Presentation On PH Measurement Technique

What is pH Electrode?
pH electrodes are electrochemical sensors. The sensor itself is similar to a battery. It generates a voltage output and has a useful service and shelf life. There are many types of pH electrodes used for different applications. The basic design of the electrode is as shown in the picture;
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What is pH Electrode?
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OFFSET - Theoretically, when electrode is placed in 7.00 buffer at 25C a pH electrode produces zero millivolts which the pH meter reads as 7.00 pH. The difference between these perfect readings and the electrode's actual reading is called the offset error. SPAN - A perfect pH electrode, at 25C produces 59.16mV per pH unit. The difference between this perfect reading and the electrode's actual reading is called the span error. These theoretical values are not always achieved, even with brand new electrodes. New pH electrode performance specifications should meet the following criteria: TYPICAL SPECIFICATION - Offset: 7.00 +/- 0.2 pH (+/12mV) SPAN: Better than 95%, i.e. between 56.2 and 59.2 mV
pH Electrode Care and Maintenance

Handling During shipment it is possible that air bubbles may go into the glass bulb. To remove air bubbles, shake down the electrode in the same manner as a clinical thermometer, until the glass bulb is filled with solution & bubble goes off. Rinse electrodes with distilled water before and after measuring a sample. Blot the end of the electrode with lint-free paper to remove excess water. NOTE: Never wipe the electrode to remove excess water - wiping can create static charges that interfere with correct pH measurement.
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Conditioning After removing the electrode from storage bottle or protective cap, place the electrode in a clean container containing one of the liquids i.e. 4.0 M KCl or pH 7.0 buffer with some amount of saturated KCl added to it. Soak electrode for 30 minutes if left dry. NOTE: Never condition the electrode in distilled water or DI water - long term exposure to pure water will damage the special glass membrane. After conditioning the sensor, rinse the electrode with distilled or DI water. The electrode is ready for calibration and measurement.
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Storing The sensor should never be stored dry. Always keep pH electrode moist. Proper pH electrode storage maximizes electrode performance and extends electrode life. It is best to store electrodes in clean containers filled with pH storage solution ( i.e. 3M KCl or 4pH soln. with some amount of KCl added to it.) Do not store an electrode in distilled or DI water - this will cause ions to leach out of the glass bulb and render your electrode useless. This is to be followed mainly for Gel filled Epoxy body sealed electrode.
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Cleaning The solution used to clean pH electrode depends on the presence of possible contaminants. Mechanically intact electrodes may show slow response due to coating or clogging. Use the guide below to choose the appropriate cleaning solution options: For general cleaning: Soak the pH electrode in 0.1 M HCl or 0.1 M HNO3 for 20 minutes. Then rinse well in tap water before use. For removing stubborn deposits and bacteria: Soak the pH electrode in a 1:10 dilution of laundry bleach for 10 minutes. Then rinse thoroughly before use. For removal of oil and grease: Rinse the pH electrode in mild detergent or methyl alcohol. Wash in water before use. For removal of protein deposits: Soak the pH electrode in 1% pepsin in 0.1m HCl for 5 minutes. Rinse well in water before use. CAUTION: Proper eyewear and hand gloves must be used when handling strong chemicals. After any of the cleaning procedures, it is good practice to thoroughly rinse the pH electrode with DI water, drain and refill the reference chamber if necessary before use.
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What LabServ Offers?

LabServOffers Best Suitable models of pH Meters to cater various segments of industries; AcuStar AcuStar V AcuStar+ V
Why LabServ pH Meter Only?

User Friendly Software In Dialogue Mode Calibration Status on Display Electrode diagnostics Very Good Accuracy & Precisions Auto / Manual Temperature Compensation Option of 5 point calibration in AcuStar+ V Alpha Numeric Entries For Authenticity 40 Reading Memory Data Logging Mode in AcuStar V & AcuStar+ V (Optional) PC & Printer Compatibility in AcuStar V & AcuStar+ V Meets All GLP Norms (i.e. For Calibration & Result Reports) Complies to USP / EP & DIN Standards Excellent After Sales Support
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Print out Formats

Calibration Print Out Printout (Data Logging)
Competition
Eutech pH 510 Price ~ 22,000/ Orion 3 Star Comparable against AcuStar Price~ 28,000/- Printout is not fully GLP compliant. AcuStar V direct connectivity of printer thru parallel port. Printout is fully GLP compliant
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What is pH Electrode?

pH Electrode Care and Maintenance

pH Electrode Care and Maintenance

pH Electrode Care and Maintenance

pH Electrode Care and Maintenance

What LabServ Offers?

Why LabServ pH Meter Only?

Print out Formats

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