Standard Practice For Determination of Long-Term Strength For Geosynthetic Reinforcement
Standard Practice For Determination of Long-Term Strength For Geosynthetic Reinforcement
Standard Practice For Determination of Long-Term Strength For Geosynthetic Reinforcement
PP = Polypropylene
QPL = Qualified Products List
RF = Combined reduction factor to account for long-term degradation due
to installation damage, creep, and chemical/biological aging
RFCR = Strength reduction factor to prevent long-term creep rupture of the
reinforcement
RFD = Strength reduction factor to prevent rupture of the reinforcement due to long-
term chemical and biological degradation
RFID = Strength reduction factor to account for installation damage to the reinforcement
Tal = The long-term tensile strength which will not result in rupture of the
reinforcement during the required design life, calculated on a load per unit of
reinforcement width basis
Tult = The ultimate tensile strength of the reinforcement determined from wide width
tensile tests
UV = Ultraviolet light
WSDOT = Washington State Department of Transportation
Definitions
Apertures The open spaces formed between the interconnected network of
longitudinal and transverse ribs of a geogrid.
Class 1 Structure Typically includes geosynthetic walls or slopes that support bridge
abutments, buildings, critical utilities, or other facilities for which
the consequences of poor performance or failure would be severe.
In general, geosynthetic walls greater than 6 m (20 ft) in height and
reinforced slopes greater than 9.2 m (30 ft) in height will be considered
to be Class 1.
Class 2 Structure All geosynthetic walls and slopes not considered to be Class 1.
Confined Testing Geosynthetic testing in which the specimen is surrounded and confined
by soil to simulate conditions anticipated for the geosynthetic in use.
Effective Design Temperature
The temperature that is halfway between the average yearly air
temperature and the normal daily air temperature for the warmest
month at the wall site.
Hydrolysis The reaction of water molecules with the polymer material, resulting in
polymer chain scission, reduced molecular weight, and strength loss.
In-isolation Testing Geosynthetic testing in which the specimen is surrounded by air or a
fluid (not soil).
Installation Damage Damage to the geosynthetic such as cuts, holes (geotextiles only),
abrasion, fraying, etc., created during installation of the geosynthetic
in the backfill soil.
Load Level For creep or creep rupture testing, the load applied to the test specimen
divided by Tlot, the short-term ultimate strength of the lot or roll of
material used form the creep testing.
Nonaggressive Environment
For geosynthetic walls and slopes, soils which have a d50 of 4.75 mm
or less, a maximum particle size of 31.5 mm or less, a pH of 4.5 to 9,
and an effective design temperature of 30o C or less.
Oxidation The reaction of oxygen with the polymer material, initiated by heat,
UV radiation, and possibly other agents, resulting in chain scission and
strength loss.
Post-consumer Recycled Material
Polymer products sold to consumers which have been returned by the
consumer after use of the products for the purpose of recycling.
Product Line A series of products manufactured using the same polymer in which
the polymer for all products in the line comes from the same source,
the manufacturing process is the same for all products in the line, and
the only difference is in the product weight/unit area or number of
fibers contained in each reinforcement element.
Sample A portion of material which is taken for testing or for record purposes,
from which a group of specimens can be obtained to provide
information that can be used for making statistical inferences about the
population(s) from which the specimens are drawn.
Specimen A specific portion of a material or laboratory sample upon which a test
is performed or which is taken for that purpose.
Survivability The ability of a geosynthetic to survive a given set of installation
conditions with an acceptable level of damage.
8. ASTM D-1248 – Standard Specification for Polyethylene Plastics Extrusion Materials for
Wire and Cable
9. ASTM D-4101 – Standard Specification for Polypropylene Injection and Extrusion
Materials
10. WSDOT Test Method T 926 – Geogrid Brittleness Test
11. ISO/DIS 10722-1 - Procedure for simulating damage during installation. Part 1: Installation
in granular materials
12. ASTM D5818 – Standard Practice for Obtaining Samples of Geosynthetics from a Test
Section for Assessment of Installation Damage
13. ASTM D2488 – Standard Practice for Description and Identification of Soils (Visual-
Manual Procedure)
14. ASTM D1557 – Standard Test Methods for Laboratory Compaction Characteristics of Soil
Using Modified Effort (56,000 ft-lbf/ft3)(2700 kN-m/m3)
15. AASHTO T96 - Resistance to Degradation of Small-Size Coarse Aggregate by Abrasion
and Impact in the Los Angeles Machine
16. ASTM D6992 – Accelerated Tensile Creep and Creep-Rupture of Geosynthetic Materials
Based on Time-Temperature Superposition Using the Stepped Isothermal Method
17. ASTM D5262 – Standard Test Method for Evaluating Unconfined Tension Creep Behavior
of Geosynthetics
18. ISO/FDIS 9080:2001 - Plastic piping and ducting systems – Determination of long-term
hydrostatic strength of thermoplastics materials in pipe form by extrapolation.
19. ASTM D2837 – Standard Test Method for Obtaining Hydrostatic Design Basis for
Thermoplastic Pipe Materials
20. ASTM D4355 – Standard Test Method for Deterioration of Geotextiles from Exposure to
Ultraviolet Light and Water (Xenon-Arc Type Apparatus)
21. ASTM D4603 – Standard Test Method for Determining Inherent Viscosity of
Poly(Ethylene Terephthalate) (PET) by Glass Capillary Viscometer
22. GRI-GG7 – Carboxyl End Group Content of PET Yarns
23. GRI-GG8 – Determination of the Number Average Molecular Weight of PET Yarns Based
on a Relative Viscosity Value
24. ASTM D3045 – Standard Practice for Heat Aging of Plastics Without Load
25. ASTM D 3417-99 - Enthaplies of Fusion and Crystallinization of Polymers by DSC
26. ENV ISO 13438:1999 - Geotextiles and Geotextile-Related Products - Screening Test
Method for Determining the Resistance to Oxidation
27. ASTM D 3895 – Standard Test Method for Oxidative-Induction Time of Polyolefins
by Differential Scanning Calorimetry
28. ASTM D 5885 – Standard Test Method for Oxidative Induction Time of Polyolefins by
High-Pressure Differential Scanning Calorimetry
Per mutual agreement between the testing laboratory, the geosynthetic manufacturer, and the
approval authority, “equivalent" ISO standards and practices may be used in lieu of ASTM,
AASHTO, or GRI standards and practices where equivalent procedures are available.
Temperature scan should start 10° C below, continue through, and stop 10° C above
the melt range. Recommended test parameters are as follows:
Homo- Sample Latent Heat, ΔH° DSC Scan Speed
Melt Range (°C)
Polymer Size (mg) (cal/gm) (°C/min)
PP 7.5 100-165 45 10
PET 10 200-245 30 10
Other values of sample size, melt range, and DSC scan speed can be used with
justification.
f. Tensile test results for specimens taken for each retrieval from the incubation
chambers.
g. Tensile test results, including tensile strength, strain at peak load, and 5 percent
secant or offset modulus, for both virgin material and degraded material should
include individual test results for each specimen, typical load-strain curves which
are representative of the specimens tested, including associated calibration data as
necessary to interpret the curves (curves in which strain and load/unit width are
already calculated are preferred), the average value for each sample, the coefficient
of variation for each sample, and a description of any deviations from the standard
tensile test procedures required by Appendix D.
h. A detailed description of the data characterization and extrapolation procedures used,
including data plots illustrating these procedures and their theoretical basis.
i. Results of any chemical tests taken (e.g., OIT or HPOIT, molecular weight, product
weight/unit area, etc.), and any scanning electron micrographs taken, to verify the
significance of any degradation in strength observed.
j. Results of biological degradation testing, if performed.
k. RFD, and a description of the method used to determine RFD for the product.
5. Evaluation of Product Lines
If determining the long-term strengths for a product line, the data required under “General
Product Information” must be obtained for each product. Product specific information
for creep and durability must be obtained for at least one product in the product line to
qualify the product line for Class 1 structures or aggressive environments, or in the case
of Class 2 structures to allow the use of a total long-term strength reductfion factor of less
than 7 (see description of environment aggressiveness and Class 1 and Class 2 structures
in “Determination Of Long-Term Geosynthetic Strength” later in this Standard Practice).
Additional product specific information for creep and durability shall also be obtained for
each product in the product line in accordance with Appendices B, C and D regarding use
of long-term data for “similar” products. This data is to be used to determine long-term
strengths for each product in the product line.
In general, product specific installation damage data must be obtained for each product
in the line. However, it is permissible to obtain installation damage data for only some of
the products in the product line if interpolation of the installation damage reduction factor
between products is feasible. Interpolation of the product specific installation damage
reduction factor RFID between tested products can be based on the weight per unit area
or undamaged tensile strength of each product, provided that the progression of weight
per unit area or tensile strength as compared to the progression of RFID for each tested
product is consistent. For coated geogrids, the weight of coating placed on the fibers or
yarns may influence the amount of installation damage obtained (Sprague, et al., 1999). In
that case, the installation damage reduction factor may need to be correlated to the coating
weight instead. If it is determined that the RFID values obtained for a product line are not
correlated with product weight per unit area, undamaged tensile strength, coating weight,
or some other product parameter, and the variance of RFID between any two products in the
product line is 0.1 or more, then each product in the product line shall be tested.
Tal = The long-term tensile strength that will not result in rupture of the
reinforcement during the required design life, calculated on a load per unit
of reinforcement width basis
Tult = the ultimate tensile strength (MARV) of the reinforcement determined from
wide width tensile tests
RF = a combined reduction factor to account for potential long-term degradation
due to installation damage, creep, and chemical/biological aging
RFID = a strength reduction factor to account for installation damage to the
reinforcement
RFCR = a strength reduction factor to prevent long-term creep rupture of the
reinforcement
RFD = a strength reduction factor to prevent rupture of the reinforcement due to
chemical and biological degradation
See Appendices A through D for protocols to use to determine RF from product specific
data. Unless otherwise indicated in the contract specifications for a given project, the
design temperature used to determine RF and Tal from product specific data shall be
assumed to be 20° C (68° F).
The value selected for Tult is the minimum average roll value (MARV) for the product to
account for statistical variance in the material strength. Tult should be based on a wide width
tensile strength (i.e., ASTM D4595 for geotextiles or ASTM D6637 for geogrids). Other
sources of uncertainty and variability in the long-term strength include installation damage
(Appendix A), creep extrapolation (Appendices B and C), and chemical degradation
(Appendix D). It is assumed that the observed variability in the creep rupture envelope
is 100% correlated with the short-term tensile strength, as the creep strength is typically
directly proportional to the short-term tensile strength within a product line (see Appendix
B and Note 7 in Appendix B if this is not the case). Therefore, the MARV of Tult adequately
takes into account that source of variability. For additional discussion of this issue, see
Note 2 below.
Note 2: The product strength variability is not taken into account by using the creep limited
strength, Tl, directly or in normalizing Tl by Tlot (see Appendix B). Tl only accounts for
extrapolation uncertainty. Furthermore, Tlot is specific to the lot of material used for the
creep testing. Normalizing by Tlot makes the creep reduction factor RFCR applicable to the
rest of the product line, as creep strength is typically directly proportional to the ultimate
tensile strength, within a product line.. As shown below, it is not correct to normalize
the creep strength Tl using Tult, the MARV of the tensile strength for the product, nor is it
correct to use Tl directly in the numerator to calculate Tal.
and
In the former case, the creep strength is not indexed to the actual tensile strength of the
material used in the creep testing, and since there is a 50% chance that Tult will be less than
or equal to Tlot, using Tult in this case would result in an unconservative determination of
RFCR. In the latter case, where Tl is used directly as a creep reduced strength, the product
strength variability is not taken into account, since Tl is really a mean creep strength.
Hence, RFCR must be determined as shown in Equation B.4-1 (see Appendix B), and the
MARV must be used for Tult when determining Tal. Note that the use of the MARV for Tult
may not fully take into account the additional variability caused by installation damage. For
the typical degree of installation damage observed in practice, this additional variability
is minor and can be easily handled through the overall safety factor used in design of
reinforced structures. For durability (RFD), additional variability does not come into play
if a default reduction factor is used. If a more refined durability analysis is performed,
additional variability resulting from chemical degradation may need to be considered.
The type and amount of data to be obtained, and the approach used to determine the long-
term design strength, will depend on the geosynthetic wall or reinforced slope class and the
aggressiveness of the environment.
For most soil conditions in the USA, the environment will likely be chemically
nonaggressive. A possible exception to this is immediately behind a concrete wall face,
where pH levels could possibly be elevated above a pH of 9. However, recent research has
indicated that for well drained backfills, the pH adjacent to a concrete face stays below 9
in the long-term (Koerner, et al., 2001, Koerner, et al., 2002). In any case, the long-term
strength determination must account for the environment at the face. However, there are
specific geological regions in the USA that are more likely to have chemically aggressive
conditions as described in Elias (2000). Examples include salt affected soils in the arid
western (especially southwest) regions of the USA, acid-sulphate soils that are commonly
found in the Appalachian region of the USA, and calcareous soils commonly found in
Florida, Texas, New Mexico, and many western states.
The wall or slope contract specifications will identify if the environment is anticipated
to be aggressive and the reason for the aggressive environment designation (i.e., backfill
gradation, site chemistry, or site temperature). If aggressive conditions are not identified
in the contract specifications, and the contract specifications provide soil chemical criteria
that are consistent with nonaggressive conditions as described herein, the environment
should be considered to be nonaggressive to determine the longterm strength. However, the
backfill should be tested prior to use to verify that it is nonaggressive.
4. Requirements for Class 1 Walls and Slopes to Determine Tal
RFID and RFCR shall be determined from product specific data for all geosynthetics used
in Class 1 walls and slopes. See submission requirements for installation damage and
creep data provided in this document. The product specific data for these reduction factors
shall be interpreted/extrapolated in accordance with Appendices A, B, and C. RFD shall
be determined from long-term product specific data, or a default value may be used as
described below. See submission requirements for durability data provided herein. Long-
term product specific data for RFD should be interpreted in accordance with Appendix D. If
adequate long-term durability data is not available, a default reduction factor for RFD may
be used if the environment is nonaggressive and if the product meets the minimum polymer
and physical property requirements provided in Table 1. In this case, a default value for
RFD of 1.3 may be used for PET, HDPE, and PP geosynthetics.
Note 3: The default value for RFD of 1.3, which can be used for products that meet the
minimum property requirements in Table 1, was determined based on FHWA (1997) and
Elias, et. al. (1997) and in consideration of the relatively cool climate which exists in the
state of Washington, where effective design temperatures are always less than 20o C (68o
F) and are likely to be on the order of 10o C (50o F) or less. A higher default value of 1.5
for products which meet the property requirements in Table 1 may be desirable for more
temperate climates which still meet the requirements for a nonaggressive environment,
especially to address polyolefin oxidative degradation, as the potential for this type of
degradation, even for products which meet the property requirements in Table 1, becomes
more uncertain at higher temperatures due to the lack of protocols which can accurately
identify the amount or effectiveness of end use antioxidants present. The UV resistance
criteria provided in Table 1 only provides a rough indication of the effectiveness of end use
antioxidants in polyolefins (see additional commentary following Table 1).
Table 1
Minimum Requirements for Geosynthetic Products to Allow Use of Default Reduction Factor for
Long-Term Degradation.
Criteria to Allow Use of Default
Polymer Type Property Test Method
RF*
PP and HDPE UV Oxidation ASTM D4355 Min. 70% strength retained after
Resistance 500 hrs in weatherometer
PET UV Oxidation ASTM D4355 Min. 50% strength retained after
Resistance 500 hrs in weatherometer if
geosynthetic will be buried within
one week, 70% if left exposed
for more than one week.
PP and HDPE Thermo- Oxidation ENV ISO 13438:1999, Min. 50% strength retained after
Resistance Method A (PP) or B (HDPE) 28 days (PP) or 56 days (HDPE)
PET Hydrolysis Inherent Viscosity Method Min. Number Average Molecular
Resistance (ASTM D4603 and GRI Test Weight of 25,000
Method GG8), or Determine
Directly Using Gel
Permeation Chromatography
PET Hydrolysis GRI Test Method GG7 Max. Carboxyl End Group
Resistance Content of 30
All Polymers Survivability 1Weightper Unit Area 1Min. 270 g/m2
(ASTM D5261)
All Polymers % Post-Consumer Certification of Materials Maximum of 0%
Recycled Material Used
by Weight
*Polymers not meeting these requirements may be used if product specific test results
obtained and analyzed in accordance with Appendices A, B, C, and D are provided.
1Alternatively, a default RFD = 1.3 may be used if product specific installation damage
testing is performed and it is determined that RFID is 1.7 or less, and if the other
requirements in Table 1 are met.
Note 4: The requirements provided in Table 1 utilize currently available index tests and
are consistent with current AASHTO design specifications (AASHTO, 2004, 2002), with the
exception of the oven aging test, which is a new requirement. These index tests can provide
an approximate measure of relative resistance to long-term chemical degradation of
geosynthetics. Values selected as “minimum” criteria to allow use without additional long-
term testing are based on values for such properties reported in the literature. These values
are considered indicative of good long-term performance or represent a readily available
current standard within the industry that signifies that a product has been enhanced for
long-term environmental exposure.
Quality Assurance Requirements for Products that have been Through Initial
Acceptance
1. Data Verification Requirements
The following information about each product shall be submitted for verification purposes:
a. Geosynthetic type and structure.
b. Spacing and dimensions of geogrid elements. The receiving laboratory should verify
these dimensions upon receipt of the sample(s) using hand measurement techniques.
This is especially critical for strength determination based on a single or limited
number of ribs in the specimens tested.
c. Polymer(s) used for fibers, ribs, etc.
d. Polymer(s) used for coating, if present.
e. Roll size (length, width, and area).
f. Typical lot size.
g. Polymer source(s) used for product.
h. For HDPE and PP, primary resin ASTM type, class, grade, and category (for HDPE
use ASTM D-1248, and for PP use ASTM D-4101).
j. % post-consumer recycled material by weight.
k. Minimum weight per unit area for product (ASTM D5261).
l. MARV for ultimate wide width tensile strength (ASTM D4595 or ASTM D6637).
If SIM is used for this creep rupture testing, it shall have been demonstrated for the
initial acceptance testing that the reduced specimen width typically used for SIM
testing does not have a significant effect on the creep rupture results, and provided
that the validity of SIM for the product through comparison of SIM data with
“conventional” creep rupture data was established for the initial product acceptance
testing.
The ultimate tensile strength of the lot or roll of material used in the creep testing
obtained in accordance with ASTM D4595 or ASTM D6637 shall be obtained
to normalize the creep rupture loads in accordance with Appendix B or C. The
information required in part 3 of “Data Requirements for Initial Product Acceptance”
as it applies to the QA testing shall be obtained and included in the test report for this
QA testing.
Note 5: If “conventional” creep testing is performed for QA purposes, it is assumed
that the product has not changed relative to what was tested for initial product
acceptance purposes, thereby allowing the assumption to be made that the shift
factors obtained through the initial product acceptance testing are valid for the QA
testing. Requiring new “conventional” creep test shift factors to be re-established
would result in the need to fully repeat the test program for the initial product
acceptance, which would not be practical for QA purposes. Regarding the fourth
creep test data point, the requirement to use only data obtained at the reference
temperature if “conventional” creep testing is performed provides a second check
that eliminates the need for this shift factor assumption and any inaccuracies
associated with that assumption.
C. Durability Testing
If only index durability testing was conducted to allow use of a default value for
RFD for the initial product acceptance testing, only index durability testing need be
conducted for QA purposes. In this case, durability testing for QA purposes shall
consist of the determination of molecular weight based on GRI-GG7 and carboxyl
end group content based on GRI-GG8 for polyesters, UV resistance based on ASTM
D4355 for polyolefins and PET’s), and an oven aging exposure test per ENV ISO
13438:1999 for polyolefin geosynthetics. Regarding the oven aging test, control
and post-exposure specimens shall be tested for tensile properties (ASTM D4595 or
ASTM D6637). The results of this oven aging testing will be used only to compare
a product with itself, and to meet the minimum requirements in Table 1. In addition,
geogrid brittleness shall be evaluated per WSDOT Test Method T 926.
If long-term performance durability testing was conducted to justify the use of a
lower RFD or to justify use in aggressive environments for initial product acceptance,
a minimum of five specimens shall be exposed to the most aggressive environment
used in the initial product acceptance testing at the highest temperature tested, for
a minimum of 2,000 hours. These specimens, and unexposed specimens from the
same roll of material, shall be tested for tensile properties (ASTM D4595 or ASTM
D6637). In addition, for polyolefins, either oxidative induction time per ASTM D
3895 or high pressure oxidative induction time per ASTM D 5885 shall be conducted
for each specimen tested (before and after exposure), and for PET’s, molecular weight
(ASTM D4603 and GRI:GG8) and specimen weight per unit area (ASTM D5261)
shall be conducted for each specimen tested (before and after exposure).
WSDOT Materials Manual M 46-01.27 Page 19 of 74
April 2017
T 925 Standard Practice for Determination of Long-Term Strength for Geosynthetic Reinforcement
5. Quality Assurance (QA) Criteria for Comparison to Initial Product Acceptance Test Results
The acceptability of the QA test results to allow a product or product line to maintain its
prior acceptance status is established based on the statistical significance, or lack thereof,
of the difference between the QA test results and the initial product acceptance test results.
The criteria and methods for determining the statistical significance between the QA and
initial product acceptance test results are as follows:
A. Short-term Index Tensile Testing
For wide width tensile strength, the mean of the test results for the sample for each
product tested shall be greater than or equal to the MARV reported for the product.
B. Installation Damage Testing
If the mean of the average strength of the sample after damage as a percent of the
undamaged strength is less than the average value obtained for the same product and
condition during the product acceptance phase, the maximum difference between the
two means shall be no greater that what is defined as statistically insignificant based
on a one-sided student-t distribution at a level of significance of 0.05. In this case, t is
determined as follows:
(P − P ) − δ n1n2 (n1 + n2 − 2 )
2 =
1 2
tα / 2, n1 + n2 −(3)
(n1 − 1)s 2
1 + (n2 − 1)s 2
2
(n1 + n2 )
where,
tα/2,n1+n2-2 = value of the t-distribution for the installation damage samples
P1 = the mean of the strength retained after installation damage
(i.e., Tdam/Tlot) obtained for initial product acceptance
P2 = the mean of the strength retained after installation damage
(i.e., Tdam/Tlot) obtained for QA testing
δ = the difference in the means for the populations corresponding to
the sample means P1 and P2 (assumed equal to zero for this test)
s1 = the standard deviation corresponding to P1
s2 = the standard deviation corresponding to P2
n1 = the number of data points corresponding to P1
n2 = the number of data points corresponding to P2
tα/2,n1+n2-2 calculated using Equation 3 shall be no greater than t determined from the
applicable Student t table (or from the Microsoft EXCEL function TINV(α,n-2)) at
α = 0.05 and n1+n2-2 degrees of freedom. If this is not true, the difference between
P1 and P2 is determined to be statistically significant, and P1 > P2 , two additional
samples from the same installation condition shall be tested and P2 recalculated and
statistically compared to P1. If the QA test results are still too low, a full installation
damage study for initial product acceptance must be completed in accordance with
Appendix A, and new values of RFID established.
(4)
ª
« 1
log t L = log t reg − tα / 2,n −2 1 + +
P−P
2
( ) º
» ×σ
«
¬
n
¦ Pi − P ( ) 2
»
¼
and
{¦ [(P − P )(log t − log t )]} 2
¦ [log t − log t ] −
2 i i
¦ (P − P )
i 2
(5)
i
σ =
n−2
where:
log tL = lower bound prediction limit
treg = time corresponding to the load level from the initial product
acceptance creep rupture envelope at which QA creep tests were
performed (e.g., at 500 and 100,000 hrs after time shifting)
tα/2,n-2 = value of the t distribution determined from applicable Student
t table (or from the Microsoft EXCEL function TINV(α,n-2)) at
α/2 = 0.05 and n-2 degrees of freedom (this corresponds to the
95% one-sided prediction limit)
n = the number of rupture or allowable run-out points in the original
test sample (i.e., for initial product acceptance)
P = load level obtained at treg from the regression line developed from
the initial product acceptance testing
P = the mean rupture load level for the original test sample (i.e., all
rupture or run-out points used in the regression to establish the
rupture envelope for initial product acceptance)
Pi = the rupture load level of the i’th point for the rupture points used
in the regression for establishing the rupture envelope for initial
product acceptance
log t = the mean of the log of the rupture time for the original test sample
(i.e., all rupture or run-out points used in the regression to establish
the rupture envelope for initial product acceptance)
ti = the rupture time of the i’th point for the rupture points used in the
regression for establishing the rupture envelope for initial product
acceptance
The comparison between the QA test results and the initial product acceptance test
results is illustrated conceptually in Figure 1. Once log tL has been determined at
each specified load level, compare this value to the log rupture time (i.e., log tQA)
obtained for each QA creep rupture test at the specified load level (e.g., 500 and
100,000 hours). If log tQA < log tL for any of the QA creep rupture test results, perform
two additional tests at the load level P for the specified treg where this QA criteria
was not met and compare those results to log tL. If for these two additional tests this
criterion is not met, perform adequate additional creep rupture testing to establish a
new rupture envelope for the product in accordance with initial product acceptance
requirements (Appendix B). This new rupture envelope will form the baseline for any
future QA testing.
P500
x
P100000 x x x
95% prediction limit
for acceptance data
- from acceptance testing
x – from QA testing 500
0
1 10 100 1,000 10,000 100,000 1,000,000
Rupture Time (after time shifting), t (hrs)
Figure 1. Conceptual illustration of the comparison of QA creep rupture test results to
initial product acceptance creep rupture test results.
D. Creep Strain Testing for Prediction of Creep Limit
The comparison between the creep data obtained for the initial product acceptance
testing and the QA creep data shall be performed at a specified strain. The specified
strain will depend on the strains observed in all of the creep tests (initial product
acceptance and QA). Select a strain that will intercept all of the creep curves as much
as possible. Preferably, the strain level should be approximately 5 to 10% or more,
and as close to the instability limit strain as possible. Where the selected strain level
intersects each creep curve, determine the time required to reach the specified strain.
Plot the load level as a function of the logarithm of time to reach the specified strain
for the initial product acceptance data, and perform a regression for this data set.
The log times to the specified strain level for the QA creep data shall be determined
at a load level that corresponds to 500 hours and 50,000 hours on the initial product
acceptance creep envelope. This is illustrated conceptually in Figure 2. The log of the
time to reach the same specified strain for each of the four QA creep data points shall
be equal to or greater than the 95% lower prediction limit of the variable, log time,
established by the Student’s t test of the original product acceptance data set, using
Equations 4 and 5 (see part “c” above).
Once log tL has been determined at each specified load level, compare this value to
the log time to reach the specified strain (i.e., log tQA) obtained for each QA creep
test at the specified load level (e.g., 500 and 50,000 hours). If log tQA < log tL for any
of the QA creep rupture test results, perform two additional tests at the load level P
for the specified treg where this QA criteria was not met and compare those results
to log tL. If for these two additional tests this criterion is not met, perform adequate
additional creep testing to establish a new creep stiffness curve for the product in
accordance with initial product acceptance requirements (Appendix C). This new
creep stiffness curve will form the baseline for any future QA testing.
(a)
P7
P6
t1 t2 t3 P5 t4 t5
P4 P3
H
Strain, H
P2
P1
(b)
P7 Regression line for
P6 acceptance testing
Load or Load level, P
P500
x P5
P50000
P4 P3
x
x x
95% prediction limit
for acceptance data
- from acceptance testing
x – from QA testing 500 50000
0
1 10 100 1,000 10,000 100,000
Time to H % Strain, t (hrs)
Figure 2. Conceptual illustration of the comparison of QA creep strain test results to initial
product acceptance creep strain test results (a) creep strain curves, and (b) envelope of time
to the specified strain.
References
AASHTO, 2002, Standard Specifications for Highway Bridges, American Association of
State Highway and Transportation Officials, Seventeenth Edition, Washington, D.C., USA.
AASHTO, 2004, LRFD Bridge Design Specifications, with Interims, American Association
of State Highway and Transportation Officials, Third Edition, Washington, D.C., USA.
Allen, T.M., 1991, “Determination of Long-Term Strength of Geosynthetics: a State-of-the-
Art Review”, Proceedings of Geosynthetics ‘91, Atlanta, GA, USA, Vol. 1, pp. 351-379.
Elias, V., 2000, Corrosion/Degradation of Soil Reinforcements for Mechanically
Stabilized Earth Walls and Reinforced Soil Slopes, FHWA-NHI-00-044, Federal Highway
Administration, Washington, D.C.
Elias, V., DiMaggio, J., and DiMillio, A., 1997, “FHWA Technical Note on the
Degradation-Reduction Factors for Geosynthetics,” Geotechnical Fabrics Report, Vol. 15,
No. 6, pp. 24-26.
Federal Highway Administration (FHWA), 1997, “Degradation Reduction Factors for
Geosynthetics,” Federal Highway Administration Geotechnology Technical Note.
Geosynthetic Research Institute, 1998, “Carboxyl End Group Content of Polyethylene
Terephthalate (PET) Yarns,” GRI Test Method GG7.
Geosynthetic Research Institute, 1998, “Determination of the Number Average Molecular
Weight of Polyethylene Terephthalate (PET) Yarns based on a Relative Viscosity Value,”
GRI Test Method GG8.
Koerner, G. R., Hsuan, Y. G., and Hart, M., 2001, Field Monitoring and Laboratory Study
of Geosynthetics in Reinforcement Applications, GRI Report #26, Geosynthetic Research
Institute, Drexel University, Philadelphia, PA, USA, 116 pp.
Koerner, G. R., Hsuan, Y. G., and Koerner, R. M., 2002, “Field Measurements of Alkalinity
(pH) Levels Behind Segmental Retaining Walls, or SRW’s,” 7th International Geosynthetics
Conference, Nice, France, Delmas, Gourc, and Girard, ed’s, Vol. 4, pp. 1443-1446.
Koerner, R. M. and Koerner, G. R., 1990, “A quantification and assessment of installation
damage to geotextiles.” Proc. Fourth Intl. Conf. on Geotextiles, Geomembranes, and
Related Products, The Hague, pp. 597-602.
Risseeuw, P, and Schmidt, H. M., 1990, “Hydrolysis of HT Polyester Yarns at Moderate
Temperatures,” Proceedings of the Fourth International Conference on Geotextiles,
Geomembranes, and Related Products, The Hague, pp. 691-696.
Sprague, C. J., Allen, S., and Thornton, S., 1999, “Installation Damage Testing, Sensitivity
Assessment and Derivation of RFID,” Geosynthetics ’99, Boston, MA, USA, pp. 1123-
1132.
Van Zanten, V., ed., 1986, Geotextiles and Geomembranes in Civil Engineering, Wiley-
Halsted.
Wadsworth, H., 1998, Handbook of Statistical Methods for Engineers and Scientists,
McGraw-Hill, 688 pp.
7. Samples subjected to installation damage shall be tested for tensile strength and
deformation characteristics in accordance with ASTM D4595, or ASTM D6637. The
number of specimens tested should be in accordance with ASTM D4595 or D6637.
Single rib tests such as GRI:GG1 shall not be used for installation damage evaluation,
as it is difficult to assess the effect of severed ribs on the strength and stiffness of
damaged materials. Test results from damaged specimens shall be compared to tensile
test results obtained from undamaged (i.e., not exposed to installation conditions)
specimens taken from the same lot, and preferably the same roll, of material as the
damaged specimens.
8. The installation damage reduction factor RFID is then determined as follows:
Tlot
RFID (A-1)
Tdam
where, Tlot is the average lot specific tensile strength before exposure to installation,
and Tdam is the average lot specific tensile strength after installation. In no case should
RFID be less than 1.1.
9. To select an appropriate reduction factor for design, the project site installation
conditions must be related to the installation test conditions. To relate the installation
damage test conditions to the actual site conditions, primary consideration will be
given to the backfill characteristics (d50 particle size, potential for oversize material,
particle angularity, and overall gradation), and to a lesser degree the method of
spreading the backfill over the geosynthetic, the type of compaction equipment,
and initial backfill lift thickness over the geosynthetic, provided that the initial lift
thickness is 150 mm (6 in.) or more. The actual installation conditions used in the
test must be clearly stated in the test report, specifically identifying any deviations
from typical geosynthetic reinforcement installation practices in full scale structures,
and the impact those deviations may have on the values of RFID determined. Typical
installation conditions, for the purposes of this protocol, are generally described
as follows:
• The geosynthetic is placed on a subgrade prepared as described in step 2.
• Backfill material is placed and spread on the geosynthetic using full scale
spreading and compaction equipment commonly used in wall or reinforced slope
construction (e.g., loaded dump trucks, dozers such as a D-6 or larger, etc.).
• Backfill is compacted using a full scale vibratory drum roller (i.e., one that
someone can drive, not a smaller walk behind unit typically used to compact near
the face of a wall to prevent distortion of facing elements during compaction).
If it is not possible to conduct the installation damage test in a way that fully
simulates these “typical” installation conditions (i.e., installation conditions in the
test are less severe than the conditions described above, for example, use lighter
equipment, less movement of soil over the geosynthetic as the backfill is spread,
etc.), data must be provided that demonstrates the effect the use of these less severe
installation conditions would have on RFID.
10. If the installation damage test is conducted for a specific project, the actual backfill
material planned for use in the geosynthetic structure should be used for the test. If
the purpose of the installation damage testing is to generate RFID values for general
use for future projects (i.e., the testing is not intended to be project specific), a range
of soil backfill gradations/types should be used in the testing. The range of backfill
materials selected should permit interpolation as needed to match the specific soil
to be used as reinforced soil backfill. In general, the backfill materials tested should
range from soil classified as a sand to coarse gravel (e.g., d50 sizes ranging from 0.5
to 25 mm). The backfill materials selected should be angular to subangular and shall
be durable. The coarse sand and gravel portions of the backfill material should have
a Los Angeles Wear (LA Wear) percent loss after 500 revolutions (AASHTO T96) of
no more than 35 percent. Additional installation damage tests may be conducted with
a less durable backfill material, at the discretion of the manufacturer and the approval
authority. If tests are conducted using a backfill material that does not meet the LA
Wear requirement stated above, the condition of the backfill shall be evaluated for
changes in angularity and gradation after each use. If changes in these two parameters
are observed, the aggregate shall be immediately replaced with fresh material. This
gradation/angularity evaluation should be conducted periodically even for more
durable backfill material. Note that if the backfill materials available in the region for
which the approval authority has jurisdiction consistently cannot meet the maximum
LA Wear requirement of 35 percent loss, a less durable aggregate may be used for all
the backfill materials tested, at the discretion of the approval authority.
11. Values of RFID may be estimated for a specified soil gradation using interpolation
as illustrated in Figure A-1. The d50 size of the soil has commonly been used for
interpolating between soil backfills for determination of RFID. Other combinations
of soil particle size and factors that account for soil angularity and durability may
be considered for this correlation and interpolation procedure per mutual agreement
between the geosynthetic manufacturer and the approval authority. The range of
backfill gradations, angularity, and durability will affect the range of applicability of
the RFID values obtained from the testing. RFID values should not be extrapolated
beyond the coarsest backfill soil tested.
1.6
1.4
Figure A-1. Interpolation of RFID for a soil with d50 = 2 mm from installation damage
data obtained for soils with d50 = 0.02, 0.5 and 10 mm (Note: 1in. = 0.0254 mm).
12. Not all products within a product line need to be tested for installation damage. As a
minimum, the weakest (lightest) and strongest (heaviest) products within the product
line, plus at least one additional intermediate strength (weight) product should be
used to characterize RFID for the product line (note: if the strongest product within the
product line is not tested, all heavier products will be assumed to have the same value
of RFID as the heaviest product tested). An example of this interpolation procedure
is provided in Figure 2. For coated polyester geogrids, the coating thickness or
coating mass per unit area relative to the mass per unit area of the product should be
considered for the purpose of correlating RFID between products rather than product
unit weight or tensile strength alone. It is acceptable to obtain the coating mass/unit
area through the use of manufacturer Quality Control (QC) data on the lot specific
mass/unit area of the uncoated material (i.e., the weight of the “greige-good”),
subtracting that mass/unit area from the total mass/unit area of the finished product.
Therefore, the total mass per unit area of the sample used in the installation damage
testing should be obtained in accordance with ASTM D5261.
1.8
1.6
Note 1: Creep results in time dependent deformation that may continue to occur as long as
the reinforcement is loaded. At low to intermediate load levels, depending on the polymer
type, the creep rate will continue to decrease with time and may eventually stabilize, at
least within the ability to measure creep. At higher load levels, creep will continue until
rupture occurs.
In general, two types of creep tests are conducted: stress or creep rupture, and creep strain.
Creep strains do not have to be monitored in creep rupture testing (strain measurement
in this type of test is recommended, however), though creep strain tests can be carried
to rupture. Rupture data is necessary if the creep reduction factor for ultimate limit state
conditions, RFCR, is to be determined. Creep rupture test results, if properly accelerated
and extrapolated, can also be used to investigate the effects of stress cracking and the
potential for a ductile to brittle transition to occur. This transition to brittle behavior, if it
occurs, can cause a geosynthetic to fail in creep at lower loads and strains than anticipated
from evaluating only creep strain and rate data.
B.1 Overview of Extrapolation Approach to Determine the Ultimate Limit State Creep
Limit, T1
Considering that typical design lives for permanent MSE structures are 75 years or more,
extrapolation of creep data will be required. Current practice allows creep data to be
extrapolated up to one log cycle of time beyond the available data without some form of
accelerated creep testing, or possibly other corroborating evidence (Jewell and Greenwood,
1988; Koerner, 1990). Based on this, unless one is prepared to obtain 7 to 10 years of creep
data, temperature accelerated creep data, or possibly other corroborating evidence, must be
obtained.
It is well known that temperature accelerates many chemical and physical processes
in a predictable manner. In the case of creep, this means that the creep strains under a
given applied load at a relatively high temperature and relatively short times will be
approximately the same as the creep strains observed under the same applied load at a
relatively low temperature and relatively long times. Temperature affects time to rupture
at a given load in a similar manner. This means that the time to a given creep strain or to
rupture measured at an elevated temperature can be made equivalent to the time expected to
reach a given creep strain or to rupture at in-situ temperature through the use of a time shift
factor.
The ability to accelerate creep with temperature for polyolefins such as polypropylene
(PP) or high density polyethylene (HDPE) has been relatively well defined (Takaku, 1981;
Bush, 1990; Popelar, et. al., 1991). Also for polyolefins, there is some risk that a “knee” in
the stress rupture envelope due to a ductile to brittle transition could occur at some time
beyond the available data (Popelar, et. al., 1991). Therefore, temperature accelerated creep
data is strongly recommended for polyolefins. However, in practice, a ductile to brittle
transition for polyolefin geosynthetic reinforcement products has so far not been observed,
likely due to the highly oriented nature of polymer resulting from the processing necessary
to make fibers and ribs. In general, the degree of orientation of the polymer is an important
factor regarding the potential for ductile to brittle transitions.
For polyester (PET) geosynthetics, available evidence indicates that temperature can also
be used to accelerate PET creep, based on data provided by den Hoedt, et. al., 1994 and
others. However, the creep rupture envelopes for PET geosynthetics tend to be flatter than
polyolefin creep rupture envelopes, and accurate determination of time-shift factors can
be difficult for PET geosynthetics because of this. This may require greater accuracy in
the PET stress rupture data than would be required for polyolefin geosynthetics to perform
accurate extrapolations using elevated temperature data. This should be considered if using
elevated temperature data to extrapolate PET stress rupture data. Note that a “knee” in the
stress rupture envelope of PET does not appear to be likely based on the available data and
the molecular structure of polyester.
If elevated temperature is used to obtain accelerated creep data, it is recommended that
minimum increments of 10° C be used to select temperatures for elevated temperature
creep testing. The highest temperature tested, however, should be below any transitions for
the polymer in question. If one uses test temperatures below 70 to 75° C for polypropylene
(PP), high density polyethylene (HDPE), and PET geosynthetics, significant polymer
transitions will be avoided. If higher temperatures must be used, the effect of any
transitions on the creep behavior should be carefully evaluated. One should also keep in
mind that at these high temperatures, significant chemical interactions with the surrounding
environment are possible, necessitating that somewhat lower temperatures or appropriate
environmental controls be used. These chemical interactions are likely to cause the creep
test results to be conservative. Therefore, from the user’s point of view, potential for
chemical interactions is not detrimental to the validity of the data for predicting creep
limits. However, exposure to temperatures near the upper end of these ranges could affect
the stress-strain behavior of the material due to loss of molecular orientation, or possibly
other effects that are not the result of chemical degradation. Therefore, care needs to be
exercised when interpreting results from tests performed at temperatures near the maximum
test temperatures indicated above. In general, if the stiffness of the material after exposure
to the environment is significantly different from that of the virgin material, the stress-
strain properties, and possibly the strength, of the material may have been affected by the
exposure temperature in addition to the chemical environment. If the stiffness has been
affected, the cause of the stiffness change should be thoroughly investigated to determine
whether or not the change in stiffness is partially or fully due to the effect of temperature,
or alternatively not use the data obtained at and above the temperature where the stiffness
was affected.
Unless otherwise specified or required by site specific temperature data, an effective design
temperature of 20o C (Tamb) should be assumed.
A number of extrapolation and creep modeling methods have been reported in the literature
(Findley, et. al., 1976; Wilding and Ward, 1978; Wilding and Ward, 1981; Takaku, 1981;
McGown, et. al., 1984; Andrawes, et. al., 1986; Murray and McGown, 1988; Bush, 1990;
Popelar, et. al., 1991; Helwany and Wu, 1992). Many of the methods discussed in the
literature are quite involved and mathematically complex.
Two creep extrapolation techniques are provided herein for creep rupture evaluation: the
conventional method, which utilizes a simplified visual/graphical approach, temperature
acceleration of creep, regression techniques, and statistical extrapolation, and the Stepped
Isothermal Method (SIM). This does not mean that the more complex mathematical
modeling techniques cannot be used to extrapolate creep of geosynthetics; they are simply
not explained herein. These two techniques are described in more detail as follows:
B.2 Step-By-Step Procedures for Extrapolating Creep Rupture Data – Conventional
Method
Step 1: Plot the creep rupture data as log time to rupture versus log load level, as shown
in Figure B.2-1. Do this for each temperature in which creep rupture data is available. For
some materials, a semi-log rather than a log-log plot could be used. The plotting method
that provides the best and most consistent fit of the data should be used. In general,
approximately 12 to 18 data points (i.e., combined from all temperature levels tested
to produce the envelope for a given product, with a minimum of 4 data points at each
temperature) are required to establish a rupture envelope (Jewell and Greenwood, 1988;
ASTM D2837). The data points should be evenly distributed through each log cycle of
time. Rupture points with a time to rupture of less than 5 hours should in general not be
used, unless it can be shown that these shorter duration points are consistent with the rest
of the envelope (i.e., they do not contribute to non-linearity of the envelope). As a guide,
three of the test results should have rupture times (not shifted by temperature acceleration)
of 10 to 100 hours, four of the test results should have rupture times between 100 and 1,000
hours, and four of the test results should have rupture times of 1,000 to 10,000 hours, with
at least one additional test result having a rupture time of approximately 10,000 hours (1.14
years) or more. It is recommended that creep strain be measured as well as time to rupture,
since the creep strain data may assist with conventional time-temperature shifting and in
identifying any change in behavior that could invalidate extrapolation of the results.
Step 2: Extrapolate the creep rupture data. Elevated temperature creep rupture data can
be used to extrapolate the rupture envelope at the design temperature through the use of a
time shift factor, aT. If the rupture envelope is approximately linear as illustrated in Figure
B.2-1(a), the single time shift factor aT should be adequate to perform the time-temperature
superposition.
Note 2: This time-temperature superposition procedure assumes that the creep-rupture
curves at all temperatures are linear on a semi-logarithmic or double logarithmic scale
and parallel. It has been found empirically that the curves for PET are semi-logarithmic
and approximately parallel, or double logarithmic and approximately parallel in the
case of HDPE and PP. It should be pointed out that the theory of Zhurkov (1965), which
assumes that the fracture process is activated thermally with the additional effect of applied
stress, predicts that the creep-rupture characteristics should be straight when plotted on a
double logarithmic diagram, and that their gradients should be stress-dependent.
Use of a single time shift factor to shift all the creep rupture data at a given temperature,
termed “block shifting,” assumes that the shift factor aT is not highly stress level dependent
and that the envelopes at all temperatures are parallel, allowing an average value of aT
to be used for all of the rupture points at a given temperature. While research reported in
the literature indicates that aT may be somewhat stress level dependent and that the curves
at all temperatures are not completely parallel, this assumption tends to result in a more
conservative assessment of the creep reduction factor RFCR (Thornton and Baker, 2002).
t = 1 hr
100 1,000 10 hrs
10,000 hrs 100 hrs
P6
10 P5 1,000 hrs
1 P4
P5
Strain, H
10,000 hrs
Load, P
P3
P2
P1
100
T1
T1 < T2 < T3
80 T2
aT2
T3 aT3
Load Level, P (%)
60
Pd
40
20
tmax
td
0
1 10 100 1,000 10,000 100,000 1,000,000
Time to Rupture, t (hrs)
Figure B.2-2. Extrapolation of Stress Rupture Data and the Determination of the Creep
Limit Load.
The time to rupture for the elevated temperature rupture data is shifted in accordance with
the following equation:
tamb = (telev)(aT) (B.2-1)
where, tamb is the predicted time at the ambient or temperature to reach rupture under the
specified load, telev is the measured time at elevated temperature to reach a rupture under
the specified load, and aT is the time shift factor. aT can be approximately estimated using a
visual/graphical approach as illustrated in figures B.2-1 and B.2-2. The preferred approach,
however, is to use a computer spreadsheet optimization program to select the best shift
factors for each constant temperature block of data to produce the highest R2 value for the
combined creep rupture envelope to produce the result in Figure B.2-2.
Note 3: Incomplete tests may be included, with the test duration replacing the time to
rupture, but should be listed as such in the reported results, provided that the test duration,
after time shifting, is 10,000 hours or more. The rule for incomplete tests is as follows.
The regression should be performed with and without the incomplete tests included. If the
incomplete test results in an increase in the creep limit, keep the incomplete tests in the
regression, but if not, do not include them in the regression, in both cases for incomplete
tests that are 10,000 hours in duration after time shifting or more. Record the duration of
the longest test which has ended in rupture, or the duration of the longest incomplete test
whose duration exceeds its predicted time to failure: this duration is denoted as tmax.
It is preferred that creep rupture data be extrapolated statistically beyond the elevated
temperature time shifted data using regression analysis (i.e., curve fitting) up to a maximum
of one log cycle of time for all geosynthetic polymers (greater extrapolation using only
statistical methods is feasible, but uncertainty in the result increases substantially and must
be taken into account). Therefore, adequate elevated temperature data should be obtained to
limit the amount of statistical extrapolation required.
Note 4: There may be situations where extrapolation to create a creep rupture envelope
at a lower temperature than was tested is necessary. Situations where this may occur
include the need to elevate the ambient temperature to have greater control regarding the
temperature variations during the creep testing (i.e., ambient laboratory temperature may
vary too much), or for sites where the effective design temperature is significantly lower
than the “standard” reference temperature used for creep testing (e.g., northern or high
elevation climates). In such cases, it is feasible to use lower bound shift factors based
on previous creep testing experience to allow the creep rupture envelope to be shifted to
the lower temperature, as shift factors for the materials typically used for geosynthetic
reinforcement are reasonably consistent. Based on previous creep testing experience
and data reported in the literature (Chow and Van Laeken 1991; Thornton, et al. 1998;
Thornton, et al. 1998a; Lothspeich and Thornton 2000; Takemura 1959; Bush, 1990;
Popelar, et al. 1990; Wrigley, et al. 2000; Takaku 1980; Thornton and Baker 2000), shift
factors for HDPE and PP geosynthetics are typically in the range of 0.05 to 0.18 decades
(i.e., log cycles of time) per 1o C increase in temperature (i.e., a 10o C increase would
result in a time shift factor of 12 to 15) and 0.05 to 0.12 decades per 1o C increase in
temperature for PET geosynthetics. It is recommended that if shifting the creep rupture
envelope to temperatures below the available data is necessary, that a shift factor of 0.05
decades per 1o C increase in temperature for PP, HDPE, and PET be used. This default
shift factor should not be used to shift the creep rupture data more than 10o C.
Step 3: Once the creep data has been extrapolated, determine the design, lot specific,
creep limit load by taking the load level at the desired design life directly from the
extrapolated stress rupture envelope as shown in Figure B.2-2. If statistical extrapolation
beyond the time shifted stress rupture envelopes (PP or HDPE), or beyond the actual data
if temperature accelerated creep data is not available, is necessary to reach the specified
design life, the calculated creep load Tl should be reduced by an extrapolation uncertainty
factor as follows:
Tl = Pcl/(1.2)x-1 (B.2-3)
where Pcl is the creep limit load taken directly from the extrapolated stress rupture
envelope, and “x” is the number of log cycles of time the rupture envelope must be
extrapolated beyond the actual or time shifted data, and is equal to log td – log tmax as
illustrated in Figure B.2-2. The factor (1.2)x-1 is the extrapolation uncertainty factor. If
extrapolating beyond the actual or time shifted data less than one log cycle, set “x-1” equal
to “0”. This extrapolation uncertainty factor only applies to statistical extrapolation beyond
the actual or time shifted data using regression analysis and assumes that a “knee” in the
rupture envelope beyond the actual or time shifted data does not occur.
Note 5: A condition on the extrapolation is that there is no evidence or reason to believe
that the rupture behavior will change over the desired design life. It should be checked that
at long durations, and at elevated temperatures if used:
• There is no apparent change in the gradient of the creep-rupture curve
• There is no evidence of disproportionately lower strains to failure
• There is no significant change in the appearance of the fracture surface.
Any evidence of such changes, particularly in accelerated tests, should lead to the
exclusion of any reading where either the gradient, strain at failure or appearance of the
failure is different to those in the test with the longest failure duration. Particular attention
is drawn to the behavior of unoriented thermoplastics under sustained load, where a
transition in behavior is observed in long-term creep-rupture testing (i.e., the so called
“ductile to brittle transition – Popelar, et al., 1991). The effect of this transition is that
the gradient of the creep-rupture curve becomes steeper at the so-called “knee” such that
long-term failures occur at much shorter lifetimes than would otherwise be predicted. The
strain at failure is greatly reduced and the appearance of the fracture surface changes
from ductile to semi-brittle. If this is observed, any extrapolation should assume that the
“knee” will occur. For the method of extrapolation reference should be made to ISO/FDIS
9080:2001, ASTM D2837, and Popelar, et al. (1991).
This extrapolation uncertainty factor also assumes that the data quality is good, data scatter
is reasonable, and that approximately 12 to 18 data points which are well distributed
(see Step 1 for a definition of well distributed) defines the stress rupture envelope for the
product. If these assumptions are not true for the data in question, this uncertainty factor
should be increased. The uncertainty factor may also need to be adjusted if a method other
than the one presented in detail herein is used for extrapolation. This will depend on how
well that method compares to the method provided in this appendix. This extrapolation
uncertainty factor should be increased to as much as (1.4)x if there is the potential for a
“knee” in the stress rupture envelope to occur beyond the actual or time shifted data, or
if the data quality, scatter, or amount is inadequate. Furthermore, if the data quantity or
distribution over the time scale is inadequate, it may be necessary to begin applying the
extrapolation uncertainty factor before the end of the time shifted data.
Note 6: Based on experience, the R2 value for the composite (i.e., time shifted) creep
rupture envelope should be approximately 0.8 to 0.9 or higher to be confident that Equation
B.2-3 will adequately address the extrapolation uncertainty. If the R2 value is less than
approximately 0.6 to 0.7, extrapolation uncertainty is likely to be unacceptably high, and
additional testing and investigation should be performed. In general, such low R2 values
are typically the result of data that is too bunched up, unusually high specimen to specimen
variability, or possibly poor testing technique.
B.3 Procedures for Extrapolating Creep Rupture Data – Stepped Isothermal Method (SIM)
An alternative creep strain/rupture analysis and extrapolation approach that has recently
become available for geosynthetics is the Stepped Isothermal Method (SIM) proposed,
illustrated, and investigated by Thornton, et. al. (1997), Thornton, et. al. (1998), Thornton,
et. al. (1998), and Thornton and Baker (2002). SIM has been applied successfully to PET
geogrids and PP geotextiles. SIM utilizes an approach similar to the Williams-Landell-
Ferry, or WLF, approach to creep extrapolation (Ferry, 1980), where master creep curves
for a given material are produced from a series of short-term tests (i.e., creep test durations
on the order of a few hours) on the same specimen over a wide range of temperatures (i.e.,
while the load on the specimen is held constant, the temperature is increased in steps). The
sections of creep curve at the individual temperatures are shifted in time and combined to
form a continuous prediction of the creep strain at the starting temperature.
Though the general principles of this method have been in use for many years in the
polymer industry (Ferry, 1980), it has been only recently that this approach has been used
for geosynthetics. Though this approach was initially developed to extrapolate creep strain
data, it has been adapted to produce stress rupture data by taking the specimen to rupture
once the highest test temperature is reached. In effect, through time shifting of the creep
strain data obtained prior to rupture, the rupture point obtained has an equivalent shifted
time that is several orders of magnitude greater than the actual test time, which could be on
the order of only a few days.
The method is conducted in accordance with ASTM D 6992. Key issues are the very
short test time used for this method, potential use of temperatures that are well above
transitions in the geosynthetic material, and its complexity. Key technical advantages of
the method, however, include more accurate determination of time shift factors, since the
same specimen is used at the same load level at all of the temperatures (the “conventional”
method must deal with the effect of specimen to specimen variability when determining the
shift factors), and that time shift factors between temperatures are determined at the same
load level, eliminating the effect of load level in the determination of the shift factors (in
the “conventional” method, the shift factors used are in fact an average value for a wide
range of loads).
SIM can be considered for use in generating and extrapolating geosynthetic creep and creep
rupture data provided this method is shown to produce results which are consistent with
the “conventional” extrapolation techniques recommended in this appendix. To this end,
creep-rupture testing shall be conducted using conventional tests (ASTM D5262) and SIM
tests (ASTM D6992). At least six SIM rupture tests and six conventional rupture tests and
shall be conducted one of the products in the product line being evaluated. Of the six SIM
rupture tests, four shall have rupture times (shifted as appropriate) between 100 and 2000
hours and two shall have rupture times greater than 2000 hours. All of the conventional
creep rupture points shall be obtained at the reference temperature (i.e., not temperature
shifted). Creep rupture plots shall be constructed, regression lines computed and the log
times to rupture determined at a load level that corresponds to 1,000 hours and 50,000
hours on the conventional creep rupture envelope, for the two data sets. The log time to
rupture for the SIM regression at this load level shall be within the upper and lower 90%
confidence limits of the mean conventional regressed rupture time at the same load level
using Student’s t test.
The confidence limit for the regression performed for the conventional creep rupture data is
given by (Wadsworth, 1998):
¦ (P − P )
i 2 (B.3-2)
i
σ=
n−2
where:
log tL = lower and upper bound confidence limit. The + or – term in Equation
B.2-1 results in the lower and upper bound confidence limits, respectively.
treg = time corresponding to the load level from the conventional creep rupture
envelope at which the comparison between the two envelopes will be
made (e.g., at 1,000 and 50,000 hrs after time shifting)
tα,n-2 = value of the t distribution determined from applicable Student t table
(or from the Microsoft EXCEL function TINV(α,n-2)) at α = 0.10
and n-2 degrees of freedom (this corresponds to the 90% two-sided
prediction limit).
n = the number of rupture or allowable run-out points in the original test
sample (i.e., the conventional creep rupture data)
P = load level obtained at treg from the regression line developed from the
conventional creep rupture testing
P = the mean rupture load level for the original test sample (i.e., all rupture or
run-out points used in the regression to establish the conventional creep
rupture envelope)
Pi = the rupture load level of the i’th point for the rupture points used in the
regression for establishing the conventional creep rupture envelope
log t = the mean of the log of rupture time for the original test sample (i.e.,
all rupture or run-out points used in the regression to establish the
conventional creep rupture envelope)
ti = the rupture time of the i’th point for the rupture points used in the
regression for establishing the conventional creep rupture envelope
Once log tL, both upper and lower bound, has been determined at the specified load level,
compare these values to the log rupture time (i.e., log tSIM) obtained for the SIM creep
rupture envelope test at the specified load level (e.g., 1,000 and 50,000 hours). The value
of log tSIM at the two specified load levels must be between the upper and lower bound
confidence limits (log tL). If this requirement is not met, perform two additional SIM tests
at each load level P for the specified treg where this comparison was made and develop
a new SIM creep rupture envelope using all of the SIM data. If for the revised SIM
regression envelope resulting from these additional tests this criterion is still not met,
perform adequate additional conventional creep rupture testing to establish the complete
rupture envelope for the product in accordance with this appendix).
If the criterion provided above is met, the SIM testing shall be considered to be consistent
with the conventional data, and SIM may be used in combination with the conventional
data to meet the requirements of Section B.2 regarding the number of rupture points and
their distribution in time and maximum duration. Therefore, the combined data can be used
to create the creep rupture envelope as shown in Figure B.2-2. In that figure, the SIM data
shall be considered to already be time shifted. Equation B.2-3 is then used to determine Tl.
B.4 Determination of RFCR
The creep reduction factor, RFCR , is determined by comparing the long-term creep
strength, Tl , to the ultimate tensile strength (ASTM D4595 or ASTM D6637) of the sample
tested for creep (Tlot). The sample tested for ultimate tensile strength should be taken from
the same lot, and preferably the same roll, of material that is used for the creep testing. For
ultimate limit state design, the strength reduction factor to prevent long-term creep rupture
is determined as follows:
P95
Tal (B.4-1)
RFID u RFD
where, Tlot is the average lot specific ultimate tensile strength (ASTM D4595 or ASTM
D6637) for the lot of material used for the creep testing. Note that this creep reduction
factor takes extrapolation uncertainty into account, but does not take into account
variability in the strength of the material. Material strength variability is taken into account
when RFCR, along with RFID and RFD, are applied to Tult to determine the long-term
allowable tensile strength, as Tult is a minimum average roll value. The minimum average
roll value is essentially the value that is two standard deviations below the average value.
B.5 Use of Creep Data from “Similar” Products and Evaluation of Product Lines
Long-term creep data obtained from tests performed on older product lines, or other
products within the same product line, may be applied to new product lines, or a similar
product within the same product line, if one or both of the following conditions are met:
• The chemical and physical characteristics of tested products and proposed products are
shown to be similar. Research data, though not necessarily developed by the product
manufacturer, should be provided which shows that the minor differences between the
tested and the untested products will result in equal or greater creep resistance for the
untested products.
• A limited testing program is conducted on the new or similar product in question and
compared with the results of the previously conducted full testing program.
For polyolefins, similarity could be judged based on molecular weight and structure of the
main polymer (i.e., is the polymer branched or crosslinked, is it a homopolymer or a blend,
percent crystallinity, etc.), percentage of material reprocessed, tenacity of the fibers and
processing history, and polymer additives used (i.e., type and quantity of antioxidants or
other additives used). For polyesters and polyamides, similarity could be judged based on
molecular weight or intrinsic viscosity of the main polymer, carboxyl end group content,
percent crystallinity, or other molecular structure variables, tenacity of the fibers and
processing history, percentage of material reprocessed or recycled, and polymer additives
used (e.g., pigments, etc.). The untested products should also have a similar macrostructure
(i.e., woven, nonwoven, extruded grid, needlepunched, yarn structure, etc.) and fiber
dimensions (e.g., thickness) relative to the tested products. It should be noted that percent
crystallinity is not a controlled property and there is presently no indication of what an
acceptable value for percent crystallinity should be.
For creep evaluation of a similar product not part of the original product line, this limited
testing program should include creep tests taken to at least 1,000 to 2,000 hours in length
before time shifting if using the “conventional” creep testing approach, with adequate
elevated temperature data to permit extrapolation to 50,000 hours or more. If it has been
verified that SIM can be used, in accordance with Section B.3, durations after time shifting
due to elevated temperature up to a minimum of 50,000 hours are required. A minimum
of 4 data points per temperature level tested should be obtained to determine time shift
factors and to establish the envelope for the similar product. These limited creep test
results must show that the performance of the similar product is equal to or better than the
performance of the product previously tested. This comparison must demonstrate that there
is no statistical difference between the old product regression line and the regression line
obtained for the similar product at a time of 2,000 hours (not temperature accelerated) and
50,000 hours (after time shifting) using a student-t distribution at a confidence level of 0.10
(see Equation B.3-1). If no statistical difference is observed, the results from the full testing
program on the older or similar product could be used for the new/similar product. If this
is not the case, then a full testing and evaluation program for the similar product should be
conducted.
Similarly, for extension of the creep data obtained on one product in the product line
(i.e., the primary product tested, which is typically a product in the middle of the range of
products in the product line) to the entire product line as defined herein, a limited creep
testing program must be conducted on at least two additional products in the product line.
The combination of the three or more products must span the full range of the product line
in terms of weight and/or strength. The limited test program described in the preceding
paragraph should be applied to each additional product in the product line. The loads
obtained for the data in each envelope should then be normalized by the lot specific
ultimate tensile strength, Tlot. All three envelopes should plot on top of one another, once
normalized in this manner, and the two additional product envelopes should be located
within the confidence limits for the product with the more fully developed creep rupture
envelope (i.e., the “primary” product) as described above for “similar” products. If this
is the case, then the creep reduction factor for the product line shall be the lesser of the
reduction factor obtained for the product with the fully developed rupture envelope and
the envelope of all three products combined, and normalization using the ultimate tensile
strength shall be considered acceptably accurate.
If this is not the case, then the creep rupture envelopes for the other two products, plus
enough other products within the product line, to establish the trend in RFCR as a function
of product weight or ultimate tensile strength, so that the RFCR for the other products within
the product line can be accurately interpolated. Furthermore, Tal must be determined in
accordance with Note 7.
Note 7: Note that normalization using the ultimate lot specific tensile strength may not be
completely accurate for some geosynthetic products regarding characterization of creep
rupture behavior, and other normalization techniques may be needed (Wrigley, et al.,
1999). In such cases, individual creep reduction factors for each product in the product
line may need to be established through fully developed creep rupture envelopes for
representative products obtained at the low, middle, and high strength end of the product
series. Once the creep limited strength, Pcl and the creep reduction factors are established
for each product, in this case, product variability must still be taken into account. In
such cases, Tal must be the lesser of the determination from Equation 1 and the following
determination:
P95
Tal
RFID u RFD
where,
P95 = the tensile strength determined from the 95% lower bound prediction limit
for the creep rupture envelope at the specified design life (see Equations 4 and
5 in “Quality Assurance (QA) Criteria for Comparison to Initial Product
Acceptance Test Results”)
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Rupture
PP/HDPE
End of secondary
creep, begin tertiary
PET creep
Arithmetic Time
Figure C.1-1. Conceptual illustration of creep strain behavior, and the determination of the
strain at the beginning of tertiary creep from creep strain data.
The instability limit strain is defined as the strain beyond which the material exhibits signs
of instability, i.e., approaches failure (Andrawes, et. al., 1986). When extrapolating creep
strain data, it is important to not extrapolate the data to strain levels that are in excess of
the instability limit strain, as doing so would produce invalid results. The determination of
this limit strain can be the most difficult part of assessing the creep rupture limit from creep
strain data. The actual rupture strain, which occurs at the end of tertiary creep, for a given
material at a given load level is difficult to measure as well as to identify. A more consistent
and more easily measured instability limit strain would be the strain level where tertiary
creep begins as illustrated in Figure C.1-1. However, if rupture occurs during the primary
or secondary creep stage (e.g., PET) the instability limit strain is the rupture strain.
Another tool that can be useful in determining the strain at the beginning of tertiary creep
is the Sherby-Dorn plot, as illustrated in Figure C.1-2. A Sherby-Dorn plot is a well known
plotting technique used in polymer science (McGown et al. 1984a). Each curve represents a
specific geosynthetic layer in a wall or a specific geosynthetic specimen tested at a specific
load level. Creep strain rates observed under constant load are plotted against the total
strain in the specimen or layer measured at the time the creep strain rate was calculated.
The creep strain rate is simply the slope of the creep strain curve at a given point in time
(see Figure C.1-2a). Curves that are linear or concave downward indicate that only primary
creep is occurring, and that stabilization (no rupture) is likely. Curves that are concave
upward indicate secondary or tertiary creep is occurring, and that rupture is likely. The
closer the curves are located to the bottom left corner of the plot (Figure C.1-2), the better
the creep performance of the material. The closer the curves are to the upper right corner,
the more likely creep rupture will occur.
H2
't2
't1
'H2
'H1
Strain
H1
'H
Creep strain rate =
't
Load level = P2
Arithmetic Time
(a) Determination of creep strain rate.
Strain
H1
0.1
H2
Tertiary creep
0.01 begins
Strain Rate
0.001
Steady state
0.0001 (secondary) creep rate
Outward sweep indicates potential for
secondary creep to develop
0.00001
Downward sweep indicates only primary creep
will occur
Note that some interpretation of the creep curves through curve fitting is required to
determine strain rates, since local jumps in the measured creep strain curves can cause wide
variations in calculated creep strain rates. The jumps in the curves are typically the result of
the short increments of time used in the calculations and the small magnitude of changes in
strain readings that may be at the limit of the resolution of the measuring devices. Hence,
the slope of the measured creep curves must be taken over fairly long increments of time to
be meaningful.
Tertiary creep begins where the creep strain rate (based on an arithmetic time scale)
begins to increase. The strain at the beginning of tertiary creep is located where the creep
strain rate begins to increase after reaching a minimum value, at least for polyolefin
geosynthetics. A minimum and then an increasing creep strain rate is very difficult to see
for polyester geosynthetics on this type of plot. Therefore, Sherby-Dorn plots tend to not be
very useful for polyester geosynthetics.
To determine the long-term instability limit strain, the measured creep strain and time
near creep rupture (i.e., at the beginning of tertiary creep) for various load levels must
be obtained. These strains are plotted versus time to the beginning of tertiary creep (the
rupture phase) on a semi-log plot (i.e., log time), or possibly a log-log plot, to establish
the trend in the data. In general, strains near rupture for times to the rupture phase from 10
hours up to approximately 10,000 hours should be obtained so that the data need only be
extrapolated two log cycles of time or less. A minimum of one data point per log cycle of
time should be obtained to define the trend, but more data points are likely to be needed to
establish the trend.
Typical near rupture strain trends for various geosynthetic polymers are illustrated in Figure
C.1-3. Strain near rupture which increases as time to the rupture phase increases may be
indicative of ductile behavior, whereas strain near rupture which decreases as time to the
rupture phase increases may be indicative of brittle behavior (i.e., localized crack growth).
If ductile behavior is observed, a transition to brittle behavior is possible. If such a shift to
brittle behavior occurred, the strain near rupture increase occurring as time to the rupture
phase increases (ductile behavior) could be lost as behavior becomes more brittle. Until
more is known, it is recommended that strains near rupture which appear to be increasing
as time to the rupture phase increases not be depended upon when assessing the long-term
instability limit strain. Therefore, if the strain near rupture increases as time to the rupture
phase increases, which appears to be typical of polypropylene (PP) geosynthetics (Takaku,
1981; Allen, 1991, Thornton and Baker, 2002), the short-term (i.e., rupture times on the
order of 10 hours) strain near rupture should be used as the instability limit strain. If the
strain near rupture decreases as time to the rupture phase increases, which appears to be
typical of high density polyethylene (HDPE) geosynthetics (Ingold, et. al., 1994; Allen and
Bathurst, 1996) and polyester (PET) geosynthetics (Krumm, 1988; Allen and Bathurst,
1996), extrapolate (up to a maximum of two log cycles) to the strain near rupture at the
specified design life using visual extrapolation, regression analysis, or time-temperature
superposition if elevated temperature data is available, and reduce that strain by a reduction
factor of 1.1 to account for potential uncertainty. This reduction factor could be adjusted
depending on the amount and quality of the strain near rupture data. The determination of
the long-term instability strain limit is conceptually illustrated in Figure C.1-3.
Strain at Beginning
Design life
of Tertiary Creep
HDPE Ht
Instability strain limit = Ht/1.1
PET
Instability strain limit = Ht/1.1
Strain at Beginning
of Tertiary Creep
PP
H0
Instability strain limit = H0
Log Time
Figure C.1-3. Typical Near Rupture Behavior for Various Geosynthetic Polymers in Terms
of Measured Strain.
If inadequate data is available to extrapolate measured strains near rupture to the long-
term strain near rupture and the material type is likely to have strains near rupture which
decrease with increasing time to the rupture phase (e.g., HDPE and PET), an acceptable
alternative to estimate the instability limit strain is to take the peak strain measured from
a wide width load-strain test (ASTM D4595 or ASTM D6637) and reduce it by a factor of
2.0.
Another tool that is useful for characterizing and working with creep strain data is the
isochronous curve. Each isochronous (i.e., constant time) curve is created by taking
load and strain levels from each creep curve at a given constant time and plotting them
to form an isochronous curve. Some curve fitting may be necessary to account for
specimen variability and to create a reasonably smooth curve. For HDPE, this curve
fitting is reasonably straight-forward to do. However, for PET, the isochronous curves
characteristically have an “s” shape at low strains resulting from load and strain dependent
changes in the crystalline and between crystal arrangement of molecules within the
polymer (Jewell and Greenwood, 1988; den Hoedt, et al, 1994). PP geosynthetics may also
have inherent abrupt non-linearities in their isochronous curves at certain strain or load
levels as observed by McGown, et al. (1984). Such changes in the curves resulting from
physical processes in the polymer must be considered when constructing isochronous from
creep strain data. Note that isochronous curves are not an extrapolation tool, but instead
t = 1 hr
100 1,000 10 hrs
10,000 hrs 100 hrs
P6
10 P5 1,000 hrs
1 P4
P5
Strain, H
10,000 hrs
Load, P
P3
P2
P1
t = 1 hr 10 hrs
100 hrs
Stiffness, J
Load, P
Entire curve determined
1,000 hrs
at H1 (load level varies)
10,000 hrs
P1 J1 = P1/H J1 = P1/H
H1
t = 1,000 hrs
H Strain, H Time, t (log scale)
(a) Creep stiffness determined at constant strain level.
t = 1 hr
10 hrs
100 hrs
Entire curve
Stiffness, J
Load, P
P1 J1 = P1/H
P1
t = 1,000 hrs
J1 = P1/H Strain, H Time, t (log scale)
(PP), high density polyethylene (HDPE), and PET geosynthetics, significant polymer
transitions will be avoided. One should also keep in mind that at these high temperatures,
significant chemical interactions with the surrounding environment are possible,
necessitating that somewhat lower temperatures or appropriate environmental controls
be used. These chemical interactions are likely to cause the creep test results to be
conservative. Therefore, from the user’s point of view, potential for chemical interactions
is not detrimental to the validity of the data for predicting creep limits. However, exposure
to temperatures near the upper end of these ranges could affect the stress-strain behavior
of the material due to loss of molecular orientation, or possibly other effects that are not
the result of chemical degradation. Therefore, care needs to be exercised when interpreting
results from tests performed at temperatures near the maximum test temperatures indicated
above. In general, if the stiffness of the material after exposure to the environment is
significantly different from that of the virgin material, the stress-strain properties, and
possibly the strength, of the material may have been affected by the exposure temperature
in addition to the chemical environment. If the stiffness has been affected, the cause of the
stiffness change should be thoroughly investigated to determine whether or not the change
in stiffness is partially or fully due to the effect of temperature, or alternatively not use the
data obtained at and above the temperature where the stiffness was affected.
A number of extrapolation and creep modeling methods have been reported in the literature
(Findley, et. al., 1976; Wilding and Ward, 1978; Wilding and Ward, 1981; Takaku, 1981;
McGown, et. al., 1984a; Andrawes, et. al., 1986; Murray and McGown, 1988; Bush, 1990;
Popelar, et. al., 1991; Helwany and Wu, 1992). Many of the methods discussed in the
literature are quite involved and mathematically complex.
Two creep extrapolation techniques are provided herein for creep rupture evaluation: the
conventional method, which utilizes a simplified visual/graphical approach, temperature
acceleration of creep, regression techniques, and statistical extrapolation, and the Stepped
Isothermal Method (SIM). This does not mean that the more complex mathematical
modeling techniques cannot be used to extrapolate creep of geosynthetics; they are simply
not explained herein.
The two techniques identified above are described in more detail in Appendix B, and as
follows:
C.2.1 Step-By-Step Procedures for Extrapolating Creep Strain Data – Conventional
Method
Step 1: Plot the creep data. Plot the data as a semilog plot (log of time) or as an arithmetic
plot (time). Do this separately for each temperature if data at elevated temperatures is
available. For examples, see Figure C.1-1.
Step 2: Determine the instability limit strain (see Section C.1).
Step 3: Construct isochronous curves, as shown in Figure C.1-4.
Step 4: Develop creep stiffness curves for each temperature in which creep data is
available, all at the same load level or strain level (see Figure C.1-5). Develop these
stiffness curves at a strain level near the instability strain limit, or at a load level that
results in a strain near the end of the specified design life that is approximately equal to
the instability strain limit. These creep stiffness curves can then be used to perform time-
temperature superposition for the purpose of creep extrapolation. Note that more accurate
time-temperature shift factors are likely to be obtained if the creep stiffness curves are
produced at a constant load level (Figure C.1-5b) rather than constant strain level (Figure
C.1-5a), as doing so avoids the additional uncertainty caused by the stress level dependence
of the shift factors. In fact, using constant load level creep stiffness curves to determine
shift factors should produce nearly identical results to the Stepped Isothermal Method
(SIM), except that specimen to specimen variability will still be present (SIM eliminates
the specimen to specimen variability when determining shift factors, since only one
specimen is used – See Appendix B for more information on SIM).
Step 5: Extrapolate the creep data. For all geosynthetics, creep strain or stiffness data can
be extrapolated statistically using regression analysis (i.e., curve fitting), or creep data can
be accelerated by temperature to allow extrapolation using time-temperature superposition
principles. It is well known that temperature accelerates many chemical and physical
processes in a predictable manner. In the case of creep, this means that the creep strains
under a given applied load at a relatively high temperature and relatively short times will
be approximately the same as the creep strains observed under the same applied load at a
relatively low temperature and relatively long times. This means that the time to a given
creep strain or stiffness measured at an elevated temperature can be made equivalent to the
time expected to reach a given creep strain or stiffness at in-situ temperature through the
use of a time shift factor. Therefore, elevated temperature creep strain or stiffness data is
made into equivalent in-situ temperature data as follows:
tamb = (telev)(aT) (C.2.1-1)
where, tamb is the predicted time at in-situ temperature to reach a specified creep stiffness or
strain under the specified load, telev is the measured time at elevated temperature to reach a
specified creep stiffness or strain under the specified load, and aT is the time shift factor. For
example, this means that if the time to reach a creep stiffness Jcl at elevated temperature is
10,000 hours, the creep stiffness will also be Jcl at in-situ temperature at a time of (10,000)
(aT) hours. In this way, the creep stiffness curve at in-situ temperature can be extrapolated
to longer times.
The magnitude of the time shift factor can be determined graphically as illustrated in
Figure C.2.1-1, or regression analysis of the composite creep stiffness curve can be used
to optimize the shift factors to produce the highest R2 value for all of the time shifted data.
Adjust aT such that the creep stiffness curves at elevated temperature line up with the
creep stiffness curve at the design (in-situ) temperature. Note that the magnitude of the
shift factors for a given product can be different at different stages of creep (i.e., primary,
secondary, or tertiary creep) and different load levels (see Appendix B). This should be
considered when determining shift factors. See Note 4 in Appendix B, Section B.2 for
additional considerations regarding the use of time shift factors.
Step 6: Once the creep data has been extrapolated, determine the design, lot specific, creep
limit load as follows:
Tl = (Jcl)(εi) (C.2.1-2)
where, Jcl is the creep stiffness at the desired design life and temperature, and εi is the
instability limit strain. If statistical extrapolation beyond the time shifted creep stiffness
curves, or beyond the actual data if temperature accelerated creep data is not available, is
necessary to reach the specified design life, the calculated creep load Tl should be reduced
by an extrapolation uncertainty factor as follows:
Tl = (Jcl)(εi)/(1.2)x-1 (C.2.1-3)
where “x” is the number of log cycles of time the creep stiffness data must be extrapolated.
Extrapolations greater than two log cycles of time are not recommended (see Appendix B
for a more detailed explanation). The factor (1.2)x-1 is the extrapolation uncertainty factor.
If extrapolating beyond the actual or time shifted data less than one log cycle, set “x-1”
equal to “0”. This extrapolation uncertainty factor only applies to statistical extrapolation
beyond the actual or time shifted data using regression analysis and assumes that a shift
from ductile to brittle behavior beyond the actual or time shifted data does not occur. This
extrapolation uncertainty factor also assumes that the data quality is good, data scatter
is reasonable, and that a minimum of 5 load levels for each temperature are tested. The
load levels should be well distributed within the load range tested, and at least one to
two load levels should be high enough to produce rupture within the test time at each test
temperature. If these assumptions are not true for the data in question, this uncertainty
factor should be increased. The uncertainty factor may also need to be adjusted if a method
other than the one presented in detail herein is used for extrapolation. This will depend on
how well that method compares to the method provided in this appendix. This extrapolation
uncertainty factor should be increased to as much as (1.4)x if there is the potential for a shift
from ductile to brittle behavior to occur beyond the actual or time shifted data, or if the data
quality, scatter, or amount is inadequate (see Appendix B, Notes 5 and 6). Furthermore,
if the data quality is inadequate, it may be necessary to begin applying the extrapolation
uncertainty factor before the end of the time shifted data.
300
200
100
0
1 10 100 1,000 10,000 100,000 1,000,000
Time, t (hrs)
(a) Creep stiffness curves and determination of shift factors.
500 T1
Creep Stiffness, J (kN/m)
T2
400 Temperat ure:
aT2
T3 T1 < T2 < T3
300 aT3
Section C.1, determine the load Pcl directly from the isochronous curve and calculate the
creep limit load Tl.
C.3 Determination of RFCR
The creep reduction factor, RFCR , is determined by comparing the long-term creep
strength, Tl , to the ultimate tensile strength (ASTM D4595 or ASTM D6637) of the sample
tested for creep. The sample tested for ultimate tensile strength should be taken from the
same lot, and preferably the same roll, of material that is used for the creep testing. For
ultimate limit state design, the strength reduction factor to prevent long-term creep rupture
is determined as follows:
Tlot (C.3-1)
RFCR
T1
where, Tlot is the average lot specific ultimate tensile strength (ASTM D4595 or ASTM
D6637) for the lot of material used for the creep testing. Note that this creep reduction
factor takes extrapolation uncertainty into account, but does not take into account
variability in the strength of the material. Material strength variability is taken into account
when RFCR, along with RFID and RFD, are applied to Tlot to determine the long-term
allowable tensile strength, as Tult is a minimum average roll value. The minimum average
roll value is essentially the value that is two standard deviations below the average value.
C.4 Estimation of Long-Term Creep Deformation
In-isolation creep strain data can be used to estimate post-construction strains and
deformations (see Allen and Bathurst, 2002b). Since load levels in full scale structures as
a percent of the ultimate tensile strength are generally quite low, adequate creep data must
be obtained at low load levels (typically in the range of 2 to 20% of ultimate). The key to
accurate estimation of creep strains in full scale structures is an accurate prediction of the
load level.
Step 1: Estimate the load levels in the reinforcement layer(s). Current design specifications
(AASHTO 2004, 2002) use the Simplified Method to estimate reinforcement loads in walls,
or slope stability analysis techniques (Elias, et al., 2001) to assess reinforcement loads in
reinforced slopes. Loads should be estimated for this purpose without any factor of safety
or load factor applied. Based on the results obtained by Allen and Bathurst (2002a), the
methods provided in current design specifications and guidelines tend to significantly over-
predict reinforcement load levels in geosynthetic structures. A new method (the K-Stiffness
Method) has been developed by Allen et al. (2003) that appears to predict reinforcement
loads in geosynthetic structures much more accurately.
Step 2: From the available creep strain data, create isochronous curves (see Section C.1
and Figure C.1-4).
Step 3: Use the isochronous curves to create a creep strain curve at the desired load level,
by selecting the strains at each time at the selected constant load level.
Step 4: Select the portion of the creep strain curve that is applicable to the post-
construction strains in the full scale structure, accounting for the time required to build the
structure (see Figure C.4-1).
The slack tension, To, applied to the specimen based on the governing tensile test (e.g.,
ASTM D4595 or D6337) will likely be too large for creep stiffness testing due to the very
low loads that are likely for this type of testing. A maximum slack tension of approximately
10 percent of the anticipated load at 2 percent strain or 9 N (2 lbf), whichever is less, is
recommended for single rib or narrow width specimens. For full width specimens (i.e., per
ASTM D5262), a maximum slack tension of approximately 10 percent of the anticipated
load at 2 percent strain or 70 N (15 lbf), whichever is less, is recommended. Since these
maximum slack tension values differ from what is specified in ASTM D4595 and ASTM
D6637, a special set of tensile tests may need to be conducted for use with the low strain
creep stiffness testing program. ASTM D4595 and ASTM D6637 allow both the slack
tension and the slack displacement, do, to be set to zero for calculation purposes. For low
strain creep stiffness testing, the slack displacement should be set to zero, but the slack
tension should be left at its full value for stiffness calculation purposes.
Step 1: Obtain creep strain data for at least one load level low enough to produce a
strain level at the end of structure construction (assume to be 1,000 hrs unless otherwise
specified by the approval authority). Per agreement between the approval authority and the
reinforcement manufacturer, load levels to produce additional 1,000 hour strain levels may
be tested. A minimum of two specimens per product at each load level shall be tested.
To establish the load levels needed to produce the desired 1,000 hour strains for each
product, conduct a series of 1,000 second ramp and hold (R+H) tests. An initial estimate
of the load levels needed for the R+H tests can be obtained from the tensile tests used to
establish Tlot for each product tested. Test a load level that is likely to produce a strain of
approximately 2 percent at 1,000 hours, and then two other load levels to bracket the 2
percent load level (e.g., at load levels that would yield approximately 1 percent strain and 3
to 4 percent strain at 1,000 hours). Do three replicate R+H tests at each of those load levels,
plotting the load level as a function of the estimated strain at 1,000 hours, assuming a log
linear extrapolation is valid for the R+H test results. Perform a regression analysis of that
data to obtain a more accurate estimation of the load level required to produce a strain of
2 percent at 1,000 hours, and run three replicate R+H tests at that load level. If one of the
load levels used for the R + H tests does not produce an estimated strain of 2 percent at
1,000 hours, a fourth set of three replicate R+H tests may be needed, estimating the load
level based on a regression of the R+H tests for the first three load levels. Then conduct
two full 1,000 hour creep tests at the R+H load level that results in the closest estimate to 2
percent strain at 1,000 hours.
Note 1: It is desirable to conduct the full 1,000 hour creep tests at the R+H load levels
tested so that a direct comparison can be made between the 1,000 hour creep tests and the
R+H tests. If the creep observed in the 1,000 hour creep tests is in fact log linear, the R+H
tests can then be used for quality assurance testing in the future.
Step 2: Use the 1,000 hour creep test results, and any other available creep strain data
for the same lot of material, to create isochronous creep curves as shown in Figure C.1-4,
if the 1,000 hour creep stiffness tests do not achieve a strain of 2 percent (or other specified
strain) at 1,000 hours..
Step 3: Create creep stiffness curves at the desired constant strain level (typically
2%) as shown in Figure C.1.5, and extrapolate to the desired time as necessary using
the “conventional” approach illustrated in Figure C.2.1-1 or using SIM, if SIM has been
determined to be applicable. In general, extrapolation should not be necessary if the
“conventional” approach is used. Be sure to extrapolate the creep stiffness curve to the
desired effective design temperature. The “conventional” approach (ASTM D 5262) shall
be used unless comparative testing is conducted that demonstrated SIM (ASTM D6992) is
providing results that are consistent with the "conventional" approach as defined in T 925.
Step 4: Obtain the creep stiffness, JEOC or JDL, at the desired time from the creep stiffness
curve as shown in Figure C.2.1-1.
C.6 Evaluation of Product Lines
Appendix B Section B.5 shall be used as the basis to apply creep strain data to product lines
for determination of RFCR. For creep stiffness assessment, a minimum of three products
in the product line spanning the range of products in the line shall be tested as described
in Section C.5. To interpolate to other products between the products tested, determine
Tlot for each product tested, plotting the creep stiffness values obtained in Section C.5 as a
function of Tlot. Creep stiffness values for other products in the product line not tested can
be interpolated based on their tensile strength.
References
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Art Review”, Proceedings of Geosynthetics ‘91, Atlanta, GA, USA, Vol. 1, pp. 351-379.
Allen, T. M., and Bathurst, R. J., 1996, “Combined Allowable Strength Reduction Factor
for Geosynthetic Creep and Installation Damage”, Geosynthetics International, Vol. 3, No.
3, pp. 407-439.
Allen, T.M., and Bathurst, R.J., 2002a, “Soil Reinforcement Loads in Geosynthetic
Reinforced Walls at Working Stress Conditions”, Geosynthetics International,
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Walls, and Implications for Design”, in press with Geosynthetics International,
Geosynthetics International, Vol. 9, Nos. 5-6, pp. 567-606.
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Working Stress Method for Prediction of Reinforcement Loads in Geosynthetic Walls”,
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of Polyester Geogrids at Elevated Temperatures,” Proceedings of the Fifth International.
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Slopes Reinforced by Polymer Materials”, Geotextiles and Geomembranes, Vol. 7, Nos. 1
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Koerner, R. M., 1990, “Determination of the Long-Term Design Strength of Stiff
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Time Behavior of Tensar Geogrids”, Proceedings of the Symposium on Polymer Grid
Reinforcement in Civil Engineering, Paper No. 1.2, pp. 1-7.
McGown, A., Paine, N., and DuBois, D.D., 1984a, “Use of Geogrid Properties in Limit
Equilibrium Analysis”, Proceedings of the Symposium on Polymer Grid Reinforcement in
Civil Engineering, Paper No. 1.4, pp. 1-5.
Popelar, C.H., Kenner, V.H., and Wooster, J.P., 1991, “An Accelerated Method for
Establishing the Long Term Performance of Polyethylene Gas Pipe Materials”, Polymer
Engineering and Science, Vol. 31, pp. 1693-1700.
Takaku, A., 1981, “Effect of Drawing on Creep Fracture of Polypropylene Fibers”, Journal
of Applied Polymer Science, Vol. 26, pp. 3565-3573.
Thornton, J. S., Allen, S. R., and Thomas, R. W., 1997, “Approaches for the Prediction of
Long Term Viscoelastic Properties of Geosynthetics from Short Term Tests,” Geosynthetics
‘97, IFAI, Long Beach, CA, Vol. 1, pp. 277-291.
Thornton, J. S., Allen, S. R., Thomas, R. W., and Sandri, D., 1998, “The Stepped Isothermal
Method for Time-Temperature Superposition and Its Application to Creep Data of Polyester
Yarns,” Sixth International Conference on Geotextiles, Geomembranes, and Related
Products, Atlanta, GA, pp. 699-706.
Thornton, J. S., Paulson, J., and Sandri, D., 1998, “Conventional and Stepped Isothermal
Methods for Characterizing Long-Term Creep Strength of Polyester Geogrids,” Sixth
International Conference on Geotextiles, Geomembranes, and Related Products, Atlanta,
GA, pp. 691-698.
This appendix provides guidance regarding the performance of long-term product specific
durability testing that may be conducted for product acceptance in lieu of the durability
index testing as described in “Determination of Long-term Geosynthetic Strength for Initial
Product Acceptance” as provided in this protocol. The procedures that follow are required
if it is desired to use a value of RFD less than the default minimum of 1.3, or to determine
RFD for environments that are defined as aggressive.
This appendix has been developed to address polypropylene (PP), polyethylene (PE or
HDPE), and polyester (PET) geosynthetics. While the chemical and biological durability
procedures and criteria provided herein may also be applicable to other polymers (for
example, hydrolysis testing as described herein is likely applicable to polyamide and PVA
geosynthetics), additional investigation will be required to establish a detailed protocol
and acceptance criteria for these other polymers. These other polymers may be considered
for evaluation using this protocol once modifications to the chemical/biological durability
aspects of this protocol have been developed and are agreed upon by the approval authority.
The product specific durability studies for the determination of RFD should be conducted
in, or if necessary extrapolated to, the chemical/biological environment anticipated in the
reinforced backfill. The anticipated temperature of the environment is also a key variable in
assessing the durability of a given product, as temperature can have an exponential effect
on the rate of product property change. For the purposes of these guidelines, the effective
design temperature is defined as the temperature that is halfway between the average yearly
air temperature and the normal daily air temperature for the highest month at the wall
site. Higher design temperatures may need to be considered for structures with southern
exposures. The effective design temperature will be assumed to be 20° C (68° F), if the
design temperature is not specifically identified in the contract specifications. Therefore,
determine RFD at a temperature of 20°C (68° F) as a minimum. Determination of RFD at
higher temperatures is optional.
Standards are currently not available for determining the effect of chemical/biological
activity on long-term geosynthetic reinforcement strength. However, long-term product
specific durability testing can be conducted in a manner that is likely to produce safe
results. Geosynthetic durability can be evaluated using either retrieval and testing of
geosynthetics in actual installations, or through long-term accelerated laboratory testing.
Use of field retrieval data from actual installations requires that the baseline, in terms of
tensile strength before and immediately after installation, and possibly other properties,
be known with certainty, and that the observation period be of sufficient length to permit
extrapolation to the desired design life. The field retrieval approach is in general fraught
with practical and technical difficulties (see Allen and Elias, 1996, Elias, 2000, and Elias,
2001). Furthermore, long periods of time may be needed for polyolefins to establish trends
that can be extrapolated due to the presence of antioxidants, as no loss in strength will be
observed until the antioxidants are used up. Elias (2001) suggests that 30 years of in-
service time may be required to obtain adequate observational data for polyolefins, and
even PET products may require 20 years of in-service observations or more to accomplish
this. Because of the very long observation periods required, long-term laboratory durability
testing is the more practical approach to dealing with the durability issue. An overview of
an appropriate laboratory testing approach for each geosynthetic polymer type is provided.
For polyolefin products in which the fibers/ribs do not exhibit micro-cracks or crazes as
manufactured, long-term chemical durability testing may consist of elevated temperature
oven aging tests to evaluate potential for oxidation effects (FHWA, 1997; Elias, et. al.,
1997; Salman, et. al., 1998; Elias, et al., 1999). A magnification of x2,000 to x3,000 may
be needed to observe whether or not micro-cracks or crazes are present (Salman, et. al.,
1997). If micro-cracks or crazes are present, elevated temperatures may significantly
affect the molecular structure of polyolefins in the vicinity of the micro-cracks/crazes,
making extrapolation of elevated temperature oxidation behavior to the behavior of the
as-manufactured product at ambient temperatures very difficult (Salman, et. al., 1998).
For polyolefins in which the fibers/ribs exhibit micro-cracks or crazes, a means other than
elevated temperature may be needed to accelerate oxidation behavior. Salman, et. al. (1998)
suggest that elevated oxygen concentration and pressure at ambient temperature may prove
to be an effective accelerator in lieu of elevated temperature, especially for geosynthetic
products in which the fibers/ribs exhibit micro-cracks or crazes as manufactured. In
addition, Schröder et al (2002) have performed extensive testing and development of a
protocol utilizing elevated oxygen pressure to address this issue. However, long-term
validation of the protocol and final development of the protocol as a test standard are yet to
be performed.
If oven aging tests are conducted, a forced air oven is strongly recommended to keep the
environment inside the oven as uniform as possible during the entire test duration and to
keep oxidation products from building up inside the oven, considering the long durations
that are likely to be required. Temperature uniformity inside the oven should be maintained
at + 1%. An oven with horizontal air flow is recommended. Specimens should be placed in
the oven parallel to the air flow and spaced no closer together than 13 mm (0.5 in.) apart
(Allen and Elias, 1996; Elias, et al., 1999). The specimens should not be framed to prevent
shrinkage, if shrinkage occurs, as doing this will create load in the specimen, making
the resulting data difficult to interpret. Note that oxidation testing using forced air ovens
will produce conservative estimates of long-term product strength due to the rapid air
circulation and the relatively high oxygen content in the oven relative to the oxygen content
in the ground. If the geosynthetic supplier wishes to submit data at a lower oxygen content
than that of air (approximately 21% O2), use of such data for approval of a given product
may require that the structure be declared experimental, requiring that instrumentation
be placed in the ground to verify the actual oxygen content in the structure backfill.
Alternatively, the geosynthetic supplier could submit data from previously constructed
structures with similar backfill in which the actual oxygen content in the structure backfill
was measured.
For polyesters, long-term chemical durability testing should consist of elevated temperature
immersion tests to evaluate potential for hydrolysis effects. A reactor similar to that
illustrated in Elias, et al. (1999) is recommended for incubating the geosynthetic specimens.
A description of the test protocol is provided by Elias, et al. (1999). The reactor should be
capable of maintaining temperature uniformity (+ 1%) and stability during long-term use.
A minimum solid/liquid ratio of 1:40 should be used to size the reactor and to determine
the maximum number of specimens that can be placed in the reactor. Measures should be
taken to minimize possibilities for oxidation and reaction with carbon dioxide during the
long-term incubation (e.g., replace any air inside the reactor with nitrogen, use de-aired
water, keep system well sealed, etc.). Specimens should be suspended in the solution on
a hanger made of a material that will not react with or contaminate the immersion fluid
and specimens (e.g., Teflon, stainless steel, etc.). The specimens should not be framed
to prevent shrinkage, if shrinkage occurs so that an unknown amount of tension is not
placed on the specimens. Specimens should each be separated by a distance of at least 13
mm (0.5 in.). The solution should be intensively stirred to ensure solution uniformity. For
coated polyester products, the immersion tests should be conducted without the coating
or the coated specimen ends should not be recoated (i.e., the ends of the core polymer
should be left exposed to the immersion liquid). Elevated temperatures should be used to
accelerate the degradation process, which allows the data to be extrapolated to the desired
design life. Hydrolysis data should be submitted for the product at a pH of approximately
7 (i.e., neutral conditions - distilled water), at a pH of 9 or more, and at a pH of 4 or less
to facilitate the determination of RFD. RFD should be determined at a pH of 7 and at an
alkaline pH (i.e., a pH of 9) as a minimum. If very acidic soils are anticipated (i.e., a pH
near the bottom limit of pH = 4 for conditions defined as nonaggressive), RFD should be
determined at a pH of 4 as well.
Note that EPA 9090 testing, or the ASTM equivalent (ASTM D5322), is not considered
adequate for a laboratory testing program to provide an estimate of RFD. However, EPA
9090 or ASTM D5322 testing can be used as a first cut screening tool. That is, if any
significant degradation of the strength of the product in question is observed for the
chemical environment tested, the product would be disqualified for use in that chemical
environment unless longer term testing conducted in accordance with this appendix is
performed. EPA 9090 testing (or ASTM D5322) could also be used verify the effects
of certain environmental variables which are known, based on the literature, to not
significantly affect the given material. For example, low or high pH is known, based on the
literature, to have little effect on polyolefins. This type of testing could be used to verify
that the low or high pH does not affect the tensile strength of a polyolefin product, to allow
that product to be used in environments that have a pH outside the range defined as a
nonaggressive environment.
The long-term chemical durability testing program should be conducted and interpreted
using the following guidelines:
• Incubation temperatures for the testing should be high enough to adequately accelerate
the degradation process but below any major transitions in polymer behavior (e.g.,
glass transition, melting). Maximum recommended test temperatures to avoid major
transitions are on the order of 70 to 75o C for polypropylene, high density polyethylene,
and polyester, except as discussed above for polyolefin products which have micro-
cracks or crazes as manufactured. However, exposure to temperatures near the upper
end of these ranges could affect the stress-strain behavior of the material due to loss
of molecular orientation, or possibly other effects that are not the result of chemical
degradation. Therefore, care needs to be exercised when interpreting results from
strength testing after exposure to temperatures near the maximum test temperatures
indicated above. In general, if the stiffness of the material after exposure to the
environment is significantly different from that of the virgin material, the stress-strain
properties, and possibly the strength, of the material may have been affected by the
exposure temperature in addition to the chemical environment. If the stiffness has
been affected, the cause of the stiffness change should be thoroughly investigated to
determine whether or not the change in stiffness is partially or fully due to the effect
of temperature, or alternatively not use the data obtained at and above the temperature
where the stiffness was affected. It is additionally recommended that the Arrhenius
plot of the data be checked for linearity (see the discussion of Arrhenius modeling
which follows). As a minimum, two to three data points above and below the suspected
transition should be obtained and the plot checked for linearity through the entire range
of temperatures, if it is desired to validate the use of data above the suspected transition
for Arrhenius modeling and extrapolation purposes.
• A minimum of three to four test temperatures are recommended, typically spaced
monotonically at 10o C increments (e.g., see ASTM D3045), except as discussed above
for some polyolefin products.
• At the lowest test temperature (e.g., 30 to 50o C), incubation times of 2 to 4 years
should be anticipated to get data adequate for long-term extrapolation.
• Enough retrievals (e.g., a minimum of three to four retrievals) should be made
at a given test condition to adequately define the property loss as a function of
incubation time.
• As a minimum, degradation should be tracked using the tensile strength of the
specimens retrieved from the incubation chambers. Full wide width (ASTM D4595
or ASTM D6637) specimens are preferred; however, single rib or yarn specimens can
be used.
• It is also recommended that degradation be tracked by chemical means, if possible, as
well as through the use of scanning electron microscope (SEM) micrographs to verify
the significance of the mechanical property degradation observed.
• The statistical variation of the measured properties after degradation are likely to be
greater than what would be observed for the virgin material. This may require that the
number of specimens per retrieval be greater than what the property variation for the
virgin material would indicate.
• Extrapolation of chemical durability data for polymers typically utilizes an Arrhenius
approach, though there is evidence which suggests that the Arrhenius model does not
always work well for geosynthetics. Assuming Arrhenius modeling is appropriate,
the slope of the strength degradation versus time plots (transformed mathematically
to be linear through zero, first, or second order Arrhenius equations) can be used to
characterize the degradation behavior as a function of temperature, allowing the slope
at the desired design temperature to be estimated through the Arrhenius extrapolation.
The equation order which best fits the data should be used (see Salman, et. al., 1998,
for details). The strength retained at a given time at the design temperature can be
calculated directly from the linear equation with the extrapolated slope. Note that
Arrhenius modeling could also be conducted as a function of reactant (oxygen)
concentration and pressure instead of temperature (Shelton and Bright, 1993; Salman,
et. al., 1998). The extrapolation concept would be similar to that used for temperature.
See Shelton and Bright (1993), Salman, et. al. (1997), and Salman, et. al. (1998), Elias,
et al. (1999), Elias (2000) for guidance on Arrhenius modeling techniques as applied
to geosynthetics. Also note that since the extrapolation is being conducted over several
log cycles of time, uncertainty in the data should be considered when determining the
retained strength at the design life and design environment.
• For polyolefin oxidation, Arrhenius modeling will likely need to be conducted in two
steps, as there are two main phases in the oxidation process for polyolefins: 1) the
induction phase, where antioxidant consumption is the primary activity and little, if
any, product strength loss occurs, and 2) the main polymer oxidation phase, where
oxidative degradation of the polyolefin occurs, resulting in strength loss, and can
generally be described by the kinetics of a Basic Auto-oxidation Scheme (Salman,
et. al., 1997; Elias, et al., 1999). An Arrhenius model for the first phase should be
developed so that the induction period tind at the design temperature or reactant (i.e.,
oxygen) concentration can be estimated. A second Arrhenius model should then be
developed using only the data after the induction period, and time in this case would
begin at the end of the induction period at each temperature or reactant concentration
tested. This second Arrhenius model is then extrapolated to the design temperature or
reactant concentration to estimate the strength loss anticipated at the desired design
life minus the induction period. Analysis of the remaining antioxidant content provides
an additional method of measuring the duration of Step 1, particularly at lower
temperatures and long durations, since changes in the antioxidant content take place
ahead of the reduction in strength. Note that if the estimated induction period at the
design environment is greater than the desired design life, this second phase Arrhenius
modeling is unnecessary.
• Once the tensile strength at a given design life and design temperature has been
estimated from the test data, determine RFD as follows:
Tlot (D-1)
RFD
TD
where, Tlot is the average lot specific ultimate tensile strength for the lot of material
used for the durability testing, and TD is the extrapolated (i.e., to the required design
life) lot specific tensile strength after degradation based on the laboratory aging tests.
In no case should RFD be less than 1.1.
Biological degradation has not proved a serious factor in the service life of geosynthetics.
This is because the high molecular weight polyethylene, polyester, polypropylene and
polyamide used are not easily broken down by bacteria and fungi. The high tensile
strength of soil reinforcements prevents them from damage by roots of burrowing animals
such as rabbits. For this reason it is not in general necessary to apply consider biological
degradation in defining RFD. However, the possibility of biological degradation should
be reviewed if new polymers other than those described are used. Biological durability,
if specifically requested by the approval authority, should be evaluated based on ASTM
D3083-89, except the test should be modified to use ASTM D4595 or ASTM D6637 as the
tensile test method. If any significant tensile strength loss is observed, as determined using
ASTM D4595 or ASTM D6637, additional longer term testing should be performed before
the product is further considered for use in reinforcement applications (see Bright, 1993).
If, as an alternative to long-term laboratory testing, the geosynthetic manufacturer prefers
to submit data from long-term field retrievals, the following requirements must be met:
• A minimum of three retrievals must be obtained over a minimum time period
adequate to permit extrapolation to the required design life (i.e., the first retrieval is
taken right after installation, the second retrieval is taken at some time during the
middle of this period, and the third retrieval is taken at the end of the minimum study
period).
• The retrieved samples shall be evaluated both physically and chemically to determine
changes in strength, fiber/yarn/rib appearance, and polymer chemistry. Lot specific
baseline data for the exhumed geosynthetic regarding strength and polymer properties
must be available for comparison. The soil environment in which the geosynthetic
was placed must also be well defined in terms chemistry, moisture, temperature,
gradation, and approximate geosynthetic stress level. Enough specimens for each
retrieval must be taken to account for statistical variance in the properties measured.
See Elias (2000, 2001) for a more detailed description of the procedures required to
obtain the needed information to determine RFD using this approach.
• The polymer and physical characteristics of the exhumed material must meet the
requirements for use in determining RFD for “similar” products as described later in
this appendix.
can become relatively rapid at high temperatures in the vicinity of the glass transition
temperature or above for the polymer, which is on the order of 70° C to 80° C (160° F to
180° F). The polymer does not need to be submerged for hydrolysis to occur, as hydrolysis
can occur in moderate to high humidity conditions, though the reaction rate becomes
slower as the humidity decreases (McMahon, et. al., 1959).
Hydrolysis appears to be the result of both a surface erosional phenomenon as well as
a diffusional process of water to the polymer fiber core. These two phenomena have
given rise to the terms “outer” and “inner” hydrolysis. Outer, or surficial, hydrolysis is
dominant in high pH conditions and is characterized by loss in fiber cross-sectional area
with minimal reduction in the molecular weight of the polymer that remains (Anderson, et.
al., 1992; Jailloux, et. al., 1992). Inner, or diffusional controlled hydrolysis is dominant in
neutral and acidic conditions and is characterized by significant losses in molecular weight
of the polymer with minimal surficial erosion or damage (Anderson, et. al., 1992; Jailloux,
et. al., 1992).
Rupture of a polymer when under stress is either ductile or brittle in nature. The ductile
failure mode occurs when stresses are high enough to cause tie molecules to stretch out,
lamellae to separate and start unfolding, resulting in fracture of the spherulites and
plastic flow of the molecular structure (Lustiger, 1983). When failure occurs in a brittle
manner, stress levels are usually lower, allowing sufficient time for tie molecules to slowly
disentangle themselves from adjacent spherulites, initiating crack formation followed by
slow crack growth (Bright, 1993).
ESC is the result of an accelerated crack initiation and growth process occurring when
a polymer is subjected concurrently to a particular chemical environment and long-term
stress. This accelerated crack initiation and growth process can result in premature brittle
failure. ESC results in molecular chain disentanglement rather than chain breakage or
chemical change.
Evaluation of ESC has been focused on polyethylene due to its use in various critical
applications (e.g., telephone transmission cables, natural gas pipe) and the potential
sensitivity of some polyethylenes to this phenomenon. The literature indicates that other
polymers used for geosynthetics may also experience some sensitivity to this phenomenon
(Bright, 1993).
The results of previous studies show that polyethylene resistance to ESC can be improved
by increasing its average molecular weight, decreasing its molecular weight distribution,
increasing its crystalline content, reducing the crystallite and/or spherulite size, increasing
the degree of orientation, and using copolymerization (Wrigley, 1987). Therefore, the
potential for ESC in a given polymer can be controlled.
ESC is closely related to the more general phenomenon of stress cracking. The difference
between the two is that the chemical present for ESC accelerates the chain disentanglement
process, whereas in stress cracking no accelerating chemical is present. Chemicals
identified in the literature that can accelerate the stress cracking process include water,
weak acids and bases, alcohols, metallic soaps, and solvents (Wrigley, 1987). Water, and to
some extent weak acids and bases, are “chemicals” which need to be considered for ESC
in typical in-soil environments.
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