DR 2700

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DOC026.53.

00809

DR 2700
USER MANUAL

08/2013, Edition 4

© HACH Company, 2007–2008, 2013. All rights reserved. Printed in Germany.


Table of Contents
Section 1 Specifications ........................................................................................................................................ 5
Section 2 General Information .............................................................................................................................. 7
2.1 Safety information .............................................................................................................................................. 7
2.1.1 Use of hazard information ......................................................................................................................... 7
2.1.2 Precautionary labels ................................................................................................................................. 7
2.1.3 Chemical and Biological Safety ................................................................................................................ 8
2.2 Overview of product ........................................................................................................................................... 8
Section 3 Installation ............................................................................................................................................. 9
3.1 Unpack the instrument ....................................................................................................................................... 9
3.2 Operating environment ...................................................................................................................................... 9
3.2.1 Power connections .................................................................................................................................. 10
3.3 Connection ....................................................................................................................................................... 10
3.4 Cell compartments, Cell adapters, Light Shield and Protective Cover ............................................................. 12
3.4.1 Cell compartments and adapters ............................................................................................................ 12
3.4.2 Installation of the sample cell adapters ................................................................................................... 13
3.4.3 Use of the light shield for measurements ................................................................................................ 14
3.4.4 Protective Cover ..................................................................................................................................... 16
3.5 Mobile use of the DR 2700 for field analysis .................................................................................................... 17
3.5.1 Position the Protective Cover .................................................................................................................. 18
3.6 Beam path ........................................................................................................................................................ 19
Section 4 Start Up ................................................................................................................................................ 21
4.1 Power the instrument on and off ...................................................................................................................... 21
4.2 Language selection .......................................................................................................................................... 21
4.3 Self-Check ....................................................................................................................................................... 21
Section 5 Standard Operations ........................................................................................................................... 23
5.1 Overview .......................................................................................................................................................... 23
5.1.1 Tips for the use of the touch screen ........................................................................................................ 23
5.1.2 Use of the alphanumeric keypad ............................................................................................................ 23
5.1.3 Main Menu .............................................................................................................................................. 24
5.2 Instrument Setup mode .................................................................................................................................... 25
5.2.1 Operator ID ............................................................................................................................................. 25
5.2.2 Sample ID ............................................................................................................................................... 26
5.2.3 Date and time .......................................................................................................................................... 27
5.2.4 Display and sound preferences .............................................................................................................. 27
5.2.5 Power Management ................................................................................................................................ 27
5.2.6 PC and printer ......................................................................................................................................... 29
5.2.6.1 Printer setup ............................................................................................................................... 29
5.2.6.2 Print data .................................................................................................................................... 31
5.2.6.3 HACH Data Trans ....................................................................................................................... 31
5.2.7 Password ................................................................................................................................................ 32
5.2.7.1 Password deactivation ................................................................................................................ 33
5.3 Store, recall, send and delete data .................................................................................................................. 35
5.3.1 The data log ............................................................................................................................................ 35
5.3.1.1 Auto/manual data storage ........................................................................................................... 35
5.3.1.2 Recall stored data from the data log ........................................................................................... 35
5.3.1.3 Send data from the data log ....................................................................................................... 36
5.3.1.4 Delete stored data from the data log .......................................................................................... 37

1
Table of Contents

5.4 Stored Programs .............................................................................................................................................. 38


5.4.1 Select a saved test/method; enter user-specific basic data .................................................................... 38
5.4.2 Stored program options .......................................................................................................................... 38
5.4.3 Use of program timers ............................................................................................................................ 40
5.4.4 Set the dilution factor .............................................................................................................................. 41
5.4.5 Run a standard adjust ............................................................................................................................. 41
5.4.6 Set the chemical form ............................................................................................................................. 42
5.4.6.1 Change of the default setting of the chemical form .................................................................... 43
5.4.7 Run a reagent blank ................................................................................................................................ 43
5.4.8 Analysis of samples ................................................................................................................................ 44
5.4.9 Add stored programs to the favorite programs list .................................................................................. 45
Section 6 Advanced Operations ......................................................................................................................... 47
6.1 User Programs ................................................................................................................................................. 47
6.1.1 Program a user method .......................................................................................................................... 47
6.1.1.1 Single wavelength settings ......................................................................................................... 49
6.1.1.2 Multi wavelength settings ............................................................................................................ 50
6.1.1.3 Calibration settings for single and multi wavelength mode ......................................................... 52
6.1.1.4 Store a user program .................................................................................................................. 56
6.1.1.5 Additional user-defined parameters and functions ..................................................................... 56
6.1.2 Free programming program type ............................................................................................................ 58
6.1.2.1 Measurement process ................................................................................................................ 58
6.1.2.2 Enter a new element of a measuring sequence ......................................................................... 59
6.1.2.3 Enter the calibration formula (evaluation formula) ...................................................................... 61
6.1.2.4 Enter variables ............................................................................................................................ 64
6.1.2.5 Save a free programming user program ..................................................................................... 64
6.1.3 Select a user program ............................................................................................................................. 65
6.1.4 Add, edit and delete user programs from the favorites list ...................................................................... 65
6.1.4.1 Add to Favorites .......................................................................................................................... 66
6.1.4.2 Edit .............................................................................................................................................. 66
6.1.4.3 Delete ......................................................................................................................................... 66
6.2 Favorite Programs ........................................................................................................................................... 67
6.2.1 Recall a favorite program ........................................................................................................................ 67
6.2.2 Delete a favorite program ....................................................................................................................... 67
6.3 Standard Addition – monitoring/checking results ............................................................................................. 68
6.3.1 Complete a standard addition ................................................................................................................. 69
6.4 Single Wavelength (absorbance, concentration and transmittance measurements) ....................................... 73
6.4.1 Set up single wavelength mode .............................................................................................................. 73
6.4.2 Take single wavelength measurements .................................................................................................. 75
6.5 Multi-Wavelength mode – measurements at more than one wavelength ........................................................ 76
6.5.1 Set the reading mode at different wavelengths ....................................................................................... 76
6.5.2 Complete a measurement in the multi wavelength mode ....................................................................... 79

2
Table of Contents

6.6 System checks ................................................................................................................................................. 79


6.6.1 Instrument information ............................................................................................................................ 80
6.6.2 Upgrade of the instrument software ........................................................................................................ 80
6.6.3 Optical checks ......................................................................................................................................... 81
6.6.3.1 Wavelength check ...................................................................................................................... 81
6.6.3.2 Stray light check ......................................................................................................................... 82
6.6.3.3 Absorbance check ...................................................................................................................... 83
6.6.3.4 Verification kit ............................................................................................................................. 84
6.6.4 Output checks ......................................................................................................................................... 86
6.6.5 Lamp history ........................................................................................................................................... 86
6.6.6 Factory service ........................................................................................................................................ 86
6.6.7 Service time ............................................................................................................................................ 87
6.6.8 Instrument Backup .................................................................................................................................. 88
Section 7 Maintenance ........................................................................................................................................ 91
7.1 Cleaning requirements ..................................................................................................................................... 91
7.1.1 Spectrophotometer ................................................................................................................................. 91
7.1.2 Display .................................................................................................................................................... 91
7.1.3 Sample cells ............................................................................................................................................ 91
7.2 Insert or change of the battery ......................................................................................................................... 92
7.2.1 Information about using the battery ........................................................................................................ 93
7.2.1.1 Dispose of the lithium battery ..................................................................................................... 93
7.2.1.2 Optimal operation of the battery ................................................................................................. 94
7.2.1.3 Lifespan of the battery ................................................................................................................ 94
7.2.1.4 Load the battery/Operating time ................................................................................................. 94
7.3 Lamp replacement ........................................................................................................................................... 95
Section 8 Troubleshooting .................................................................................................................................. 99
Section 9 Replacement Parts ............................................................................................................................ 101
Section 10 Contact Information ........................................................................................................................ 103
Section 11 Limited Warranty ............................................................................................................................. 105
Index .................................................................................................................................................................... 107

3
Table of Contents

4
Section 1 Specifications
Specifications are subject to change without notice.

Performance Specifications

Operating Mode Transmittance (%), Absorbance and Concentration

Source Lamp Gas-filled Tungsten (visible)

Wavelength Range 400–900 nm

Wavelength Accuracy ± 1.5 nm

Wavelength Reproducibility < 0.1 nm

Wavelength Resolution 1 nm

Wavelength Calibration Automatic at startup

Wavelength Selection Automatic, based on method selection

Spectral Bandwidth < 5 nm

Photometric measuring range ± 3.0 Ext in Wavelength Range 400–900 nm


0.005 Abs at 0.0–0.5 Abs
Photometric Accuracy
1% at 0.50–2.0 Abs
< 0.5% ≤2 Abs
Photometric Linearity ≤ 1% at > 2 Abs
with neutral glass at 546 nm
Stray Light < 0.1% T at 500 nm with filter OG570/3

Data storage 200 measured values (result, date, time, sample ID, user ID)

User programs 10

Physical and Environmental Specifications

Width 220 mm (8.6 in)

Height 135 mm (5.3 in)

Depth 330 mm (12.9 in)


4.06 kg (8.95 Ibs) without battery
Weight
4.38 kg (9.66 Ibs) with battery
Operating Requirements 10–40 °C (50–104 °F), max. 80% relative humidity (non-condensing)

Storage Requirements -40–60 °C (-40–140 °F) max. 80% relative humidity (non-condensing)

Additional technical data


15 VDC- / 30VA
Mains connection Plug-in power supply unit: (100–240 VAC/50–60 Hz)
Lithium battery pack,11.1 V, 4.4 Ah, rechargeable
Use only shielded cable with max. length of 3 m.
Interfaces 1 x USB type A
1 x USB type B
IP 41 with closed lid
Enclosure Rating
IP 42 with Protective Cover in place
Safety class Safety class II

5
Specifications

6
Section 2 General Information

2.1 Safety information


Please read this entire manual before unpacking, setting up or
operating this equipment. Pay attention to all danger, warning and
caution statements. Failure to do so could result in serious injury to
the operator or damage to the equipment.
Make sure that the protection provided by this equipment is not
impaired, do not use or install this equipment in any manner other
than that specified in this manual.

2.1.1 Use of hazard information

DANGER
Indicates a potentially or imminently hazardous situation
which, if not avoided, will result in death or serious injury.

WARNING
Indicates a potentially or imminently hazardous situation
which, if not avoided, could result in death or serious injury.

CAUTION
Indicates a potentially hazardous situation that may result in
minor or moderate injury.

Important Note: Indicates a situation which, if not avoided, may


cause damage to the instrument. Information that requires special
emphasis.

Note: Information that supplements points in the main text.

2.1.2 Precautionary labels


Read all labels and tags attached to the instrument. Personal injury
or damage to the instrument could occur if not observed. A symbol,
if noted on the instrument, will be included with a danger or caution
statement in the manual.

This symbol, if noted on the instrument, references the instruction manual for operation and/or safety information.

Electrical equipment marked with this symbol may not be disposed of in European public disposal systems after
12 August of 2005. In conformity with European local and national regulations (EU Directive 2002/96/EC),
European electrical equipment users must now return old or end-of life equipment to the Producer for disposal at no
charge to the user.
Note: For return for recycling, please contact the equipment producer or supplier for instructions on how to return
end-of-life equipment, producer-supplied electrical accessories and all auxiliary items for proper disposal.

7
General Information

2.1.3 Chemical and Biological Safety

DANGER
Potential Chemical/ Biological Exposure Hazards. Handling
chemical samples, standards and reagents can be dangerous.
Users of this product are advised to familiarize themselves
with safety procedures and the correct use of chemicals, and
to carefully read all relevant Material Safety Data Sheets.

Normal operation of this instrument may involve the use of


hazardous chemicals or biologically harmful samples.
• The user must observe all cautionary information printed on the
original solution containers and safety data sheet prior to their
use.
• All waste solutions must be disposed in accordance with local
and national law.
• The type of protective equipment must be selected according to
the concentration and amount of the dangerous substance at
the specific workplace.

2.2 Overview of product


The DR 2700 spectrophotometer is a VIS spectrophotometer with a
wavelength range of 400 to 900 nm. The instrument comes with a
complete set of application programs and multi-language support.
The DR 2700 spectrophotometer contains the following application
modes: Stored Programs (pre-installed tests), User Programs,
Favorite Programs, Single Wavelength Mode and Multi-Wavelength
Mode.
The DR 2700 spectrophotometer provides digital readouts in direct
concentration units, absorbance, or percent transmittance.
When a user-generated or programmed method is selected, the
on-screen menus and prompts direct the user through the test.
This menu system also can be used to generate reports, statistical
evaluations of generated calibration curves, and to report
instrument diagnostic checks.

8
Section 3 Installation
WARNING
Electrical and Fire Hazards. Use only the provided power
supply. Only qualified personnel should conduct the tasks
described in this section of the manual.

3.1 Unpack the instrument


The DR 2700 Spectrophotometer comes packaged with the
following items:
• DR 2700 spectrophotometer
• Plug-in power supply, including 4 adapters for EU, GB, USA,
AUS/China
• Two square glass cells, 10 mL, matched
• 3 different cell adapters (A, B and C)
• Light Shield
• Protective Cover
• DR 2700 Basic User Manual
Further information, detailed user manuals and documentation are
available on the website of the manufacturer.
Note: If any of these items are missing or damaged, contact the
manufacturer or a sales representative immediatly.

3.2 Operating environment


The following conditions are necessary to ensure correct
instrument operation and accurate results:
• Place the instrument firmly on an even surface. Do not push
any objects under the instrument.
• Maintain an ambient temperature of 10 to 40 ºC (50 to 104 ºF)
for proper instrument operation.
• The relative humidity should be less than 80%; moisture should
not condense on the instrument.
• Leave at least a 15 cm (6 in.) clearance at the top and on all
sides for air circulation to avoid overheating of electrical parts.
• Do not operate or store the instrument in extremely dusty,
damp or wet locations.
• Keep the surface of the instrument, the cell compartment and
all accessories clean and dry at all times. Splashes or spills on
and in the instrument should be cleaned up immediately (see
section 7.1 on page 91).
Important Note: Protect the instrument from temperature
extremes, including heaters, direct sunlight and other heat sources.

9
Installation

3.2.1 Power connections


Only the provided external power supply LZV798 has to be used.
Install the correct adapter plug on the supplied external power
supply (Figure 1) by sliding the adapter on until it "clicks" into
position. Correctly mounted, both housing of power supply and plug
are in line. Plug the external power supply cord into the connector
on the back panel of the instrument, then plug the supply into a
power outlet (100–240 V~ / 50–60 Hz). Press the power switch on
the back of the instrument to initialize power.

3.3 Connection
The DR 2700 has two USB interfaces as a standard feature,
located on the back of the instrument (Figure 1).
The USB Type A interface is used for communications with a
printer, USB memory stick or keyboard. A USB memory stick is
used to update instrument software.
The USB Type B interface is used for communications with a PC.
The optional Hach Data Trans software (see section 5.2.6.3 on
page 31) must be installed on the PC for this use.
A USB hub may be used to connect several accessories at a time.
Note: USB cables must not be longer than 3 meters (10 feet).

These USB interfaces enable data and graphics to be output to a


Printer and a PC and upgrade of instrument software (see
section 6.6.2 on page 80).

10
Installation

Figure 1 Interfaces
1 On/Off switch 4 Cover
2 USB type B 5 USB type A
3 Plug in power supply

11
Installation

3.4 Cell compartments, Cell adapters, Light Shield and Protective Cover
3.4.1 Cell compartments and adapters
The DR 2700 has two cell compartments (Figure 2). Only one
sample cell type at a time can be used for a measurement.

Cell compartment #1
• 13-mm and 16-mm round cells

Cell compartment #2
Cell compartment #2 uses adapters to accommodate different
sample cell types.
• 1-inch square or 50-mm rectangular cells (can be inserted
directly into the cell compartment without using an adapter).
• Adapter A: 10-mm square cells
• Adapter B: Pour-Thru cells (refer to the instruction sheet
supplied with the Pour-Thru cell) and multi-path cells
Note: Pour-Thru Cell must be used with Adapter B, not Adapter C.

• Adapter C: One-inch round cells and AccuVac® Ampules


Note: One-inch round cells and AccuVac Ampules must be used with
Adapter C, not Adapter B.

Figure 2 Cell compartments


1 Cell compartment #1 2 Cell compartment #2

12
Installation

Figure 3 Sample cell adapters


1 10 mm square sample cell adapter (A) 3 1 inch round sample cell adapter (C)
2 1 inch Pour-Thru adapter (B)

3.4.2 Installation of the sample cell adapters

1. Open the cell compartment.

2. Select the correct adapter for the sample cell type.

3. Insert the adapter so the arrow on top of the adapter points to


the left (Figure 4 on page 14) and the orientation tab fits the
groove in the compartment opening. The sample cell type
imprint should be legible on the adapter (Figure 3).

Note: The arrow on top of the adapter indicates the direction of the
light beam path.

13
Installation

Figure 4 Installation of a sample cell adapter

3.4.3 Use of the light shield for measurements


The light shield (Figure 5 on page 15) prevents light interference
when using 13 mm and 16 mm vial tests and must be in place
before measurements can be taken in cell compartment #1. The
light shield is required only when using 13 mm or 16 mm vial tests.

14
Installation

The DR 2700 is shipped with the light shield installed. Remove the
light shield before using cell compartment #2. The light shield can
be stored in the Protective Cover (Figure 7 on page 16)

Figure 5 Light Shield

Installation of the light shield

1. Open the cell compartment.

2. Insert the light shield so the arrow on the light shield points to
the left and the orientation tab fits the groove in the
compartment opening (Figure 6).

Figure 6 Light Shield in place


1 Light Shield

15
Installation

3.4.4 Protective Cover

Figure 7 Protective Cover


1 Protective Cover 3 Protective Cover with inserted sample cell adapter A in
2 Protective Cover (inside view) position A.
The inside of the Protective Cover is intended to house
the sample cell adapters. The recesses for holding the
sample cell adapters are marked with the corresponding
letters.

16
Installation

3.5 Mobile use of the DR 2700 for field analysis


If the DR 2700 spectrophotometer is used to carry out field
analysis, it may be necessary to take a number of measures to
compensate for the fluctuating ambient light conditions.
You should take the measures described below if the following
warning is displayed after you take a measurement:
Error: Too much ambient light! Move device into shade or
close the lid!
General measure:
Shield the instrument from the sun by standing so that your shadow
falls on it, and carry out the measurement again. If the warning
appears again, take the following measures.
Measures:
Measurements in a 10 mL round cell, a rectangular cell or
AccuVac Ampules
Close the lid of the cell compartment and carry out the
measurement.
Measurements in a 13 or 16 mm cell or a 25 mL square cell
To obtain consistent measurement conditions in all weather
conditions, place the Protective Cover on the open cell
compartment (see Figure 8 Position the Protective Cover on page
18) and carry out the measurement.
Important Note: When you carry out measurement in 25 mL
square cells, take care that there is no adapter in the Protective
Cover.

The enclosure rating of the photometer increases from IP41 to IP42


when the Protective Cover is in place.

17
Installation

3.5.1 Position the Protective Cover

Figure 8 Position the Protective Cover

1. After you have inserted the zero solution cell or the sample cell,
position the Protective Cover over the open cell compartment.
The lettering "Protective Cover" must be readable from the
display side of the instrument.

2. Press the Protective Cover lightly into the correct position until
the cell compartment is completely sealed and the Protective
Cover cannot slip off.

3. Carry out the measurement.

Note: The Protective Cover can simultaneously be used to house the


different cell adapters. The cell adapter recesses in the Protective Cover
are marked with the corresponding letters and arrows of the adapter. The
arrows in the Protective Cover and on the adapters indicate the direction of
insertion.

18
Installation

3.6 Beam path


Figure 9 shows the beam path of the DR 2700:

Figure 9 Beam path


1 Tungsten lamp 8 Splitter mirror
2 Entrance slit 9 Reference-element
3 Heat-protection glass 10 Cell compartment #2
4 Grating 11 Lens
5 Exit slit 12 Measurement element
6 Lens 13 Cell compartment #1
7 Filter wheel 14 LED

19
Installation

20
Section 4 Start Up

4.1 Power the instrument on and off


1. Plug in to the power supply (laboratory analysis) or insert the
battery (field analysis).

2. The push-button switch on the back of the instrument switches


the instrument on (press for about 1 second) and off (press for
about 3 to 5 seconds). An acoustic signal confirms that the
instrument has been switched off.

Note: Do not turn the instrument off and on in rapid succession. Always
wait about 20 seconds before turning the instrument on again, otherwise
the electronic and mechanical systems will be damaged.

4.2 Language selection

The spectrophotometer software includes several language


options. The first time the instrument is turned on, the language
selection screen will appear.

1. Select the desired language.

2. Press OK to confirm the language selection. The self check will


start automatically.

Change the language setting


The instrument functions in the selected language until the option is
changed.

1. While turning the instrument on, touch the screen at any point
until the list for selecting a language appears
(about 30 seconds).

2. Select the required language.

3. Press OK to confirm. The test program subsequently starts


automatically.

4.3 Self-Check

Each time the instrument is powered up, a series of diagnostic tests


are performed automatically to ensure operation of major system
components.
This procedure, which takes approximately two minutes, checks the
system, lamp, filter adjustment, wavelength calibration and voltage.
Each test that functions correctly is confirmed with a check mark.
The Main Menu is displayed when power-up diagnostics are
completed.

21
Start Up

If the instrument detects any deviation relative to the last


calibration, a system check has to be carried out.

1. Remove the cell from the cell compartment and close the lid.

2. Then press Start.

The system check is carried out (duration approx. 6 minutes).


Note: Further error messages during self check, see Section 8 on page 99.

22
Section 5 Standard Operations

5.1 Overview
5.1.1 Tips for the use of the touch screen
The entire screen is touch-activated. To make a selection, press the
screen with a fingernail, fingertip, pencil eraser or a stylus. Do not
press the screen with a sharp object, such as the tip of a ball
point pen.
• Do not place anything on top of the screen, to prevent damage
or scratching on the screen.
• Press keys, words or icons to select them.
• Use scroll bars to move up and down long lists very quickly.
Press and hold the scroll bar, then move up or down to move
through the list.
• Highlight an item from a list by pressing it once. When the item
has been successfully selected, it will be displayed as reversed
text (light text on a dark background).

5.1.2 Use of the alphanumeric keypad

This display is used to enter letters, numbers and symbols as


needed when programming the instrument. Unavailable options are
disabled (grayed out). The icons on the right and left of the screen
are described in Table 1.
The central keypad changes to reflect the chosen entry mode.
Press a key repeatedly until the desired character appears on the
screen. A space can be entered by using the underscore on the
YZ_ key.
Note: A USB keyboard (with US keyboard layout) can be used for input
(see Section 9 on page 101).

Table 1 Alphanumeric keypad


Icon / key Description Function
When entering alphabetic characters (ex. user-entered units), this key allows to
ABC/abc Alphabetic
toggle between upper and lower case letters.
#% Symbols Punctuation, symbols and numerical sub- and superscripts may be entered.

123 Numeric For entering regular numbers.

CE Clear Entry Clear the entry.


Moves back one position. This deletes the character previously entered in the new
Left Arrow Backspace
position.
Moves to the next space in an entry when two adjacent characters occur on the
Right Arrow Advance
same key.

23
Standard Operations

5.1.3 Main Menu

A variety of modes may be selected from the ”Main Menu“. The


following table briefly describes each menu option.

Table 2 ”Main Menu“ Options DR 2700


Option Function
Stored programs are pre-programmed methods that make use of HACH reagents.
Stored Programs The DR 2700 Procedures Manual contains illustrated, step-by-step procedures for analysis using
HACH programs.
User programs make "made to measure analysis" possible:
- Users can program methods they have developed themselves
User Programs
- Existing HACH methods can be stored as user programs. The tests can then be modified to suit
the user's requirements.
Favorite Programs List of methods/tests selected by the user to suit his own requirements.
Single wavelength measurements are:
Absorbance measurements: The light absorbed by the sample is measured in absorbance
units.
Single Wavelength Transmittance measurements (%): The percentage of the light that passes through the sample
and reaches the detector is measured.
Concentration measurements: A concentration factor can be entered to enable the measured
absorbance values to be converted into concentration values.
In the multi-wavelength mode, absorbance (Abs) or percentage transmittance (%T) is measured
Multi Wavelength at up to four wavelengths, and absorbance differences and absorbance relationships are
calculated. Simple conversions into concentrations can also be carried out.
The system checks menu offers a number of options, including optical checks, output checks,
System Checks
lamp history, instrument update, service time and instrument backup.
Recall Data Stored data can be called up, filtered, transmitted and deleted.
In this mode, user-specific or method-specific settings can be entered: Operator-ID, Sample-ID,
Instrument Setup
Date & Time, Display & Sound, Power Management, PC & Printer and Password.

24
Standard Operations

5.2 Instrument Setup mode

1. Select Instrument Setup in the ”Main Menu“.

A selection of functions appears in order to configure the functions


of the instrument.

5.2.1 Operator ID
Use this option to enter up to 30 sets of operator initials (up to
5 characters each) into the instrument. This feature helps record
which operator measured each sample.

1. Press Operator ID in the Instrument Setup.

2. Press New to enter a new Operator ID.

3. Use the alphanumeric keypad to enter a new Operator ID.

4. Press OK to confirm.

5. The display shows the chosen Operator ID.

6. Press OK. The instrument will return to the Instrument Setup


screen and show the selected operator identifier.

7. The chosen Operator ID is activated.

Note: Press Delete to remove an Operator ID from the list.

Note: Alternatively, enter or change an Operator ID in measurement mode.


In the results screen, press Options>More>Instrument Setup or if an
Operator ID is already assigned, select the "Operator ID symbol
immediately in the results screen.

25
Standard Operations

5.2.2 Sample ID
Use this option to enter up to 30 Sample Identification tags (up to
13 characters each) into the instrument. Sample IDs can be used to
specify the sample location or other sample specific information.

1. Press Sample ID in the Instrument Setup.

2. Press New to enter a new Sample ID.

3. Use the alphanumeric keypad to enter a new Sample ID.

Note: Sample IDs can also be entered with a USB keyboard.

4. Press OK to confirm.

5. To number the Sample IDs sequentially (e.g. Inflow (01 etc.)),


select Add Number.

• Use the arrow keys to specify the first number of the


sequence.
• Use the key between the arrow keys to enter the first
number of the sequence using the alphanumeric keypad.

6. Press OK to return to "Instrument Setup".

7. The Sample ID is activated. Each Sample ID is automatically


numbered in ascending order after a measurement. The
number is shown in parentheses behind the Sample ID.

Note: To remove a Sample ID, highlight the ID and press Delete.

Note: A Sample ID can be entered or changed in measurement mode. In


the results screen, press Options>More>Instrument Setup. If a Sample
ID is already assigned, select the Sample ID symbol in the results screen.

26
Standard Operations

5.2.3 Date and time

1. Press Date & Time in the Instrument Setup.

2. The date and time are subdivided over a number of fields.


Press the appropriate field and use the arrow keys to change
the value.

3. Press OK to confirm. The instrument will return to


Instrument Setup.

5.2.4 Display and sound preferences

1. Press Display & Sound in the Instrument Setup.

The following options will be displayed:


• Display Contrast—Adjusts the display brightness to suit
lighting conditions.
• Screen touch—Activates//Deactivates a short beep each time
the screen is pressed (Default:off).
• Reading done—Activates/Deactivates a sound when a
reading is complete (Default: short beep every time a reading is
complete).
• Timer—Adjusts the length of the timer sound. Select Short or
Long. Long beeps are recommended for noisy environments.

2. Press OK to confirm. The instrument will return to


Instrument Setup.

5.2.5 Power Management


The DR 2700 can run on mains or battery power.
Note: The battery is not part of the standard scope of delivery.

1. Select Power Management in the ”Instrument Setup“ menu.

The battery symbol indicates the charge status of the battery


in %.

Note: The timer settings in the Power Management menu are only
active when the instrument is running on battery power.

27
Standard Operations

2. Select one of the options under Standby mode to set the


length of the idle period that can elapse before the instrument
switches to the Standby mode when running on battery power.

Note: In standby mode, the backlighting of the screen is switched off.


Touching the display causes the lighting to switch on again.

3. Select one of the options under Auto off to set the length of the
idle period that can elapse before the instrument automatically
switches off when running on battery power.

Note: After the instrument switches itself off automatically, you have to
press the push-button switch on the back of the instrument to start it
again.

28
Standard Operations

5.2.6 PC and printer


The instrument is provided with 2 USB interfaces, which are located
on the back of the instrument (see Figure 1 on page 11). These
interfaces can be used for exporting data and graphics to a printer,
updating data and for data communication to a personal computer.
These interfaces can be used for the connection of a USB stick or
an external USB keyboard.
Note: A USB hub may be used to connect several accessories at a time.

A USB memory stick is used to upgrade data and software, see


section 6.6.2 on page 80.
Important Note: A screened USB cable must not be longer than
3 m!

Table 3 USB connector


USB Interfaces Description
This USB interface is only intended to connect the instrument to a PC (with installation of the
USB (Type B)
HACH Data Trans Software).
USB (Type A) This USB port can be used to connect a printer, a USB memory stick or a keyboard.

1. Press PC & Printer in the Instrument Setup.

A list with information about the connections opens.

5.2.6.1 Printer setup

For reasons of compatibility, the printer language must be


HP PCL 3.

2. Press Printer.

3. Press Setup to display the Printer Setup screen.

29
Standard Operations

Printer Setup:
• Resolution: Print quality
• Paper: Paper size
Note: If an optional Thermal Printer is connected, the function "Auto Send"
on/off is available.

4. Select Auto-Send: On to send all measured data automatically


to the Thermal printer.

Note: The option Auto-Send is not available for any other printer (e.g. ink
jet printer).

5. Press Resolution to select the print quality.

Select between

• 100 dpi
• 150 dpi and
• 300 dpi

6. Press OK to confirm.

Note: Press OK again to return to the PC & Printer menu.

30
Standard Operations

7. Press Paper to select the paper size.

Select between

• Letter
• Legal
• Executive
• A4

8. Press OK to confirm.

Note: Press OK again to return to the PC & Printer menu.

5.2.6.2 Print data

1. Press Recall Data in the Main Menu.

2. Select the data source, where the data to be printed are stored.

3. A list is displayed. Data can be filtered. For more information


see section 5.3.1.2 on page 35.

4. Press the PC & Printer icon to send the data (table, curve)
immediately to the printer.

5. Highlight Single point or Filtered data or All data and press


OK to confirm.

Sending Data... is displayed until the data have been printed.

5.2.6.3 HACH Data Trans


The optional HACH Data Trans software must be installed on the
PC for the subsequent to work for measurement data.

1. Press PC & Printer in the Instrument Setup.

2. Select PC.

3. Press Setup to display the PC Setup screen.

For further installation instructions, refer to the HACH Data


Trans user manual.

31
Standard Operations

4. Select Auto-Send: On to send all measured data automatically


to the PC.

Note: If Auto-Send: Off is selected, the PC & Printer icon must be


pressed, in order to send data to the PC.

Note: The remote function is only for monitoring the data transfer.

5.2.7 Password
The Password menu contains a variety of security settings to
control access to various functions. For example, prevent
unauthorized changes to stored programs or instrument
configurations.

1. Press Password in the Instrument Setup menu.

2. In order to highlight the Security List assign a password. Press


Set Password.

3. Use the alphanumeric keypad to enter a new Password (up to


10 characters each) and press OK to confirm.

The access to the Security List is activated.

32
Standard Operations

4. Press Security List to lock various functions for unauthorized


users.

5. Highlight the desired functions to control.

6. Confirm the Security List with OK to return to the Password


menu.

7. Press On to highlight the new settings of the Security List.

8. Enter the new Password again to confirm.

9. Press OK to return to Instrument Setup.

Note: The alphanumeric keypad to the Password inquiry appears when a


user tries to reach a locked setting.

5.2.7.1 Password deactivation

1. Press Password in the Instrument Setup.

2. Use the alphanumeric keypad to enter the former Password


and press OK to confirm.

33
Standard Operations

3. Press Off to deactivate the settings of the Security List.

4. Press OK to return to Instrument Setup.

Note: Use this function to delete the former Password or to enter a new
one.

34
Standard Operations

5.3 Store, recall, send and delete data


5.3.1 The data log
The Data Log will store up to 200 readings taken in the modes:
Stored Programs, User Programs, Favorite Programs, Single
Wavelength and Multi Wavelength. A complete record of the
analysis is stored, including the Date, Time, Results, Sample ID,
and Operator ID.

5.3.1.1 Auto/manual data storage


The data storage parameter indicates whether data are to be stored
automatically or manually (in which case the user has to decide
which data to store).

1. Press Store: On/Off in the Options menu.

• With the Store On setting, all measurement data are stored


automatically.
• With the Store: Off setting, no measurement data are
stored. However, this setting can be changed to Store: On
in the result display through configuration. The reading
currently shown in the display is then stored.
Note: When the instrument's memory (data log) is full, the oldest data are
automatically deleted allowing the new data to be stored.

5.3.1.2 Recall stored data from the data log

1. Press Recall Data in the Main Menu.

2. Press Data Log.

A listing of the stored data is displayed.

3. Press Filter: On/Off.

35
Standard Operations

4. The function Filter Settings is used to search for specific


items.

1. Highlight On to turn on the filters to select data by

• Sample ID
• Operator ID
• Start Date
• Parameter

or any combination of the four.

2. Press OK to confirm the selection. The chosen items are listed.

3. Press View Details to get more information.

5.3.1.3 Send data from the data log


Data is sent from the data log as CSV (Comma Separated Value)
files through a USB memory stick to a file named DATALOG. The
file can then be processed using a spreadsheet program. The file
name will be formatted as:
DLYear_Month_Day_Hour_Minute_Second. CSV.
To send data to a Printer, see section 5.2.6.2 on page 31.

1. Plug in the USB device (Figure 1 on page 11).

2. Press Recall Data from the Main Menu. Press Options and
then the PC & Printer icon.

3. Select the data to send to the memory stick and press OK.

Note: The number in parenthesis is the total number of data sets


assigned to this selection.

To send measurement data to a PC:


The optional HACH Data Trans software must be installed on the
PC, see section 5.2.6.3 on page 31.

36
Standard Operations

5.3.1.4 Delete stored data from the data log

1. Press Recall Data in the Main Menu.

2. Press Data Log>Options>Delete.

3. Highlight Single Point or Filtered data or All data and press


OK to confirm.

Note: The number in parentheses is the total number of data sets


assigned to this selection.

37
Standard Operations

5.4 Stored Programs


The instrument contains more than 130 programmed procedures.
They can be accessed through the Stored Programs menu.

5.4.1 Select a saved test/method; enter user-specific basic data

1. Press Stored Programs in the Main Menu to view an


alphabetical list of stored programs with program numbers.

The Stored Programs list will appear.

2. Highlight the required test.

Note: Select the program number by name or use the arrow keys to
scroll through the list quickly and highlight the program or press
Select by number to search for a specific program number. Use the
alphanumeric keypad to enter the test number and press OK.

3. Press Start to run the program. After a program is selected, the


screen for that parameter will appear.

Note: All corresponding data (wavelength, factors and constants) are


already preset.

4. Follow the chemical procedures described in the corresponding


Procedures Manual.

5.4.2 Stored program options

1. From the Main Menu, select Stored Programs. Select the


necessary method and press Start.

2. Press Options for Parameter Setup. Refer to Table 4 for stored


program descriptions.

Table 4 Stored programs options


Options Description

More For further Options

38
Standard Operations

Table 4 Stored programs options (continued)


Options Description
With the Store On setting, all measurement data are stored automatically. With the Store Off
Store Off/On
setting, no measurement data are stored.
% Trans/Conc/Abs To switch to % transmittance, concentration or absorbance readings

Send Data icon /


To send Data to a printer, computer or USB memory stick (Type A)
Send Data
This functions as a stopwatch. It helps to ensure that the steps of an analysis are correctly timed
(e.g. reaction times, wait times, etc., can be exactly specified). When the specified time has
Timer icon
elapsed, an acoustic signal is emitted. The use of the timer has no influence on the measurement
program.
A corrective dilution factor can be entered in order to account for certain properties.
The number entered at the dilution factor prompt will be multiplied by the result to compensate for
Dilution Factor Off/On the adjustment. For example, if the sample has been diluted by a factor of 2, enter 2. The default
setting of the dilution factor is turned off.
Note: When a dilution is in effect, the dilution icon will appear on the display.
This enables the accuracy of the measurements to be checked. The procedure for a test
Standard Addition
parameter contains a detailed explanation of how to use this function.
The procedure for a test parameter indicates whether a standard adjustment is necessary and, if
Standard Adjust
so, how to proceed.
Chemical Form Some of the stored tests/methods allow to select the chemical form and the measuring range.
Some of the stored tests/methods include the "Reagent Blank" function. This enables the reagent
blank value to be added to or subtracted from the subsequent readings. The reagent blank value
Reagent Blank shifts the calibration curve along the y-axis, without changing the shape or gradient of the curve.
The effect corresponds to a y-axis intercept of the calibration straight line. This is made clear by
the following equation: Concentration = [(Conc. factor) * Abs] – (reagent blank value).
Save as User Program To store the selected parameters as a User Program, see section 6.1 on page 47.

Recall Data Call up saved measurement data, see section 5.3 on page 35.

Instrument Setup Basic data of the instrument, see section 5.2 on page 25.

39
Standard Operations

5.4.3 Use of program timers


Some procedures do not require the use of timers. Other
procedures require several timers. These timers are
pre-programmed into each Stored Program, along with a
description of the activity to be performed during the timed period.

1. Press the Timer icon on the display.

2. Press OK to start the first timer.

The timer will count down on the screen.

3. To start the next timed activity for the Stored Program, press
the Timer icon and OK.

Note: Press Close to view the measurement screen while the timer is
running. The time will be shown left side bottom instead of the date.

Note: Press Cancel to stop the timer midway through the countdown.

Note: The Timer will beep when the end of the running time is
reached.

A general purpose timer is also available in many programs. When


the timer icon is visible, press the icon and select General Timer.
A new screen will appear. Enter the length of the timed interval and
press OK to start the timer. The timer will beep when the timed
interval ends.

40
Standard Operations

5.4.4 Set the dilution factor


The Dilution Factor function is used to calculate the original
concentration of a sample that has been diluted by a known ratio.
Dilution can be used to bring the sample concentration within the
test range.

1. Press Options>More…>Dilution Factor.

The number entered at the dilution factor prompt will be


multiplied by the result to compensate for the adjustment.

For example, if the sample has been diluted by a factor of 2,


enter 2. The default setting of the dilution factor is turned off.

2. Press OK to confirm. Press again OK.

3. Press Return to return to the result display.

4. Confirm ’Store present reading again?’ to save the current


measured value if necessary.

Note: When a dilution is in effect, the dilution icon will appear on the
display.

Note: If using undiluted samples, turn the dilution factor off again.

5.4.5 Run a standard adjust


The Standard Adjust function allows the calibration curve for a
stored program to be adjusted based on analysis of a known
standard solution. The Accuracy Check section of written
procedures often suggests a standard solution concentration for
this purpose.

41
Standard Operations

Read a standard before setting Standard Adjust to On.

1. Follow the entire procedure, using a known standard for the


sample.

2. After reading the concentration, press


Options>More>Standard Adjust.

3. If Standard Adjust is set to Off, turn it On.

The Current Reading will show the concentration. The box on


the right will show the default standard value for the test, as
mentioned in the procedure.

4. If the measurement used a standard concentration that is


different from the one displayed in the box, press the box on the
right to enter a different standard value and enter the new
value. Press OK to confirm.

5. Press Adjust to enable the Standard Adjust. The Standard


Adjust icon will appear.

Note: The adjustment must be within certain limits, which vary with
each program. The allowable percentage is shown after "Adjustment“.

Note: When a Standard Adjust is in effect, the Standard Adjust icon


will appear on the display.

5.4.6 Set the chemical form


Some Stored Programs allow a variety of chemical forms to
be selected.
Press the unit (e.g. mg/L) or the chemical representation of the
evaluation form (e.g. Al3+). A list of available evaluation forms is
displayed. Select the required form by pressing the corresponding
entry in the list.
Note: When the program is exited, the evaluation form reverts to the
standard setting.

An alternative way of changing the standard setting:

42
Standard Operations

1. Press Options>More>Chemical Form.

2. Select the Chemical Form.

Note: The stoichiometric conversion of the measurement result is


carried out automatically.

Note: The selected Chemical Form will appear on the display. Test
results will be calculated and displayed in this chemical form.

5.4.6.1 Change of the default setting of the chemical form

1. Insert the sample cell or blank (depending on the working


procedure) into the cell compartment.

2. In the result display, press Options>More>Chemical Form.

3. A list of available evaluation forms appears. Select the new


default setting.

4. Press Save as Default.

The current result and all further measurements will be displayed in


the new chemical form.

5.4.7 Run a reagent blank


Some of the stored tests/methods include the "Reagent Blank"
function. This enables the reagent blank value to be measured and
then taken into account in calculating the measurement result.

Measurement/analysis of a reagent blank:

1. Prepare the test/method in accordance with the (working)


procedure. Instead of a sample, deionized water is used to
determine the reagent blank value.

2. Select the test. If required by the (working) procedure, insert


the cell with deionized water into the cell compartment. Press
Zero.

3. Insert the prepared sample cell into the cell compartment.


Press Read. The result is displayed.

43
Standard Operations

4. Press Options>More>Reagent Blank.

5. Press On to highlight the Reagent Blank function.

6. The concentration shown on the key is the measured value of


the reagent blank. To use this value for more analyses of this
parameter, press OK.

7. To enter a previously recorded reagent blank value, press the


key and use the alphanumeric keypad.

8. Press OK.

Note: The Reagent Blank function is deactivated when the measurement


program is left. To use the same blank value later for other tests using the
same reagent lot, enter the value per step 7.

Note: The results calculated using the reagent blank value must lie within
the limits of the measuring range of the test/method.

Note: The reagent blank icon is shown in the result display (see arrow)
when the function is active.

5.4.8 Analysis of samples

1. Press Stored Programs and select a program.

2. Insert the blank cell into the sample cell holder.

3. Press Zero.

44
Standard Operations

4. Remove the blank cell and insert sample cell into the cell
compartment.

5. Press Read. The result will be displayed.

6. For data storage, see section 5.3.1 on page 35.

5.4.9 Add stored programs to the favorite programs list


The Favorites menu simplifies test selection by creating a list of the
most frequently used tests from the Stored Programs and
User Programs.

1. Press Stored Programs in the Main Menu. The Stored


Programs list will appear.

2. Highlight the selection by pressing it or Select by Number to


search for the program by number.

3. Press Add to Favorites and press OK to confirm.

The program can now be selected from Favorite Programs


menu in the Main Menu.

45
Standard Operations

46
Section 6 Advanced Operations

6.1 User Programs


User programs provide the opportunity to complete "made to
measure" analysis.
The User Programs database is empty when the instrument leaves
the factory and is used to accommodate programs created by users
specific needs. Here are a few examples of entries:
• Programming of user-created procedures. The analysis
procedure must be developed first, before it can be
programmed. The user must define or determine the program
sequences, calculation formulas, measurement wavelengths,
factors, measuring range limits, etc.
• Modified tests
• Assignment of user programs to the favorites menu for
frequently used tests.
• Creation of a specific selection of methods and tests.
Press User Programs in the Main Menu and then
Program Options. The Program Options menu contains several
input and editing options (Table 5):

Table 5 Program options user programs


Options Description
Select New to program a new user program.
New Note: The first time Program Options is selected, only the New option is available. The other
options remain inactive (grey) until the first program has been created.
Add to favorites Select Add to favorites to add an existing user program to the list of frequently used programs.

Edit Select Edit to modify an existing program


Select Delete to remove a program from the list of user programs. The program will be
Delete
simultaneously deleted from the Favorites list.

6.1.1 Program a user method


All input steps and their significance and options are explained in
the following sections.

1. Select New in the Program Options menu.

47
Advanced Operations

Program Number:
Specific test number, with which the program can subsequently be
called up from the selection list in the User Programs menu or the
Favorites menu.

2. Use the alphanumeric keypad to enter a program number


between 950 and 959. The lowest available number appears
automatically.

3. Press OK.

Note: If the program number is already assigned to another user


program, a message appears, asking whether the existing program
should be replaced. Press OK to overwrite the existing program.

Program Name:

4. Use the alphanumeric keypad to enter a program name. The


name can be a maximum of 28 characters long.

5. Press Back to go back to the previous program point or press


Next to continue with the input of the program data.

Program Type:

6. Select the required option (Table 6) and press Next.

7. If the Single Wavelength (section 6.1.1.1 on page 49) or Multi


Wavelength (section 6.1.1.2 on page 50) is selected, define the
units, wavelength, absorbance formula, wavelength λx,
concentration factor Kx, concentration resolution, chemical
form and calibration equation.
More information on Free Programming parameters see
section 6.1.2 on page 58.

Table 6 Program descriptions


Program Type Description

Single Wavelength Measurements at a defined wavelength


In the Multi Wavelength mode, absorbance values can be measured at up to four wavelengths
Multi Wavelength
and the results can be mathematically processed to obtain sums, differences and relationships.
This is an advanced form of programming for original user-developed methods. In Free
Free Programming Programming, the user defines the measurement process, variables and calculations involved in
obtaining a reading.

48
Advanced Operations

6.1.1.1 Single wavelength settings


If the Single Wavelength mode is selected, the following
parameters can be defined:

Units:
Select the required unit from the list and press Next.
Note: Units of measure not included in this list can be added in the edit
program under Program Options, Edit. Select Units, Edit and then New.

Wavelength (single wavelength program type):


Use the alphanumeric keypad to enter the measurement
wavelength. The entered wavelength must be in the range from
400–900 nm.
Press Next to proceed.

Concentration resolution (number of decimal places)


Select the required number of decimal places from the displayed
list and press Next.

49
Advanced Operations

Chemical form:
Enter the chemical formula used in the display to represent the
analysis parameter.
Use the alphanumeric keypad to enter the chemical form and press
Next to enter Calibration settings.

6.1.1.2 Multi wavelength settings


If the Multi Wavelength mode is selected, the following parameters
can be defined:

Units:
Select the required unit from the list and press Next.
Note: Units of measure not included in this list can be added in the edit
program under Program Options, Edit. Select Units, Edit and then New.

Absorbance formula (multi-wavelength program type):


The Absorbance Formula menu is used to define the wavelengths
and the coefficients used in the formula. The absorbance formula
defines the calculation for the multi-wavelength measurement.
Press the appropriate key to edit the input.
Press the Formula key.
In the displayed list, select the formula for the program and press
OK to confirm.

50
Advanced Operations

List of available absorbance formulas


A1 is the absorbance at wavelength 1,
A2 is the absorbance at wavelength 2 and so on
K1 is the factor at wavelength 1,
K2 is the factor at wavelength 2 and so on
If a subtraction has to be completed, the factors can be entered
with a minus sign.

Wavelength λx:
Press a λx key and use the alphanumeric keypad to enter a
wavelength. Press another λx key and enter the next wavelength. If
necessary, repeat until all the wavelengths for the formula have
been entered. The wavelengths must be in the range from
400–900 nm. Press OK.

Concentration Factor Kx
Multiplication factor for converting absorbance values into
concentration values.
Press a factor key and use the alphanumeric keypad to enter a
factor. If the formula includes more than one factor, press another
factor key and enter another factor and repeat until all the factors
have been entered. Press OK. When all the relevant data have
been entered, press Next.
Note: Up to 5 digits can be entered, including a maximum of 4 decimal
places to the right of the decimal.

Concentration resolution (number of decimal places)


Select the required number of decimal places from the displayed
list and press Next.

51
Advanced Operations

Chemical form:
Enter the chemical formula used in the display to represent the
analysis parameter.
Use the alphanumeric keypad to enter the chemical form and press
Next to enter Calibration settings.

6.1.1.3 Calibration settings for single and multi wavelength mode


A method is calibrated by determining the absorbance values of
several standard solutions of known concentration.
There are three ways to create and store a calibration curve.
Instructions for each method follows (Table 7).

Table 7 Calibration settings


Mode Descriptions
A calibration table is created by entering the concentration values and the absorbance values of
Enter values the analyte solution. The absorbance values are plotted versus standard concentrations and the
calibration curve is displayed as a graph (page 52).
A calibration table is created by entering the concentration values of the standard solutions and
Read Standards then measuring the absorbance of the analyte solutions. The absorbance values are plotted
versus standard concentrations and the calibration curve is displayed as a graph (page 54).
If the calibration curve can be determined from the mathematical relationship between
concentration and absorbance by linear regression, etc., the corresponding formula can be
Enter Formula
selected (linear, 2nd or 3rd order polynomial) from a list and the appropriate factors can be
entered (page 55).

Calibration by entering calibration values


Enter concentration/absorbance

1. Select the Enter Values and press Next.

52
Advanced Operations

2. To enter the standard concentrations and corresponding


absorbance values in the displayed table, press the "+" symbol.
Use the alphanumeric keypad to enter the values.

Press OK and enter the corresponding absorbance value.


Press OK.

The entered data are displayed in the table. Repeat the


sequence for each data point to enter it.

3. To change a value in the table, highlight the appropriate line,


press the unit key (e.g. mg/L) or Abs and enter the changed
value via the alphanumeric keypad.

4. When the data have all been entered, press Graph.

Note: The correlation coefficient (r2) is shown on the left below the
axes.

5. The linear equation corresponds to the standard setting. Press


Next Curve to display the polynomial 2nd order curve. Press
Next Curve again, to display the polynomial 3rd order curve.

6. Press Force 0 to change the setting from Off to On. The curve
now passes through the origin of the coordinate system.

Note: This may have an adverse effect on the correlation coefficient


(r2).

7. Press Table to display the table again.

8. When the table has been completed and the curve type has
been chosen, press Done when the graph is displayed or Exit
when the table is displayed. Go to section 6.1.1.4 on page 56.

53
Advanced Operations

Calibration by reading standards

1. Press Read Standards and press Next.

2. To enter the standard concentrations in the displayed table,


press the "+" symbol. Use the alphanumeric keypad to enter
the standard concentration. Press OK.

3. Press the "+" symbol again (see arrow) and enter the next
standard concentration. Repeat this sequence until all standard
conentrations (maximum of 24 solutions) have been entered.

4. Highlight the line with the appropriate concentration and insert


the cell with the corresponding standard solution.

5. Insert the zero solution into the cell compartment. Press Zero.

6. Insert the first standard solution into the cell compartment.


Press Read.

Insert the second standard solution into the cell compartment.


Press Read.

Repeat this sequence until all the standard solutions have been
measured (maximum of 24 solutions).

The entered and measured data are displayed in the table.


Note: To delete a standard concentration, highlight the appropriate line and
press the Delete icon.

The timer icon shown in the display helps to ensure, when


necessary, that the steps of an analysis are correctly timed (e.g.
reaction times, wait times, etc., can be exactly specified). When the
specified time has elapsed, an acoustic signal is emitted. The use
of the timer has no influence on the measurement program.

7. When the data have all been entered and the measurements
have all been completed, press Graph.

8. The linear curve corresponds to the standard setting. Press


Next Curve to display the polynomial 2nd order curve.Press
Next Curve again to display the polynomial 3rd order curve.

54
Advanced Operations

9. Press Force 0 to change the setting from Off to On. The curve
then passes through the origin of the coordinate system.

Note: This may have an adverse effect on the correlation coefficient


(r2).

10. Press Table to display the table again.

11. When the table has been completed and the curve type has
been chosen, press Done when the graph is displayed or Exit
when the table is displayed. Go to section 6.1.1.4 on page 56.

Calibration by entering the formula

1. Press Enter Formula and press Next.

2. Press the formula key.

A list of available formulas (linear and 2nd and 3rd order


polynomial) is displayed. Up to 4 coefficients can be entered,
depending on the selected formula. Press the required formula.

3. Depending on the selected formula, the required coefficients (a,


b, c...) are displayed. Press the coefficient keys and enter the
corresponding values via the alphanumeric keypad. After each
entry, press OK to confirm.

Note: The coefficients can have 5 digits and can have a positive or a
negative sign.

55
Advanced Operations

6.1.1.4 Store a user program

The input of the basic data is complete. An overview of the variable


program data is displayed.

1. To enter more specifications or change existing ones, highlight


the appropriate line and press Edit.

2. Select Store to save the user program.

3. Press the PC & Printer icon to send the program data to a


printer or to a USB memory stick (connect the USB memory
stick to the USB interface first).

Note: The test data will be formatted in the preinstalled PrgData folder
as a .csv and as a .lst file.

4. To transfer the program data from one instrument to another


create a new folder on the USB memory stick named dbhlc
and copy the .lst files into this folder. (see section 6.6.2 on
page 80).

6.1.1.5 Additional user-defined parameters and functions


In addition to the previously defined basic data, additional
parameters and functions can be defined for user programs:
• measuring range upper and lower limits
• timer functions
• chemical forms

Upper and lower limits of the measuring range


It is possible to enter a maximum (upper) and minimum (lower)
measurement value. An error message is displayed if a reading is
above the upper limit or below the lower limit.

1. Highlight the appropriate line in the overview of the program


data and press Edit.

2. Set On and press the 0.000 key to enter the measuring range
limit. Confirm the entry by pressing OK.

56
Advanced Operations

Timer 1 / Timer 2 / Timer 3 / Timer 4:


This function can define time intervals for up to four timers. Timer
designations such as Shake, Wait and Swirl can be assigned.

1. Highlight the appropriate line in the overview of the program


data and press Edit.

2. The timers are activated or deactivated with the check boxes in


the left part of the display. In the next column, a selection can
be made from a list of names that designate the corresponding
work step. In the third column, the times for each timer are
entered (in mm:ss).

Chemical form 2 / chemical form 3 / chemical form 4:


If a Chemical Form 1 has been defined, up to three additional
alternative forms can be entered here.

1. Highlight the appropriate line in the overview of the program


data and press Edit.

2. The chemical forms are activated or deactivated with the check


boxes in the left part of the display.

3. Press the left key to enter another chemical form with the
alphanumeric keypad and press OK to confirm. Press the right
key to enter the conversion factor to calculate the concentration
of the additional chemical form from the concentration of
Chemical Form 1 and press OK to confirm.

4. Press Store to save the program data. Press Cancel to return


to the Main Menu.

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6.1.2 Free programming program type


Free Programming is an advanced option for entering original
user-developed methods. When the Free Programming option is
selected, an overview of the specifications of the programmed test
is displayed. Each input option can be modified to develop the user
method. Refer to Table 8 for more information. To modify an input
option, select the appropriate line and press Edit.
Important Note: Perform steps 1–6 of Programming a New User
Method (section 6.1.1 on page 47) before proceeding with Free
Programming.

Highlight the line containing the program point that is to be edited or


defined and press Edit.

Table 8 Definitions of the program points


Program point Description

Name Name of the analysis parameter

Version An abbreviation or version number assigned by the user is entered here.


Exact definition of the test: the number of wavelengths at which measurements are made, the
Measurement Process number of absorbance measurements needed, the keys to be used, any waiting periods between
measurements, etc.
Formula Definition of the formulas with which the test result is calculated.
The number of variables shown in the display depends on the definition of the measurement
Variables process and the formulas. Input of the numerical values of the wavelengths, factors, constants,
etc.
Used to enter abbreviations and defined times for up to four timers. Highlight the appropriate line
Timer 1, Timer 2, and press Edit. The timers are activated or deactivated with the control boxes on the left of the
Timer 3, Timer 4 display. In the next column, a selection can be made from a list of names that describe the
corresponding work step. In the third column, the times for each active timer are entered.

6.1.2.1 Measurement process


The measurement process defines the handling and the
measurements of the test:
• At which and how many wavelengths should measurements be
completed
• How many absorbance measurements must be completed?
• When should the zero measurement and the sample
measurement be completed?
• Are waiting times necessary between measurements?

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• Should individual program sequences be repeated?


The elements of a measuring sequence, such as zero and sample
measurements and the timer(s) (reaction times, waiting times, etc.)
are individually defined.

6.1.2.2 Enter a new element of a measuring sequence


Important Note: Each component of the measurement process
must be entered in the order in which it will be completed.

1. Highlight the Measurement Process line in the data overview


and press Edit.

2. Press Edit again and then New.

Content and definition of the keys

[Z] key / Zeroing

1. Press the [Z] key to program a zero measurement. Confirm


with OK.

2. Press New and then Zeroing... and use the alphanumeric


keypad to enter the wavelength at which the zero measurement
is to be completed. Press OK and confirm the input by pressing
OK again.

3. If zero measurements are to be carried out at a number of


wavelengths, repeat the above two steps for each wavelength.

Note: The entered measurement sequence is displayed.

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Advanced Operations

Process Timer key

1. Press the Process Timer key to enter any waiting, reaction or


handling times that have to be taken into account. Use the
alphanumeric keypad to enter the time. Press OK and confirm
the input by pressing OK again.

Note: This time is integrated into the measurement process.

Note: The entered measurement sequence is displayed.

[R] key / Reading...

1. Press the [R] key to program a measurement of the substance


that is to be analyzed. Confirm with OK.

2. Press New and then Reading... and use the alphanumeric


keypad to enter the wavelength at which the measurement is to
be completed. Press OK and confirm the input by pressing OK
again.

3. If measurements are to be completed at a number of


wavelengths, repeat the above two steps for each wavelength.

Note: The entered measurement sequence is displayed.

{ } key
Elements of the measurement sequence that are to be repeated
are placed in brackets.
The left bracket "{"marks the start of the sequence that is to be
repeated and the right bracket "}" marks the end.
Note: The key showing the right bracket remains inactive until a left bracket
is entered.

1. Press {.

2. Press the key that defines the sequence that is to be repeated:


[Z] or [R]. Confirm with OK.

3. Press New and then press Zeroing... or Reading... and use


the alphanumeric keypad to enter the wavelength at which the
measurement should be completed. Press OK and confirm the
input by pressing OK again.

4. Press } to end the sequence.

Note: If an action such as a zero measurement recurs at different


stages of a measurement sequence, the series of actions is numbered
sequentially (e.g. Z1, Z2, etc.).

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Deleting an element of a measuring sequence


Select the appropriate line and press Delete. The element is
deleted.

Inserting an element of a measuring sequence


Select the line in the measuring sequence where the insertion is be
made and press New.
A new element can be entered at the selected position.
When the input is complete, press OK in the "Measurement
Process" display. The data overview is then displayed.

6.1.2.3 Enter the calibration formula (evaluation formula)


The calibration formula (evaluation formula) defines the calculation
and display of intermediate and final results. The previously defined
elements of the measuring sequence are the basis for calculating
the concentrations.

Enter calibration formula C1

1. Highlight the Formula line in the data overview and press Edit.

2. Highlight the line C1: Off and press Edit.

3. Select C1: Off again and press Edit. The display changes to
C1: On.

4. Highlight the next line C1 = to define the formula and press


Edit.

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Refer to Table 9 for detailed information on the Edit


formula keys.
Note: The evaluation formula is built up successively in the display in
accordance with the input.

Note: The arrow key deletes the most recently entered element of the
formula.

Table 9 Edit formula key descriptions


Screen Key Description

Press the Abs/Variables key to select, from the


displayed list, the required element of the defined
Abs/Variables measuring sequence and therefore the corresponding
measurement wavelength, so that this can be taken into
account in the formula.

New Number Press New Number to enter a new factor or constant.

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Table 9 Edit formula key descriptions (continued)


Screen Key Description
Press +– ÷x, to enter a mathematical operation.
Select the operation and press OK to confirm.
The available choice of mathematical operations
depends on the defined formula.
This means that functions such as "( )" or "ln"/"log" etc.
are only active if a term in parentheses or the calculation
of a logarithm is mathematically permissible in the
defined formula (this also applies to the basic
mathematical operations).
The following mathematical operations are available:
+– ÷x
• + (Addition)
• – (Subtraction)
• ÷ (Division)
• x (Multiplication)
• ^ (Exponent)
• Ln (Natural logarithm)
• Log (Common logarithm)

Press >=< to include logic statements/links/conditions in


the formula. The following functions are available:
= (Equal to), < (Less than), > (Greater than), <= (Less
than or equal to), >= (Greater than or equal to), IF,
THEN, ELSE
>=< When the evaluation formula C1 has been entered
completely, press OK to confirm. Press OK again to
return to the Formula display.
When the formula C1 has been entered and confirmed,
the parameter name, upper and lower limits of the
measuring range and display result (yes, no) can be
entered.

Enter the next calibration formula (C2 or Cn)

1. Highlight C2: Off and press Edit.

2. Select C2: Off again and press Edit. The display switches to
C2: On.

3. Highlight the next line C2 = to define the formula and press


Edit.

In addition to the keys described in Table 9, only one other function


is available:

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Advanced Operations

Select Conc. key


If an already defined formula, in this case C1, is to be taken into
account in the formula for C2, press Select conc.
Enter the number of the formula (e.g. 1 for C1) and press OK to
confirm.
Cn can now be linked with a mathematical operation.
Note: The Cn concentrations that are to be calculated are numbered in
sequence: C1, C2, C3, etc.

Note: When the first Cn formula has been defined, the Formula list is
automatically extended by Cn+1.

6.1.2.4 Enter variables

1. Highlight the Variables line in the data overview and press


Edit.

2. Select the variable to be edited, press Edit and use the


alphanumeric keypad to enter the data specified in the working
procedure (for F1, F2, λ1, U1 etc.). Press OK to confirm each
entry.

Abbreviation of Variables:
F1: Factor 1
F2: Factor 2
λ1: Wavelength 1
U1: Conversion Factor 1 for the first chemical form
U2: Conversion Factor 2 for the further chemical form etc.

6.1.2.5 Save a free programming user program

1. Press Store to save the entered data. The data can be stored
under any data point (Measurement sequence, Formula, Timer,
etc.).

2. Press the PC & Printer icon to send the program data to a


printer or to a USB memory stick (connect the USB memory
stick to the USB interface first).

Note: The test data will be formatted in the preinstalled PrgData folder
as a .csv and as a .lst file.

3. To transfer the program data from one instrument to another


create a new folder on the USB memory stick named dbhlc
and copy the .lst files into this folder (see section 6.6.2 on
page 80).

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Advanced Operations

6.1.3 Select a user program

1. Press User Programs in the Main Menu to view an


alphabetical list of user programs with program numbers.

The User Programs list will appear.

Note: Use the scroll bar to scroll through the list quickly.

Note: Highlight the selection by pressing it or press Select by


Number to search for the program by number.

2. Press Start to run the program.

6.1.4 Add, edit and delete user programs from the favorites list
The most frequently used tests/methods in the User Program menu
can also be added to the list of favorites to simplify their selection.

1. Press User Programs in the Main Menu.

The User Programs list will appear.

2. Highlight the selection by pressing it or press Select by


Number to search for the program by number.

Note: Use the scroll bar to scroll through the list quickly. Use the
alphanumeric keypad to enter the test number (program number) and
press OK to confirm.

3. Press Program Options.

4. Press Add to Favorites, Edit or Delete and press OK to


confirm.

Note: If the stored program is deleted in User Programs, it will also be


deleted in Favorites Programs.

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Advanced Operations

6.1.4.1 Add to Favorites

1. Press Add to Favorites and press OK to confirm.

The program is added to the Favorites.

6.1.4.2 Edit

1. Press Edit and press OK to confirm.

An overview of the specifications of the programmed test is


displayed. More information about the input options is provided
in the section 6.1.2 on page 58.

6.1.4.3 Delete

1. Press Delete and press OK to confirm.

The program is deleted from the list of User Programs.

Note: If the stored program is deleted in User Programs, it will also be


deleted in Favorites Programs.

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Advanced Operations

6.2 Favorite Programs


The most frequently used tests/methods in the Stored Programs
menu and the User Programs menu can also be added to the list
of favorites to simplify their selection.
To add Stored Programs and/or User Programs to the favorites
list or the favorite programs, see section 6.1.4 on page 65.

6.2.1 Recall a favorite program

1. Press Favorite Programs in the Main Menu.

The Favorite Programs list will appear.

2. Highlight the selection by pressing it.

Note: Use the scroll bar to scroll through the list quickly.

Note: Press Select by Number to search for the program by number.


Use the alphanumeric keypad to enter the test number (program
number) and confirm the input by pressing OK.

3. Press Start.

6.2.2 Delete a favorite program

1. Press Favorite Programs in the Main Menu.

The Favorite Programs list will appear.

2. Highlight the selection by pressing it.

Note: Use the scroll bar to scroll through the list quickly.

Note: Press Select by Number to search for the program by number.


Use the alphanumeric keypad to enter the test number (program
number) and confirm the input by pressing OK.

3. Press Remove Program and press OK to confirm.

Note: If a Favorite Programs is deleted, it will stay in the User


Programs or Stored Programs.

Note: If the stored program is deleted in User Programs, it will also be


deleted in Favorites Programs.

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6.3 Standard Addition – monitoring/checking results


The accuracy of measured values (their correspondence with the
actual concentration of the analyte in the sample) and their
precision (correspondence of the measurement results obtained
from several samples containing the same concentration of the test
analyte) can be determined or improved using the standard addition
method.
This method (also referred to as spiking) serves to identify
sample-specific interference factors, e.g. substances in the sample
that falsify the analysis (sample matrix effect), a defective
measuring instrument or contaminated reagents.

Method:
A defined amount (concentration) of a standard solution of the test
substance is added to the sample. The detection rate should be
close to 100%.

Measured value after a standard addition


Detection rate = -------------------------------------------------------------------------------------------------------------
Expected value after a standard addition

Detection rate Conclusion


Probability that the measurement results are correct
100%
is high.
Assumption: The analysis was falsified by
substances in the sample (sample matrix effect)
Test to determine whether a sample matrix effect
< 100%
is present:
Use distilled water instead of the sample. Add
standard solution as described in the procedure.
Detection rate Conclusion
Ions in the sample are
interfering with the
100%
analysis, causing false
results to be obtained.
No interfering ions -
≠ 100% consider other
interference factors.

Measures to identify other interference factors:

Checklist:

1. Check if the procedure is completed correctly:

a. Are the reagents added in the correct order?

b. Is enough time allowed for color development?

c. Is the correct glassware in use?

d. Is the glassware clean?

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e. Does the test require the sample to be at a certain


temperature?

f. Was the pH of the sample in the correct range?

g. Is the pipette volume correct?

2. Check the used reagents by repeating the standard addition


procedure with freshly prepared reagents.

Detection rate Conclusion


The originally used reagents were defective.
Check the standard solution:
100%
Repeat the standard addition procedure with a
freshly prepared standard solution.
Detection rate Conclusion
The originally used
100% standard solution was
defective.

If none of these measures resolves the problem, please contact the


manufacturer or a sales representative.

6.3.1 Complete a standard addition


Carry out the standard addition in accordance with the
corresponding procedure.
There are two different methods:

Peak volume (Standard addition):


Defined volumes of a standard solution are added step by step to
an already analyzed sample. The sample is measured again after
each addition.

Sample volume:
A defined volume of a standard solution of known concentration is
added to the volume of sample specified in the procedure and the
sample is measured after each addition. In most cases three
different standard solutions are prepared and the procedure is
repeated for each of them.
Note: The units and chemical forms used for the sample are used for the
standard solutions. Be careful to ensure that to use the correct units for
subsequent entries.

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Peak volume/sample volume methods

1. Select Stored Programs in the main menu. Select the required


program.

2. Press Start.

3. Analyze a sample without added standard solution in


accordance with the instructions in the Procedures Manual.
When the measurement is complete, leave the sample cell in
the sample cell holder.

4. Press Options>More>Standard Addition.

An overview of the data of the standard addition procedure is


displayed.

5. Press OK to accept the standard values for standard


concentration, sample volume (total) and standard addition
volume. Press Edit to change any of these values.

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6. Press the key of the value to change it. Use the alphanumeric
keypad to change the value. Press OK to confirm.

7. Press the keys to enter the standard addition volumes. Use the
alphanumeric keypad to enter the new data and press OK.

Description of the table of readings


• The first column shows the standard addition volume. 0 mL
stands for a sample containing no added standard.
• The second column shows the reading of the samples with and
without added standard.
• The third column shows the detection rate of the added
standard.
Note: The black highlighted line is active.

8. The reading of the sample in the instrument, without added


standard, is automatically shown under 0 mL.

9. Prepare the standard addition solution as described in the


procedure.

10. Use the arrow keys to select the first standard addition volume
in the table and insert the cell with the corresponding volume of
added standard into the cell compartment. Press Read.

Repeat the procedure from step 8 with all the other standard
addition solutions.

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11. After all the standard addition solutions have been measured,
press Graph.

The regression line through the standard addition data points is


displayed.

The correlation coefficient r2 indicates how close the data


points are to the line.

If the correlation coefficient = 1, the curve is linear.

The concentration shown above the curve is the estimated


concentration of the sample without the added standard.

Note: In the curve menu, the name on the Curve key switches to
Table. Press Table to display all the data in the table again.

12. Press Ideal line to display the relationship between the added
standard solutions and the ideal line (detection rate 100%).

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6.4 Single Wavelength (absorbance, concentration and transmittance


measurements)
The Single Wavelength mode can be used in three ways. For
sample measurements at a single wavelength, the instrument can
be programmed to measure the absorbance, % transmittance or
concentration of the analyte.
Absorbance measures the amount of light absorbed by the sample,
in units of absorbance.
% transmittance measures the percent of the original light that
passes through the sample and reaches the detector.
Turn the concentration factor on to select a specific multiplier for
converting absorbance readings to concentration. In a graph of
concentration versus the absorbance, the concentration factor is
the slope of the line.

6.4.1 Set up single wavelength mode


Press Single Wavelength in the Main Menu. Press Options for
Parameter Setup.

Table 10 Single wavelength setup options


Options Description

More For further Options


With the Store On setting, all measurement data are stored automatically. With the Store Off
Store Off/On
setting, no measurement data are stored.
% Trans/Abs To switch to % transmittance, concentration or absorbance readings
To enter the measurement wavelength. Use the alphanumeric keypad to enter the measurement
λ Wavelength
wavelength. The entered wavelength must be in the range from 400–900 nm.
This functions as a stopwatch. It helps to ensure that the steps of an analysis are correctly timed
(e.g. reaction times, wait times, etc., can be exactly specified). When the specified time has
Timer icon
elapsed, an acoustic signal is emitted. The use of the timer has no influence on the measurement
program.
Concentration Factor Multiplication factor for converting absorbance values into concentration values.

Concentration
To select the position of the decimal point in the calculated concentration readings.
Resolution

Save as User Program To store the selected parameters as a User Program, see section 6.1 on page 47

Recall Data Call up saved measurement data, see section 5.3 on page 35.

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Table 10 Single wavelength setup options (continued)


Options Description

Instrument Setup Basic data of the instrument, see section 5.2 on page 25.

Concentration factor:

1. Press Concentration Factor: Off in the Options menu. Press


On to highlight this feature.

2. Press the ”Factor“ key and use the alphanumeric keypad to


enter the factor by which absorbance readings are to be
multiplied. Press the ”Unit“ key to select the units for
concentration measurements or to create a new unit.

3. Press OK to confirm.

Concentration resolution:

1. Press Concentration Resolution in the Options menu.

2. Select the resolution and press OK to confirm.

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6.4.2 Take single wavelength measurements

1. Insert the blank cell into the sample cell holder. Press Zero.

Note: The Read key is only active after the zero measurement has
been completed.

2. Insert the sample cell into the sample cell holder. Press Read.

3. For data storage, see section 5.3.1 on page 35.

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6.5 Multi-Wavelength mode – measurements at more than one wavelength


In the multi-wavelength mode, absorbance values can be
measured at up to four wavelengths and the results can be
mathematically processed to obtain sums, differences and
relationships.
Absorbance measures the amount of light absorbed by the sample,
in units of absorbance.
% Transmittance measures the percent of the original light that
passes through the sample and reaches the detector.
Turning on the concentration factor allows selection of a specific
multiplier for converting absorbance readings to concentration. In a
graph of concentration versus the absorbance, the concentration
factor is the slope of the line. Concentration is calculated using a
single factor for each wavelength, which is input by the user.

6.5.1 Set the reading mode at different wavelengths


Press Multi Wavelength in the Main Menu. Press Options for
Parameter Setup.

Table 11 Multi-wavelength setup options


Options Description

More For further Options


With the Store On setting, all measurement data are stored automatically. With the Store Off
Store Off/On
setting, no measurement data are stored.
% Trans/Abs To switch to % transmittance, concentration or absorbance readings
To enter the measurement wavelength. Use the alphanumeric keypad to enter the measurement
λ Wavelength
wavelength. The entered wavelength must be in the range from 400–900 nm.
This functions as a stopwatch. It helps to ensure that the steps of an analysis are correctly timed
(e.g. reaction times, wait times, etc., can be exactly specified). When the specified time has
Timer icon
elapsed, an acoustic signal is emitted. The use of the timer has no influence on the measurement
program.
Concentration Factor Multiplication factor for converting absorbance values into concentration values.

Concentration
To select the position of the decimal point in the calculated concentration readings.
Resolution

Absorbance Formula Calculation basis for evaluating samples

Save as User Program To store the selected parameters as a User Program, see section 6.1 on page 47

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Table 11 Multi-wavelength setup options (continued)


Options Description

Recall Data Call up saved measurement data, see section 5.3 on page 35.

Instrument Setup Basic data of the instrument, see section 5.2 on page 25.

λ / Absorbance formula:

1. Press Absorbance Formula.

2. The formula selected in the top key determines the number of


wavelength and coefficent keys that will appear below. To
change the absorbance formula, press the top key, select a
formula from the displayed list and press OK. When a new
formula is selected, the number of variables below changes to
match.

The following formulas are available:

K1A1+K2A2
K1A1+K2A2+K3A3
K1A1+K2A2+K3A3+K4A4
K1A1/K2A2
(K 1 A 1 + K 2 A 2 ) / K 3 A 3
(K 1 A 1 + K 2 A 2 ) / (K 3 A 3 + K 4 A 4 )

A 1 refers to the absorbance at wavelength 1


A 2 refers to the absorbance at wavelength 2, etc.
K 1 refers to the coefficient at wavelength 1
K 2 refers to the coefficient at wavelength 2, etc.
Coefficients can be set negative where subtraction is required.

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3. To change a wavelength, press one of the ”λx:“ keys. Enter the


desired wavelength coefficient into the numeric keypad.
Press OK to confirm.

4. To change a coefficient, press one of the ”KX:“ keys. Enter the


desired coefficient into the numeric keypad.
Press OK to confirm.

Note: The instrument allows entry of up to 5 significant digits, with a


maximum of 4 significant digits after the decimal point.

Concentration factor:

1. Press Concentration Factor: Off in the Options menu. Press


On to highlight this feature.

2. Press the ”Factor“ key to enter the factor by which


absorbance readings are to be multiplied. Press the ”Unit“ key
to select the units for concentration measurements or to create
a new unit.

3. Press OK to confirm.

Concentration resolution:

1. Press Concentration Resolution in the Options menu.

2. Select the resolution and press OK to confirm.

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6.5.2 Complete a measurement in the multi wavelength mode

1. Insert the blank cell into the sample cell holder. Press Zero.

Note: The Read key does not become active until the zero
measurement has been completed.

2. Insert the sample cell into the sample cell holder. Press Read.

3. For data storage, see section 5.3.1 on page 35.

6.6 System checks

1. Press System Checks in the Main Menu.

The System Checks menu contains instrument information and


various performance tests.

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6.6.1 Instrument information

1. Press Instrument Information in the System Checks menu.

2. The model, serial number and software version are displayed.

6.6.2 Upgrade of the instrument software


To obtain the software for the update from the Internet at
www.hach.com:

1. Go to http://www.hach.com.

2. On the DR 2700 product page, click Lab System


Software/Software Update Downloads under Downloads.

3. Locate the appropriate download and save it on your computer.


Open the ZIP file and follow the "Read Me" instructions for
saving the file(s) to the USB memory stick.

4. On the DR 2700, press Instrument Update in the System


Checks menu.

5. Connect the USB stick to the USB interface on the DR 2700


(section 3.3 on page 10). Press OK.The link is established
automatically and the software is updated.

6. Press OK to return to the System Checks menu.

Note: When the instrument software has been updated, a prompt to restart
the instrument is displayed.

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6.6.3 Optical checks


For each optical check, the measured results must be evaluated
against user-specific requirements. The check options do not
define tolerances.

1. Press Optical Checks in the System Checks menu.

The Optical Checks menu contains programs for checking the


wavelength accuracy, stray light and photometric accuracy.
An optional test filter set (Verification Kit) (Section 9 on page 101)
containing 4 precision glass filters, target values, tolerances and
instructions is available and is recommended as an aid for carrying
out comprehensive in-house instrument checks.

6.6.3.1 Wavelength check


The Wavelength Check test is used to check wavelength accuracy
at 807 nm.

1. Press Wavelength Check in the Optical Checks menu.

2. Insert the adapter (A) for 10-mm rectangular cells in the cell
compartment #2 and insert the sample cell (Neodym or
BG20/2) in the adapter. Close the cell compartment.
Press Start.

3. The result is displayed and is to be compared with the


nominal/standard data (given in the quality control certificate) of
the sample cell.

4. Press Cancel to return to Optical Checks.

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6.6.3.2 Stray light check


The Stray Light test is used to measure the stray light in the
instrument at 500 nm.

1. Press Stray Light Check in the Optical Checks menu.

2. Remove any sample cell from the cell compartment.

3. Insert the adapter (A) for 10-mm rectangular cells in the cell
compartment #2. Press Zero.

4. Insert the sample cell or reference filter into the cell


compartment #2. Close the cell compartment. Press Start.

5. The ”Average“ is calculated from 100 successive absorbance


measurements. The result is displayed and is to be compared
with the nominal/standard data (given in the quality control
certificate) of the sample cell.

Note: Failings and passings will be defined by the user.

6. Press Cancel to return to Optical Checks.

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6.6.3.3 Absorbance check

The Absorbance Check test is used to test the photometric


accuracy and repeatability of the instrument.
This test can be used to test absorbance at any wavelength by a
specific sample or test filter set (Refer to section 6.6.3.4 on
page 84).

1. Press Absorbance Check in the Optical Checks menu.

2. Press λ to input the wavelength.

3. Input the wavelength and press OK to confirm.

4. Remove any sample cell from the cell compartment and press
Zero.

5. Insert sample cell into the cell compartment and press Read.

6. 5 Replicates of blanking and reading lead to results.

7. The result is displayed and is to be compared with the


nominal/standard data of the sample cell.

8. Press Cancel to return to Optical Checks.

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6.6.3.4 Verification kit


The Verification Kit, LZV770, (see Section 9 on page 101) is
designed for periodic monitoring of scattered light, photometric
accuracy and the wavelength accuracy of the spectrophotometer.
When results exceed allowable tolerances (given in the quality
control certificate), contact the manufacturer.

1. Press Verification Kit in the Optical Checks menu.

2. Press Nominal Values.

3. Press Edit.

An automatic menu guidance queries values (filters,


wavelength, nominal values and tolerances) given in the quality
control certificate, to the following specifications:

• Stray Light
• Photometrical accuracy
• Wavelength accuracy

4. Press OK when all values are entered and the overview is


displayed.

5. Press Verification.

6. Insert the adapter A (Figure 3 on page 13) in cell


compartment #2.

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7. Remove any cells from the cell compartment and press Start.

8. Insert the different filter in the given order one after the other.
Press Next after inserting a filter.

After the last measurement the results are displayed.

9. Press PC & Printer icon to send the data to a USB memory


stick, PC or to a printer.

The files will be stored automatically as CSV file (Comma


Separated Value). The file name will be formatted as
“Verification.csv“.

85
Advanced Operations

6.6.4 Output checks


If a printer is connected a test printing of the current screen will be
printed.

6.6.5 Lamp history


The Lamp History menu provides the amount of time that the lamp
has been on (Hours).

After a lamp is replaced and the Lamp History is reset, the display
of the total operating time is reset to 0.

1. Press Lamp History in the System Checks menu.

2. Press Reset VIS and the Visible Lamp will be reset.

3. Press OK to return to System Checks.

6.6.6 Factory service

The Factory Service menu is password protected. This menu is not


intended for customer use.

86
Advanced Operations

6.6.7 Service time


In order to ensure a regular inspection, an automatic memory
reference for the service times can be entered. After switching the
instrument on this memory reference will be activated and indicated
at the appropriate time.

1. Press Service Time in the System Checks menu.

2. Select On and then Last Service to enter the date of the last
inspection.

3. Press OK to confirm.

4. Select Next Service to determine a specific period of time up to


the next inspection.

5. Press OK to confirm.

If the next service is due, the message "Next service is due!" is


displayed after switching on the instrument.

6. Press OK to return to the Main Menu.

Contact the manufacturer or distributor to arrange an appointment


for the next service.

87
Advanced Operations

6.6.8 Instrument Backup


Before the next service date the Instrument Backup menu offers
the possibility to store all programs, measuring data, Operator ID,
Sample ID, passwords and all adjustable data on a USB stick.

1. Press Instrument Backup in the System Checks menu.

2. Connect the USB memory stick (section 3.3 on page 10).

3. Press Store to start a Backup.

Note: If the USB stick is not connected, the message "Please insert USB
Memory" is displayed. Connect a USB stick, in order to store the data.
Press OK to confirm and press Store again.

Note: If the Backup was already stored before, the message "Data already
exists. Overwrite?" is displayed. Press OK to overwrite the data.

88
Advanced Operations

If the file was stored the message Instrument Backup is stored to


USB stick will be displayed.

4. Press OK to return to the System Checks menu.

Restore backup data:


Important Note: All current data will be overwritten when restoring
the Backup file!

1. Press Instrument Backup in the System Checks menu.

2. Connect the USB memory stick containing the Backup


(section 3.3 on page 10).

3. Press Restore to pass back the data.

Note: If the USB stick is not connected, the message "Please insert USB
Memory" is displayed. Connect a USB stick, in order to store the data.
Press OK to confirm and press Restore again.

89
Advanced Operations

4. Press OK to confirm after the message “Instrument Backup


from S/N XXXXXXX. Restore?“ is displayed.

5. After the backup start the instrument again.

90
Section 7 Maintenance
CAUTION
Potential Chemical, Biological Eye and Skin Hazards.
Only qualified personnel should conduct the tasks described
in this section of the manual.

Important Note: Remove any cells that are still in the instrument
and dispose of them or their contents using an approved disposal
method.

7.1 Cleaning requirements


CAUTION
Potential Pinch, Eye, Burn and Chemical Hazards.
Always disconnect power from the instrument before
attempting any cleaning operations.

Important Note: Under no circumstances should the instrument,


display or the accessories be cleaned with solvents such as white
spirit, acetone, etc.

7.1.1 Spectrophotometer
• Clean the enclosure, sample cell compartments and all
accessories with a soft damp cloth. A mild soap solution can
also be used. Do not get excess water in the sample cell
compartments. Do not insert a brush or sharp object into Cell
Compartment #1 to avoid damaging the mechanical
components.
• Dry the cleaned parts carefully with a soft cotton cloth.

7.1.2 Display
• Take care not to scratch the display. Do not touch the screen
with ball pens, pencils or similar pointed objects.
• Clean the display with a soft, lint-free and oil-free cotton cloth.
Diluted window cleaner liquid can also be used.

7.1.3 Sample cells

CAUTION
Potential Chemical/ Biological Exposure Hazards.
Use proper laboratory practices whenever there is a risk of
chemical exposure.

1. After performing a procedure, clean glass sample cells with


cleaning agents.

2. Afterwards, rinse the sample cells several times with tap water
and then thoroughly with deionized water.

Important Note: Glass sample cells that have been used for
organic solvents (such as chloroform, benzene, toluene, etc.) must
be rinsed with acetone before being treated with cleaning agents. In
addition, another rinse with acetone is necessary as a final
treatment step before the sample cells are dried.

91
Maintenance

7.2 Insert or change of the battery

1. Remove the cell from the cell compartment.

2. Switch the instrument off.

3. Unplug the power cord.

4. Turn the instrument over carefully and place it on a soft surface.

5. Use a screwdriver or a coin to remove the screw from the


cover.

6. Remove the cover and place it to one side.

CAUTION
For quality and safety reasons, only the manufacturer’s lithium
batteries (LZV551) should be used for this instrument. Use of
non-instrument-specific battery types may impair the
functioning of and/or damage the instrument electronics by
overloading them, or depending on battery types can even
result in fire or explosion hazards.

7. Carefully push the battery from right to left into the


compartment, with the labeled face upward.

92
Maintenance

8. Push in the battery so that the contacts of the instrument can


be plugged into the socket of the battery.

Important Note: Take care that the battery contacts are always
clean. Soiled contacts can result in contact heating and voltage
drop, interfering with the proper operation of the
spectrophotometer.

9. Use a screwdriver or a coin to replace the screw securing the


cover.

10. Carefully stand the instrument upright.

11. Plug in power supply again – the Instrument is now ready for
use. The battery charges up.

7.2.1 Information about using the battery

7.2.1.1 Dispose of the lithium battery


A lithium battery allows the DR 2700 to be used as a portable
instrument.

Please dispose the batteries of in compliance with the


country-specific regulations (information about the charge status of
the battery can be found in the "Instrument Setup” menu under
5.2.5 Power Management on page 27).

CAUTION
Pay special attention to the following information for the
Lithium battery pack:

• Do not short-circuit the contacts.


• Keep the battery away from fire.
• Do not expose the battery to temperatures above 60°C (such
temperatures may occur, for example, in a car left in the sun, or
in direct sunlight).
• Take care that the battery does not become wet.
• Take care that the battery is not exposed to impacts, blows, etc.
Do not drop it. Do not step on it.
• Do not take the battery apart or modify it in any way.

93
Maintenance

• The performance of the battery decreases with the


temperature.

7.2.1.2 Optimal operation of the battery


The battery is charged automatically when the plug-in power supply
on the back of the instrument is connected and is plugged into a
mains socket (100–240 Volt/50–60 Hz).

CAUTION
Use only the manufacturer's specified external power supply
to operate the instrument and charge the internal lithium
battery pack. The specified power supply and it's plug shape,
it voltage rating (12V, 2A) and it's electromagnetic
characteristics are critical to assuring the DR 2700's
performance and the safety of the user.

Important Note: We advise charging the battery at an ambient


temperature between 10°C and 30°C, as this is the range in which it
can be most effectively charged to 100%.

7.2.1.3 Lifespan of the battery


The battery has a limited lifespan. The more it is used, the more its
capacity is reduced. If a fully charged battery only allows the
instrument to be used for a relatively short time, replace the battery
with a new one.
Note: You need not run down the battery completely before recharging it. If
you recharge the battery when it still has some residual charge, this does
not reduce its capacity!

7.2.1.4 Load the battery/Operating time


The time required to charge a newly installed battery is about
3.5 hours.

Operating time of a fully charged battery:


Charge: If a battery is charged to 100% capacity, and the user
carries out 10 measurements per day, and the instrument is left on
after each measurement for the full 15 minutes before it
automatically switches off, the battery can be used for 6 to 7 days
before it needs recharging.

94
Maintenance

7.3 Lamp replacement

CAUTION
To avoid a possible electric shock, disconnect the instrument
from the power source before servicing the lamp.

1. Remove the cell from the cell compartment.

2. Switch the instrument off.

3. Unplug the power cord.

WARNING
Burn Hazard. Wait until the lamp cools down. Contact with the
hot lamp can cause burns.

4. Turn the instrument over carefully and place it on a soft surface.

5. Use a screwdriver or a coin to remove the screw from the


cover.

6. Remove the cover and place it to one side.

7. If there is a battery in the instrument, push it out and put it to


one side too, see section 7.2.1 on page 93.

8. Use a screwdriver (slotted or cross-headed) to remove the


screws from the lamp fitting.

95
Maintenance

WARNING
Burn Hazard. Wait until the lamp cools down. Contact with the
hot lamp can cause burns.

9. Lift the lamp fitting carefully.

10. Put both screws to one side.

11. Push up on the pressure spring.

12. Remove the halogen lamp complete with the plug panel.

96
Maintenance

13. Carefully unplug the halogen lamp from the plug panel.

Important Note: Hold the lamp by the fitting only. Avoid touching
the glass, as substances on the skin can bake onto the lamp bulb
and thus accelerate the aging process of the lamp.

14. Plug a new halogen lamp to the panel.

15. Insert the halogen lamp with the half rounded part pointing
down.

16. Press the plug with slight pressure into the direction of the
halogen lamp and push the pressure spring down, so that it will
engage.

17. Carefully insert the lamp fitting again.

18. Use a screwdriver (slotted or cross-headed) to replace the


screws to secure the lamp fitting.

19. Put the battery back in place, see section 7.2.1 on page 93.

20. Use a screwdriver or a coin to screw the back cover to the


instrument.

21. Carefully stand the instrument upright.

22. Plug in the power supply.

23. Reset the Lamp History, see section 6.6.5 on page 86.

97
Maintenance

98
Section 8 Troubleshooting

Problem/Display screen Likely Cause Action

Attention! Measurements with round vials or tubes Insert the light shield.
Please insert the light shield. generally require the light shield. Press OK.
Dilute the sample and repeat the
Absorbance > 3.5! The measured absorbance exceeds 3.5
measurement
Calculated concentration is higher than Dilute the sample and repeat the
Concentration too high!
999999 measurement
Error Check the lamp and replace it if
Selfcheck stopped. necessary.
Self Check Test stops while starting the
Please check the lamp.
instrument Close the lid.
Please close the lid.
Error [xx] Press Start Again.

Error
Self Check Test stops while starting the Remove the cell.
Selfcheck stopped.
instrument Press OK.
Please remove the cell

Error
Contact the manufacturer or a sales
Selfcheck stopped.
Electronic defect representative and indicate the error
Hardware error.
number
Error [x]
Remove cell.
It’s recommended to execute a
Close the lid.
Full System Check The instrument needs a new
Please remove cell. Full System Check. Press Start. If the Full System Check
Please close the lid. fails, please contact the manufacturer or
distributor.
Negative result! The calculated result is negative Check the concentration of the sample
Check the programming
Error in the test database / user
No evaluation! Contact the manufacturer or a sales
database
representative
The measured absorbance is above the Dilute the sample and repeat the
Over measuring range
calibration range of the test measurement
Check the lamp and replace it if
Please check the lamp. The lamp output is too low
necessary
Too much ambient light! Reduce ambient light. (Avoid direct sun
The instrument sensors detects to much
Move device into shade light.)
ambient light.
or close the lid! Close the lid.
If possible, select a test with a lower
The measured absorbance is below the
Under measuring range measurement range or use a cell with a
calibration range of the test
longer path length
Fluctuating light conditions during the Close the lid or place the Protective
Unstable lighting conditions!
measurement Cover on the cell compartment (2)

99
Troubleshooting

100
Section 9 Replacement Parts

Description Cat. No.


Battery, rechargeable lithium LZV551
Cell Adapter A, 10 mm square LZV583
Cell Adapter B, Pour-Thru Cell LZV585
Cell Adapter C, 1 inch round LZV584
Dust Cover HYH019
Filter set, certified, for self-checks (4 precision glass filters with target values) LZV770
Hach Data Trans (PC software for data transfer) LZY274
Lamp, tungsten LZV565
Light Shield LZV646
Pour-Thru Cell Kit 5940400
Power Supply, external LZV798
Protective Cover/adapter holder LZV642
Sample Cell, 10-mL, 1-inch glass square matched pair 2495402
Sample Cell, 25-mL, 1-inch glass square matched pair with stoppers 2612602
Sample Cell, 10-mL round glass, with cap, each 2122800
Sample Cell, multi-path 10 and 25 mL, plastic, with caps, pk/6 5940506
Sample cell, 25 mL, 1-inch square plastic, with cap, pk/12 2410212
USB-Interface Cable (1 m) LZV567
USB-Keyboard (keyboard layout: US) LZV582
USB-Memory Stick 2946900

101
Replacement Parts

102
Section 10 Contact Information
HACH Company Repair Service in the Repair Service in Canada: Repair Service in
World Headquarters United States: Hach Sales & Service Latin America, the
P.O. Box 389 HACH Company Canada Ltd. Caribbean, the Far East,
Loveland, Colorado Ames Service 1313 Border Street, Unit 34 Indian Subcontinent, Africa,
80539-0389 U.S.A. 100 Dayton Avenue Winnipeg, Manitoba Europe, or the Middle East:
Tel (800) 227-HACH Ames, Iowa 50010 R3H 0X4 Hach Company World
(800) -227-4224 Tel (800) 227-4224 Tel (800) 665-7635 Headquarters,
(U.S.A. only) (U.S.A. only) (Canada only) P.O. Box 389
Fax (970) 669-2932 Fax (515) 232-3835 Tel (204) 632-5598 Loveland, Colorado,
[email protected] Fax (204) 694-5134 80539-0389 U.S.A.
www.hach.com [email protected] Tel +001 (970) 669-3050
Fax +001 (970) 669-2932
[email protected]

HACH LANGE GMBH HACH LANGE LTD HACH LANGE LTD HACH LANGE GMBH
Willstätterstraße 11 Pacific Way Unit 1, Chestnut Road Hütteldorfer Str. 299/Top 6
D-40549 Düsseldorf Salford Western Industrial Estate A-1140 Wien
Tel. +49 (0)2 11 52 88-320 GB-Manchester, M50 1DL IRL-Dublin 12 Tel. +43 (0)1 912 16 92
Fax +49 (0)2 11 52 88-210 Tel. +44 (0)161 872 14 87 Tel. +353(0)1 460 2522 Fax +43 (0)1 912 16 92-99
[email protected] Fax +44 (0)161 848 73 24 Fax +353(0)1 450 9337 [email protected]
www.hach-lange.de [email protected] [email protected] www.hach-lange.at
www.hach-lange.co.uk www.hach-lange.ie
HACH LANGE GMBH HACH LANGE FRANCE HACH LANGE NV/SA DR. LANGE NEDERLAND
Rorschacherstrasse 30a S.A.S. Motstraat 54 B.V.
CH-9424 Rheineck 8, mail Barthélémy Thimonnier B-2800 Mechelen Laan van Westroijen 2a
Tel. +41 (0)848 55 66 99 Lognes Tel. +32 (0)15 42 35 00 NL-4003 AZ Tiel
Fax +41 (0)71 886 91 66 F-77437 Marne-La-Vallée Fax +32 (0)15 41 61 20 Tel. +31(0)344 63 11 30
[email protected] cedex 2 [email protected] Fax +31(0)344 63 11 50
www.hach-lange.ch Tél. +33 (0) 820 20 14 14 www.hach-lange.be [email protected]
Fax +33 (0)1 69 67 34 99 www.hach-lange.nl
[email protected]
www.hach-lange.fr
HACH LANGE APS HACH LANGE AB HACH LANGE S.R.L. HACH LANGE SPAIN S.L.U.
Åkandevej 21 Vinthundsvägen 159A Via Rossini, 1/A Edificio Seminario
DK-2700 Brønshøj SE-128 62 Sköndal I-20020 Lainate (MI) C/Larrauri, 1C- 2ª Pl.
Tel. +45 36 77 29 11 Tel. +46 (0)8 7 98 05 00 Tel. +39 02 93 575 400 E-48160 Derio/Bizkaia
Fax +45 36 77 49 11 Fax +46 (0)8 7 98 05 30 Fax +39 02 93 575 401 Tel. +34 94 657 33 88
[email protected] [email protected] [email protected] Fax +34 94 657 33 97
www.hach-lange.dk www.hach-lange.se www.hach-lange.it [email protected]
www.hach-lange.es
HACH LANGE LDA HACH LANGE SP. ZO.O. HACH LANGE S.R.O. HACH LANGE S.R.O.
Av. do Forte nº8 ul. Krakowska 119 Zastrčená 1278/8 Roľnícka 21
Fracção M PL-50-428 Wrocław CZ-141 00 Praha 4 - Chodov SK-831 07 Bratislava –
P-2790-072 Carnaxide Tel. +48 801 022 442 Tel. +420 272 12 45 45 Vajnory
Tel. +351 214 253 420 Zamówienia: +48 717 177 707 Fax +420 272 12 45 46 Tel. +421 (0)2 4820 9091
Fax +351 214 253 429 Doradztwo: +48 717 177 777 [email protected] Fax +421 (0)2 4820 9093
[email protected] Fax +48 717 177 778 www.hach-lange.cz [email protected]
www.hach-lange.pt [email protected] www.hach-lange.sk
www.hach-lange.pl
HACH LANGE KFT. HACH LANGE S.R.L. HACH LANGE HACH LANGE SU
Vöröskereszt utca. 8-10. Str. Căminului nr. 3, 8, Kr. Sarafov str. ANALİZ SİSTEMLERİ
H-1222 Budapest XXII. ker. et. 1, ap. 1, Sector 2 BG-1164 Sofia LTD.ŞTİ.
Tel. +36 1 225 7783 RO-021741 Bucureşti Tel. +359 (0)2 963 44 54 Ilkbahar mah. Galip Erdem
Fax +36 1 225 7784 Tel. +40 (0) 21 205 30 03 Fax +359 (0)2 866 15 26 Cad. 616 Sok. No:9
[email protected] Fax +40 (0) 21 205 30 17 [email protected] TR-Oran-Çankaya/ANKARA
www.hach-lange.hu [email protected] www.hach-lange.bg Tel. +90312 490 83 00
www.hach-lange.ro Fax +90312 491 99 03
[email protected]
www.hach-lange.com.tr

103
Contact Information

HACH LANGE D.O.O. ΗΑCH LANGE E.Π.Ε. HACH LANGE D.O.O. HACH LANGE MAROC
Fajfarjeva 15 Αυλίδος 27 Ivana Severa bb SARLAU
SI-1230 Domžale GR-115 27 Αθήνα HR-42 000 Varaždin Villa 14 – Rue 2 Casa
Tel. +386 (0)59 051 000 Τηλ. +30 210 7777038 Tel. +385 (0) 42 305 086 Plaisance
Fax +386 (0)59 051 010 Fax +30 210 7777976 Fax +385 (0) 42 305 087 Quartier Racine Extension
[email protected] [email protected] [email protected] MA-Casablanca 20000
www.hach-lange.si www.hach-lange.gr www.hach-lange.hr Tél. +212 (0)522 97 95 75
Fax +212 (0)522 36 89 34
[email protected]
www.hach-lange.ma

HACH LANGE OOO


Finlyandsky prospekt, 4A
Business Zentrum “Petrovsky
fort”, R.803
RU-194044, Sankt-Petersburg
Tel. +7 (812) 458 56 00
Fax. +7 (812) 458 56 00
[email protected]
www.hach-lange.com

104
Section 11 Limited Warranty

Hach Company warrants its products to the original purchaser against any defects that are due to faulty
material or workmanship for a period of one year from date of shipment unless otherwise noted in the
product manual.

In the event that a defect is discovered during the warranty period, Hach Company agrees that, at its
option, it will repair or replace the defective product or refund the purchase price excluding original
shipping and handling charges. Any product repaired or replaced under this warranty will be warranted
only for the remainder of the original product warranty period.

This warranty does not apply to consumable products such as chemical reagents; or consumable
components of a product, such as, but not limited to, lamps and tubing.

Contact Hach Company or your distributor to initiate warranty support. Products may not be returned
without authorization from Hach Company.

Limitations
This warranty does not cover:

• Damage caused by acts of God, natural disaster, labor unrest, acts of war (declared or undeclared),
terrorism, civil strife or acts of any governmental jurisdiction

• Damage caused by misuse, neglect, accident or improper application or installation

• Damage caused by any repair or attempted repair not authorized by Hach Company
• Any product not used in accordance with the instructions furnished by Hach Company

• Freight charges to return merchandise to Hach Company

• Freight charges on expedited or express shipment of warranted parts or product

• Travel fees associated with on-site warranty repair


This warranty contains the sole express warranty made by Hach Company in connection with its
products. All implied warranties, including without limitation, the warranties of merchantability and fitness
for a particular purpose, are expressly disclaimed.

Some states within the United States do not allow the disclaimer of implied warranties and if this is true in
your state the above limitation may not apply to you. This warranty gives you specific rights, and you
may also have other rights that vary from state to state.

This warranty constitutes the final, complete, and exclusive statement of warranty terms and no person
is authorized to make any other warranties or representations on behalf of Hach Company.

Limitation of Remedies
The remedies of repair, replacement or refund of purchase price as stated above are the exclusive
remedies for the breach of this warranty. On the basis of strict liability or under any other legal theory, in
no event shall Hach Company be liable for any incidental or consequential damages of any kind for
breach of warranty or negligence.

105
Limited Warranty

106
Index

A O
Absorbance Check .................................................. 83 Operator ID .............................................................. 24
Absorbance Formula ......................................... 76, 77 create ................................................................ 24
Alphanumeric keypad .............................................. 23 delete ................................................................. 25
Audio signals ........................................................... 27 Optical Checks ...................................... 81, 82, 83, 84
B Output Checks ......................................................... 86
Basic data ................................................................ 38 P
C Password ................................................................. 32
Calibration formula ................................................... 61 activate .............................................................. 32
Calibration Settings .................................................. 52 PC and Printer ................................................... 29, 31
Cells ......................................................................... 91 Print data .................................................................. 31
Chemical Form .................................................. 39, 42 Printer Setup ............................................................ 29
Cleaning Program ................................................................... 47
Display ............................................................... 91 R
Spectrophotometer ............................................ 91 Reagent Blank ................................................... 39, 43
Concentration Factor ............................ 73, 74, 76, 78 Recall Data ..................................................39, 73, 77
Concentration Resolution ..................... 73, 74, 76, 78 S
D Safety Information ...................................................... 7
Data ......................................................................... 35 Sample ID ................................................................ 26
delete ........................................................... 35, 37 create ................................................................ 26
recall .................................................................. 35 delete ................................................................. 26
send ................................................................... 35 Save as User Program .................................39, 73, 76
store .................................................................. 35 Security List ............................................................. 32
Data Log .................................................................. 35 Self Check ................................................................ 21
Date and Time ......................................................... 26 Send Data .......................................................... 36, 39
Dilution Factor .................................................... 39, 41 Service Time ............................................................ 87
Display ............................................................... 23, 91 Single Wavelength ................................ 49, 52, 73, 74
Display and Sound ................................................... 27 Software ............................................................. 80, 81
F Specifications ............................................................. 5
Factory Service ........................................................ 86 Standard Addition .............................................. 39, 68
Favorites ......................................................45, 66, 67 Standard Adjust ................................................. 39, 41
delete ........................................................... 66, 67 Stored Data .............................................................. 35
edit ..................................................................... 66 Stored Programs ...................... 38, 39, 41, 42, 43, 45
recall .................................................................. 67 send Data .......................................................... 39
Filter Settings ........................................................... 36 Stray Light Check ..................................................... 82
Free programming ..........................58, 59, 61, 64, 66 System Checks 21, 24, 79, 81, 82, 83, 84, 86, 87, 88
H T
HACH Data Trans .............................................. 31, 36 Timer ..................................................... 27, 39, 73, 76
Hazard Information .................................................... 7 Touch Screen ........................................................... 23
I U
Instrument Backup ............................................. 88, 89 Unpack the instrument ............................................... 9
Instrument Information ............................................. 80 Update ............................................................... 80, 81
Instrument Setup .........................................39, 74, 77 User Programs ......................................................... 47
Interfaces ................................................................. 29 V
Internet ............................................................... 80, 81 Variables .................................................................. 64
L Verification Kit .......................................................... 84
Lamp, see VIS-Lamp VIS-Lamp
Language ................................................................. 21 Lamp Control
M Lamp History ..................................................... 86
Main Menu ............................................................... 24 W
Maintenance ............................................................ 91 Warranty ................................................................ 105
Measurement Process ............................................. 58 Wavelength ........................................................ 73, 76
Measuring sequence ............................................... 59 Wavelength Check ................................................... 81
Multi Wavelength ..................... 50, 52, 76, 77, 78, 79

107

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