Is 15388 2003 PDF
Is 15388 2003 PDF
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IS 15388:2003
Indian Standard
SILICA FUME SPECIFICATION
ICS91.100.
I5
0 BIS 2003
BUREAU
MANAK
August 2003
OF
BHAVAN,
INDIAN
STANDARDS
9 BAHADUR
SHAH
NEW DELHI 110002
ZAFAR
MARG
Price Group 4
Sectional Committee,
CED 2
FOREWORD
This Indian Standard was adopted by the Bureau of Indian Standards, after the draft finalized by the Cement and
Concrete Sectional Committee had been approved by the Civil Engineering Division Council.
Si Iica fume is very fine pozzolanic material composed of ultra fine, amorphous glassy sphere (average diameter,
0.10-0. 15~m) of silicon dioxide (Si02) produced during the manufacture of silicon or ferro-silicon by electric
arc furnaces at temperature of over 2 000C. The micro silica is formed when SiO gas produced in the furnace
mixes with oxygen, oxidizes to Si02, condensing into the pure spherical particles of micro silica that form the
major part of the smoke or fume from the furnace. These fumes are collected and bagged called silica fume. It is
also known as condensed silica fume and micro silica. The Committee also felt that chloride content in silica
fume shall be declared by the manufacturer so that different samples of silica fume can be compared and Engineerin-Charge is in knowledge of the amount of chloride entering into concrete through silica fume.
This standard has been formulated
use in the country.
[n the preparation of this standard, due weightage has been given to the international coordination among the
standards and practices in different countries in addition to relating it to the practices in the field in this country.
For this, assistance has been derived from the following:
a)
ASTM C 1240-2000 Standard specification for use of silica fume as a mineral admixture in hydraulic
cement concrete, mortar and grout; issued by the American Society for Testing and Material
b)
EN 197-1:2001
cements
The composition
of the Committee
responsible
specifications
for formulation
and conformity
For the purpose of deciding whether a particular requirement of this standard is complied with, the final value,
observed or calculated, expressing the result of a test, shall be rounded off in accordance with IS 2: 1960 Rules
for rounding off numerical values (revisecf). The number of significant places retained in the rounded off value
shou]d be the same as that of the specified value in this standard.
IS 15388:2003
Indian Standard
SILICA FUME SPECIFICATION
Table 1 Chemical
1 SCOPE
This standard covers the chemical and physical
requirements of silica fume for use in concrete and
other systems containing hydraulic cement.
s]
2 REFERENCES
1727:1967
4082:1996
4305:1967
6491:1972
Characteristic
4)
Requirements
(2)
i)
Requirements
(Clause
SiOz ,
Min
percentby mass,
(3)
Test
Method
(4)
85.0
IS 1727
ii)
3.0
see
Note 1
iii)
4.0
1S 1727
iv)
1.5
See
Notes
2 and 3
NOTES
Title
Methods
of test for pozzolanic
materials (@W revision)
Recommendations
on stacking and
storage of construction materials and
components at site (second revision)
Glossary
of terms relating
to
pozzolana
Methods of sampling fly ash
3 TERMINOLOGY
5 PHYSICAL
REQUIREMENTS
FOR CONFERMfTY
6.1 Sampling
6.1.1 The methods and procedure of sampling of silica
fume shall be same as the method given for fly ash in
IS 6491. All samples whether grab or composite shall
have amass of at least 1 kg. Two grab/~omposite samples
shall be taken from the lot for the first 100 t of silica
fume. For each subsequent 100 t from the lot of silica
fi.tme, one sample shall be taken. However, not less than
two samples shall be taken in any sampling programme.
4 CHEMICAL
REQUIREMENTS
IS 15388:2003
7.2 A sampling device of appropriate size shall be used
to take material from the thoroughly mixed sample for
purpose of making the test specimen. At least six
random sub-samples shall be taken to prepare the test
specimen.
SI
Characteristic
No.
5)
Requi~ement
Method of
Test, Ref to
r
(2)
(1)
-!
Annex
IS
No.
(3)
(4)
(5)
i)
15
11)
Oversize percent
retained on 45 micron IS
Sieve, Max (see Note I )
10
iii)
Oversize percent
retained on 45 micron IS
Sieve, variation from
average percent, Max
(see Notes I and 2)
1727
w)
Compressive strength at
7 days as percent of
control sample, Mirr (see
Note 3)
85.0
1727
8 STORAGE
AND INSPECTION
1727
9 DELIVERY
The supply of silica fume shall be m~de in suitable
quantities mutually agreed upon between the purchaser
and the supplier. Where so required by the purchaser,
the material shall be supplied in bags (jute laminated,
multiply paper or polyethylene lines).
NOTES
I Any oqe of the tests specified in (i) or (ii) and (iii) indicated
may he adopted.
2 For (iii) the average shall consist of the ten preceding tests or
all of the preceding tests if the number is less than ten.
10 MANUFACTURERS
The supplier/manufacturer
shall satisfy himself that the
silica fume conforms to the requirements
of this
standard and, if requested by the purchaser, shall
furnish a certificate to this effect, indicating the results
of the tests carried out on the samples of silica fume.
11 MARKING
11.1 Each bag/consignment
of silica fume shall be
clearly and permanently marked with the,<ollowing
..
information
:
passing if samples
meet in all the requirements. The silica fume may be
rejected if it fails to meet any of the requirements of
this standard. In case of dissatisfaction with the results
of tests, the producer or supplier may request re-testing
of the failed consignment.
7 SAMPLE
CERTIFICATE
a)
Identifications
b)
c)
Batch/Control
d)
e)
PREPARATION
Marking
: ,,
IS 15388:2003
12 HEALTH AND SAFETY
ANNEX
shall be in good
(Table 2)
DETERMINATION
OF SPECIFIC SURFACE AREA BY GAS
ADSORPTION USING THE BET METHOD
A-1 SCOPE
This method of test specifies the determination of
total specific external and internal surface area
disperse or porous solids by measuring the amount
physically adsorbed gas according to the method
Brunauer, Emmett and Teller (BET method).
the
of
of
of
A-4 EVALUATION
OF ADSORPTION
DATA
A-3 PROCEDURE
A-3.1 Sample Preparation
Prior to the determination of an adsorption isotherm,
remove physically adsorbed material from the sample
surface by degassing, while avoiding irreversible
changes to the surface. As certain the maximum
temperature at which the sample is not affected by
rhermogravimetric
analysis or by trial experiments
using different degassing conditions
of time and
temperature. When vaccumed conditions are used,
degassing to a residual pressure of approximately 1 Pa
or better is usually sufficient. Degassing of a sample
can also be performed at elevated temperature by
flushing with helium or with adsorptive. Degassing is
PIPO
, [ l(P/PO)]
1 +Cl
.
mC
mc
P()
where
pressure of the adsorptive
with the adsorbate, Pa;
P=
Po
n=a
saturation
adsorptive,
vapour
Pa;
in equilibrium
pressure
of
mol g-;
the
IS 15388:2003
?1m
= BET parameter.
f-)
shall include
of equipment,
the
a)
Laboratory,
type
determination;
date of
b)
Characterization
of the sample, for example
source, chemical composition, purity, method
of sampling, sample division;
c)
d)
Mass of degassed
e)
Experimental
procedure
for adsorption
isotherm
determination,
for example
volumetric,
gravimetric,
chromatographic,
sample, in g;
h)
j)
k)
Reference
results.
material(s)
in mlg;
of
MATERIAL
ANNEX
(1oreword)
COMMITTEE
COMPOSITION
Representative(s)
Organization
In personal capacity ( Chandrika at 15h Cross, 63-64, East Park Road,
Mallesu,aram, Bangalore-560003)
B.G. Shirke Construction
Builders Association
Building Materials
Technology
Limited,
(Chairman)
DR H. C. VMVESVARAYA
SHRI G. R. B}{ARITKAR
Pune
SECRETARY
of India, Mumbai
& Technology
Cement Corporation
CED 2
Promotion
Council,
SHRI T. N. G(JPTA
SHJUJ. K. PRASAD(Alternate)
New Delhi
SHRI MAHESHKUMAR
SHKI1. K. WAITAL (A/terns/e)
MEMBERSECRBTARY
DIRECTOR(CIVIL) (Ahernate)
Central Building
Institute,
DR C. L. VERMA
DR B. K. RAO (Alternate)
Research
Central
Central
Road Research
Central
Central
Water Commission,
Directorate
Institute.
Department
DIRECTOR(CMDD) (N&W)
DEPUTYDISECTOR(CMDD) (NW&S)
& Disposals,
Army Headquarters,
New Delhi
New Delhi
DR S. S. AMETA
DR D. K. RAI (Alternate)
Limited,
institute,
SHRJ J. P. DESAI
SHRI B. K. JAGETIA(Alternate)
Ahmedabad
Corporation
SHRI A. K. JAJ~
COL SUDHIRTAMHANEY
(RETD) (A/terns/c)
Mumbai
Consultancy
Corporation
(India)
SHRI J. SARUP
SHRI P. K. JAIPURIAR(Alternate)
Ltd, Noida
SHRI V. SURESH
SHRI V. ARUL KUMAR(Alternate)
SHRI L. N. APTE
SHRI D. SRINIVASAN
(Alternate)
Mumbai
DR VIMALKUMAR
SHRI MUKf3H MATHUR(Alternate)
SHRI S. A. RE~OI
SHRI M. U. SHAH(Alfernafe)
Mumbai
Limited,
PROF T. S. NA~ARAJ
Bangalore
Roorkce
PROF A. K. JAIN
Kharagpur
DR ASHOKKUMARGHOSH
(Ahernate)
SHRI V. BALSUBIWMANIAN
SHRJR. P. SINGH(Alternafe)
Bangalore
Grasim Industries
Hospital
DIRECTOR
SHIUP. L. KASHYAP(Alternate)
New Delhi
Branch,
Geological
HEAO
DIRECTOR(Alternate)
New Delhi
General of Supplies
India Limited,
CHIEF ENGINEER(DESIGN)
SUPERINTENDING
ENGINEER(S&S) (Alternate)
New Delhi
Research
Engineer-in-Chiefs
Gammon
Roorkee
DR S. S. SEHJLA
New Delhi
& Ecological
DR N. BHANUMATHIDAS
SHIUN. KALIDAS(A/ternate)
Balance,
(Continued
on page 6)
IS 15388:2003
Organization
Larsen & Toubro Limited,
Madras Cements
SHRI C. R. V. SUBRAMANWM
Snru S. CHOWDHtJRY
(A[ternOte)
Mumbai
DR N. BHANUMATHIDAS
Ltd, Chennai
Highways,
SHSUC. C. BHATTACHARYA
SHIUI. K. pANoEY(A/ternate)
New Delhi
Materials,
DR S. C. MAITI
DR (SHRIMATI)S. LAKMI(Afternate)
Ballabgarh
SHRI D. K. KANUNGO
SHIUB. R. MEE~A (Alternate)
DR S. C. AHLUWALIA
SUPERtNTENDING
ENCINEER(DESIGN)
EXECUTIVE
ENOINEER(Alternate)
Research,
Sardar Saro\ar
Structural
Chennai
Narmada
Engineering
The Associated
Organization,
Nigam Limited,
Research
fhe Institution
of Engineers
SHRI T. N. Tlwmt
DR D. GHOSH(Alternate)
Limited, Mumbai
SHRI S. GOPINATH
SHRI R. ARUNACHALAM
(Alternate)
SHRI P. R. C. NAIR
SHRI P. D. KELKAR(Alternate)
Limited, Mumbai
DR H. C. VtsvF.svARAYA
SHRJD. C. CHATURVEDI
(Alternate)
(India), Bangalore
SHRI S. GOPALAKRJSHNAN
SHJUN. P. RAIAMANE(Alternate)
Limited, Chennai
(A1/ernate)
CHIEF ENGINEER(NAVGAMDAM)
SUPEIUNTENDING
ENGtNEER(Alternate)
District Narmada
Centre, Chemrai
Cement Companies
JOINTDIRECTOR(STD) (B&S)/CB-11
JOINTDIRECTOR(STD) (B&S)/CB-I
Lucknow
SHRI Y. R. TANEJA
General
Member Secretaries
SHRI SANJAYPANT
Joint Director (CED), BIS
SHRI ALOK KESARI
Deputy Director (CED), BIS
Cement, Pozzolana
Subcommittee,
CED 2:1
(Convener)
DR H. C. VISVESVARAYA
Butldlng Materials
Cement Corporation
Central Electricity
Association,
Promotion
Hyderabad
SHRI J. K. PRASAD
SHRI L K. WATTAL
SHRIMATISARASWATHI
DEW (Alternate)
Cement Manufacturers
Central Building
Manufacturers
& Technology
Association,
Research
Institute,
Authority,
Kolkata
SHRI SOMNATHBANERIEE
Roorkee
DR B. K. RAO
DR MANJITSINOH(Alternate)
SHRI Y. K. SHARMA
SHRJMOHANKUMAR(Alternate)
New Delhi
CHIEF ENGINEER(CDO)
SUPERINTENDING
ENGINEER(S&S) (Alternate)
New Delhi
(Contittued on page 7)
IS 15388:2003
Representative(s)
OrganizatiOtl
Central Road Research
Institute,
Research
SHRI S. S. SE~HRA
SHRI SATANDER
KUMAR(Alternate)
New Delhi
Station,
DIRECTOR
Stou N. CHANDRASBKARAN
(Alternate)
New Delhi
DIRITTOR(C&MDD-11)
DEPUTYDKWCTOR(CMDD-H)
New Delhi
(Al[erna/c)
DR K. C. NARANG
SHRI C. S. SHARMA(Alternate)
Stiru
HmA LAL
Branch, Chandigarh
LT-COL DWJENORAKUMAR(Alternate)
Fly Ash Mission.
Gammon
Department
India Limited,
Cimsim Industries
Limited,
Engineering
lndlan Concrete
New Delhi
Institute,
SHRI A. K. JAIN
COL SUDHIRTAMHANEY
(RETD) (Alferwak,)
Mumbai
%RI J. P. DESAI
SHRI B. K. JACiETIA(Alferna[e)
Ltd, Ahmedabad
Research
Institute,
DIRFCTOR
SHRI J. K. PAT~L(A/fernafe)
Vadodara
DR C. S. VISWANATHA
PROF M. S. SHETTY(Alternate)
Chennai
PROF T. S. NAGARAJ
Bangalore
DR VIMALKUMAR
SHRI MUKWH MATHUR(Alternate)
SHRI S. A. RLDDI
Murnbai
DR ASHOKKUMARGHOSH
Kharagpur
Limited,
Mumbai
SHRI K. K. TAPAJUA
SHP.JA. K. PRASHAR(Alternate)
Mumbai
SHRI S. CHOWDHURY
Iodorama Cement
Madras Cements
DR N. BHANUMATHIDAS
Ltd, Chennai
kMaharashtra Engineering
Ministry of Commerce
Research
Institute,
DIRECTOR
RESEARCHOFFICER(Alternafe)
Nasik
SHRI P. K. JAIN
SHFUSHAISHKUMAR(Alternate)
& Highways,
SHSUV. VELAYUTHAM
SHRI 1. K. PANDEY(Alternate)
New Delhi
Materials,
DR K. MOHAN
DR (SHRIMATI)S. LAXMI(Alternate)
Ballabgarh
SHRI B. R, MEENA
SHRI B. K. MANDAL(Alternate)
Orissa Cement
DR S. C. AHLUWALIA
SUPERINTENDING
ENGINEER(DESIGN)
SENIORDFPUTYCHIEF ENGINEER(Alterna/e)
Chennai
Organization,
DEPUTYDIRECTOR(B&F)
ASSISTANTDESIGNENGINEER(B&F) (Akowafe)
Lucknow
SHRI K. SUMA~THBABU
Limited, Chennai
Cement Company
Construction
SHRI T. N. TIWARI
DR D. GHOSH(Alternate)
Ltd, Mumbai
Company
Limited,
SHRI A. P. PHADKE
SHRI D. M. SAVUR(A[fernafe)
Mumbai
of Zndian
Standards
marking
and quality
Act,
1986
certification
to promote
of goods
Copyright
BIS has the copyright of all its publications. No part of these publications may be reproduced in any form
without the prior permission
in writing of BIS. This does not preclude the free use, in the course of
implementing
the standard, of necessary details, such as symbols and sizes, type or grade designations.
Enquiries relating to copyright be addressed to the Director (Publications), BIS.
Review of Indian Standards
Amendments are issued to standards as the need arises on the basis
periodically; a standard along with amendments is reaffirmed when
needed; if the review indicates that changes are needed, it is taken
should ascertain that they are in possession of the latest amendments
BIS Catalogue and Standards: Monthly Additions.
This Indian Standard has been developed
Amendments
Amend No.
Text Affected
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23237617
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