Splitting Tensile Strength of Intact Rock Core Specimens: Standard Test Method For
Splitting Tensile Strength of Intact Rock Core Specimens: Standard Test Method For
Splitting Tensile Strength of Intact Rock Core Specimens: Standard Test Method For
1
D 3967
with a thickness-to-diameter ratio (t/D) between 0.2 and 0.75.
The diameter of the specimen shall be at least 10 times greater
than the largest mineral grain constituent. A diameter of 50 mm
(115⁄16 in.) (NX wireline core) will generally satisfy this
criterion.
NOTE 5—When cores smaller than the specified minimum must be
tested because of the unavailability of material, notation of the fact shall
be made in the test report.
NOTE 6—If the specimen shows apparent anisotropic features such as
bedding or schistosity, care shall be exercised in preparing the specimen
so that the orientation of the loading diameter relative to anisotropic
features can be determined precisely.
6.2 Number of specimens—At least ten specimens shall be
tested to obtain a meaningful average value. If the reproduc-
ibility of the test results is good (coefficient of variation less
than 5 %), a smaller number of specimens is acceptable.
6.3 The circumferential surface of the specimen shall be
smooth and straight to 0.50 mm (0.020 in.).
6.4 Cut the ends of the specimen parallel to each other and
at right angles to the longitudinal axis. The ends of the
specimen shall not deviate from perpendicular to the core axis
by more than 0.5°. This requirement can be generally met by
cutting the specimen with a precision diamond saw.
6.5 Determine the diameter of the specimen to the nearest
0.25 mm (0.01 in.) by taking the average of at least three
measurements, one of which shall be along the loading
diameter.
6.6 Determine the thickness of the specimen to the nearest
0.25 mm (0.01 in.) by taking the average of at least three
FIG. 1 One of the Proposed Testing Setup for Splitting Tensile
measurements, one of which shall be at the center of the disk.
Strength 6.7 The moisture conditions of the specimen at the time of
test can have a significant effect upon the indicated strength of
closely in the spherical seat, but the design shall be such that the rock. The field moisture condition for the specimen shall be
the bearing face can be rotated and tilted through small angles preserved until the time of test. On the other hand, there may
in any direction. be reasons for testing specimens at other moisture contents,
4.2.4 Rigid Seating—If a spherical seat is not used, the faces including zero, and preconditioning of specimen when mois-
of the bearing blocks shall be parallel to 0.0005 mm/mm of the ture control is needed. In any case, tailor the moisture content
block diameter. This criterion shall be met when the blocks are of the test specimen to the problem at hand and report it in
in the loading device and separated by approximately the accordance with 9.1.6.
diameter of the test specimen.
4.3 Bearing Strips (0.01 D thick cardboard cushion, where 7. Procedure
D is the specimen diameter; or up to 0.25 in. thick plywood 7.1 Marking—The desired vertical orientation of the speci-
cushion are recommended to place between the machine men shall be indicated by marking a diametral line on each end
bearing surfaces (or supplementary bearing plates; if used) and of the specimen. These lines shall be used in centering the
the specimen to reduce high stress concentration. specimen in the testing machine to ensure proper orientation,
NOTE 4—Experiences have indicated that test results using the curved and they are also used as the reference lines for thickness and
supplementary bearing plates and bearing strips, as specified in 4.2.2 and diameter measurements.
4.3, respectively, do not significantly differ from each other, but there may
NOTE 7—If the specimen is anisotropic, take care to ensure that the
be some consistent difference from the results of tests in which direct
marked lines in each specimen refer to the same orientation.
contact between the specimen and the machine platen is used.
7.2 Positioning—Position the test specimen to ensure that
5. Sampling the diametral plane of the two lines marked on the ends of the
5.1 The specimen shall be selected from the core to repre- specimen lines up with the center of thrust of the spherically
sent a true average of the type of rock under consideration. This seated bearing surface to within 1.25 mm (0.05 in.).
can be achieved by visual observations of mineral constituents,
NOTE 8—A good line loading can often be attained by rotating the
grain sizes and shape, partings, and defects such as pores and
specimen about its axis until there is no light visible between the specimen
fissures. and the loading platens. Back lighting helps in making this observation.
6. Test Specimens 7.3 Loading—Apply a continuously increasing compressive
6.1 Dimensions—The test specimen shall be a circular disk load to produce an approximately constant rate of loading or
2
D 3967
deformation such that failure will occur within 1 to 10 min of be more precisely determined when possible and reported as
loading, which should fall between 0.05 and 0.35 MPa/s (500 either water content or degree of saturation.
and 3000 psi/min) of loading rate, depending on the rock type. 9.1.7 Splitting tensile strength of each specimen as calcu-
lated, average splitting tensile strength of all specimens,
NOTE 9—Results of tests by several investigators indicate that rates of
loading at this range are reasonably free from rapid loading effects. standard deviation or coefficient of variation.
9.1.8 Type and location of failure. A sketch of the fractured
8. Calculation specimen is recommended.
8.1 The splitting tensile strength of the specimen shall be
calculated as follows: 10. Precision and Bias
st 5 2P/pLD (1) 10.1 An interlaboratory study was conducted in which
seven laboratories each tested five specimens of four different
and the result shall be expressed to the appropriate number
rocks. The specimens were cored by a single laboratory from a
of significant figures (usually 3),
common set of samples and randomly distributed to the testing
where: laboratories for testing. The study was carried out in accor-
st 5 splitting tensile strength, MPa (psi), dance with Practice E 691. Details of the study are given in ISR
P 5 maximum applied load indicated by the testing ma- Research Report No. PS #D18.12-R01, 1992, and its Adden-
chine, N (or lbf), dum, 1994. The table below gives the repeatability limit
L 5 thickness of the specimen, mm (or in.), and (within a laboratory) and reproducibility limit (between labo-
D 5 diameter of the specimen, mm (or in.). ratories) for the method.
9. Report 10.1.1 The probability is approximately 95 % that two test
results obtained in the same laboratory on the same material
9.1 The report shall include as much of the following as
will not differ by more than the repeatability limit. Likewise,
possible:
the probability is approximately 95 % that two test results
9.1.1 Sources of the specimen including project name and
obtained in different laboratories on the same material will not
location, and if known, storage environment. The location is
differ by more than reproducibility limit.
frequently specified in terms of the borehole number and depth
of specimen from collar of hole. TABLE Splitting Tensile Strength (MPa)
9.1.2 Physical description of the specimen including rock
Berea Salem Tennessee Barre
type; location and orientation of apparent weakness planes, Sandstone Limestone Marble Granite
bedding planes, and schistosity; large inclusions or inhomoge- Average Value 3.85 4.92 9.39 13.66
neities, if any. Repeatability Limit 1.24 1.56 3.63 4.31
Reproducibility Limit 1.37 1.74 5.38 4.98
9.1.3 Dates of sampling and testing.
9.1.4 Specimen diameter and length, conformance with 10.2 The variability of rock and resultant inability to deter-
dimensional requirements, direction of loading if anisotropy mine a true reference value prevent development of a mean-
exists. Type of contact between the specimen and the loading ingful statement of bias.
platens.
9.1.5 Rate of loading or deformation rate. 11. Keywords
9.1.6 General indication of moisture condition of the speci- 11.1 compression testing; indirect tensile strength; loading
men at time of test such as as-received, saturated, laboratory air tests; rock; splitting tensile strength; tension (tensile)
dry, or oven dry. It is recommended that the moisture condition properties/tests
The American Society for Testing and Materials takes no position respecting the validity of any patent rights asserted in connection
with any item mentioned in this standard. Users of this standard are expressly advised that determination of the validity of any such
patent rights, and the risk of infringement of such rights, are entirely their own responsibility.
This standard is subject to revision at any time by the responsible technical committee and must be reviewed every five years and
if not revised, either reapproved or withdrawn. Your comments are invited either for revision of this standard or for additional standards
and should be addressed to ASTM Headquarters. Your comments will receive careful consideration at a meeting of the responsible
technical committee, which you may attend. If you feel that your comments have not received a fair hearing you should make your
views known to the ASTM Committee on Standards, 100 Barr Harbor Drive, West Conshohocken, PA 19428.