i.e. auxiliary electrode (anode) with positive
terminal and travelling wire (cathode) with negative terminal. When voltage applied
to tool-electrode interface reaches beyond a certain value then dissociation of
electrolyte take places and formation of H2 gas bubbles at wire tool surface (i.e.
cathode) and generates electrolytic gas film around electrode surface. There is also
11 Travelling Wire Electrochemical Spark Machining: An Overview 395
O2 gas evolution and formation of oxide films on auxiliary electrode (i.e. anode)
surface during machining of non-conducting materials. When number of H2 gas
bubbles formed at the cathode becomes larger thereby resistance at tool-electrolyte
interface becomes very high, it is due to the restriction caused by the gas bubbles
insulating effect. Because of the above actions there is an increase in the Joule
heating around the wire electrode which turned electrolyte in form of vapours. So,
there is a formation of a spark in the wire-electrolyte circuit because of the
inductance similar to an electrical circuit.
Some of the researchers already worked on electro chemical spark machining and
travelling wire electro chemical spark machining. They published their research
outcome as well. Basak and Ghosh [2] investigated the electro chemical discharge
machining and concluded that material removal rate can be substantial increased by
introducing an additional inductance. Gautam and Jain [3] investigated on elec-
trochemical spark discharge machining using various tool kinematics for
enhancement of process capabilities. Jain et al. [4] concluded that electro chemical
spark machining along with abrasive cutting tools improved the machining per-
formance of electrically non-conducting materials, borosilicate glass and alumina.
Kulkarni et al. [5] studied the discharge mechanism in electro chemical discharge
machining and identified the basic mechanism of rise in temperature and material
removal with the help of experimental observations for time-varying current in the
circuit. Mediliyegedara et al. [6] studied the electro chemical discharge machining
process and concluded that the ECDM process has different advantages over ECM
and EDM because of higher machining performance. Manna and Bhattacharyya [7]
studied a dual response approach for parametric optimization of CNC wire cut
EDM during machining of particulate reinforced aluminium silicon carbide metal
matrix composite. They used Taguchi method of experimental design and the
significant factors were identified for machining performance characteristics during
WEDM of Al/SiC-MMC. Mohen and Shan [8] reviewed the electro chemical
micro-to-micro-hole drilling process and concluded that advanced hole-drilling
process like jet-electrochemical drilling can be accepted in producing large number
of quality holes in difficult to machined materials. Different authors such as
Kulkarni and Jain [9], Hwa and Ling [10], Singh et al. [11], Manna and Khas [12],
Manna and Narang [13] carried out experimental investigation on micro EDM and
electrochemical spark machining processes; they explained the effects of various
parameters on response characteristics. Theory proposed by Jain et al. [4] applied to
ECM process that H2 gas liberated and accumulated at the cathode (i.e. travelling
wire). The density of bubbles at tool increases with increase in supply voltage, and
when it becomes sufficiently high, substantial constriction of the current path takes
place at the interface of the tool and electrolyte. The constriction cause an increase
396 A. Malik and A. Manna
in the resistance of the machining region and ohmic heating of electrolyte solution
becomes significant. This leads to the onset of vapour bubble nucleation on the
electrode surface in addition to the presence of hydrogen bubbles and it increases
very rapidly with the applied voltage. It is hypothesized that as the density of
nucleation reaches a critical value, vapour blanketing of the electrode occurs. The
point of contact between the electrolyte and tool is known as ‘Bubble Bridge’,
which blow-off instantly due to intense heating. Consequently, the current through
the circuit, within a very short time span, drops to zero.
Jain et al. [14] experimentally investigated the electro chemical spark machining
(ECSM) process and described that SEM photograph of the machined piece showed
micro-cracks when machining operation were performed at high applied voltages
i.e. 70 V and above. It was due to the high thermal energy input per spark which
consequently leads to thermal cracking in the glass-epoxy composite workpiece.
Authors also claimed the visibility of globules on the protruding fibres of glass fibre
epoxy composite (Fig. 11.1) when machined at 85 V supply voltage.
The evolution of heat because of sparking melts and evaporates workpiece
material. That’s seen by the existence of globules (i.e., resolidified material) on
protruding fibres (Fig. 11.1) as explained by Jain et al. [14]. Bhuyan and Yadava
[15] experimentally investigated the performance of the TWECSM through
examined the surface finished and machined kerfs width of machined samples by
SEM (Fig. 11.2). They claimed that the shape is irregular and also large heat
affected zone (HAZ) produced on the bottom side of sliced workpiece. They also
claimed that it may be due to the high applied voltage and low wire tension, which
are responsible for formation of this kind of unusual shape. Authors also claimed
Fig. 11.1 Globules visible on the protruding fibres of glass-epoxy composites at 85 V, 25%
concentration, magnification = 100 [14]
11 Travelling Wire Electrochemical Spark Machining: An Overview 397
Fig. 11.2 SEM micrographs of a kerf width and b surface finish at 55 V applied voltage, 300 µs
pulse-on time, 250 µs pulse-off time, 250 g/l electrolyte concentration and 1.8 m/min wire feed
velocity [15]
the formation of small craters and shallow cracks on the machined surface because
of higher concentration of electrolyte.
Bhuyan and Yadav [16] optimized the travelling wire electrochemical process
parameters based on response surface methodology and claimed that the effect of
wire feed velocity and voltage on Ra keeping constant value of electrolyte con-
centration (i.e. 250 g/l) and workpiece thickness (i.e. 4 mm) respectively, authors
noticed that at the beginning decreases Ra and then gradually increase in curvilinear
pattern with change in wire feed velocity as well as change in supply voltage
(Fig. 11.3). This is because of high wire feed velocity, which is not helping for
formation of bubbles at sidewall of the tool, hence formation of low crater taking
place on the machined workpiece surface. They also explained the effect of
workpiece thickness and voltage on MRR at constant value of electrolyte con-
centration (i.e. 250 g/l) and wire feed velocity (i.e. 1.8 m/min) respectively. The
variation of MRR with voltage and workpiece thickness is quite similar in nature
398 A. Malik and A. Manna
(Fig. 11.4). The MRR increases with increase in supply voltage between electrodes.
It is due to the fact that at high voltage, the generation and accumulation of gas
bubbles at the tool sidewall are very large, which leads to generate large numbers of
sparks in the sparking zone and enhances MRR (Fig. 11.4). As workpiece thickness
increases MRR also increases the reason behind this is the shifting of discharging
zone in the vicinity of the wire to the top of the workpiece and more bubble
concentration take place on the wire passing through groove resulting in higher
discharge energy per spark and thus enhances MRR as claimed by Bhuyan and
Yadav [16].
Zhu et al. [17] used micro tungsten wire of 5 µm diameter as a tool (i.e. cathode)
for the wire electro chemical micro machining. Micro slits were machined of 15 µm
width (Fig. 11.5). They also generated several complex structures with the slit
width (20 µm) by wire electrochemical micro machining process (Fig. 11.6) at
0.125 µm/s feed rate. A small workpiece vibration of 5 Hz frequency was used for
successfully circulating electrolyte in the machining zone. The nanosecond pulses
(ns) with 4.2 V pulse amplitude, 50 ns on-time and 1 µs off-time was used for
machining of complex micro structures.
11 Travelling Wire Electrochemical Spark Machining: An Overview 399
Fig. 11.6 Micro structure cutting by micro wire electrochemical cutting [17]
Jain et al. [14] concluded that travelling wire electrochemical spark machining
(TW-ECSM) of composites using NaOH as electrolyte has been found to be a
feasible and effective process. Higher machining accuracy is obtained at lower
values of voltage and electrolyte concentration. Thermo mechanical phenomenon
has been identified as the main mechanism responsible for material removal in
TW-ECSM. There is an increase in MRR at higher voltage along with the presence
of thermal cracks, large heat affected zone and irregular machined surfaces. For
higher machining efficiency, the distance between the anode and the cathode, and
the distance between the tool and the work needs to be optimized. Also, a minimum
distance between the point of power supply and the point of contact of wire with the
workpiece is expected to improve the process performance.
Bhuyan and Yadav [16] concluded that the parameters, electrolyte concentration,
workpiece thickness, and interaction effect of parameter workpiece thickness and
wire feed velocity have significant factors for Ra. Material removal rate also
affected by wire feed velocity, voltage and interaction effect of electrolyte con-
centration and workpiece thickness and square effect of workpiece thickness.
Manna and Kundal [18] concluded that the machining characteristics gradually
declines with increase in tool depth and formed micro cracks on the sliced surface
because of thermal shocks at high voltage. Three most influential parameters are
identified i.e. DC supply voltage, electrolyte concentration and gap between cath-
ode and anode. According to the authors, experimentally acquired results revealed
that moderate DC supply voltage has reduced the tendency of cracking, and at low
gap between cathode and anode generated debris during micro slicing of Al2O3
ceramics. They claimed that the sparking starts when the travel wire touches the
work-piece immersed under the electrolyte in the machining chamber. Fins and
burrs along the sliced surfaces were witnessed by the authors this is due to the
adhering of particles dispersed from the workpiece surface during machining,
which was not flash out by the flow of di-electric fluid. They explained that it’s may
be due to low flashing pressure of electrolyte; again at high flashing pressure of
11 Travelling Wire Electrochemical Spark Machining: An Overview 401
electrolyte may vibrate the wire during traveling and generates poor surface.
Scattered and fins along the sliced surfaces were formed because of the adhering of
small particles dispersed from the work surface during slicing operation, this is due
to improper flashing of di-electric fluid in machining zone.
A travel wire electro chemical spark discharge machine (TWECSM) has been
designed, fabricated and used for experimental investigation.
The developed TWECSM has main four units such as (i) power supply unit,
(ii) wire feed unit and (iii) electrolyte flow control unit and (iv) workpiece motion
control unit. A voltage rectifier (i.e. converter cum regulator) is used to convert
single phase 220 V A.C. supply into D.C. supply voltage range of 20–200 V.
Auxiliary copper plate is connected with the positive terminal of the converter cum
regulator, which is functioning as an auxiliary anode (i.e. auxiliary electrode). Tool
(i.e. wire electrode) is connected with the negative terminal of the converter cum
regulator, which is functioning as a cathode. A step down transformer with regu-
lator is used to step down the voltage; this step down voltage is used to operate a
stepper motor which runs the wire take up unit. A Direct Current supply power of
12 V is used to operate another stepper motor which rolls the used wire around the
pulley mount on the main frame. Figure 11.8 shows the schematic diagram of
indigenously developed TWECSM.
Table 11.2 represents the different input parameters of the developed TWECSM
and their parameter levels used during experiments. Taguchi method based design
of experiment L16(45) orthogonal array is employed to carry out the experiment for
cutting of e-glass fibre epoxy composite on developed machine.
11 Travelling Wire Electrochemical Spark Machining: An Overview 403
A series of experiments has been carried out with variation of different parametric
setting value and the results are utilized for further analysis. Different graphs have
been drawn to examine the various parametric effects on the different machining
characteristics of fabricated TWECSM. Different SEM photographs demonstrate
the machining characteristics (i.e. surface texture and spark gap width) during
TWECSM operation. Figure 11.9 represents a curve showing the investigated
results obtained during slicing of e-glass fibre epoxy composite, which is electri-
cally non-conductive high corrosive resistant, less weight, high strength and high
temperature resistant material on developed TWECSM. Figure 11.9 shows that
material removal (MR, mg) increases with increase of supply DC voltage. It may be
due to the increase of potential difference between the tool (i.e. cathode) and anode
(i.e. auxiliary anode) which may discharge or liberates more numbers of electrons
per unit area of cathode and simultaneously act for making crater with dissolution
of non-conductive anode i.e. work-piece. Maximum material removal is observed at
80 V DC supply voltage. Figure 11.9 is drawn on the basis of results obtained by
slicing of workpiece (i.e. e-glass fibre epoxy composite) for continuously 60 min of
machining at constant electrolyte concentration (80 gm/l), wire speed (0.15 m/min),
404 A. Malik and A. Manna
gap between tool (i.e. cathode) and auxiliary anode (120 mm), supply current
(1.5 amp) with supply voltage variation from 40 to 80 V.
Figure 11.10 represents a curve showing the investigated results obtained during
slicing of e-glass fibre epoxy composite on developed TWECSM. Figure 11.10
shows that there is increase in material removal (MR, mg) with increase in wire
speed. Effect of wire speed is smaller on material removal. Material removal is
increases with increase in wire speed because as wire speed increases fresh wire
comes quickly in the machining zone and this may cause higher number of spark
discharge which helps to form more crater per unit time. Maximum material
removal is found at 0.35 m/min wire speed. Figure 11.10 shows effect of wire
speed based on acquired results from continuously 60 min of machining at constant
supply voltage (40 V), electrolyte concentration (80 gm/l), gap between tool (i.e.
cathode) and auxiliary anode (120 mm), supply current (1.5 amp) with variation of
wire speed from 0.15 to 0.35 m/min.
Figure 11.11 shows the effect of electrolyte concentration on spark gap width.
This is drawn on the basis of investigated results acquired during slicing of e-glass
fibre epoxy composite on developed TWECSM. Figure 11.11 shows that there is
increase in spark gap width (Wg, lm) with increase in electrolyte concentration.
Effect of electrolyte concentration on spark gap width is significantly high. It may
be due to the increase of charge carriers in the electrolytic solution due to increase
in electrolyte concentration which may discharge or liberates more numbers of ions
per unit area of cathode and simultaneously act for making crater with dissolution
of non-conductive anode i.e. work-piece. Maximum material removal is observed at
electrolyte concentration (200 gm/l). Figure 11.11 is drawn based on the results
acquired during slicing of workpiece for continuously 60 min of machining at
constant supply voltage (40 V), wire speed (0.15 m/min), gap between tool (i.e.
cathode) and auxiliary anode (120 mm), supply current (2 amp) with electrolyte
concentration variation from 40 to 200 gm/l.
Taguchi method based L16(45) orthogonal array is employed and detail experi-
ments are carried out. The acquired results are utilized for optimization of
11 Travelling Wire Electrochemical Spark Machining: An Overview 405
-0.5
S/N ratio (dB) graph
Grand mean of S/N ratio (dB)
-1
Average S/N ratio (dB )
-1.5
-2
-2.5
-3
-3.5
A1 A2 A3 A4 B1 B2 B3 B4 C1 C2 C3 C4 D1 D2 D3 D4 E1 E2 E3 E4
Machining parameters and their levels
Fig. 11.12 S/N ratio by their factor level for material removal (MR, mg)
Figure 11.13 shows Scanning Electron Micrograph (SEM) of a micro sliced section
of e-glass fibre epoxy composite workpiece using travelling wire electro chemical
406 A. Malik and A. Manna
spark machine (TWECSM). The SEM graph demonstrates the real condition of the
micro sliced surface machined at supply voltage (40 V), electrolyte concentration
(40 gm/l), wire speed (0.15 m/min), gap between tool and anode (40 mm) and
supply current (1.5 amp). Figure 11.13 shows SEM photographs sliced workpiece
for continuous 60 min machining with brass 200 lm diameter wire. From SEM
graph, it is observed that micro slicing mainly proceeds in the conical manner. From
Fig. 11.13, it is clear that there are continuous burrs and fins on the surface of the
micro sliced workpiece. Over all slicing surface finish is not good when seen at
micron level. At entry level the slicing width is 296 lm but after continuous cutting
for 60 min it is found to be only 167 lm, measured just at the end of slicing. Hence
it is proved that slicing is about conical in nature. Some fins and burs are also found
during cutting in both sides of micro sliced surface. That’s due to the irregular and
insufficient electrolyte flow. During micro slicing it is also witnessed that there is
formation of foam and gas bubbles which causes a barrier for electron’s flow and
decreases electrolyte dissolution strength.
Figure 11.14 shows SEM image of a micro sliced section of e-glass fibre epoxy
composite machined on developed TWECSM. The SEM image demonstrates the
real condition of the micro cutting surface. This machining operation was carried
out at supply voltage (40 V), electrolyte concentration (120 gm/l), wire speed
(0.25 m/min), gap between tool and anode (120 mm) and supply current (2 amp).
Figure 11.14 shows SEM photographs sliced workpiece for continuous 40 min
machining with brass wire of 200 lm diameter. It is also found that there is some
11 Travelling Wire Electrochemical Spark Machining: An Overview 407
presence of continuous burrs and fins on the surface of the micro slicing. Over all
slicing surface finish is not good when seen at micron level. At entry, the slicing
width is 238 lm but after continuous cutting for 40 min it is found that this size is
being 127 lm only, measured just at the end of slicing. It’s proved that slicing is
about conical. Some fins and burs are also found during cutting in both sides of
micro sliced surface. That’s due to the irregular and insufficient electrolyte flow.
During micro slicing it is also witnessed that there is formation of foam and gas
bubbles which causes a barrier for electron’s flow and thereby decreases the
electrolyte dissolution strength.
mathematical models can be used for selection of parameters setting in advance for
effective machining on developed TWECSM.
R2 = 0.9915
where X1 = Supply voltage (Volt)
X2 = Electrolyte conc. (gm/l)
X3 = Wire speed (m/min)
X4 = Gap between anode and cathode (mm)
X5 = Supply current (amp).
Figure 11.15 demonstrates the supply voltage (Volt) and electrolyte conc. (gm/l)
effect on material removal (MR, mg). Figure 11.15 clearly shows the effect of
parameters when machining operation was carried out at high electrolyte concen-
tration (i.e. 200 gm/l) and high supply voltage (i.e. 70 V) which reflected high
material removal. It is also observed that MR is high when the electrolyte con-
centration is 50 g/l and voltage is 40 V. There is increase in material removal with
increase in electrolyte concentration and supply voltage. This is due to generation of
higher potential difference between tool and anode at higher supply voltage, which
may discharges more number of electrons per unit area and at the same time
increases electrolyte concentration thereby increases rate of dissolution of ions from
the anode. This is because of higher current density and thereby strong dissolution
effect.
The developed mathematical model for spark gap width is
R2 = 0.9984.
Figure 11.16 shows the electrolyte conc. (gm/l) and wire speed (m/min) effect on
spark gap width (Wg, lm). Figure 11.16 clearly shows that at higher electrolyte
concentration (i.e. 200 gm/l) and at higher wire speed (i.e. 0.30 m/min) the spark
gap width is high. This is also noticed that spark gap width is low when the
11 Travelling Wire Electrochemical Spark Machining: An Overview 409
2
Material removal, mg
1.5
0.5
200 80
150 70
60
100 50
Electrolyte concentration, g/l 50 40
30 DC supply voltage, Volts
Fig. 11.15 Effect of supply voltage and electrolyte conc. on (MR, mg)
100
Spark gap width, micro meter
80
60
40
20
0.5
0.4 250
0.3 200
150
0.2 100
50
0.1 0
Wire speed, m/min Electrolyte concentration, g/l
Fig. 11.16 Effect of electrolyte conc. and wire speed on spark gap width
electrolyte concentration (i.e. 50 gm/l) and wire speed (i.e. 0.15 m/min). There is
increase in spark gap width with increase in electrolyte concentration and wire
speed.
410 A. Malik and A. Manna
Glass fibre epoxy composites, ceramics etc. are non-conductive materials which are
difficult to machine by any known unconventional machining methods like ECM,
EDM and WEDM etc. These non-conductive materials can be machined with the
help of conventional machining processes but compromise with surface texture. But
conventional machining methods are not suitable even not possible to micro slicing
as well. But a new hybrid machining process which is combination of both ECM
(i.e. electro chemical machining) and WEDM (i.e. wire electric discharge
machining) can be effectively used to machine such materials. This chapter presents
some investigated published results during machining of composites and ceramics
which proved that this hybrid machining technique can effectively use for
machining of non-conductive materials. This chapter also presents the brief about
the design and development of the particular hybrid travelling wire electro chemical
spark machine. This developed machine is utilized for slicing of non-conductive
workpiece (i.e. e-glass fibre epoxy composite). By studying different experimental
results during machining (i.e. slicing) of workpiece (i.e. e-glass fibre epoxy com-
posite) on developed TWECSM, it is believe that the developed travel wire electro
chemical spark machine can be effectively use to machine non-conductive work-
piece (i.e. e-glass fibre epoxy composite). However, it is identified that during
starting of micro cutting the micro slice width is slightly more than wire diameter
(i.e. 200 µm) but after some minutes of continuous slicing the micro slice width
decreases along the depth of cut. The micro sliced surface is irregular and poor if
experiments are carried out without proper plan and optimization of parameters.
Fins and scattered along the cutting edges of the sliced workpiece are observed
because of the adhering of small particles dispersed from the workpiece surface
during slicing of the workpiece. This is due to insufficient or improper electrolyte
flow during machining. Some burrs are noticed along the edge of micro sliced
workpiece after cutting. However, experimental results also revealed that the very
good micro slicing is possible. By optimizing machining parameters generation of
high surface texture can be possible. This hybrid machining technique can be used
for machining of PSZ, zirconia, YBa2Cu3O7−x, Si3N4, PZT etc. difficult to machine
nonconductive materials.
References
3. Gautam N. and Jain V. K. (1998); Experimental investigations into ECSD process using
various tool kinematics; Int. J. of Mach Tool Manuf, Vol. 38, pp. 15–27.
4. Jain V. K.; Choudhury S. K.; Ramesh K. M. (2002); On the machining of alumina and glass;
Int. J. of Mach Tool Manuf, Vol. 42, pp. 1269–1276.
5. Kulkarni A.; Sharan R.; Lal G. K. (2002); An experimental study of discharge mechanism in
electrochemical discharge machining; Int. J. of Mach Tool Manuf, Vol. 42, pp. 1121–1127.
6. Mediliyegedara T.K.K.R.; De Silva A.K.M; Harrison, D.K.; McGeough, J.A. (2004); An
intelligent pulse classification system for electro-chemical discharge machining (ECDM)-a
preliminary study; J. Mater Process Technol, Vol. 149, pp. 499–503.
7. Manna A. and Bhattacharyya B. (2006); Taguchi and Gauss elimination method: A dual
response approach for parametric optimization of CNC wire cut EDM of PRAl/SiC-MMC;
Int. J. Adv. Manuf. Technol, Vol. 28, pp. 67–75.
8. Mohen S. and Shan H. S. (2005); A review of electrochemical micro-to micro-hole drilling
processes; Int. J. of Mach Tool Manuf, Vol. 45, pp. 137–152.
9. Kulkarni A. and Jain V. K. (2007) “Electrochemical Discharge Machining Process” Defence
Science Journal, Vol. 57, Page 765.
10. Hwa Y. B. and Ling W. K. (2007); A study on the mirror surface machining by using a
micro-energy EDM and the electrophoretic deposition polishing; Int. J. Adv. Manuf. Technol,
Vol. 34, pp. 96–103.
11. Singh Y. P; Jain V K; Prashant Kumar and Agrawal, D. C.; (1996), Machining piezoelectric
(PZT) ceramics using an electrochemical spark machining (ECSM) process, J. Mater Process
Technol, 58: 24–31.
12. Manna Alakesh. and Khas Kanwaljit; (2009), Micro machining of electrically non-conductive
Al2O3 ceramic, Journal of Machining and Forming Technology, 1(1–2): 101–112.
13. Manna Alakesh; and Narang, Vivek; (2012), A study on micro machining of
glass-fibre-epoxy composite by ECSM process, Int. J. Adv. Manuf. Technol, 61: 1191–1197.
14. Jain V. K., Rao P. Sreenivasa, Choudhary S. K., Rajurkar K. P. (1991) “Experimental
investigations into travelling wire electrochemical spark machining (TW-ECSM) of
composites”, Journal of Engineering for Industry, Vol. 113/75.
15. Bhuyan B. K. and Yadava V. (2014) “Experimental study of traveling wire electrochemical
spark machining of borosilicate glass”, Journal of Materials and Manufacturing, Vol. 29,
pp. 298–304.
16. Bhuyan B. K. and Yadava V. (2013) “Experimental modeling and multi-objective
optimization of travelling wire electrochemical spark machining (TW-ECSM) process”,
Journal of Mechanical Science and Technology, Vol. 27(8), pp. 2467–2476.
17. Zhu D., Wang K., Qu N. S. (2007) “Micro wire electrochemical cutting by using in situ
fabricated wire electrode”, Annals of the CIRP Vol. 56, pp. 241–244.
18. Manna Alakesh and Kundal Amandeep; (2015), An experimental investigation on fabricated
TW-ECSM setup during micro slicing of nonconductive ceramic, Int. J. Adv. Manuf.
Technol, 76: 29–37.
Index
Intensifiers, 9 Magnetostrictively, 63
Inter Electrode Gap (IEG), 37, 96, 99, 278, Magnetostrive, 77
282, 296, 304, 339 Manufacture, 94
Internal cylindrical surfaces, 11 Manufacturer engineers, 117
Ion Beam Machining (IBM), 3, 27 Marking process, 247
Irregular micro-peaks, 211 Maskants, 34
Irregular topographies, 49 Maskless EMM, 294
Ishikawa diagram, 295 Mass transfer, 291, 299
Iso-frequency, 160 Mass transport, 329
Isolation transformer, 236 Material evaporation, 198
Material removal, 48
J Material Removal Rate (MRR), 3, 65, 99, 240
Jet-ECM, 14 Mechanical failure, 173
Jet-EMM, 324 Median crack, 72
Medical fields, 5
K Melt film, 259
Kerf width, 164, 270 Melt pool, 270
Kerosene, 94 Metal Anisotropic Reactive Ion etching with
Kerosene dielectric, 116 Oxidation (MARIO), 360
Kinetic energy, 30, 82 Metal hydroxides, 284
Metallic salt, 34
L Metallurgical damage, 40
Lack-of-fit test, 268 Metallurgical property, 32
Lamp current, 270 Metal oxide semiconductor field effect
Laser Beam Machining (LBM), 3, 4, 62 transistor, 151
Laser energy, 12 Methanol sulfuric acid, 348
Laser fusion cutting, 259 Mettler Toledo, 119
Laser irradiance, 257 Microcantilever, 326
Laser irradiated zone, 206 Microchannel, 43, 228, 318
Laser irradiation, 180 Microcontact, 327
Laser micro-turning, 180 Microdimple, 323
Laser peak fluence, 241 Microdrilling process, 182
Laser polarization, 25 Micro-ECDM process, 367
Laser scan passes, 211 Micro-ECM (lECM), 6, 62
Lateral cracks, 71 Micro-EDG, 108, 109
Letter H blind, 113 Microelectrodes, 185
LIGA process, 281 Micro-Electro-Mechanical-Systems (MEMS),
Limiting current density, 291 5, 10, 43
Lithography, 27, 28 Microelectrical Discharge Machining
Localization of dissolution, 362 (µ-EDM), 6, 10, 94, 107, 118
Localized current density, 346 Microelectrochemical discharge machining, 43
Localized deformation, 71 Microfabrication, 146
Localized joule heating, 150 Microfeature, 2, 12, 43, 66, 180
Localized temperature, 95 Microfixtures, 276
Lost wax method, 6 Microfluidic channels, 243
Low-frequency tool vibration, 315 Microfluidics, 17
Lubrication film, 48 Microfuel cells, 5
Microgear, 39
M Microgear dies, 176
Machine controller unit, 307 Micrographs, 140
Machine spindle, 68 Microgroove, 5, 45, 184
Machining accuracy, 309, 316 Microhemisphere, 319
Machining efficiency, 101, 134 Microhole, 5, 119
Machining zone, 49, 82, 115, 131, 146 Microhole generation, 141
418 Index