87728001EN
87728001EN
87728001EN
Manual
8.772.8001EN / 2019-11-29
Metrohm AG
CH-9100 Herisau
Switzerland
Phone +41 71 353 85 85
Fax +41 71 353 89 01
[email protected]
www.metrohm.com
Manual
8.772.8001EN / 2019-11-29
Technical Communication
Metrohm AG
CH-9100 Herisau
[email protected]
Table of contents
1 Introduction 1
1.1 Instrument description ......................................................... 1
1.1.1 Model versions ........................................................................ 1
1.1.2 Connectors .............................................................................. 1
1.1.3 Intended use ........................................................................... 1
1.2 About the documentation ................................................... 2
1.2.1 Symbols and conventions ........................................................ 2
1.3 Safety instructions ................................................................ 3
1.3.1 General notes on safety ........................................................... 3
1.3.2 Electrical safety ........................................................................ 3
1.3.3 Tubing and capillary connections ............................................. 4
1.3.4 Flammable solvents and chemicals ........................................... 4
1.3.5 Recycling and disposal ............................................................. 4
4 Operation 14
5 Operation and maintenance 15
5.1 General notes ...................................................................... 15
5.1.1 Care ...................................................................................... 15
5.1.2 Maintenance by Metrohm Service .......................................... 15
5.2 Pump tubings ...................................................................... 16
5.2.1 Selecting the pump tubing ..................................................... 16
5.2.2 Suitability test for tubing materials ......................................... 17
5.2.3 Tubing dimensions ................................................................. 17
5.2.4 Tubing lifetime ....................................................................... 17
5.2.5 PharMed® pump tubing data sheet ....................................... 18
5.2.6 Viton® pump tubing data sheet ............................................ 19
5.3 Tubings ................................................................................ 20
6 Troubleshooting 21
6.1 Problems .............................................................................. 21
7 Technical specifications 22
7.1 Peristaltic pump .................................................................. 22
7.2 Power supply ...................................................................... 22
7.3 Interfaces and connectors ................................................. 22
7.4 Ambient temperature ......................................................... 22
7.5 Reference conditions .......................................................... 23
7.6 Dimensions/material ........................................................... 23
8 Accessories 24
Index 25
Table of figures
Figure 1 Front 772 Pump Unit ......................................................................... 6
Figure 2 Inserting the tubing olives ................................................................. 7
Figure 3 Installing the pump tubing ................................................................ 8
Figure 4 Fastening the pressure clamp in place ................................................ 8
Figure 5 Connecting the tubings ..................................................................... 9
Figure 6 Screwing the union nuts tightly ....................................................... 10
Figure 7 772 Pump Unit directly on the Sample Processor ............................. 11
Figure 8 772 Pump Unit via the Remote Box and 731 Relay Box .................... 12
Figure 9 Direction of rotation ........................................................................ 13
Figure 10 Calculation formula for the permeability (C) ..................................... 19
1 Introduction
Each version includes different accessories according to its use (see chap-
ter 8, page 24).
1.1.2 Connectors
The 772 Pump Unit needs 16 - 24 V DC voltage.
Power is supplied to the pump via the direct connection to a Sample Pro-
cessor (e.g. 814 or 815) or to the 731 Relay Box (connection via adapter
cable 6.2160.010).
CAUTION
NOTE
This symbol highlights additional information and
tips.
WARNING
WARNING
WARNING
Supply voltage
WARNING
WARNING
CAUTION
Leaks in tubing and capillary connections are a safety risk. Tighten all
connections well by hand. Avoid applying excessive force to tubing con-
nections. Damaged tubing ends lead to leakage. Appropriate tools can
be used to loosen connections.
Check the connections regularly for leakage. If the instrument is used
mainly in unattended operation, then weekly inspections are manda-
tory.
WARNING
More details about the disposal of your old instrument can be obtained
from your local authorities, from waste disposal companies or from your
local dealer.
2
5
3
7
6
7 Connection cable
With M8 plug for connection to a Sample
Processor.
3 Installation
3.1.2 Checks
Immediately after receipt, check whether the shipment has arrived com-
plete and without damage by comparing it with the delivery note.
3.1.3 Location
The instrument has been developed for operation indoors and may not be
used in explosive environments.
Place the instrument in a location of the laboratory which is suitable for
operation and free of vibrations and which provides protection against
corrosive atmosphere and contamination by chemicals.
The instrument should be protected against excessive temperature fluctua-
tions and direct sunlight.
NOTICE
Selecting the correct pump tubing is very important for its function and
lifetime (see chapter 5, page 15).
2 Insert the tubing olives (6.1820.050) into the two tubing ends.
3 Clamp the pump tubing 1 into the pump head according to the
drawing below such that the tubing and the tubing olives are fas-
tened by the tubing clips 2 and 3. The tubing must be as centered
on the roller as possible.
3
Figure 3 Installing the pump tubing
4 Press on the pressure clamp 5 and fasten it in place using the locking
lever 4.
5 Tighten the clamping screw 4 so that the pump tubing cannot slip.
With the pump running, gently tighten the clamping screw until the
liquid flows evenly. After a run-in period, correct the setting again if
necessary.
NOTICE
Do not clamp the pump tubing too tightly or apply too much pres-
sure, as this causes greater wear to the pump tubing and the
pump will generate excessive pump pressure.
NOTICE
Which of the two tubings to use depends largely on the solvent used.
PVC tubing is more flexible and has the advantage of making less noise
during the pumping operation. It must be noted that the PVC tubing is
not resistant to solvents.
1 Cut the inlet tubing and outlet tubing to the suitable length.
2 Connect the tubings to the tubing olives of the pump tubing using
union nuts.
NOTICE
WARNING
Voltage
The 772 Pump Unit needs 16 - 24 V DC voltage. It can be connected
directly to Sample Processor models 814, 815, 855 or 864.
When using the 772 Pump Unit in an automation system with remote
control, we recommend using a 731 Relay Box for the power supply.
1 2
Figure 7 772 Pump Unit directly on the Sample Processor
NOTICE
The Sample Processor 824 Easy Sample Changer does not have an M8
socket. However, the adapter cable 6.2160.010 can be used for the
connection. For details about connecting the 772 Pump Unit to the
adapter cable, refer to the manual for the 824 Easy Sample Changer.
1 2 3 4 5 6
Figure 8 772 Pump Unit via the Remote Box and 731 Relay Box
NOTICE
3 Inlet
NOTICE
For information on controlling the 772 Pump Unit using the 731 Relay
Box and a suitable control device, refer to the manual of the 731 Relay
Box.
4 Operation
The 772 Pump Unit does not have its own operating units. It is operated
and controlled via the main instrument in the linked system.
CAUTION
WARNING
Aggressive liquids
Leaking liquids can pose a risk of injury and damage instruments.
■ Use suitable tubing only.
■ Regularly check tubing for proper fastening and for damage and
wear.
NOTICE
In every case, the user has sole responsibility with regard to suitability
and safety of pump tubing. Therefore, it is extremely important that
before each use, the safety and effectiveness of tubing is tested based
on application-specific laboratory, field or clinical tests.
NOTICE
NOTICE
■ If the tubing is not tightened sufficiently around the rotor, this has a
negative impact on the lifetime of the tubing, as in this case the tub-
ing tends to fold up. If the tubing is tightened too much, the flow is
restricted.
■ The tubing will last longer if the pressure clamp is detached when
the pump is not in use.
■ In order to achieve good repeatability of flow rate following a
change in tubing, it is imperative that you always select the same
tubing length.
Before changing tubing:
■ Pump all of the liquid out of the tubing so that none remains.
■ Pull out the connection cable of the peristaltic pump to prevent acci-
dental starting of the pump.
■ Detach the pressure clamp, open the tubing clamps and remove the
tubing.
N2 80
Bases Outstanding
Solvents Limited
Vacuum Good
O2 14
N2 5
5.3 Tubings
The tubing requires regular inspection in order to work properly:
■ Do not kink PTFE tubing.
■ Ensure resistance to solvents.
■ Check the tubing regularly for any damage.
6 Troubleshooting
6.1 Problems
Problem Cause Remedy
The flow is not set The flow is too strong or Loosen or tighten the locking lever with the
correctly. too weak. clamping screw.
The liquid is not The inlet tubing and the Switch the tubings so that the inlet tubing
aspirated, but just outlet tubing have been goes into the solution and the outlet tubing
"bubbles" instead. switched. goes into the waste canister.
The peristaltic pump The connecting cable is not Connect the connecting cable.
is not running. connected.
The peristaltic pump The pressure clamp is set Set the correct pressure using the locking lever
is pumping too little insufficiently or not at all. and clamping screw.
or not at all.
The tubing clamp is pinch- Fasten the tubing end piece and the tubing
ing off the tubing. olive in the tubing clip correctly. The tubing
clamp must clamp the tubing in the area of
the tubing olive.
The tubing connec- The tubings are not Check the screw connectors.
tion of the inlet tub- screwed on correctly.
ing and/or outlet
tubing is dripping.
The tubing connec- The pressure is too high. Loosen the locking lever of the pressure clamp
tion of the pump slightly.
tubing is dripping or
If necessary, also use a cable tie to tie down
spraying.
the cable ends at the tubing olives.
7 Technical specifications
7.6 Dimensions/material
Width 100 mm
Height 210 mm
Depth 260 mm
Weight 3.20 kg (without accessories)
Material
Housing, upper Polyurethane, coated
part
Bottom part of Steel sheet, stove-enameled
housing
8 Accessories
Up-to-date information on the scope of delivery and optional accessories
for your product can be found on the Internet. You can download this
information using the article number as follows:
NOTICE
Index
C M Pump tubing ............................ 16
Connect Material .................................... 23 Dimensions ......................... 17
731 Relay Box .................... 11 Model versions ........................... 1 Lifetime .............................. 17
Peristaltic pump .................. 10 Mount .................................. 7
Sample Processor ................ 11 O Select ................................. 16
Operation ................................. 14 Suitability test ..................... 17
D
Dimensions .............................. 23 P S
Peristaltic pump Safety instructions ...................... 3
E Direction of rotation ........... 22 Service ....................................... 3
Electrostatic charge .................... 4 Flow rate ............................ 22 Supply voltage ............................ 3
Power supply
F Power consumption ............ 22 T
Front of the instrument .............. 6 Voltage .............................. 22 Tubing
Problems .................................. 21 Maintenance ...................... 20
I
Instrument description ................ 1