DR 5000 Maintanance
DR 5000 Maintanance
DR 5000 Maintanance
00654
DR 5000
USER MANUAL
January 2008, Edition 3
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Table of Contents
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Table of Contents
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Table of Contents
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Section 1 Specifications
Specifications are subject to change without notice.
Performance specifications
Spectral bandwidth 2 nm
User programs 50
Operating requirements 10–40 °C (50–104 °F), max. 80% relative humidity (non-condensing)
Storage requirements –25–60 °C (–13–140 °F) max. 80% relative humidity (non-condensing)
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Specifications
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Section 2 General Information
DANGER
Indicates a potentially or imminently hazardous situation
which, if not avoided, will result in death or serious injury.
WARNING
Indicates a potentially or imminently hazardous situation
which, if not avoided, could result in death or serious injury.
CAUTION
Indicates a potentially hazardous situation that may result in
minor or moderate injury.
Important Note: Indicates a situation which, if not avoided, may
cause damage to the instrument. Information that requires special
emphasis.
This symbol, if noted on the instrument, references the instruction manual for operation and/or safety information.
Electrical equipment marked with this symbol may not be disposed of in European public disposal systems after
12 August of 2005. In conformity with European local and national regulations (EU Directive 2002/96/EC),
European electrical equipment users must now return old or end-of life equipment to the Producer for disposal at no
charge to the user.
Note: For return for recycling, please contact the equipment producer or supplier for instructions on how to return
end-of-life equipment, producer-supplied electrical accessories and all auxiliary items for proper disposal.
This symbol indicates that the instrument contains a Class 1 LASER device.
LASER CLASS 1 Data: 0.3 mW; λ = 650 nm
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General Information
DANGER
Potential Chemical/ Biological Exposure Hazards. Handling
chemical samples, standards and reagents can be dangerous.
Users of this product are advised to familiarize themselves
with safety procedures and the correct use of chemicals, and
to carefully read all relevant Material Safety Data Sheets.
CAUTION
The UV lamp generates UV light.
Do not look directly at an operating lamp without wearing UV
protective eye glasses.
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General Information
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General Information
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Section 3 Installation
WARNING
Electrical and Fire Hazards. Use only the provided power
supply. Only qualified personnel should conduct the tasks
described in this section of the manual.
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Installation
3.3 Connection
The DR 5000 has three USB interfaces as a standard feature,
located on the back of the instrument (Figure 1).
The USB Type A interfaces are used for communications with a
printer, USB memory stick or keyboard. A USB memory stick is
used to update instrument software.
The USB Type B interface is used for communications with a PC.
The optional Hach Data Trans software (see section 5.2.6.3 on
page 31) must be installed on the PC for this use.
A USB hub may be used to connect several accessories at a time.
Note: USB cables must not be longer than 3 meters (10 feet).
Figure 1 Interfaces
1 USB type A 4 Fuse
2 USB type B 5 Plug in power supply
3 On/Off switch
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Installation
3.4 Cell compartment, Multi Cell Holder, 100 mm Cell Adapter (optional)
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Installation
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Installation
2. Identify the correct opening for the selected cell type in the
Multi Cell Holder.
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Installation
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Section 4 Start Up
Note: Do not turn the instrument off and on in rapid succession. Always
wait about 20 seconds before turning the instrument on again, otherwise
the electronic and mechanical systems will be damaged.
1. While turning the instrument on, touch the screen at any point
until the list for selecting a language appears (about
30 seconds).
4.3 Self-Check
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Start Up
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Section 5 Standard Operations
5.1 Overview
5.1.1 Tips for the use of the touch screen
The entire screen is touch-activated. To make a selection, press the
screen with a fingernail, fingertip, pencil eraser or a stylus. Do not
press the screen with a sharp object, such as the tip of a ball
point pen.
• Do not place anything on top of the screen, to prevent damage
or scratching on the screen.
• Press keys, words or icons to select them.
• Use scroll bars to move up and down long lists very quickly.
Press and hold the scroll bar, then move up or down to move
through the list.
• Highlight an item from a list by pressing it once. When the item
has been successfully selected, it will be displayed as reversed
text (light text on a dark background).
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Standard Operations
Stored programs are pre-programmed methods that make use of HACH reagents and LANGE
Stored Programs (HACH cuvette tests and pipette tests.
LANGE Programs) The DR 5000 Procedures Manual contains illustrated, step-by-step procedures for analyses
using HACH programs. The working procedures for LANGE tests are included in the test packs.
User programs make "made to measure analysis" possible:
–Users can program methods they have developed themselves
User Programs
–Existing HACH and LANGE methods can be stored as user programs. The LANGE tests can
then be modified to suit the user's requirements.
Favorite Programs List of methods/tests created by the user to suit his own requirements.
Single wavelength measurements are:
Absorbance measurements: The light absorbed by the sample is measured in absorbance
units.
Single Wavelength Transmittance measurements (%): The percentage of the light that passes through the sample
and reaches the detector is measured.
Concentration measurements: A concentration factor can be entered to enable the measured
absorbance values to be converted into concentration values.
In the multi-wavelength mode, absorbance (Abs) or percentage transmittance (%T) is measured
Multi Wavelength at up to four wavelengths and absorbance differences and absorbance relationships are
calculated. Simple conversions into concentrations can also be carried out.
A wavelength scan shows how the light from a sample is absorbed over a defined wavelength
spectrum.This function can be used to determine the wavelength at which the maximum
Wavelength Scan
absorbance value can be measured.The absorbance behavior is displayed graphically during the
scan.
Time Course The time scan records the absorbance or % transmittance at a wavelength over a defined time.
The system checks menu offers a number of options, including optical checks, output checks,
System Checks
lamp history, instrument update, service time and instrument backup.
Recall Data Stored data can be recalled, filtered, sent and deleted.
In this mode, user-specific or method-specific settings can be entered: Operator-ID, Sample-ID,
Instrument Setup
Date & Time, Display & Sound, Lamp Control, PC & Printer, Password, and Module Options.
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Standard Operations
5.2.1 Operator ID
Use this option to enter up to 30 sets of operator initials (up to
5 characters each) into the instrument. This feature helps record
which operator measured each sample.
4. Press OK to confirm.
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Standard Operations
5.2.2 Sample ID
Use this option to enter up to 30 Sample Identification tags (up to
13 characters each) into the instrument. Sample IDs can be used to
specify the sample location or other sample specific information.
4. Press OK to confirm.
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Standard Operations
Option 1
In the result display, press Options>More>Instrument Setup. If a
Sample ID is already assigned, select the Sample ID symbol in the
result display.
Option 2
With an USB keyboard (with US keyboard layout) or a scanner a
Sample ID can be directly entered in the result display.
Note: This sample ID will not be added to the list
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Standard Operations
4. Press the field below Save to select the lamp burning time.
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Standard Operations
Note: After this period of time the lamp automatically turns off, after no
measurement has been made outside the corresponding range (UV/VIS).
6. Touch OK to confirm.
Note: The selected program that requires a lamp has highest priority. If the
lamp in the Lamp Control was turned off, the lamp will be turned on
automatically if it is needed for the stored program.
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Standard Operations
When the lamp is warmed up and ready, the UV icon stops flashing.
Note: If both lamps are On, the icon UV-VIS is displayed in the selected
Measurement Mode.
Note: Alternatively you can touch the UV- or VIS-Lamp icon on the
measurement screen to change the actual setting.
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Standard Operations
2. Press Printer.
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Standard Operations
Printer Setup:
• Resolution: Print quality
• Paper: Paper size
Note: If an optional Thermal Printer is connected, the function "Auto Send"
on/off is available.
Note: The option Auto-Send is not available for any other printer (e.g. ink
jet printer).
Select between
• 100 dpi
• 150 dpi and
• 300 dpi
6. Press OK to confirm.
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Standard Operations
Select between
• Letter
• Legal
• Executive
• A4
8. Press OK to confirm.
2. Select the data source, where the data to be printed are stored.
4. Press the PC & Printer icon to send the data (table, curve)
immediately to the printer.
2. Select PC.
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Standard Operations
Note: The remote function is only for monitoring the data transfer.
5.2.7 Password
The Password menu contains a variety of security settings to
control access to various functions. For example, prevent
unauthorized changes to stored programs or instrument
configurations.
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Standard Operations
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Standard Operations
Note: Use this function to delete the former Password or to enter a new
one.
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Standard Operations
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Standard Operations
• Sample ID
• Operator ID
• Start Date
• Parameter
2. Press Recall Data from the Main Menu. Press Options and
then the PC & Printer icon
3. Select the data to send to the memory stick and press OK.
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Standard Operations
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Standard Operations
5.3.2 Store, recall, send and delete data from wavelength scan and time course
The instrument can store 20 Wavelength Scans and 20 Time
Course Data sets.The data can be stored manually at the user's
discretion after viewing the data.
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Standard Operations
Option 1:
2. Press Options and then the PC & Printer icon to send the
data to a USB memory stick, to a printer or to a PC with Hach
Data Trans.
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Standard Operations
Note: The advice ”Data already exist. Overwrite?“ appears when the files
were already stored. Press OK to overwrite the stored data.
Option 2:
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Standard Operations
1. Press Recall Data from the Main Menu and then Wavelength
Scan or Time Course or Options>More>Recall Data.
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Standard Operations
Note: Select the program number by name or use the arrow keys to
scroll through the list quickly and highlight the program or press
Select by number to search for a specific program number. Use the
alphanumeric keypad to enter the test number and press OK.
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Standard Operations
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Standard Operations
3. To start the next timed activity for the Stored Program, press
the Timer icon and OK.
Note: Press Close to view the measurement screen while the timer is
running. The time will be shown left side bottom instead of the date.
Note: Press Cancel to stop the timer midway through the countdown.
Note: The Timer will beep when the end of the running time is
reached.
2. Select the required mode, then press OK, then Return to return
to the result display.
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Standard Operations
Note: The Read key is only active after the zero measurement has
been carried out.
Note: In the reading mode ”Continuous“ only the Zero key is shown to
start the reading. The reading sequence is started automatically.
3. Press Options and then the Store icon to store the displayed
data in the Data Log.
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Standard Operations
2. Press OK to confirm.
Note: When a dilution is in effect, the dilution icon will appear on the
display.
Note: If using undiluted samples, set the dilution factor off again.
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Standard Operations
Note: The adjustment must be within certain limits, which vary with
each program. The allowable percentage is shown after "Adjustment“.
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Standard Operations
Note: The selected Chemical Form will appear on the display. Test
results will be calculated and displayed in this chemical form.
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Standard Operations
8. Press OK.
Note: The results calculated using the reagent blank value must lie within
the limits of the measuring range of the test/method.
Note: The reagent blank icon is shown in the result display (see arrow)
when the function is active.
3. Press Zero.
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Standard Operations
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Standard Operations
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Standard Operations
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Standard Operations
Some tests can be used for different measuring ranges. After the
sample cuvette/vial has been inserted, a list of the different
measuring ranges is displayed.
Select the required measuring range by highlighting the appropriate
line.
Press Start Permanent if this measuring range is to apply to all
subsequent measurements.
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Standard Operations
Note: The selected chemical form is displayed, but does not become
the default. To change the default, see section 5.5.3.1.
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Standard Operations
Save as User Program To store the selected parameters as a User Program, see section 6.1 on page 65.
Call up saved measurement data, wavelength scans or time courses, see section 5.3 on
Recall Data
page 35.
Instrument Setup Basic data of the instrument, see section 5.2 on page 23.
Turbidity and color in the sample matrix can falsify the results of a
photometric analysis. The interference factors come from the
sample or are created by reactions with the reagents.
The influence of turbidity and/or color can be eliminated or reduced
by taking a sample blank reading.
In the barcode mode, a special cuvette/vial (LCW 919) containing
the sample blank is placed in cell compartment #1 after the sample
reading has been taken and is automatically measured. The
sample reading is then corrected by adding or subtracting the blank
value. The final result is displayed, with the message "After blank
value corr.".
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Standard Operations
1. Highlight the line containing Name and press Edit. Use the
alphanumeric keypad to enter the name indicated in the
working procedure.
2. Press OK to confirm.
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Standard Operations
1. Highlight the line containing Version and press Edit. Use the
alphanumeric keypad to enter the name indicated in the
working procedure.
2. Press OK to confirm.
1. Highlight the Formula line in the data overview and press Edit.
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Standard Operations
Abbreviation of Variables:
F1: Factor 1
F2: Factor 2
λ1: Wavelength 1
U1: Conversion Factor 1 for the first chemical form
U2: Conversion Factor 2 for additional chemical forms etc.
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Standard Operations
3. Press Options>More>Edit.
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Standard Operations
1. Go to http://www.hach-lange.com
5. Unpack the ZIP file and save the files to the USB memory stick.
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Standard Operations
Note: When the instrument software has been updated, a prompt to restart
the instrument is displayed.
3. Select the required application 906 from the displayed list and
press Start.
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Standard Operations
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Standard Operations
3. Press OK.
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Standard Operations
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Section 6 Advanced Operations
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Advanced Operations
Program Number:
Specific test number, with which the program can subsequently be
called up from the selection list in the User Programs menu or the
Favorites menu.
3. Press OK.
Program Name:
Program Type:
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Advanced Operations
Units:
Select the required unit from the list and press Next.
Note: Units of measure not included in this list can be added in the edit
program under Program Options, Edit. Select Units, Edit and then New.
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Advanced Operations
Chemical form:
Enter the chemical formula used in the display to represent the
analysis parameter.
Use the alphanumeric keypad to enter the chemical form and press
Next to enter Calibration settings.
Units:
Select the required unit from the list and press Next.
Note: Units of measure not included in this list can be added in the edit
program under Program Options, Edit. Select Units, Edit and then New.
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Advanced Operations
Wavelength λx:
Press a λx key and use the alphanumeric keypad to enter a
wavelength. Press another λx key and enter the next wavelength. If
necessary, repeat until all the wavelengths for the formula have
been entered. The wavelengths must be in the range from
190–1100 nm. Press OK.
Concentration Factor Kx
Multiplication factor for converting absorbance values into
concentration values.
Press a factor key and use the alphanumeric keypad to enter a
factor. If the formula includes more than one factor, press another
factor key and enter another factor and repeat until all the factors
have been entered. Press OK. When all the relevant data have
been entered, press Next.
Note: Up to five digits can be entered, including a maximum of 4 decimal
places to the right of the decimal.
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Advanced Operations
Chemical form:
Enter the chemical formula used in the display to represent the
analysis parameter.
Use the alphanumeric keypad to enter the chemical form and press
Next to enter Calibration settings.
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Advanced Operations
Note: The correlation coefficient (r2) is shown on the left below the
axes.
6. Press Force 0 to change the setting from Off to On. The curve
now passes through the origin of the coordinate system.
8. When the table has been completed and the curve type has
been chosen, press Done when the graph is displayed or Exit
when the table is displayed. Go to section 6.1.1.4 on page 74.
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Advanced Operations
3. Press the "+" symbol again (see arrow) and enter the next
standard concentration. Repeat this sequence until all standard
conentrations (maximum of 24 solutions) have been entered.
5. Insert the zero solution into the cell compartment. Press Zero.
Repeat this sequence until all the standard solutions have been
measured (maximum of 24 solutions).
7. When the data have all been entered and the measurements
have all been completed, press Graph.
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Advanced Operations
9. Press Force 0 to change the setting from Off to On. The curve
then passes through the origin of the coordinate system.
11. When the table has been completed and the curve type has
been chosen, press Done when the graph is displayed or Exit
when the table is displayed. Go to section 6.1.1.4 on page 74.
Note: The coefficients can have 5 digits and can have a positive or a
negative sign.
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Advanced Operations
Note: The test data will be formatted in the preinstalled PrgData folder
as a .csv and as a .lst file.
2. Set On and press the 0.000 key to enter the measuring range
limit. Confirm the entry by pressing OK.
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Advanced Operations
3. Press the left key to enter another chemical form with the
alphanumeric keypad and press OK to confirm. Press the right
key to enter the conversion factor to calculate the concentration
of the additional chemical form from the concentration of
Chemical Form 1 and press OK to confirm.
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Advanced Operations
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Advanced Operations
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Advanced Operations
{ } key
Elements of the measurement sequence that are to be repeated
are placed in brackets.
The left bracket "{"marks the start of the sequence that is to be
repeated and the right bracket "}" marks the end.
Note: The key showing the right bracket remains inactive until a left bracket
is entered.
1. Press {.
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Advanced Operations
1. Highlight the Formula line in the data overview and press Edit.
3. Select C1: Off again and press Edit. The display changes to
C1: On.
Note: The arrow key deletes the most recently entered element of the
formula.
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Advanced Operations
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Advanced Operations
2. Select C2: Off again and press Edit. The display switches to
C2: On.
Note: When the first Cn formula has been defined, the Formula list is
automatically extended by Cn+1.
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Advanced Operations
Abbreviation of Variables:
F1: Factor 1
F2: Factor 2
λ1: Wavelength 1
U1: Conversion Factor 1 for the first chemical form
U2: Conversion Factor 2 for the further chemical form etc.
1. Press Store to save the entered data. The data can be stored
under any data point (Measurement sequence, Formula, Timer,
etc.).
Note: The test data will be formatted in the preinstalled PrgData folder
as a .csv and as a .lst file.
Note: Use the scroll bar to scroll through the list quickly.
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Advanced Operations
6.1.4 Add, edit and delete user programs from the favorites list
The most frequently used tests/methods in the User Program menu
can also be added to the list of favorites to simplify their selection.
Note: Use the scroll bar to scroll through the list quickly. Use the
alphanumeric keypad to enter the test number (program number) and
press OK to confirm.
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Advanced Operations
6.1.4.2 Edit
6.1.4.3 Delete
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Advanced Operations
Note: Use the scroll bar to scroll through the list quickly.
3. Press Start.
Note: Use the scroll bar to scroll through the list quickly.
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Advanced Operations
Method:
A defined amount (concentration) of a standard solution of the test
substance is added to the sample. The detection rate should be
close to 100%.
Checklist:
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Advanced Operations
Sample volume:
A defined volume of a standard solution of known concentration is
added to the volume of sample specified in the procedure and the
sample is measured after each addition. In most cases three
different standard solutions are prepared and the procedure is
repeated for each of them.
Note: The units and chemical forms used for the sample are used for the
standard solutions. Be careful to ensure that to use the correct units for
subsequent entries.
2. Press Start.
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Advanced Operations
6. Press the key of the value to change it. Use the alphanumeric
keypad to change the value. Press OK to confirm.
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Advanced Operations
7. Press the keys to enter the standard addition volumes. Use the
alphanumeric keypad to enter the new data and press OK.
10. Use the arrow keys to select the first standard addition volume
in the table and insert the cuvette with the corresponding
volume of added standard into the cell compartment.
Press Read.
Repeat the procedure from point 8 with all the other standard
addition solutions.
11. After all the standard addition solutions have been measured,
press Graph.
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Advanced Operations
Note: In the curve menu, the name on the Curve key switches to
Table. Press Table to display all the data in the table again.
12. Press Ideal line to display the relationship between the added
standard solutions and the ideal line (detection rate 100%).
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Advanced Operations
Concentration
To select the position of the decimal point in the calculated concentration readings.
Resolution
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Advanced Operations
Concentration factor:
3. Press OK to confirm.
Concentration resolution:
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Advanced Operations
Reading mode:
2. Select the required mode, then press OK, then Return to return
to the result display.
Note: The Read key is only active after the zero measurement has
been completed.
Note: In the reading mode ”Continuous“ only the Zero key is shown to
start the reading. The reading sequence is started automatically.
3. Press Options and then the Store icon to store the displayed
data in the Data Log.
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Advanced Operations
Concentration
To select the position of the decimal point in the calculated concentration readings.
Resolution
Save as User Program To store the selected parameters as a User Program, see section 6.1 on page 65
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Advanced Operations
λ / Absorbance formula:
K1A1+K2A2
K1A1+K2A2+K3A3
K1A1+K2A2+K3A3+K4A4
K1A1/K2A2
(K 1 A 1 + K 2 A 2 ) / K 3 A 3
(K 1 A 1 + K 2 A 2 ) / (K 3 A 3 + K 4 A 4 )
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Advanced Operations
Concentration factor:
3. Press OK to confirm.
Concentration resolution:
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Advanced Operations
Note: The Read key does not become active until the zero
measurement has been completed.
Note: Zero and Read are disabled until the cell compartment is
closed.
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Advanced Operations
Integral: On/Off The integral gives the area and the derivative of the integral gives the original function
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Advanced Operations
λ Setting wavelength
2. Press the upper left key to open the numeric keypad and select
the minimum wavelength. Press OK to confirm.
3. Press the upper right key to open the numeric keypad and
select the maximum wavelength. Press OK to confirm.
Note: Do not select the same wavelength for minimum and maximum.
Note: Scan recordings of high resolution data take a longer time than
recordings of low resolution data.Selecting a larger step allows the
instrument to scan faster, but decreases the resolution of the collected
data.
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Advanced Operations
Cursor mode
2. The selection for this menu item determines what data are
displayed in the table. Highlight Track or Peak/Valley.
3. Press OK to confirm.
Integral
The Integral applies to the whole wavelength range of the scan.
3. Press OK to confirm.
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Advanced Operations
Note: For the next scan measurement the setting for the Integral will be
On.
Note: If manual scaling is selected, use the alphanumeric keypad to set the
limits ymin. and ymax.. The graph is adjusted to display only the values in the
selected range. If automatic scaling is selected, the instrument sets the
limits automatically so that the total range can be displayed.
4. Press OK.
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Advanced Operations
Curve Icon Choice of Cursor Mode Peak/Valley (cursor moves between minimum/maximum absorbance
(Choice of Cursor Mode) values) or Cursor Mode Tracking (cursor moves over each data point of the scan).
The arrow keys are used (right/left) to move the cursor (depending on the selected mode) to the
next data point. The data of the data point (wavelength/absorbance or transmittance value) are
Arrow keys highlighted on the x and y axes.
Note: Press any point on the curve to display the associated data.
This function is used to magnify the section of the curve in the vicinity of the cursor. The original
Zoom Icon
curve size can be restored by pressing the zoom icon again.
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Advanced Operations
Option 1:
Note: After selecting a reference scan the Reference: Off key in the
Options menu turns into Reference: On.
Note: Only scans that have the same wavelength range and step can
be displayed using the overlay option. This process can be repeated
until all matching scans are displayed.
Note: A black and an gray box are shown in the left corner of the
display. The gray box relates to the reference scan and the black one
relates to the current wavelength scan.
4. Press the black or gray small box in the left upper corner on the
screen to switch between the actual wavelength scan and
reference scan.
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Advanced Operations
Option 2:
Note: After selecting a reference scan the Reference: Off key in the
Options menu turns into Reference: On.
Note: Only scans that have the same wavelength range and step can
be displayed using the overlay option. This process can be repeated
until all matching scans are displayed.
5. Press the black or gray small box in the left upper corner on the
screen to switch between the actual wavelength scan and
reference scan.
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Advanced Operations
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Advanced Operations
2. Input the total time and the reading time and press OK to
confirm.
Note: In total 500 measuring steps are possible. To select a total time and
a time interval that would cause this number of measurements to be
exceeded, the time interval is defined automatically and the OK key is
inactivated.
Note: If manual scaling is selected, use the alphanumeric keypad to set the
limits ymin. and ymax.. The graph is adjusted to display only the values in the
selected range. If automatic scaling is selected, the instrument sets the
limits automatically so that the total range can be displayed.
4. Press OK to confirm.
Note: During the measurement the Zero and Read keys change to
Mark and Stop.
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Advanced Operations
• Select Mark to mark the next data point collected. This mark is
not used by the instrument, but is available for the user and
may indicate a significant event, such as the addition of a
sample or other reagent. The mark is also shown in the table.
• Select Stop to stop taking sample readings.
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Advanced Operations
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Advanced Operations
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Advanced Operations
1. Go to http://www.hach-lange.com
5. Unpack the ZIP file and save the files to the USB memory stick.
Note: When the instrument software has been updated, a prompt to restart
the instrument is displayed.
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Advanced Operations
4. Press Start.
Note: During the warm-up phase of the UV lamp, the message ”Lamp
Warmup...“ is displayed.
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Advanced Operations
4. Press Zero.
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Advanced Operations
6. Press Start.
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Advanced Operations
4. Press Zero.
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Advanced Operations
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Advanced Operations
4. Press Start.
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Advanced Operations
This test takes a reading every minute for one hour. Every
15 minutes, linear regression is used to calculate the slope
(rate of change) for the previous 15 minute interval.
6. The last reading and slope for each 15 minute interval are
displayed. At the end of the hour, the overall values are
calculated and displayed. The test proceeds to completion.
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Advanced Operations
3. Press Edit.
• Stray Light
• Photometrical accuracy
• Wavelength accuracy
5. Press Verification.
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Advanced Operations
8. Insert the different filter in the given order one after the other
with the filter glass facing the front of the instrument. Press
Next after inserting a filter and closing the cell compartment.
After a lamp is replaced and the Lamp History is reset, the display
of the total operating time is reset to 0.
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Advanced Operations
2. Select On and then Last Service to enter the date of the last
inspection.
3. Press OK to confirm.
5. Press OK to confirm.
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Advanced Operations
Note: If the USB stick is not connected, the message "Please insert USB
Memory" is displayed. Connect a USB stick, in order to store the data.
Press OK to confirm and press Store again.
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Advanced Operations
Note: If the Backup was already stored before, the message "Data already
exists. Overwrite?" is displayed. Press OK to overwrite the data.
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Advanced Operations
Note: If the USB stick is not connected, the message "Please insert USB
Memory" is displayed. Connect a USB stick, in order to store the data.
Press OK to confirm and press Restore again.
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Advanced Operations
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Section 7 Maintenance
CAUTION
Potential Chemical, Biological Eye and Skin Hazards.
Only qualified personnel should conduct the tasks described
in this section of the manual.
Important Note: Remove any cuvettes/cells that are still in the instrument
and dispose of them or their contents using an approved disposal method.
7.1.1 Spectrophotometer
• Clean the enclosure, cuvette/sample cell compartments and all
accessories with a soft damp cloth. A mild soap solution can
also be used. Do not get excess water in the cuvette/sample
cell compartments. Do not insert a brush or sharp object into
Cell Compartment #1 to avoid damaging the mechanical
components.
• Dry the cleaned parts carefully with a soft cotton cloth.
7.1.2 Display
• Take care not to scratch the display. Do not touch the screen
with ball pens, pencils or similar pointed objects.
• Clean the display with a soft, lint-free and oil-free cotton cloth.
Diluted window cleaner liquid can also be used.
125
Maintenance
The Lamp compartment is on the left side behind the display and is
provided with ventilation on the back side. The tungsten and
deuterium (UV) lamp are installed in the lamp compartment. On the
back side a fan is installed for cooling of electric components.
The ventilation system operates automatically.
Refer to section 7.2.1 on page 126, section 7.2.2 on page 127 and
Figure 8 on page 128 for instructions on replacing the tungsten
lamp and deuterium lamp (UV).
DANGER
The instrument must remain switched off until the change of
lamp has been completed.
WARNING
Burn Hazard. Wait until the lamp cools down. Contact with the
hot lamp can cause burns.
4. Place the cover and the attached fan carefully beside the
instrument (take special care with the fan cable).
Important Note: The lamp should only be held by the lamp socket.
Avoid touching the glass.
8. Insert the tungsten lamp into the lamp compartment. Push the
spring down.
9. Check that the spring and the lamp socket are positioned
correctly.
10. Use a screwdriver to screw the back cover onto the instrument
again.
126
Maintenance
13. Reset the Lamp History, see section 6.8.5 on page 119.
DANGER
The instrument must remain switched off until the change of
lamp has been completed.
WARNING
Burn Hazard. Wait until the lamp cools down. Contact with the
hot lamp can cause burns.
4. Place the cover and the attached fan carefully beside the
instrument (take special care with the fan cable).
7. Holding the lamp socket, lift the deuterium lamp up out of the
lamp compartment (remove the complete unit, including the
cable).
Important Note: Do not touch the glass envelope on the new lamp.
If it is touched, clean with alcohol.
10. Insert the deuterium lamp in the socket so that the safety
contact clicks into place.
11. Use a screwdriver to screw the back cover onto the instrument
again.
14. Reset the Lamp History, see section 6.8.5 on page 119.
127
Maintenance
DANGER
Failed fuses are generally an indication of a problem with the
equipment. If fuse failure continues, contact a service
representative for instructions on how to return the equipment
for repair. Do not attempt to repair the equipment yourself.
128
Maintenance
3. Pull out the plastic base over the power cable socket.
4. Lift the instrument and check the color of the filter mat. Replace
the filter mat if is dark gray or black.
8. Remove the old air filter pad and replace it with a new air filter
pad (Figure 10, item 2).
129
Maintenance
130
Section 8 Troubleshooting
Error The cuvette is soiled or there are Clean the cuvette; allow the particles to
Clean Cuvette undissolved particles in the cuvette settle
Negative result! The calculated result is negative Check the concentration of the sample
Check the programming
Error in the test database / user
No evaluation! Contact the manufacturer or a sales
database
representative
The measured absorbance is above the Dilute the sample and repeat the
Over measuring range
calibration range of the test measurement
If possible, select a test with a lower
The measured absorbance is below the
Under measuring range measurement range or use a cuvette
calibration range of the test
with a longer path length
131
Troubleshooting
132
Section 9 Replacement Parts
Description Cat.-No.
Sipper Module DR 5000 LZV485
Peltier temperature controlled Module DR 5000 LZV513
Pour-Thru Module DR 5000 LZV479
Multi-Cell Holder DR 5000 A23618
Carousel Holder (Sample changer) A23620
USB-Keyboard (keyboard layout: US) LZV582
USB-Barcode Scanner (handset scanner) LZV566
Hach Data Trans (PC software for data transfer) LZY274
Brewery Analysis Software LZV570
Software Drinking Water Application LZV571
Tubing Inlet Sipper DR 5000 (PHARMED) for Drinkingwater Applications LZV580
Tubing Inlet Sipper DR 5000 LZV780
Pour Thru Tube Kit LZV569
USB-Memory Stick LZV568
USB-Interface Cable, (1 m) LZV567
Tungsten (VIS) Lamp A23778
Deuterium (UV) Lamp A23792
Fuse A23772
Filter Pad A23766
Certified test filter set for self-checks (Verification Kit)
LZV537
(6 precision glass filters with target values)
Semi-Micro Cell OS / 50 mm LZP269
Macro Cell OG / 20 mm LZP331
Sample Cell, 1 cm Square Glass, (10 mm path length) matched pair 2095100
Sample Cell, 1 cm Square Quartz, (10 mm path length) matched pair 4822800
Sample Cell, 50 mm Rectangular Glass 2629250
Sample Cell, 50 mm Rectangular Quartz 2624450
Sample Cell, 100 mm Rectangular Glass 2629201
Sample Cell, 100 mm Rectangular Quartz 2624401
Sample Cell, 1" Round Plastic, (1 cm path length) 10 mL, w/cap 4864302
Sample Cell, 1" Square Glass, 10 mL, matched sets 2495402
Sample Cell, 1" Square Glass, 10&25 mL, matched sets 2665902
Sample Cell, 1" Square Plastic 2410212
Pour Thru Cell, 1x1 cm (Quartz/160 µL/glass center height 10 mm) A24209
Pour Thru Cell, 1x1 cm (Quartz/450 µL/glass center height 10 mm) LZV510
Pour Thru Cell, 5x1 cm (Quartz/370 µL/glass center height 10 mm) LZV649
Pour Thru Cell, 1" Square (1" path length) 5913700
Adapter for 100 mm Sample Cell LZY421
Dust Cover LZV728
133
Replacement Parts
134
Section 10 Contact Information
HACH Company Repair Service in the Repair Service in Canada: Repair Service in
World Headquarters United States: Hach Sales & Service Latin America, the
P.O. Box 389 HACH Company Canada Ltd. Caribbean, the Far East,
Loveland, Colorado Ames Service 1313 Border Street, Unit 34 Indian Subcontinent, Africa,
80539-0389 U.S.A. 100 Dayton Avenue Winnipeg, Manitoba Europe, or the Middle East:
Tel (800) 227-HACH Ames, Iowa 50010 R3H 0X4 Hach Company World
(800) -227-4224 Tel (800) 227-4224 Tel (800) 665-7635 Headquarters,
(U.S.A. only) (U.S.A. only) (Canada only) P.O. Box 389
Fax (970) 669-2932 Fax (515) 232-3835 Tel (204) 632-5598 Loveland, Colorado,
[email protected] Fax (204) 694-5134 80539-0389 U.S.A.
www.hach.com [email protected] Tel +001 (970) 669-3050
Fax +001 (970) 669-2932
[email protected]
HACH LANGE GMBH HACH LANGE LTD HACH LANGE LTD HACH LANGE GMBH
Willstätterstraße 11 Pacific Way Unit 1, Chestnut Road Hütteldorferstr. 299/Top 6
D-40549 Düsseldorf Salford Western Industrial Estate A-1140 Wien
Tel. +49 (0)2 11 52 88-320 GB-Manchester, M50 1DL IRL-Dublin 12 Tel. +43 (0)1 9 12 16 92
Fax +49 (0)2 11 52 88-210 Tel. +44 (0)161 872 14 87 Tel. +353(0)1 46 02 5 22 Fax +43 (0)1 9 12 16 92-99
[email protected] Fax +44 (0)161 848 73 24 Fax +353(0)1 4 50 93 37 [email protected]
www.hach-lange.de [email protected] [email protected] www.hach-lange.at
www.hach-lange.co.uk www.hach-lange.ie
DR. BRUNO LANGE AG HACH LANGE FRANCE HACH LANGE SA DR. LANGE NEDERLAND
Juchstrasse 1 S.A.S. Motstraat 54 B.V.
CH-8604 Hegnau 33, Rue du Ballon B-2800 Mechelen Laan van Westroijen 2a
Tel. +41(0)44 9 45 66 10 F-93165 Noisy Le Grand Tél. +32 (0)15 42 35 00 NL-4003 AZ Tiel
Fax +41(0)44 9 45 66 76 Tél. +33 (0)1 48 15 68 70 Fax +32 (0)15 41 61 20 Tel. +31(0)344 63 11 30
[email protected] Fax +33 (0)1 48 15 80 00 [email protected] Fax +31(0)344 63 11 50
www.hach-lange.ch [email protected] www.hach-lange.be [email protected]
www.hach-lange.fr www.hach-lange.nl
HACH LANGE APS HACH LANGE AB HACH LANGE S.R.L. HACH LANGE S.L.U.
Åkandevej 21 Vinthundsvägen 159A Via Riccione, 14 Edif. Arteaga Centrum
DK-2700 Brønshøj SE-128 62 Sköndal I-20156 Milano C/Larrauri, 1C- 2ª Pl.
Tel. +45 36 77 29 11 Tel. +46 (0)8 7 98 05 00 Tel. +39 02 39 23 14-1 E-48160 Derio/Vizcaya
Fax +45 36 77 49 11 Fax +46 (0)8 7 98 05 30 Fax +39 02 39 23 14-39 Tel. +34 94 657 33 88
[email protected] [email protected] [email protected] Fax +34 94 657 33 97
www.hach-lange.dk www.hach-lange.se www.hach-lange.it [email protected]
www.hach-lange.es
HACH LANGE LDA HACH LANGE SP.ZO.O. HACH LANGE S.R.O. HACH LANGE S.R.O.
Av. do Forte nº8 ul. Opolska 143 a Lešanská 2a/1176 Roľnícka 21
Fracção M PL-52-013 Wrocław CZ-141 00 Praha 4 SK-831 07 Bratislava –
P-2790-072 Carnaxide Tel. +48 (0)71 342 10-83 Tel. +420 272 12 45 45 Vajnory
Tel. +351 214 253 420 Fax +48 (0)71 342 10-79 Fax +420 272 12 45 46 Tel. +421 (0)2 4820 9091
Fax +351 214 253 429 [email protected] [email protected] Fax +421 (0)2 4820 9093
[email protected] www.hach-lange.pl www.hach-lange.cz [email protected]
www.hach-lange.pt www.hach-lange.sk
HACH LANGE KFT. HACH LANGE S.R.L. HACH LANGE HACH LANGE SU
Hegyalja út 7-13. Str. Leonida, nr. 13 8, Kr. Sarafov str. ANALİZ SİSTEMLERİ
H-1016 Budapest Sector 2 BG-1164 Sofia LTD.ŞTİ.
Tel. +36 (06)1 225 7783 RO-020555 Bucuresti Tel. +359 (0)2 963 44 54 Hilal Mah. 75. Sokak
Fax +36 (06)1 225 7784 Tel. +40 (0) 21 201 92 43 Fax +359 (0)2 866 04 47 Arman Plaza No: 9/A
[email protected] Fax +40 (0) 21 201 92 43 [email protected] TR-06550 Çankaya/ANKARA
www.hach-lange.hu [email protected] www.hach-lange.bg Tel. +90 (0)312 440 98 98
www.hach-lange.ro Fax +90 (0)312 442 11 01
[email protected]
www.hach-lange.com.tr
135
Contact Information
136
Section 11 Warranty, liability and complaints
The manufacturer warrants that the product supplied is free of
material and manufacturing defects and undertakes the obligation
to repair or replace any defective parts at zero cost.
The warranty period for instruments is 24 months. If a service
contract is taken out within 6 months of purchase, the warranty
period is extended to 60 months.
With the exclusion of the further claims, the supplier is liable for
defects including the lack of assured properties as follows: all those
parts that can be demonstrated to have become unusable or that
can only be used with significant limitations due to a situation
present prior to the transfer of risk, in particular due to incorrect
design, poor materials or inadequate finish will be improved or
replaced, at the supplier's discretion. The identification of such
defects must be notified to the supplier in writing without delay,
however at the latest 7 days after the identification of the fault. If the
customer fails to notify the supplier, the product is considered
approved despite the defect. Further liability for any direct or
indirect damages is not accepted.
If instrument-specific maintenance and servicing work defined by
the supplier is to be performed within the warranty period by the
customer (maintenance) or by the supplier (servicing) and these
requirements are not met, claims for damages due to the failure to
comply with the requirements are rendered void.
Any further claims, in particular claims for consequential damages
cannot be made.
Consumables and damage caused by improper handling, poor
installation or incorrect use are excluded from this clause.
137
Warranty, liability and complaints
138
Index
A L
Absorbance Check .................................................115 Language ................................................................. 19
Absorbance Formula ......................................... 94, 95 LCW 906 .................................................................. 61
Alphanumeric keypad .............................................. 21 Liability ................................................................... 137
Application ............................................................... 61 M
Audio signals ........................................................... 25 Main Menu ............................................................... 22
B Maintenance .......................................................... 125
Barcode Programs .......................................53, 54, 55 Manual Update ......................................................... 50
edit ..................................................................... 55 Mark ....................................................................... 107
Basic data ................................................................ 42 Measurement Process .................................56, 57, 76
C Measuring sequence ................................................ 77
Calibration formula ................................................... 79 Multi Wavelength ............... 22, 68, 70, 94, 95, 96, 97
Calibration Settings .................................................. 70 N
Chemical Form ............................................43, 47, 55 Name ....................................................................... 56
Chemical form .................................................... 53, 54 Noise Check ............................................................112
Cleaning O
Display ............................................................. 125 Operating environment ............................................ 13
Spectrophotometer .......................................... 125 Operator ID .............................................................. 23
Complaints ............................................................. 137 creating .............................................................. 23
Concentration Factor ............................ 91, 92, 94, 96 delete ................................................................. 23
Concentration Resolution ..................... 91, 92, 94, 96 Optical Checks ....... 110, 111, 112, 114, 115, 116, 117
Continuous Reading .......................................... 43, 45 Output Checks ........................................................119
Cursor Mode .................................................... 98, 100 P
Cuvettes/cells ........................................................ 125 Password ................................................................. 32
D activate .............................................................. 32
Data PC and Printer ................................................... 29, 31
delete ........................................................... 35, 37 Print data .................................................................. 31
recall .................................................................. 35 Printer Setup ............................................................ 29
send ................................................................... 35 Printing data ............................................................. 31
store .................................................................. 35 Program ................................................................... 65
Data Storage ............................................................ 38 Programm overview ................................................. 22
Date ......................................................................... 25 R
Date and Time ......................................................... 25 Reading Mode ....................................... 43, 44, 92, 93
Dilution Factor ..............................................43, 46, 55 Reagent Blank ................................................... 43, 48
Display ............................................................. 21, 125 Recall Data ................22, 38, 43, 55, 92, 95, 99, 105
Display and Sound ................................................... 25 Reference Scan ............................................... 98, 103
Drift Check ..............................................................116
S
F Safety Information ...................................................... 9
Factory Service ...................................................... 120 Sample blank ........................................................... 55
Favorites ............................................... 22, 51, 83, 85 Sample ID ................................................................ 24
delete ........................................................... 84, 85 create ................................................................ 24
edit ..................................................................... 84 delete ................................................................. 24
recall .................................................................. 85 Save as User Program .......................... 43, 55, 92, 94
Filter Settings ........................................................... 36 Scale & Units .................................. 99, 101, 105, 106
Formula .............................................................. 56, 57 Security List ............................................................. 32
Free programming ................... 76, 77, 79, 82, 83, 84 Select View ............................................................ 100
H Send Data .....................................36, 43, 55, 98, 105
HACH Data Trans .............................................. 31, 36 Service Time .......................................................... 120
Hazard Information .................................................... 9 Single Reading ......................................................... 43
I Single Wavelength .......22, 43, 45, 67, 70, 91, 92, 93
Instrument Backup ......................................... 121, 122 Software ........................................................... 60, 110
Instrument Information ........................................... 109 Standard Addition .............................................. 43, 86
Instrument Setup .......22, 23, 43, 55, 92, 95, 99, 105 Standard Adjust ................................................. 43, 46
Integral ............................................................. 98, 100 Stored Data .............................................................. 35
Interfaces ................................................................. 29 Stored Programs ..........22, 42, 43, 46, 47, 48, 50, 51
Internet ............................................................. 60, 110 send Data .......................................................... 43
139
Stray Light Check ...................................................114
System Check ........................................................ 120
System Checks 22, 109, 111, 112, 114, 115, 116, 117,
................................................................119, 120, 121
T
Time & Interval ............................................... 105, 106
Time Course ..........22, 38, 39, 40, 41, 105, 107, 108
Time Course Scan Reading ................................... 106
Timer .................................. 25, 43, 55, 56, 58, 91, 94
Touch Screen .......................................................... 21
U
Unpack the instrument ............................................. 13
Update .......................................................56, 60, 110
User Programs ................................................... 22, 65
V
Variables ......................................................56, 58, 82
Verification Kit .........................................................117
Version ............................................................... 56, 57
View Table ............................................................. 105
W
Warranty ................................................................ 137
Wavelength ........................................................ 91, 94
Wavelength Check .................................................. 111
Wavelength Range .................................................. 99
Wavelength Scan .......22, 38, 39, 40, 41, 98, 99, 102
Wavelength setting ................................................ 105
Wavelength spectrum .............................................. 98
140