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Model 700

Gas Chromatograph
System Reference Manual

Applies to Both
Daniel Danalyzer Model 700
Rosemount Analytical Model 700

Part Number 3-9000-521


Revision J

SEPTEMBER 2005
Model 700 Gas Chromatograph
System Reference Manual

NOTICE

DANIEL MEASUREMENT AND CONTROL, INC. AND ROSEMOUNT ANALYTICAL, INC.


(COLLECTIVELY, “SELLER”) SHALL NOT BE LIABLE FOR TECHNICAL OR EDITORIAL ERRORS IN
THIS MANUAL OR OMISSIONS FROM THIS MANUAL. SELLER MAKES NO WARRANTIES,
EXPRESSED OR IMPLIED, INCLUDING THE IMPLIED WARRANTIES OF MERCHANTABILITY AND
FITNESS FOR A PARTICULAR PURPOSE WITH RESPECT TO THIS MANUAL AND, IN NO EVENT,
SHALL SELLER BE LIABLE FOR ANY SPECIAL OR CONSEQUENTIAL DAMAGES INCLUDING,
BUT NOT LIMITED TO, LOSS OF PRODUCTION, LOSS OF PROFITS, ETC.

PRODUCT NAMES USED HEREIN ARE FOR MANUFACTURER OR SUPPLIER IDENTIFICATIO


ONLY AND MAY BE TRADEMARKS/REGISTERED TRADEMARKS OF THESE COMPANIES.

THE CONTENTS OF THIS PUBLICATION ARE PRESENTED FOR INFORMATIONAL PURPOSES


ONLY, AND WHILE EVERY EFFORT HAS BEEN MADE TO ENSURE THEIR ACCURACY, THEY
ARE NOT TO BE CONSTRUED AS WARRANTIES OR GUARANTEES, EXPRESSED OR IMPLIED,
REGARDING THE PRODUCTS OR SERVICES DESCRIBED HEREIN OR THEIR USE OR
APPLICABILITY. WE RESERVE THE RIGHT TO MODIFY OR IMPROVE THE DESIGNS OR
SPECIFICATIONS OF SUCH PRODUCTS AT ANY TIME.

SELLER DOES NOT ASSUME RESPONSIBILITY FOR THE SELECTION, USE OR MAINTENANCE
OF ANY PRODUCT. RESPONSIBILITY FOR PROPER SELECTION, USE AND MAINTENANCE OF
ANY SELLER PRODUCT REMAINS SOLELY WITH THE PURCHASER AND END-USER.

DANIEL AND THE DANIEL LOGO ARE REGISTERED TRADEMARKS OF DANIEL INDUSTRIES,
INC. THE ROSEMOUNT AND ROSEMOUNT ANALYTICAL LOGO THE ARE REGISTERED
TRADEMARKS OF ROSEMOUNT ANALYTICAL, INC. THE EMERSON LOGO IS A TRADEMARK
AND SERVICE MARK OF EMERSON ELECTRIC CO.

COPYRIGHT © 2005 BY DANIEL MEASUREMENT AND CONTROL, INC., HOUSTON, TEXAS,


U.S.A.

All rights reserved. No part of this work may be reproduced or copied in any form or by any
means - graphic, electronic, or mechanical — without first receiving the written permission of
Daniel Measurement and Control, Inc. Houston, Texas, U.S.A.
WARRANTY

1. LIMITED WARRANTY: Subject to the limitations contained in Section 2 herein and except as
otherwise expressly provided herein, Daniel Measurement and Control, Inc. and Rosemount
Analytical, Inc., (collectively“Seller”) warrants that the firmware will execute the programming
instructions provided by Seller, and that the Goods manufactured or Services provided by Seller
will be free from defects in materials or workmanship under normal use and care until the
expiration of the applicable warranty period. Goods are warranted for twelve (12) months from
the date of initial installation or eighteen (18) months from the date of shipment by Seller,
whichever period expires first. Consumables and Services are warranted for a period of 90 days
from the date of shipment or completion of the Services. Products purchased by Seller from a
third party for resale to Buyer ("Resale Products") shall carry only the warranty extended by the
original manufacturer. Buyer agrees that Seller has no liability for Resale Products beyond making
a reasonable commercial effort to arrange for procurement and shipping of the Resale Products. If
Buyer discovers any warranty defects and notifies Seller thereof in writing during the applicable
warranty period, Seller shall, at its option, promptly correct any errors that are found by Seller in
the firmware or Services, or repair or replace F.O.B. point of manufacture that portion of the
Goods or firmware found by Seller to be defective, or refund the purchase price of the defective
portion of the Goods/Services. All replacements or repairs necessitated by inadequate
maintenance, normal wear and usage, unsuitable power sources, unsuitable environmental
conditions, accident, misuse, improper installation, modification, repair, storage or handling, or
any other cause not the fault of Seller are not covered by this limited warranty, and shall be at
Buyer's expense. Seller shall not be obligated to pay any costs or charges incurred by Buyer or
any other party except as may be agreed upon in writing in advance by an authorized Seller rep-
resentative. All costs of dismantling, reinstallation and freight and the time and expenses of
Seller's personnel for site travel and diagnosis under this warranty clause shall be borne by Buyer
unless accepted in writing by Seller. Goods repaired and parts replaced during the warranty
period shall be in warranty for the remainder of the original warranty period or ninety (90) days,
whichever is longer. This limited warranty is the only warranty made by Seller and can be
amended only in a writing signed by an authorized representative of Seller. Except as otherwise
expressly provided in the Agreement, THERE ARE NO REPRESENTATIONS OR WARRANTIES OF
ANY KIND, EXPRESSED OR IMPLIED, AS TO MERCHANTABILITY, FITNESS FOR PARTICULAR
PURPOSE, OR ANY OTHER MATTER WITH RESPECT TO ANY OF THE GOODS OR SERVICES. It
is understood that corrosion or erosion of materials is not covered by our guarantee.

2. LIMITATION OF REMEDY AND LIABILITY: SELLER SHALL NOT BE LIABLE FOR DAMAGES
CAUSED BY DELAY IN PERFORMANCE. THE SOLE AND EXCLUSIVE REMEDY FOR BREACH OF
WARRANTY HEREUNDER SHALL BE LIMITED TO REPAIR, CORRECTION, REPLACEMENT OR
REFUND OF PURCHASE PRICE UNDER THE LIMITED WARRANTY CLAUSE IN SECTION 1
HEREIN. IN NO EVENT, REGARDLESS OF THE FORM OF THE CLAIM OR CAUSE OF ACTION
(WHETHER BASED IN CONTRACT, INFRINGEMENT, NEGLIGENCE, STRICT LIABILITY, OTHER
TORT OR OTHERWISE), SHALL SELLER'S LIABILITY TO BUYER AND/OR ITS CUSTOMERS
EXCEED THE PRICE TO BUYER OF THE SPECIFIC GOODS MANUFACTURED OR SERVICES
PROVIDED BY SELLER GIVING RISE TO THE CLAIM OR CAUSE OF ACTION. BUYER AGREES
THAT IN NO EVENT SHALL SELLER'S LIABILITY TO BUYER AND/OR ITS CUSTOMERS EXTEND
TO INCLUDE INCIDENTAL, CONSEQUENTIAL OR PUNITIVE DAMAGES. THE TERM
"CONSEQUENTIAL DAMAGES" SHALL INCLUDE, BUT NOT BE LIMITED TO, LOSS OF
ANTICIPATED PROFITS, LOSS OF USE, LOSS OF REVENUE AND COST OF CAPITAL.
TABLE OF CONTENTS i
Model 700

TABLE OF CONTENTS

INTRODUCTION 1.1 DESCRIPTION OF MANUAL ............................1-1

1.2 SYSTEM DESCRIPTION..................................1-1


Analyzer Assembly ........................................1-2
Controller Assembly ......................................1-5
Sample Conditioning System (SCS) .................1-8
1.2.1 Functional Description ...................................1-9
1.2.2 Available Functions ..................................... 1-11

1.3 SOFTWARE DESCRIPTION ........................... 1-13


BOS .......................................................... 1-13
MON2000.................................................. 1-14

1.4 THEORY OF OPERATION ............................. 1-15


1.4.1 Thermal Conductivity Detector (TCD) ............ 1-15
1.4.2 Flame Ionization Detector (Micro-FID) ............ 1-18
1.4.3 LSIV .......................................................... 1-19
1.4.4 Methanator ................................................ 1-21
1.4.5 Data Acquisition ......................................... 1-22
1.4.6 Peak Detection ........................................... 1-23

1.5 BASIC ANALYSIS COMPUTATIONS .............. 1-26


1.5.1 Conc Analysis - Response Factor................... 1-26
1.5.2 Conc Calc - Mole Percentage
(without Normalization) ................................ 1-28
1.5.3 Conc Calc in Mole Percentage
(with Normalization) .................................... 1-29

1.6 ADDITIONAL RESOURCES ........................... 1-30

SEP 2005 INTRODUCTION


ii TABLE OF CONTENTS
Model 700

1.7 GLOSSARY ................................................ 1-31


Auto Zero .................................................. 1-31
Baseline ..................................................... 1-31
Carrier Gas ................................................. 1-31
Chromatogram............................................ 1-31
Component ................................................ 1-32
Condulet .................................................... 1-32
CTS .......................................................... 1-32
DCD .......................................................... 1-32
DSR .......................................................... 1-32
DTR .......................................................... 1-32
FID............................................................ 1-33
LSIV .......................................................... 1-33
Methanator ................................................ 1-33
Response Factor ......................................... 1-33
Retention Time ........................................... 1-33
RI.............................................................. 1-34
RLSD......................................................... 1-34
RTS........................................................... 1-34
RxD, RD, or Sin .......................................... 1-34
TCD .......................................................... 1-34
TxD, TD, or Sout ........................................ 1-34

EQUIPMENT 2.1 EQUIPMENT DESCRIPTION ............................ 2-1


DESCRIPTION AND
2.1.1 Upper Enclosure............................................ 2-2
SPECIFICATIONS
2.1.2 Lower Enclosure ........................................... 2-8
2.1.3 Flow Panel Assembly................................... 2-10

2.2 EQUIPMENT SPECIFICATIONS ...................... 2-10


2.2.1 Utilities ...................................................... 2-10
2.2.2 Electronic Hardware .................................... 2-13
2.2.3 Micro Heat Sink Oven .................................. 2-18
2.2.4 Software.................................................... 2-19

INSTALLATION AND 3.1 PRECAUTIONS AND WARNINGS ................... 3-1


SETUP
3.1.1 Hazardous Environments ................................ 3-2
3.1.2 Power Source Wiring ..................................... 3-3
3.1.3 Card Cage Removal ....................................... 3-4
3.1.4 Signal Wiring .............................................. 3-10

EQUIPMENT DESCRIPTION AND SPECIFICATIONS SEP 2005


TABLE OF CONTENTS iii
Model 700

3.1.5 Electrical and Signal Ground ......................... 3-11


3.1.6 Electrical Conduit ........................................ 3-13
3.1.7 Sample System Requirements ....................... 3-14
Line Length: ............................................... 3-15
Sample Line Tubing Material: ....................... 3-15
Dryers and Filters: ....................................... 3-16
Pressure Regulators and Flow Controllers: ...... 3-16
Pipe Threads, Dressing:................................ 3-16
Valving: ..................................................... 3-16

3.2 PREPARATION............................................ 3-16


3.2.1 Site Selection ............................................. 3-17
3.2.2 Unpacking the Unit...................................... 3-17
3.2.3 Model 700 Installation Arrangements............. 3-18
Wall Mount ................................................ 3-18
Pole Mount................................................. 3-19
Floor Mount................................................ 3-19
3.2.4 Required Tools and Components ................... 3-19
3.2.5 Supporting Tools and Components ................ 3-21

3.3 MODEL 700 INSTALLATION......................... 3-23


3.3.1 DC Power Supply ........................................ 3-23
3.3.2 Optional AC – DC Power Converter ............... 3-25
3.3.3 Sample and Gas Lines.................................. 3-28

3.4 SETTING THE COM ID ................................. 3-33


3.4.1 Inspect or Change the Com ID ...................... 3-33
3.4.2 Preparing for Serial Connections.................... 3-37
3.4.3 FTB Connection (RS-232)............................. 3-40
3.4.4 PC to GC Cable Short Distance
Connection (RS-232) ................................... 3-41
3.4.5 Long Distance Connection (RS-422,
RS-485) ..................................................... 3-48
3.4.6 GC-Printer Wiring ........................................ 3-50

SEP 2005 INSTALLATION AND SETUP


iv TABLE OF CONTENTS
Model 700

3.4.7 Discrete Digital I/O Wiring ............................ 3-51


Discrete Digital Inputs.................................. 3-51
Discrete Digital Outputs ............................... 3-52
3.4.8 Analog Input Wiring..................................... 3-54
3.4.9 Analog Output Wiring .................................. 3-55
3.4.10 Optional Boards .......................................... 3-57
Optional WinSystems Modem ....................... 3-57
Optional Radicom Modem Settings ................ 3-58
Ethernet Settings ........................................ 3-59

3.5 LEAK CHECKS AND PURGING FOR


FIRST CALIBRATION ................................... 3-60
3.5.1 Initial Leak Check ........................................ 3-60
Carrier Gas Line Leak Checks........................ 3-60
Calibration Line Leak Check .......................... 3-61
Sample Lines (Streams) Leak Check .............. 3-62
3.5.2 Purging Carrier Gas Lines ............................. 3-62
3.5.3 Purging Calibration Gas Lines........................ 3-64

3.6 SYSTEM STARTUP ..................................... 3-65

MAINTENANCE AND 4.1 TROUBLESHOOTING AND REPAIR CONCEPT ... 4-1


TROUBLESHOOTING
4.2 ROUTINE MAINTENANCE............................... 4-1
4.2.1 Bimonthly Maintenance Checklist .................... 4-2
4.2.2 Routine Maintenance Procedures..................... 4-4
4.2.3 Contact Service ............................................ 4-4

4.3 ACCESS TO GC EQUIPMENT ELEMENTS ......... 4-5


4.3.1 Electrical/Electronic Components..................... 4-5
Model 700 with TCD Upper Enclosure ............. 4-6
Model 700 with TCD Lower Enclosure ............. 4-6
Model 700 with Micro-FID/TCD
Upper Enclosure............................................ 4-6
Model 700 with Micro-FID/TCD
Lower Enclosure ........................................... 4-6
4.3.2 Detector Elements, Heater Elements,
Valves and Columns ...................................... 4-7

MAINTENANCE AND TROUBLESHOOTING SEP 2005


TABLE OF CONTENTS v
Model 700

4.4 PRECAUTIONS FOR HANDLING


PC ASSEMBLIES ......................................... 4-11

4.5 GENERAL TROUBLESHOOTING..................... 4-12


4.5.1 Hardware Alarms ........................................ 4-12
4.5.2 Troubleshooting Checklist ............................ 4-14
4.5.3 Test Points Dual Methods Board and FTB ....... 4-19
4.5.4 Preamplifier ................................................ 4-22
4.5.5 Flow Balance Check .................................... 4-22
4.5.6 Temperature ............................................... 4-22
4.5.7 FID Configuration ........................................ 4-25
Baseline Drift .............................................. 4-26

4.6 LEAK CHECKS ............................................ 4-27


4.6.1 Field Service ............................................... 4-27
4.6.2 Factory Level Leak Check............................. 4-28
4.6.3 Plugged Lines, Columns, or Valves ................ 4-31

4.7 CHROMATOGRAPH VALVES........................ 4-31


4.7.1 Required Tools ............................................ 4-31
4.7.2 Chromatograph Valve Replacement Parts ....... 4-32
4.7.3 Valve Cleaning............................................ 4-32
4.7.4 TCD Oven System Removal.......................... 4-33
4.7.5 Micro-FID Removal ...................................... 4-36
4.7.6 Micro-FID Maintenance ................................ 4-39
4.7.7 Micro-FID Re-assembly................................. 4-39
4.7.8 Maintenance............................................... 4-41
4.7.9 LSIV Removal ............................................. 4-41
Replacing LSIV Seals ................................... 4-42
LSIV Disassembly........................................ 4-43
4.7.10 Methanator Maintenance.............................. 4-45
4.7.11 Valve Overhaul ........................................... 4-46
4.7.12 Oven System and Stream Switching
System Solenoid Valve Replacement ............. 4-48

SEP 2005 MAINTENANCE AND TROUBLESHOOTING


vi TABLE OF CONTENTS
Model 700

4.7.13 Solenoid Valve Replacement ......................... 4-49

4.8 TCD DETECTOR BRIDGE BALANCE ............... 4-52

4.9 MEASURE VENT FLOW ............................... 4-55

4.10 MODEL 700 ELECTRICAL COMPONENTS ...... 4-56


4.10.1 DC Power Supply Replacement Procedures..... 4-59

4.11 COMMUNICATIONS .................................... 4-61


Model 700 GC with the TCD ........................ 4-61
Model 700 GC with the Micro-FID/TCD.......... 4-61

4.12 ANALOG INPUTS/OUTPUTS ......................... 4-65


4.12.1 Model 700 Analog Inputs ............................. 4-66
4.12.2 Analog Output Adjustment ........................... 4-67
4.12.3 Model 700 Analog Outputs .......................... 4-68
Standard Analog Outputs ............................. 4-68

4.13 DISCRETE DIGITAL INPUTS/OUTPUTS .......... 4-70

4.14 RECOMMENDED SPARE PARTS.................... 4-70

4.15 UPGRADE PROCEDURES ............................. 4-71


4.15.1 Base Operating System ................................ 4-71
4.15.2 Applications ............................................... 4-71

APPENDIX A, A.1 TCD SERIAL COMMUNICATIONS....................A-1


COMMUNICATIONS
SPECIFICATIONS A.1.1 Model 700 with a TCD Comm Ports ................A-2

A.2 FID SERIAL COMMUNICATIONS .....................A-7

A.2.1 Connecting Serial Communications to the GC .A-10


RS-232 Ports..............................................A-11
RS-422 Ports..............................................A-11
RS-485 Serial Specifications.........................A-11

APPENDIX A, COMMUNICATIONS SPECIFICATIONS SEP 2005


TABLE OF CONTENTS vii
Model 700

A.2.2 FTB Serial Communications ..........................A-12


WinSystems CPU ........................................A-15
WinSystems MCM/LPM – Com4A Board ........A-19
Com4A Board Compatibility Settings .............A-23
WinSystems Ethernet Board .........................A-24
Radicom 56K Baud Modem Board .................A-25

A.3 WIRING LOCAL RS-232 COMMUNICATIONS..A-25

A.3.1 GC Serial Port and Cable Configurations.........A-25


A.3.2 GC DB 9-pin Serial Port to PC DB 9-pin Port ...A-29
A.3.3 GC DB 9-pin Serial Port to PC DB 25-pin Port .A-30
A.3.4 GC PHOENIX Plug Port to PC DB 9-pin Port ....A-31
A.3.5 GC PHOENIX Plug Port to PC DB 25-pin Port ..A-32

A.4 WIRING REMOTE RS-232


COMMUNICATIONS ....................................A-33

A.4.1 GC DB 9-pin Serial Port to Modem


DB 25-pin Port ............................................A-33
A.4.2 GC PHOENIX Plug to Modem
DB 25-pin Port ............................................A-34

A.5 EXAMPLE RS-422 PC-GC CONNECTION ........A-35

A.6 EXAMPLE RS-485 PC-GC CONNECTION ........A-37

SEP 2005 APPENDIX A, COMMUNICATIONS SPECIFICATIONS


viii TABLE OF CONTENTS
Model 700

APPENDIX B, MODEM B.1 OPTIONAL INTERNAL MODEM ....................... B-1


INSTALLATION
B.1.1 Optional Ethernet Board ................................. B-3

APPENDIX C, C.1 CARRIER GAS ..............................................C-1


MANIFOLD CARRIER
FOR GAS BOTTLES C.2 INSTALLATION AND LINE PURGING................C-2

C.3 REPLACING CARRIER CYLINDER ....................C-3

C.4 CALIBRATION GAS .......................................C-4

APPENDIX D, D.1 LIST OF ENGINEERING DRAWINGS .................D-1


ENGINEERING
DRAWINGS

Appendix B, MODEM INSTALLATION SEP 2005


LIST OF FIGURES ix
Model 700

LIST OF FIGURES

Figure 1-1 Block Diagram Upper Enclosure with TCD ........................................1-3


Figure 1-2 Block Diagram Upper Enclosure with Micro-FID.................................1-4
Figure 1-3 Block Diagram TCD Lower Enclosure ...............................................1-6
Figure 1-4 Block Diagram Micro-FID Lower Enclosure........................................1-7
Figure 1-5 Analyzer Assembly with TCD Detector Bridge ................................ 1-16
Figure 1-6 Detector Output During Component Elution .................................... 1-17
Figure 1-7 Analyzer Assembly with Micro-FID Detector Bridge ......................... 1-18
Figure 1-8 Model 700 LSIV Assembly ........................................................... 1-19
Figure 1-9 Model 700 Methanator Assembly ................................................. 1-21
Figure 2-1 Model 700 Gas Chromatograph ......................................................2-1
Figure 2-2 Upper Enclosure Assembly .............................................................2-2
Figure 2-3 TCD Oven System Assembly..........................................................2-3
Figure 2-4 Model 700 Micro-FID Upper Assembly.............................................2-4
Figure 2-5 Model 700 Methanator Upper Assembly ..........................................2-5
Figure 2-6 LSIV Assembly .............................................................................2-6
Figure 2-7 SSS Installed................................................................................2-7
Figure 2-8 Lower Enclosure Assembly.............................................................2-8
Figure 2-9 Upper Electronics with TCD Block Diagram .................................... 2-13
Figure 2-10 Upper Electronics with Micro-FID Block Diagram ............................. 2-14
Figure 2-11 Lower Electronics TCD Block Diagram ........................................... 2-15
Figure 2-12 Lower Electronics Micro-FID Block Diagram .................................... 2-16
Figure 3-1 Lower Enclosure Disassembly.........................................................3-5
Figure 3-2 Card Cage Cable Disassembly ........................................................3-6
Figure 3-3 Card Cage Assembly Screw Locations .............................................3-7
Figure 3-4 Card Cage Disassembly .................................................................3-8
Figure 3-5 Card Cage Disassembly for Power and Signal Wiring .........................3-9
Figure 3-6 Stream Inlets (Right side of unit)................................................... 3-15
Figure 3-7 DC Power Wiring ........................................................................ 3-24

SEP 2005 List of Figures


x LIST OF FIGURES
Model 700

Figure 3-8 AC/DC Power Converter .............................................................. 3-26


Figure 3-9 Calibration Gas Stream Inlet (Right side of unit) .............................. 3-31
Figure 3-10 Sample Stream Inlets (Right side of unit) ....................................... 3-32
Figure 3-11 Dip Switch................................................................................. 3-33
Figure 3-12 Oven Mounting Bracket ............................................................... 3-34
Figure 3-13 Multifunction Board Location........................................................ 3-35
Figure 3-14 Dip Switch................................................................................. 3-35
Figure 3-15 Field Termination Board ............................................................... 3-41
Figure 3-16 Configuration without Com4A Board ............................................. 3-42
Figure 3-17 Configuration with Com4A Board ............................................... 3-43
Figure 3-18 FTB Com1 and Com2 DB 9-pin Connector ..................................... 3-44
Figure 3-19 FTB Com 1 DB 9-pin Phoenix Connector........................................ 3-45
Figure 3-20 FTB Com2 DB 9-pin Phoenix Connector ......................................... 3-45
Figure 3-21 FTB Com5 DB 9-pin Phoenix Connector ......................................... 3-46
Figure 3-22 FTB Com6 DB 9-pin Phoenix Connector ......................................... 3-46
Figure 3-23 FTB Com7 DB 9-pin Phoenix Connector ......................................... 3-47
Figure 3-24 Com8 DB 9-pin Phoenix Connector GC Phoenix Plug Port ................ 3-47
Figure 3-25 GC Phoenix Plug Port to External Modem DB 25-pin Port ................. 3-48
Figure 3-26 Field Termination Board ............................................................... 3-51
Figure 4-1 Model 700 with TCD/Micro-FID Front View...................................... 4-5
Figure 4-2 CPU, Com4A, and Modem Boards .................................................. 4-7
Figure 4-3 Upper Explosion-proof Housing ....................................................... 4-8
Figure 4-4 Thermal Conductivity Detector ....................................................... 4-9
Figure 4-5 Flame Ionization Detector .............................................................. 4-9
Figure 4-6 Test Points Dual Methods Board (Cut View) ................................... 4-19
Figure 4-7 Test Points Dual Methods Board ................................................... 4-20
Figure 4-8 Test Points Field Termination Board (Cut View) .............................. 4-20
Figure 4-9 Test Points Field Termination Board .............................................. 4-21
Figure 4-10 Temperature Control Dialog.......................................................... 4-23
Figure 4-11 Chromatograph Valve Assemblies ................................................. 4-32
Figure 4-12 Micro-FID Oven System Thermal Cover ......................................... 4-33
Figure 4-13 TCD Upper Assembly Components ............................................... 4-34

List of Figures SEP 2005


LIST OF FIGURES xi
Model 700

Figure 4-14 TCD Oven System Disassembly .................................................... 4-35


Figure 4-15 Micro-FID Upper Assembly Components ........................................ 4-37
Figure 4-16 Model 700 with Micro-FID Upper Assembly ................................... 4-38
Figure 4-17 Model 700 with LSIV .................................................................. 4-43
Figure 4-18 Model 700 Optional Methanator Assembly..................................... 4-45
Figure 4-19 TCD Valve Tubing and Fittings ..................................................... 4-47
Figure 4-20 Side View TCD Oven System Mounting Bracket ............................. 4-49
Figure 4-21 Rotated TCD Upper Assembly ...................................................... 4-50
Figure 4-22 Stream Switching Assembly......................................................... 4-51
Figure 4-23 Stream Switching System Final Assembly ...................................... 4-52
Figure 4-24 Model 700 Micro-FID/TCD Preamplifier .......................................... 4-53
Figure 4-25 Model 700 TCD Bridge Balance .................................................... 4-54
Figure 4-26 Model 700 Micro-FID Bridge Balance ............................................. 4-54
Figure 4-27 Measure Flow Vents ................................................................... 4-55
Figure 4-28 Model 700 Lower Enclosure ......................................................... 4-57
Figure 4-29 Model 700 Card Stack Assembly .................................................. 4-57
Figure 4-30 Model 700 Lower Assembly......................................................... 4-58
Figure 4-31 DC Power Supply Lower Enclosure................................................ 4-59
Figure 4-32 Dip Switch................................................................................. 4-62
Figure 4-33 Multifunction Board..................................................................... 4-63
Figure 4-34 Analog Board - Inputs.................................................................. 4-66
Figure 4-35 Analog Inputs............................................................................. 4-67
Figure 4-36 FTB Board Analog Outputs........................................................... 4-68
Figure 4-37 Analog Outputs .......................................................................... 4-69
Figure 4-38 Optional Analog Board Outputs..................................................... 4-69
Figure A-1 Standard Configuration without LOI and Com4A Board..................... A-3
Figure A-2 Configuration with LOI ................................................................. A-3
Figure A-3 Configuration with Com4A Board................................................... A-4
Figure A-4 Configuration with Com4A Board and LOI ....................................... A-5
Figure A-5 FTB Com1 and Com2 DB9 Connector............................................. A-6

SEP 2005 List of Figures


xii LIST OF FIGURES
Model 700

Figure A-6 Configuration without Com4A Board ...............................................A-8


Figure A-7 Configuration with Com4A Board ...................................................A-9
Figure A-8 FTB Com1 DB 9-pin Phoenix Connector .........................................A-12
Figure A-9 FTB Com2 DB 9-pin Phoenix Connector........................................A-12
Figure A-10 FTB Com5 DB 9-pin Phoenix Connector .........................................A-13
Figure A-11 FTB Com6 DB 9-pin Phoenix Connector........................................A-13
Figure A-12 FTB Com7 DB 9-pin Phoenix Connector .........................................A-14
Figure A-13 FTB Com8 DB 9-pin Phoenix Connector .........................................A-14
Figure A-14 FTB Serial Connections................................................................A-26
Figure A-15 FTB Serial Connections................................................................A-26
Figure A-16 Phoenix Connector (J5, J6, J10, and J11) Pinout ...........................A-27
Figure A-17 DB 9-pin Connector (P2 and P3) and Pinout for Jacks .....................A-28
Figure A-18 GC DB 9-pin Port to PC DB 9-pin Port ...........................................A-29
Figure A-19 GC DB 9-pin Port to PC DB 25-pin Port..........................................A-30
Figure A-20 GC DB 9-pin Port to PC DB 25-pin Port..........................................A-31
Figure A-21 GC Phoenix Plug Port to PC DB 25-pin Port....................................A-32
Figure A-22 GC DB 9-pin Port to External Modem DB 25-pin Port .......................A-33
Figure A-23 GC Phoenix Plug Port to External Modem DB 25-pin Port .................A-34
Figure A-24 Example RS-422 Serial Cable Terminations ....................................A-35
Figure A-25 Example RS-485 Serial Cable Terminations, Line Driver
to GC Controller Com3 ................................................................A-37
Figure A-26 Example RS-485 Serial Cable Terminations, Line Driver to
GC Controller Com4....................................................................A-38
Figure B-1 Radicom 56K Baud Modem Installation ............................................ B-2
Figure C-1 Manifold for Two Carrier Gas Bottles to GC System ..........................C-1

List of Figures SEP 2005


LIST OF TABLES xiii
Model 700

LIST OF TABLES

Table 2-1 Model 700 Unit Specifications...................................................... 2-11


Table 2-2 Electronic Hardware Specification ................................................. 2-17
Table 2-3 Oven Assembly Specifications...................................................... 2-18
Table 2-4 Software Specifications ............................................................... 2-19
Table 3-1 DC Power Wiring ........................................................................ 3-24
Table 3-2 AC Wiring.................................................................................. 3-27
Table 3-3 Modbus Slave Address (Com ID) DIP Switch Settings...................... 3-36
Table 3-4 Switch Positions for Cold Start ..................................................... 3-37
Table 3-5 FTB Discrete Digital Inputs ........................................................... 3-52
Table 3-6 FTB Discrete Digital Outputs ........................................................ 3-53
Table 3-7 FTB Analog Inputs ...................................................................... 3-54
Table 3-8 FTB Analog Outputs.................................................................... 3-55
Table 3-9 Optional Analog Outputs.............................................................. 3-56
Table 3-10 J8 Modem Board Jumper Settings ................................................ 3-57
Table 3-11 J9 Modem Board Jumper Settings ................................................ 3-57
Table 3-12 J10 Modem Board Jumper Settings .............................................. 3-57
Table 3-13 J26 Radicom Modem Jumper Settings .......................................... 3-58
Table 3-14 J27Radicom Modem Jumper Settings ........................................... 3-58
Table 3-15 J30 Radicom Modem Jumper Settings .......................................... 3-58
Table 3-16 J31 Radicom Modem Jumper Settings .......................................... 3-58
Table 3-17 J1 PCM-NE2000 Ethernet Board Jumper Settings ........................... 3-59
Table 3-18 J2 PCM-NE2000 Ethernet Board Jumper Settings ........................... 3-59
Table 3-19 J3 PCM-NE2000 Ethernet Board Jumper Settings ........................... 3-59
Table 4-1 Maintenance Checklist...................................................................4-3
Table 4-2 Basic Hardware Troubleshooting via Alarms ................................... 4-12
Table 4-3 Troubleshooting Checklist ............................................................ 4-16
Table 4-4 Temperature Control Dialog.......................................................... 4-24
Table A-1 Matrix of Possible TCD Configurations Field Termination Board.......... A-1

SEP 2005 List of Tables


xiv LIST OF TABLES
Model 700

Table A-2 Matrix of Possible FID Configurations Field Termination Board ............A-7
Table A-3 Communication with WinSystems CPU..........................................A-15
Table A-4 Communication with WinSystems CPU..........................................A-16
Table A-5 Communication with WinSystems CPU..........................................A-17
Table A-6 Communication with WinSystems CPU..........................................A-18
Table A-7 Communication with WinSystems MCM/LPM –
Com4A Board (Optional) ..............................................................A-19
Table A-8 J10 Jumper Settings...................................................................A-23
Table A-9 J7 Jumper Settings.....................................................................A-23
Table A-10 J8 Jumper Settings.....................................................................A-23
Table A-11 J9 Jumper Settings.....................................................................A-23
Table A-12 Ethernet Board Pin Settings..........................................................A-24
Table A-13 J26 Radicom Modem Jumper Settings ..........................................A-25
Table A-14 J27 Radicom Modem Jumper Settings ..........................................A-25
Table A-15 J30 Radicom Modem Jumper Settings ..........................................A-25
Table A-16 J31 Radicom Modem Jumper Settings ..........................................A-25
Table A-17 Serial Ports on Field Termination Board..........................................A-27
Table A-18 Switch Settings for LD485A-MP, RS-422 to GC .............................A-36
Table A-19 Jumper Settings for LD485A-MP, RS-422 to GC ............................A-36
Table A-20 Switch Settings for LD485A-MP, RS-485 to GC .............................A-39
Table A-21 Jumper Settings for LD485A-MP, RS-485 to GC ............................A-39
Table C-1 Contents of Example Calibration Gas...............................................C-4

List of Tables SEP 2005


INTRODUCTION 1-1
Model 700

INTRODUCTION
1

This section describes the contents and purpose


of the Model 700 Gas Chromatograph System
Reference Manual, a description of the Model
700 system, an explanation of the theory of
operation, and a glossary of chromatograph
terminology.

Use this section to get acquainted with the


basic engineering of the Model 700 product.

1.1 DESCRIPTION OF MANUAL

The Model 700 Gas Chromatograph System


Reference Manual (P/N 3-9000-521) consists of
Installation, Operations, and Maintenance and
Troubleshooting Procedures. Also, included is
information about the MON2000 software
interface.

1.2 SYSTEM DESCRIPTION

The Model 700 is a high-speed gas


chromatograph (GC) system that is engineered
to meet specific field application requirements
based on typical natural gas stream
composition and anticipated concentration of
the selected components. In its standard
configuration, the Model 700 can handle up to
four streams: typically, three for sample and
one for calibration.

The Model 700 system consists of three major


parts: the Analyzer Assembly, Controller
Assembly, and Sample Conditioning System
(SCS).

Model 700 subsystems are: a Flame Ionization


Detector (Micro-FID), a Liquid Sample Injector
(LSIV) and a Methanator.

SEP 2005 Description of Manual


1-2 INTRODUCTION
Model 700

Analyzer Assembly

The Analyzer Assembly (upper enclosure)


includes columns TCD/Micro-FID detectors,
Methanator, preamplifier, preamplifier power
supply, stream switching valves, and solenoids.
See Figure 1-2 Block Diagram Upper
Enclosure for TCD details and Figure 1-5
Block Diagram Upper Enclosure for Micro-FID
details. Additionally, the Model 700 may be
equipped with the Liquid Sample Inject Valve
(LSIV) or a Methantor.

System Description SEP 2005


INTRODUCTION 1-3
Model 700

Figure 1-1 Block Diagram Upper Enclosure with TCD

SEP 2005 System Description


1-4 INTRODUCTION
Model 700

PREAMPLIFIER PCB
PREAMPLIFIER P/S PCB
INPUTS:
DC-DC CONVERTERS 1 TCD DETECTOR
24VDC INPUT 1 FID DETECTOR
24VDC POWER
OUTPUTS OUTPUTS:
+20VDC -20VDC COM (1)
100VDC (RS-232 OR RS-485)
5VDC

3.3 VDC

SERIAL I/O

SOLENOID/HEATER
DRIVER PCB

DC-DC CONVERTERS
24 VDC INPUT
OUTPUTS
5VDC
SOLENOID DRIVERS (16)
HEATERS (4 ZONES)

MULTIFUNCTION SERIAL PORT RS-232


MICRO-CONTROLLER PCB

HEATER PWM CONTROLLER


(4 ZONES)

DIGITAL INPUTS.................(5)
COM RS-232......................(1)
RTD INPUTS.......................(4)
ANALOG INPUTS 4-20mA....(4)
DIGITAL OUTPUTS..............(5) SERIAL PERIPHEERAL INTERFACE
SERIAL DAC CONTROL........(SPI)

Figure 1-2 Block Diagram Upper Enclosure with Micro-FID

System Description SEP 2005


INTRODUCTION 1-5
Model 700

Controller Assembly

The Controller Assembly (lower enclosure)


includes electronics and ports for signal
processing, instrument control, data storage,
personal computer (PC) interface, and telecom-
munications. This assembly allows the user to
control the GC functions via a PC with the
MON2000 software package (see Section 1.3).

SEP 2005 System Description


1-6 INTRODUCTION
Model 700

See Figure 1-3 and Figure 1-4 for lower


enclosure block diagrams.

Figure 1-3 Block Diagram TCD Lower Enclosure

System Description SEP 2005


INTRODUCTION 1-7
Model 700

INPUT OPTIONAL
AC POWER AC-DC
POWER SUPPLY

24 VDC

FIELD TERMINATION PCB OPTIONAL ANALOG


BUILT IN SURGE PROTECTION OUTPUT PCB
FIELD WIRING FOR THE FOLLOWING: 4 ISOLATED OR
8 NON-ISOLATED
COM 1 & 2, 5-8
ANALOG INPUTS 4-20mA.......(4)
ANALOG OUTPUTS 4-20mA....(4)
DIGITAL INPUTS.....................(5)

DIGITAL OUTPUTS (5) RELAYS


2 RELAYS FORM “A” CONTACT
3 SOLID STATE RELAYS
ANALYZER INTERCONNECT
POWER FOR STANDARD BUS
DC-DC CONVERTER SIGNALS - POWER
OUTPUTS STD-BUS
5VDC, +12VDC, -12 VDC
- 3.8VDC

CPU
MULTIFUNCTION COM 3
COM4A PCB
COM 5-8
FID & TCD PREAMPLIFIER COM 4
ETHERNET PCB

INTERNAL MODEM

OPTIONAL PC104

BOARD STACK

Figure 1-4 Block Diagram Micro-FID Lower Enclosure

SEP 2005 System Description


1-8 INTRODUCTION
Model 700

The GC-PC interface provides the user with the


greatest capability, ease-of-use, and flexibility.
One PC running MON 2000 can connect with
up to 32 chromatographs (via RS-485 serial
communications links). MON 2000 is used to
edit applications, monitor operations, calibrate
streams, and display analysis chromatograms
and reports, which can then be stored to files
on the PC hard drive or printed from either the
PC printer port or the GC printer port.

Sample Conditioning System (SCS)

The sample conditioning system is located


between the process stream and the Analyzer
Assembly sample inlet (mounted on the lower
portion of the Analyzer Assembly stand). The
standard configuration includes a Stream
Switching System and filters.

The Model 700 electronics and hardware are


housed in two explosion-proof enclosures and
meet IEC Class I, Zone 1, Ex d IIB+H2, T4
(NEC Class 1, Division 1, Groups B, C, and D)
approval for use in a hazardous environment.

System Description SEP 2005


INTRODUCTION 1-9
Model 700

1.2.1 Functional Description

A sample of the gas to be analyzed is taken


from the process stream by a sample probe
installed in the process line. The sample passes
through a sample line to the SCS where it is
filtered or otherwise conditioned. After
conditioning, the sample flows to the Analyzer
Assembly for separation and detection of the
gas components.

DANGER TO PERSONNEL AND EQUIPMENT


Do not use a PC or a printer in a hazardous area.
Serial port and Modbus communications links are
provided to connect the unit to the PC and to
connect to other computers and printers in a safe
area.
Failure to follow this warning may result in injury or
death to personnel or cause damage to the
equipment.

The chromatographic separation of the sample


gas into its components is accomplished in the
following manner. A precise volume of sample
gas is injected into one of the analytical
columns. The column contains a stationary
phase (packing) that is either an active solid or
an inert solid support that is coated with a
liquid phase (absorption partitioning). The
sample gas is moved through the column by
means of a mobile phase (carrier gas). The
selective retardation of the components takes
place in the column, causing each component to
move through the column at a different rate.
This separates the sample into its constituent
gases and vapors.

SEP 2005 System Description


1-10 INTRODUCTION
Model 700

A detector located at the outlet of the analytical


column senses the elution of components from
the column and produces electrical outputs
proportional to the concentration of each
For additional information,
see Section 1.4 component. Outputs from the detector(s) are
amplified in the Analyzer Assembly electronics,
then transmitted to the Controller Assembly
for further processing.

Output from the Controller Assembly is


normally displayed on a remotely located PC or
a printer. Connection between the Controller
Assembly and the PC can be accomplished via a
direct serial line or via a Modbus-compatible
communication interface.

Several chromatograms may be displayed via


MON2000, with separate color schemes,
allowing the user to compare present and past
data.

Use of the MON2000 software for configuration


and troubleshooting procedures is essential in
most cases. The PC may be remotely connected
via telephone, radio or satellite communica-
tions. Once installed and configured, the Model
700 can operate independently for long periods
of time.

System Description SEP 2005


INTRODUCTION 1-11
Model 700

1.2.2 Available Functions

Individual GC functions that can be initiated or


controlled by the GC system and its software,
MON2000, include (but are not limited to) the
following:

• valve activations
• timing adjustments
• stream sequences
• calibrations
• baseline runs
• analyses
• halt operation
• stream/detector assignments
• stream/component table assignments
• stream/calculation assignments
• diagnostics
• alarm and event processing
• event sequence changes
• component table adjustments
• calculation adjustments
• alarm parameters adjustments
• analog scale adjustments

SEP 2005 System Description


1-12 INTRODUCTION
Model 700

Reports and logs that can be produced,


depending upon the GC application in use,
include (but are not limited to) the following:

• Configuration Report
• Parameter List
• Analysis Chromatogram
• Chromatogram Comparison
• Alarm Log (unacknowledged and active
alarms)
• Event Log
• Various Analysis Reports

System Description SEP 2005


INTRODUCTION 1-13
Model 700

1.3 SOFTWARE DESCRIPTION

The MON2000 uses three distinct types of


software. This enables total flexibility in
defining the calculation sequence, printed
report content, format, type and amount of
data for viewing, control and/or transmission to
another computer or Controller Assembly. The
three types are:

• Baseline Operating System (BOS)


• Application configuration software
• Maintenance and Operations software
(MON2000 version 2.2 or later)

The BOS and the Application configuration


software are installed when the
Model 700 system is shipped. The application
configuration is tailored to the customer’s
process and shipped on a floppy disk. Note that
the hardware and software are tested together
as a unit before the equipment leaves the
factory. The MON2000 software program
communicates with the Model 700 system and
allows an initial site system setup (i.e.,
operational parameters, application
modifications, and maintenance).

BOS

The Baseline Operating System (BOS)


supervises operation of the Model 700 through
its internal microprocessor-based controller; all
direct hardware interface is via this control
software. It consists of a multi-tasking program
that controls separate tasks in system
operation, as well as hardware self-testing,
user application downloading, start-up, and
communications. Once configured, a Model 700
can operate as a stand alone unit.

SEP 2005 Software Description


1-14 INTRODUCTION
Model 700

MON2000

MON2000, available as a Windows-based


program, provides the human-machine
interface for maintenance, operation, and
troubleshooting. It allows the user to download
applications developed for a specific GC unit.
MON2000 provides operator control of the
connected Model 700, monitors analysis
results, and inspects and edits various
parameters that affect Model 700 operation. It
also controls display and printout of the
chromatograms and reports, and it stops and
starts automatic analysis cycling or calibration
runs.

After the equipment/software has been


installed and the operation stabilized,
automatic operation can be initiated. The link
between the MON2000 computer and the
Model 700 can either be direct, via a local serial
connection or remote, via an ethernet network,
modems, telephone lines and/or radio.

Operation of multiple Model 700


chromatographs (up to 32) with a single
MON2000 computer, via a multi-drop serial
link, is also supported.

Software Description SEP 2005


INTRODUCTION 1-15
Model 700

1.4 THEORY OF OPERATION

The following sections discuss the theory of


See Section 1.7 for operation for the Model 700, the engineering
definitions of the principles and concepts used.
terminology used in the
following explanations. 1.4.1 Thermal Conductivity Detector (TCD)

One of the detectors (located on the oven in the


Analyzer upper assembly) is a thermal
conductivity detector that consists of a
balanced bridge network with heat sensitive
thermistors in each leg of the bridge. Each
thermistor is enclosed in a separate chamber of
the detector block.

One thermistor is designated the reference


element and the other the measurement
element. See Figure 1-5 for a schematic
diagram of the thermal conductivity detector
(TCD).

SEP 2005 Theory of Operation


1-16 INTRODUCTION
Model 700

Figure 1-5 Analyzer Assembly with TCD Detector Bridge

In the quiescent condition (prior to injecting a


sample), both legs of the bridge are exposed to
pure carrier gas. In this condition, the bridge is
balanced and the bridge output is electrically
nulled. (The bridge can be balanced by the fine
and coarse adjustment potentiometers located
on the preamplifier circuit board.)

The analysis begins when a fixed volume of


sample is injected into the column by operation
of the sample valve. The sample is moved
through the column by the continuous flow of
carrier gas. As successive components elute
from the column, the temperature of the
measurement element changes.

Theory of Operation SEP 2005


INTRODUCTION 1-17
Model 700

The temperature change unbalances the bridge


and produces an electrical output proportional
to the component concentration.

The differential signal developed between the


two thermistors is amplified by the
preamplifier. Figure 1-6 illustrates the change
in detector electrical output during elution of a
component.

1 2 1

1 detector bridge balanced

component begins to elute from column


2 and is measured by thermistor

3 peak concentration of component

Figure 1-6 Detector Output During Component Elution

In addition to amplifying the differential signal


developed between the two thermistors, the
preamplifier supplies drive current to the
detector bridge. The voltage signal is converted
to a 4-20 milliampere (mA) current loop for
transmission to the Controller Assembly.

The signal is proportional to the concentration


of a component detected in the gas sample. The
preamplifier provides four different gain
channels as well as compensation for baseline
drift.

SEP 2005 Theory of Operation


1-18 INTRODUCTION
Model 700

The signals from the preamplifier are sent to


the Controller Assembly for computation,
recording on a printer, or viewing on a PC
monitor (via MON2000).

1.4.2 Flame Ionization Detector (Micro-FID)

The other detector (located on the oven in the


Analyzer Assembly) is a Flame Ionization
Detector. The Micro-FID requires a
polarization voltage and its output is connected
to the input to a high impedance amplifier
which is called an Electrometer. The burner
uses a mixture of hydrogen and air to maintain
the flame. The sample of gas to be measured is
also injected into the burner. See Figure 1-7 for
a schematic diagram of the Flame Ionization
Detector (Micro-FID).

Figure 1-7 Analyzer Assembly with Micro-FID Detector Bridge

Theory of Operation SEP 2005


INTRODUCTION 1-19
Model 700

1.4.3 LSIV

The Liquid Sample Inject Valve (LSIV)


penetrates the wall of the upper enclosure and
is held in place by a retaining ring. The
mounting arrangement is designed to ensure
integrity of the flameproof enclosure.
Model 700 LSIV Upper Enclosure

Retaining Ring Piston Housing

Retraction Actuation
Air Inlet Air Inlet

Figure 1-8 Model 700 LSIV Assembly

The outermost end houses an air operated


piston. Air at 15 to 45 psi is directed by a
solenoid valve to either advance the stem to
inject the sample or to retract the stem.

The next section houses an auxiliary stem seal


assist. A piston driven by air at 80 to 100 psi
keeps adequate load on the stem seal to
counteract wear at the high temperatures and
pressures that might be encountered. There
are two ¼"npt ports in this section; one port
retracts the sample piston and the other port
activates the seal assist.

SEP 2005 Theory of Operation


1-20 INTRODUCTION
Model 700

The innermost section houses the stem seals


and the sample chamber. There are five ¼" npt
ports in this section.

Within the enclosure cavity are the flash


chamber components surrounded with
insulating covers. At working temperatures,
the surfaces of these covers become very hot to
the touch.

The tip of the LSIV is the port where flashed


sample is taken to the oven system.

The port at right angles to the length of the


LSIV is the input for carrier gas.

The heater block, a cylinder of aluminum, is


installed off-center surrounding the flash
chamber, close to the wall of the upper
enclosure. It houses the heater and an RTD
and is retained by a jamb nut that should only
be finger tight.

Theory of Operation SEP 2005


INTRODUCTION 1-21
Model 700

1.4.4 Methanator

After all other components have been


separated from the sample, normally
undetectable CO and CO2 are sent through the
methanator. They are combined with hydrogen
to make methane in a heat generated catalytic
reaction. The methanator is also known as a
methanizer or a catalytic converter.
Model 700 Methanator Upper Enclosure

Methanator
Assembly

Figure 1-9 Model 700 Methanator Assembly

SEP 2005 Theory of Operation


1-22 INTRODUCTION
Model 700

1.4.5 Data Acquisition

Every second, exactly 40 equi-spaced data


samples are taken (i.e., one data sample every
25 milliseconds) for analysis by the Controller
Assembly. The sampling frequency of 40 Hertz
(Hz) was chosen to reduce normal mode noise
(at 60 Hz).

After each point on the chromatograph signal is


sampled, the resulting number is stored for
processing in a buffer area of the Controller
Assembly memory. During the analysis, only
the last 256 data points are available for
processing.

Because the data analysis is done as the signal


is sampled (in real-time), only a limited
number of past data samples is required to
analyze any signal.

As a part of the data acquisition process,


groups of incoming data samples are averaged
together before the result is stored for
processing. Non-overlapping groups of N
samples are averaged and stored, and thus
reduce the effective incoming data rate to 40/N
samples per second. For example, if N = 5, then
a total of 40/5 or 6 (averaged) data samples are
stored every second.

The value for the variable N is determined by


the selection of a Peak Width parameter (PW).
The relationship is

N = PW

where PW is given in seconds. Allowable values


of N are 1 to 63; this range corresponds to PW
values of 2 to 63 seconds.

Theory of Operation SEP 2005


INTRODUCTION 1-23
Model 700

The variable N is known as the integration


factor. This term is used because N determines
how many points are averaged, or integrated,
to form a single value. The integration of data
upon input, before storing, serves two
purposes:

• The statistical noise on the input signal is


reduced by the square root of N. In the case
of N = 4, a noise reduction of two would be
realized.
• The integration factor controls the
bandwidth of the chromatograph signal. It
is necessary to match the bandwidth of the
input signal to that of the analysis
algorithms in the Controller Assembly. This
prevents small, short-duration
perturbations from being recognized as true
peaks by the program. It is therefore
important to choose a Peak Width that
corresponds to the narrowest peak in the
group under consideration.

1.4.6 Peak Detection

For normal area or peak height concentration


evaluation, the determination of a peak's start
point and end point is automatic. The manual
The Controller Assembly determination of start and end points is used
software assumes that a only for area calculations in the Forced
region of signal quiescence
and stability will exist.
Integration mode. Automatic determination of
peak onset or start is initiated whenever
Integrate Inhibit is turned off. Analysis is
started in a region of signal quiescence and
stability, such that the signal level and activity
can be considered as baseline values.

SEP 2005 Theory of Operation


1-24 INTRODUCTION
Model 700

Having initiated a peak search by turning


Integrate Inhibit off, the Controller Assembly
performs a point by point examination of the
signal slope. This is achieved by using a digital
slope detection filter, a combination low pass
filter and differentiator. The output is
continually compared to a user-defined system
constant called Slope Sensitivity. A default
value of 8 is assumed if no entry is made.
Lower values make peak onset detection more
sensitive, and higher values make detection
less sensitive. Higher values (20 to 100) would
be appropriate for noisy signals, e.g. high
amplifier gain.

Onset is defined where the detector output


exceeds the baseline constant, but peak
termination is defined where the detector
output is less than the same constant.

Sequences of fused peaks are also


automatically handled. This is done by testing
each termination point to see if the region
immediately following it satisfies the criteria of
a baseline. A baseline region must have a slope
detector value less than the magnitude of the
baseline constant for a number of sequential
points. When a baseline region is found, this
terminates a sequence of peaks.

A zero reference line for peak height and area


determination is established by extending a
line from the point of the onset of the peak
sequence to the point of the termination. The
values of these two points are found by
averaging the four integrated points just prior
to the onset point and just after the
termination points, respectively.

Theory of Operation SEP 2005


INTRODUCTION 1-25
Model 700

The zero reference line will, in general, be non-


horizontal, and thus compensates for any
linear drift in the system from the time the
peak sequence starts until it ends.

In a single peak situation, peak area is the area


of the component peak between the curve and
the zero reference line. The peak height is the
distance from the zero reference line to the
maximum point on the component curve. The
value and location of the maximum point is
determined from quadratic interpolation
through the three highest points at the peak of
the discrete valued curve stored in the
Controller Assembly.

For fused peak sequences, this interpolation


technique is used both for peaks, as well as,
valleys (minimum points). In the latter case,
lines are dropped from the interpolated valley
points to the zero reference line to partition the
fused peak areas into individual peaks.

The use of quadratic interpolation improves


both area and height calculation accuracy and
eliminates the effects of variations in the
integration factor on these calculations.

For calibration, the Controller Assembly may


average several analyses of the calibration
stream.

SEP 2005 Theory of Operation


1-26 INTRODUCTION
Model 700

1.5 BASIC ANALYSIS COMPUTATIONS

Two basic analysis algorithms are included in


For additional information the Controller Assembly:
about other calculations
performed, see the • Area Analysis – calculates area under
MON2000 Software for Gas component peak
Chromatographs User
Manual (P/N 3-9000-522). • Peak Height Analysis – measures height of
component peak

1.5.1 Conc Analysis - Response Factor

Concentration calculations require a unique


response factor for each component in an
analysis. These response factors may be
manually entered by an operator or determined
automatically by the system through
calibration procedures (with a calibration gas
mixture that has known concentrations).

The response factor calculation, using the


external standard, is:

Area Ht n
ARF n = --------------n- or HRF n = -----------
Cal n Cal n

where

ARFn area response factor for component “n” in area


per mole percent

Arean area associated with component “n” in calibra-


tion gas

Caln amount of component “n” in mole percent in


calibration gas
Htn peak height associated with component “n”
mole percent in calibration gas

HRFn peak height response factor for component “n”

Basic Analysis Computations SEP 2005


INTRODUCTION 1-27
Model 700

Calculated response factors are stored by the


Controller Assembly for use in the
concentration calculations, and are printed out
in the configuration and calibration reports.

Average response factor is calculated as


follows:
k

∑ RFi
i=1
RFAVGn = ------------------
k

where

RFAVGn area or height average response factor for


component “n”

RFi area or height average response factor for


component “n” from the calibration run

k number of calibration runs used to


calculate the response factors

The percent deviation of new RF averages from


old RF average is calculated in the following
manner:

RF new – RF old
deviation = ----------------------------------- × 100
RF old

where the absolute value of percent deviation


has been previously entered by the operator.

SEP 2005 Basic Analysis Computations


1-28 INTRODUCTION
Model 700

1.5.2 Conc Calc - Mole Percentage


(without Normalization)

Once response factors have been determined by


the Controller Assembly or entered by the
operator, component concentrations are
determined for each analysis by using the
following equations:

Area Ht n
CONC n = --------------n- or CONC n = --------------
ARF n HRF n

where

ARFn area response factor for component “n” in


area per mole percent

Arean area associated with component “n” in


unknown sample

CONCn concentration of component “n” in mole


percent

Htn peak height associated with component “n”


mole percent in unknown sample

HRFn peak height response factor for component


“n”

Component concentrations may be input


through analog inputs 1 to 4 or may be fixed. If
a fixed value is used, the calibration for that
component is the mole percent that will be used
for all analyses.

Basic Analysis Computations SEP 2005


INTRODUCTION 1-29
Model 700

1.5.3 Conc Calc in Mole Percentage


(with Normalization)

The average concentration The normalized concentration calculation is:


of each component will also
be calculated when data
averaging is requested.
CONC n
- × 100
CONCN n = ---------------------------
k

∑ CONCi
i=1

where

CONCNn normalized concentration of component


“n” in percent of total gas concentration

CONCi non-normalized concentration of


component “n” in mole percent for each
“k” component

CONCn non-normalized concentration of


component “n” in mole percent

k number of components to be included in


the normalization

SEP 2005 Basic Analysis Computations


1-30 INTRODUCTION
Model 700

1.6 ADDITIONAL RESOURCES

In addition to this manual, Model 700 Gas


Chromatograph System Reference Manual,
refer to the following:

• MON2000 Software for Gas


Chromatographs User Manual
(P/N 3-9000-522). Use this manual for
installing the MON2000 and Modbus Test
(WinMB) software programs, getting
started, checking various gas
chromatograph (GC) application settings,
and configuring and monitoring your GC
system.

Additional Resources SEP 2005


INTRODUCTION 1-31
Model 700

1.7 GLOSSARY

Auto Zero

Automatic zeroing of the TCD preamplifier


may be configured to take place at any time
during the analysis when either the component
is not eluting or the baseline is steady.

The Micro-FID is automatically zeroed at each


new analysis run and can be configured to take
place anytime during the analysis when either
the component is not eluting or the baseline is
steady. The TCD is only automatically zeroed
at the start of a new analysis.

Baseline

Signal output when there is only carrier gas


going across the detectors. In a chromatogram
you should only see Baseline when running an
analysis without injecting a sample.

Carrier Gas

The gas used to push the sample through the


system during an analysis. In C6+ analysis we
use Ultra Pure (zero grade) Carrier Gas for the
carrier. This gas is 99.995 percent pure.

Chromatogram

A permanent record of the detector output. A


chromatograph is obtained from a PC
interfaced with the detector output through the
Controller Assembly. A typical chromatogram
displays all component peaks, and gain
changes. It may be viewed in color as it is
processed on a PC VGA display. Tick marks
recorded on the chromatogram by the
Controller Assembly indicate where timed
events take place.

SEP 2005 Glossary


1-32 INTRODUCTION
Model 700

Component

Any one of several different gases that may


appear in a sample mixture

For example, natural gas usually contains the


following components: nitrogen, carbon dioxide,
methane, ethane, propane, isobutane, normal
butane, isopentane, normal pentane, and
hexanes plus.

Condulet

A box with a removable cover providing access


to wiring in conduit (conduit outlet) that is part
of an optional cable entry package.

CTS

Clear to send

DCD

Data carrier detect

DSR

Data set ready

DTR

Data terminal ready

Glossary SEP 2005


INTRODUCTION 1-33
Model 700

FID

Flame Ionization Detector - The optional


Micro-FID may be used in place of one TCD for
the detection of trace compounds. The
Micro-FID requires a polarization voltage and
its output is connected to the input to a high
impedance amplifier, an Electrometer. The
sample of gas to be measured is injected into
the burner with a mixture of hydrogen and air
to maintain the flame.

LSIV

Liquid Sample Inject Valve - The optional LSIV


is used to convert a liquid sample to a gas
sample by vaporizing the liquid in a heated
chamber, then analyzing the flashed sample.

Methanator

The optional Methanator, a catalytic converter,


converts otherwise undetectable CO2 and/or
CO into methane by adding hydrogen and heat
to the sample.

Response Factor

Correction factor for each component as


determined by the calibration:

RawArea
RF = ----------------------------------------------------------------------
CalibrationConcentration

Retention Time

Time (in seconds) that elapses between the


start of analysis (0 seconds) and the sensing of
the maximum concentration of each component
by the detector.

SEP 2005 Glossary


1-34 INTRODUCTION
Model 700

RI
Ring indicator

RLSD

Received Line Signal Detect (a digital


simulation of a carrier detect).

RTS
Request to send

RxD, RD, or Sin

Receive data, or signal in

TCD
Thermal Conductivity Detectors – Detectors
that use thermal conductivity of the different
gas components to produce an unbalanced
signal across the bridge of the preamplifier.
The higher the temperature the lower the
resistance on the detectors.

TxD, TD, or Sout

Transmit data, or signal out

Glossary SEP 2005


EQUIPMENT DESCRIPTION AND SPECIFICATIONS 2-1
Model 700

EQUIPMENT DESCRIPTION AND SPECIFICATIONS


2

Use the following sections to reference the


Model 700 equipment description or specifica-
tions.

2.1 EQUIPMENT DESCRIPTION

The Model 700 consists of two copper-free


aluminium explosion-proof housings, upper
and lower, and a front flow panel assembly.
The enclosures are separated by a pipe conduit
which routes electrical wiring from the lower
enclosure to the upper enclosure. Designed to
be explosion-proof, this unit is built for
installation in hazardous locations.
See Section 3.1 for more information.

Figure 2-1 Model 700 Gas Chromatograph

SEP 2005 Equipment Description


2-2 EQUIPMENT DESCRIPTION AND SPECIFICATIONS
Model 700

2.1.1 Upper Enclosure

The Model 700 upper explosion-proof housing


All circuit boards are contains the electronic controller
connected through a (multifunction board), the Oven System, the
common ground via the Stream Switching System (SSS) and
enclosure. preamplifier assembly.

Model 700 Upper Enclosure

Insulating Cover

Preamplifier Assembly

Multifunction Board

Micro-FID Exhaust Line

Figure 2-2 Upper Enclosure Assembly

Equipment Description SEP 2005


EQUIPMENT DESCRIPTION AND SPECIFICATIONS 2-3
Model 700

A more detailed equipment list includes:

• TCD Oven System (consists of the


electronics, up to three chromatograph
valves and the stream switching system):
- column module (i.e., “oven”)
- one or two pairs thermal conductivity
detectors (TCDs)
- valve system consisting of:
› three sample-directing valves
› plastic manifold that thermally
insulates the Oven System and
connects the actuating part to the
solenoid valves attached to the plastic
manifold
- two heater zones: column with one
cartridge heater and one block with
three heaters
- two thermal cut-off switches:
(oven temperature switch) opens at
257°F (±5 °) (125 °C)
Model 700 Upper Enclosure

Figure 2-3 TCD Oven System Assembly

SEP 2005 Equipment Description


2-4 EQUIPMENT DESCRIPTION AND SPECIFICATIONS
Model 700

• Micro-FID

Model 700 FID Upper Enclosure

Micro-FID

Figure 2-4 Model 700 Micro-FID Upper Assembly

The optional Flame Ionization Detector may be


used in place of one TCD for the detection of
trace levels of compounds.

Equipment Description SEP 2005


EQUIPMENT DESCRIPTION AND SPECIFICATIONS 2-5
Model 700

• Methanator
Model 700 Methantor Upper Enclosure

Methantor

Figure 2-5 Model 700 Methanator Upper Assembly

The optional Methanator, a catalytic converter,


converts otherwise undetectable CO2 and/or
CO into methane by adding hydrogen and heat
to the sample.

SEP 2005 Equipment Description


2-6 EQUIPMENT DESCRIPTION AND SPECIFICATIONS
Model 700

Model 700 LSIV Right Side View

LSIV Assembly

Figure 2-6 LSIV Assembly

The optional Liquid Sample Inject Valve (LSIV)


is used to convert a liquid sample to a gas
sample for analysis on the Model 700 Gas
Chromatograph.

A measured sample is placed in a heated


chamber above the vaporization point of the
liquid and then it is flashed to a gas. Once
vaporized, the sample is pushed by the carrier
gas through the heated tubing into the column
train.

Equipment Description SEP 2005


EQUIPMENT DESCRIPTION AND SPECIFICATIONS 2-7
Model 700

• Stream Switching System (SSS) which


consists of:
- manifold block
- solenoid valves
- valve clamps
- temperature sensor
- oven temperature switch
- tubing
- insulation cover

Model 700 Upper Enclosure

GC Valve
Solenoids

Figure 2-7 SSS Installed

• TCD Electronics
- Dual Methods Adapter Board
- Driver I/O Board
- Multifunction Board
- Preamplifier Board
- External Locking Device

SEP 2005 Equipment Description


2-8 EQUIPMENT DESCRIPTION AND SPECIFICATIONS
Model 700

• Micro-FID Electronics
- Solenoid/Heater Driver Board
- Multifunction Board
- Preamplifier Power supply
- Driver I/O Board
- Multifunction Board

2.1.2 Lower Enclosure

The Model 700 lower enclosure consists of:

Model 700 Lower Enclosure

AC/DC Power
Converter FTB

Com1

Com2

Card Cage Assembly


(CPU, Analog,
Com4A, Modem,
Ethernet Cards)
Figure 2-8 Lower Enclosure Assembly

Equipment Description SEP 2005


EQUIPMENT DESCRIPTION AND SPECIFICATIONS 2-9
Model 700

• Card cage assembly, containing:

DANGER TO PERSONNEL AND EQUIPMENT


See power supply label prior to connection.
Check the unit power design to determine if it
is equipped for AC or DC power. Applying 110/
220 VAC to a DC power input unit will
severely damage the unit.
Failure to do so may result in injury to
personnel or cause damage to the equipment.

- WinSystems CPU board


- Com4A board (optional)
- analog board
- analog board (optional)
- digital I/O
- internal modem (optional)
The Model 700 CSA- - ethernet card (optional)
certified unit is equipped - field termination board (FTB)
with 3/4 inch cross-over
adapters. - connection for AC/DC power supply
(converter)
- internal and external ground
- external locking device
- DB pin connection for serial
communications

SEP 2005 Equipment Description


2-10 EQUIPMENT DESCRIPTION AND SPECIFICATIONS
Model 700

2.1.3 Flow Panel Assembly

The Flow Panel Assembly is attached to the


If the carrier gas pressure front of the upper enclosure and consists of the
drops below a set point, this following: (see Figure 2-2):
switch causes the analysis
to stop and activates the • carrier pressure regulator(s) and gauge(s)
analyzer failure alarm.
• sample flow meter
• Sample Vent (SV)
• Measure Vent (MV)
• actuation pressure limiting regulator
• pressure switch, mounted internally

2.2 EQUIPMENT SPECIFICATIONS

2.2.1 Utilities

Use the following table to determine the utility


specifications.

Equipment Specifications SEP 2005


EQUIPMENT DESCRIPTION AND SPECIFICATIONS 2-11
Model 700

Table 2-1 Model 700 Unit Specifications

Type Specification

unit dimensions • basic unit envelope


(P/N 20351) w - 15.2” (387 mm)
h - 41.5” (1054 mm)
d - 19.2” (488 mm)
• wall mount
w - 18.2” (463 mm)
h - 41.5” (1054 mm)
d - 19.2” (488 mm)
• pole mount
Allow 14” (360 mm
w - 18.2” (463 mm)
additional) clearance for
h - 41.5” (1054 mm)
removal of dome.
d - 25.0” (635 mm)
• floor mount
w - 18.2” (463 mm)
h - 58.0” (1470 mm)
d - 19.2” (488 mm)

unit weight • wall mount 130 lbs (59 kg)


• pole mount 135 lbs (61 kg)
• floor mount 150 lbs (68)

materials • 303 and 316 stainless steel


• 316 stainless steel and Kapton in contact with sample
• Swagelock and Valco fittings

mounting • floor mount


• pole mount:
- 2” (60.3 mm)
- 3” (89.0 mm)
- 4” (114.3 mm)
• direct wall mount

SEP 2005 Equipment Specifications


2-12 EQUIPMENT DESCRIPTION AND SPECIFICATIONS
Model 700

Table 2-1 Model 700 Unit Specifications

Type Specification

power • 24 VDC standard


• 75W (Model 700 w/TCD)
• 150W (Model 700 w/Methanator or LSIV)
• 36VDC, Sol/Drv PCB Transorb
• 90-130/180-264 VAC
• 47-63HZ (single phase)
• AC optional

Voltage range includes line


voltage variations.

instrument air not required; optional for valve


actuation, min pressure of 90 psig

environment • -18 to 55 oC (0 to 130 oF)


• 0 to 95% RH (non-condensing)
• indoor/outdoor
• pollution - degree 2 (the unit can withstand some non
conductive environmental pollutants e.g., humidity)
• max altitude 2000m

classification • For Canada: Class 1,Zone 1,Ex d IIB (+H2),T4 (pending)


• For USA: Class 1,Zone 1,AEx d IIB (+H2),T4 (pending)

international CENELEC/IEC Class 1,Zone 1, EEx d IIB(+H2) T4


(pending)
ATEX CE EEx d IIC T4
Certification number SIRA - 04ATEX1055X
Special conditions for safe use must be met. The
maximum constructional gap (ic) is less than that required
by Table 1 of IEC 60079-1:2004 as detailed below:

FLAMEPATH MAXIMUM GAP (MM) COMMENT

Fitting tube adaptor/fitting tube taper 0.000 Taper fit

Fitting tube/taper/tubes 0.132

Equipment Specifications SEP 2005


EQUIPMENT DESCRIPTION AND SPECIFICATIONS 2-13
Model 700

2.2.2 Electronic Hardware

Review the system block diagrams, Upper and


Lower Electronics, to become familiar with the
Model 700.

Figure 2-9 Upper Electronics with TCD Block Diagram

SEP 2005 Equipment Specifications


2-14 EQUIPMENT DESCRIPTION AND SPECIFICATIONS
Model 700

PREAMPLIFIER PCB
PREAMPLIFIER P/S PCB
INPUTS:
DC-DC CONVERTERS 1 TCD DETECTOR
24VDC INPUT 1 FID DETECTOR
24VDC POWER
OUTPUTS OUTPUTS:
+20VDC -20VDC COM (1)
100VDC (RS-232 OR RS-485)
5VDC

3.3 VDC

SERIAL I/O

SOLENOID/HEATER
DRIVER PCB

DC-DC CONVERTERS
24 VDC INPUT
OUTPUTS
5VDC
SOLENOID DRIVERS (16)
HEATERS (4 ZONES)

MULTIFUNCTION SERIAL PORT RS-232


MICRO-CONTROLLER PCB

HEATER PWM CONTROLLER


(4 ZONES)

DIGITAL INPUTS.................(5)
COM RS-232......................(1)
RTD INPUTS.......................(4)
ANALOG INPUTS 4-20mA....(4)
DIGITAL OUTPUTS..............(5) SERIAL PERIPHEERAL INTERFACE
SERIAL DAC CONTROL.........(SPI)

Figure 2-10 Upper Electronics with Micro-FID Block Diagram

Equipment Specifications SEP 2005


EQUIPMENT DESCRIPTION AND SPECIFICATIONS 2-15
Model 700

Figure 2-11 Lower Electronics TCD Block Diagram

SEP 2005 Equipment Specifications


2-16 EQUIPMENT DESCRIPTION AND SPECIFICATIONS
Model 700

INPUT OPTIONAL
AC POWER AC-DC
POWER SUPPLY

24 VDC

FIELD TERMINATION PCB OPTIONAL ANALOG


BUILT IN SURGE PROTECTION OUTPUT PCB
FIELD WIRING FOR THE FOLLOWING: 4 ISOLATED OR
8 NON-ISOLATED
COM 1 & 2, 5-8
ANALOG INPUTS 4-20mA.......(4)
ANALOG OUTPUTS 4-20mA....(4)
DIGITAL INPUTS.....................(5)

DIGITAL OUTPUTS (5) RELAYS


2 RELAYS FORM “A” CONTACT
3 SOLID STATE RELAYS
ANALYZER INTERCONNECT
POWER FOR STANDARD BUS
DC-DC CONVERTER SIGNALS - POWER
OUTPUTS STD-BUS
5VDC, +12VDC, -12 VDC
- 3.8VDC

CPU
MULTIFUNCTION COM 3
COM4A PCB
COM 5-8
FID & TCD PREAMPLIFIER COM 4
ETHERNET PCB

INTERNAL MODEM

OPTIONAL PC104

BOARD STACK

Figure 2-12 Lower Electronics Micro-FID Block Diagram

Equipment Specifications SEP 2005


EQUIPMENT DESCRIPTION AND SPECIFICATIONS 2-17
Model 700

Use the following table to determine the


electronic hardware specifications.

Table 2-2 Electronic Hardware Specification

Type Specification

Rating Division 1; no purge required

CPU WinSystems 386sx 33 MHz

Memory 4 MB System RAM

DiskOnChip 8 MB – 288 MB

Communication Ports 6 configurable Modbus ports; support RS-232/422/485


protocols

Optional Modem 56K Baud Telephone

Analog Inputs 4, 12-pin Phoenix on FTB

Standard Analog Outputs 4, 12-pin Phoenix on FTB

Optional Analog Outputs 8, non-isolated outputs 24-pin Phoenix


Located on Optional Analog Board
Or,
4, isolated outputs 12-pin Phoenix connector
Located on Optional Analog Board

Discrete Digital Inputs GC_IN (dedicated to pressure switch); 4 user-defined inputs

Digital Outputs (5) 2 Relays “Form A” contacts


Relay contact rating 24 VDC nominal @ 1 Amp
3 Solid State Relays - Rating of 0.375A @30 VDC on FTB - 10
pin Phoenix connector

Detector Inputs Optionally 2 micro-volume TCD inputs


1 Flame Ionization Detector (Micro-FID) input

Transient Protection over-voltage category II

SEP 2005 Equipment Specifications


2-18 EQUIPMENT DESCRIPTION AND SPECIFICATIONS
Model 700

2.2.3 Micro Heat Sink Oven

Use the following table to determine the oven


specifications.

Table 2-3 Oven Assembly Specifications

Type Specification

Valves 6-port and 10-port valves; piston-


operated diaphragms with
pneumatic actuation

Columns max of 40 feet (12 m) of micro-


packed columns; 1/16-inch
(1.6-mm) outside diameter

Solenoid Actuation • 24 VDC


• max 90 psi

Wetted Parts 316 stainless steel and kapton


diaphragm

Temperature Control • 24 VDC heat sink


• 2 zones (1 column, 1 block)
• max operating temperature of
115 °C (239 °F)

Sample System 1 zone, includes Stream Switching


System

Sample Streams • standard: max of 3 analytical


and 1 auto calibration
• optional: max of 8

Equipment Specifications SEP 2005


EQUIPMENT DESCRIPTION AND SPECIFICATIONS 2-19
Model 700

2.2.4 Software

Use the following table to determine the


The Model 700 has its own software specifications.
applications and is not
compatible with 2350/ Table 2-4 Software Specifications
2350A applications.
Type Specification

Software PC-based MON2000; runs 2350 and


2350A applications (v2.4 or later)

Firmware embedded firmware compatible with


2350/2350A applications (v1.8 or later)

Methods 4 Timed Event Tables and 4


Component Data Tables assignable to
each stream

Peak Integration • fixed time or auto slope and peak


identification
• update Retention Time upon
calibration or during analysis

SEP 2005 Equipment Specifications


2-20 EQUIPMENT DESCRIPTION AND SPECIFICATIONS
Model 700

This page is intentionally left blank.

Equipment Specifications SEP 2005


INSTALLATION AND SETUP 3-1
MODEL 700

INSTALLATION AND SETUP


3-

This section provides instructions for installing


and setting up the Model 700 Gas
Chromatograph (GC) System for Zone 1/
Division I environments.

This procedure involves the following steps:

• observe precautions and warnings


• plan site location
• obtain supplies and tools
• install GC wiring
• install GC sample and gas lines
• perform leak checks
• purge carrier gas lines
• purge calibration lines
• start up GC system

3.1 PRECAUTIONS AND WARNINGS

DANGER TO PERSONNEL AND EQUIPMENT


Install and operate all equipment as designed and is
compliant with all safety requirements.
The “Seller” does not accept any responsibility for
installations of the Model 700, or any attached
equipment, in which the installation or operation
thereof has been performed in a manner that is
negligent and/or non-compliant with applicable safety
requirements.

SEP 2005 Precautions and Warnings


3-2 INSTALLATION AND SETUP
MODEL 700

3.1.1 Hazardous Environments

DANGER TO PERSONNEL AND EQUIPMENT


Observe all precautionary signs posted on the Model 700 enclosure.
Failure to do so may result in injury to personnel or cause damage to the
equipment.

DANGER TO PERSONNEL AND EQUIPMENT


Observe all precautionary signs posted on the Model 700 enclosure.
The Model 700 enclosures are certified for Class 1, Zone 1, EEx d IIB (+H2)
T4 locations and also complies with the ATEX directive 94/9/EC EEx d IIC T4.
ATEX certified units must be installed strictly in compliance with the
requirements of ISO 60079-14.
Before opening the Model 700 assembly, reduce the risk of igniting hazardous
atmospheres by disconnecting the equipment from all power supplies. Keep
the assembly closed tightly when in operation to reduce the risk of igniting
hazardous atmospheres.
Inlet (incoming) wiring must meet local standards (i.e. in conduit with seal
fitting within 18” or via cable glands certified to ISO 60079-1). Seal all
unused entries with blanks certified to ISO 60079-1.
Observe all precautionary signs posted on the Model 700 enclosure. Failure to
do so may result in injury to personnel or cause damage to the equipment.
Please direct all health, safety and certification related questions to: Daniel
Measurement and Control, Inc. Applications Engineering Group or Rosemount
Analytical, Inc.

Precautions and Warnings SEP 2005


INSTALLATION AND SETUP 3-3
MODEL 700

Follow these precautions if installing or


operating the Model 700 instrumentation in a
hazardous area:

1. Install and operate only the Zone 1/


Division I version of the Model 700 in a
hazardous area.
2. Do not operate any printer or personal
computer (PC) that is connected to a GC
which is installed in a hazardous area. To
interface with a GC in a hazardous area,
use a PC that is located in a nonhazardous
area and remotely connected to the GC.
3. Ensure that field connections to the
analyzer are made through explosion-proof
conduit or flameproof glands.

3.1.2 Power Source Wiring

Follow these precautions when installing AC


power source wiring:

1. All wiring must conform to the CEC or


NEC, local state or other jurisdiction, and
company standards and practices.
2. Provide 24 VDC power or optional single-
phase, 3-wire, power at 115 or 230 VAC, 50-
60 Hertz.
3. Locate circuit breaker and optional power
disconnect switch in a safe area.
4. Provide the Model 700 system and any
optionally installed devices with one 15-
Amp circuit breaker for protection.
15 amps is the maximum
current for 14 AWG (wire). 5. Ensure that the 24 VDC input power is
S.E.L.V. compliant by suitable electrical
separation from other circuits.

SEP 2005 Precautions and Warnings


3-4 INSTALLATION AND SETUP
MODEL 700

6. Use multi-stranded copper conductor wire


according to the following recommenda-
tions:
• For power feed distances up to 250 feet
(76 meters), use 14 AWG (American
Wire Gauge) (18 Metric Wire Gauge),
stranded.
• For power feed distances 250 to 500 feet
(76 to 152 meters), use 12 AWG
(25 Metric Wire Gauge), stranded.
• For power feed distances 500 to 1000 feet
(152 to 305 meters), use 10 AWG
(30 Metric Wire Gauge), stranded.
• Cable entries are M32 in accordance
with ISO 965.

3.1.3 Card Cage Removal

The Model 700 card cage assembly is designed


to be disconnected and removed from the lower
enclosure to allow space for user power and
signal connections. This may be particularly
important for applications where large
numbers of I/O connections are required.

To disassemble the Card Cage,

1. Remove the lower enclosure cover and the


front flow panel assembly.

Precautions and Warnings SEP 2005


INSTALLATION AND SETUP 3-5
MODEL 700

Note: Leave the wires attached to the flow


panel assembly and allow it to hang outside
of the enclosure.

Cover

Flow Panel

Figure 3-1 Lower Enclosure Disassembly

SEP 2005 Precautions and Warnings


3-6 INSTALLATION AND SETUP
MODEL 700

2. Carefully disconnect all of the ribbon cables


from the boards in the card cage assembly
(CPU, Analog, Modem, Ethernet, etc.).
Note the location of the
ribbon cables for ease
of reassembly.

Flow Panel

Figure 3-2 Card Cage Cable Disassembly

Precautions and Warnings SEP 2005


INSTALLATION AND SETUP 3-7
MODEL 700

3. Use a Phillips head screw driver and


remove the two screws located at the top of
the card cage and one screw on the bottom
left side of the card cage (not visible in the
figure).

Card Cage
Screws

Figure 3-3 Card Cage Assembly Screw Locations

SEP 2005 Precautions and Warnings


3-8 INSTALLATION AND SETUP
MODEL 700

4. Slide the card cage assembly out of the


lower enclosure.

Figure 3-4 Card Cage Disassembly

Precautions and Warnings SEP 2005


INSTALLATION AND SETUP 3-9
MODEL 700

5. User power and signal connections may be


made with the card cage removed from the
lower enclosure.

Figure 3-5 Card Cage Disassembly for Power and Signal Wiring

SEP 2005 Precautions and Warnings


3-10 INSTALLATION AND SETUP
MODEL 700

3.1.4 Signal Wiring

Follow these general precautions for field


wiring digital and analog input/output (I/O)
lines:

DANGER TO PERSONNEL AND EQUIPMENT


Observe all precautionary signs posted on the Model
700 enclosure. Applicable to all digital and analog I/O
lines connecting to the GC: Any loop of extra cable
left for service purposes inside the GC housing must
not be placed near any AC power lines.
If this precaution is not followed, the data and control
signals to and from the GC can be adversely affected.

• Metal conduit must be used for all process


signal wiring.
• Metal conduit or cable (in compliance with
EN 60079-14) used for process signal wiring
must be grounded at conduit support points
(intermittent grounding of conduit helps
prevent induction of magnetic loops
between the conduit and cable shielding).
• All process signal wiring should be a single,
continuous length between field devices and
the GC. If, however, length or conduit runs
require that multiple wiring pulls be made,
the individual conductors must be
interconnected with suitable terminal
blocks.
• Use suitable lubrication for wire pulls in
conduit to prevent wire stress.
• Use separate conduits for AC voltage and
DC voltage circuits.
• Do not place digital or analog I/O lines in
same conduit as AC power circuits.

Precautions and Warnings SEP 2005


INSTALLATION AND SETUP 3-11
MODEL 700

• Use only shielded cable for digital I/O line


connections.
- Ground the shield at only one end.
- Shield-drain wires must not be more
than two AWG sizes smaller than the
conductors for the cable.
• When inductive loads (relay coils) are
driven by digital output lines, the inductive
transients must be diode-clamped directly
at the coil.
• Any auxiliary equipment wired to the GC
must have its signal common isolated from
earth/chassis ground.

3.1.5 Electrical and Signal Ground

Follow these general precautions for grounding


electrical and signal lines:

• For shielded signal conducting cables,


shield-drain wires must not be more than
two AWG sizes smaller than the conductors
for the cable. Shielding is grounded at only
one end.
• Metal conduit used for process signal wiring
must be grounded at conduit support points
(intermittent grounding of conduit helps
prevent induction of magnetic loops
between the conduit and cable shielding).
• A single-point ground (the outside case
ground lug) must be connected to a copper-
clad, 10-foot long, 3/4-inch diameter steel
rod, which is buried, full-length, vertically
into the soil as close to the equipment as is
practical (note: the grounding rod is not
furnished.)

SEP 2005 Precautions and Warnings


3-12 INSTALLATION AND SETUP
MODEL 700

• Resistance between the copper-clad steel


ground rod and the earth ground must not
exceed 25 Ohms.
• On ATEX certified units, the external
ground lug must be connected to the
customer’s protective ground system via
AWG 9 (6mm2) ground wire. After the
connection is made, apply a non-acidic
grease to the surface of the external ground
lug to prevent corrosion.
• The equipment-grounding conductors used
between the GC and the copper-clad steel
ground rod must be sized according to the
following specifications:

Length Wire

15 ft. (4.6 m) 8 AWG


or less stranded, insulated copper

15 to 30 ft. 6 AWG
(4.6 to 9.1 m) stranded, insulated copper

30 to 100 ft. 4 AWG


(9.1 to 30.5 m) stranded, insulated copper

• All inter-enclosure equipment-grounding


conductors must be protected by metal
conduit.
• External equipment, such as data printers,
that are connected to the GC should be
powered via isolation transformers to
minimize the ground loops caused by the
internally shared safety and chassis
grounds.

Precautions and Warnings SEP 2005


INSTALLATION AND SETUP 3-13
MODEL 700

3.1.6 Electrical Conduit

Follow these general precautions for conduit


installation:

• Conduit cutoffs must be square. Cutoffs


must be made by a cold cutting tool,
hacksaw, or by some other approved means
that does not deform the conduit ends or
leave sharp edges.
• All conduit fitting-threads, including
factory-cut threads, must be coated with a
metal-bearing conducting grease, such as
Crouse-Hinds STL or equivalent, prior to
assembly.
• Temporarily cap the ends of all conduit runs
immediately after installation to prevent
accumulation of water, dirt, or other
contaminants. If necessary, swab out
conduits prior to installing the conductors.
• Install drain fittings at the lowest point in
the conduit run; install seals at the point of
entry to the GC explosion-proof housing to
prevent vapor passage and accumulation of
moisture.
• Use liquid-tight conduit fittings, such as
Myers Scru-tite or similar, for conduits
exposed to moisture.

SEP 2005 Precautions and Warnings


3-14 INSTALLATION AND SETUP
MODEL 700

When conduit is installed in hazardous areas


(e.g., areas classified as NEC Class I, Division
1, Groups B, C, and D), follow these general
precautions for conduit installation:

DANGER TO PERSONNEL AND EQUIPMENT


Observe all precautionary signs posted on the
equipment. Consult your company policies and
procedures and other applicable requirements
documents to determine wiring and installation
practices that are appropriate for hazardous areas.
Failure to do so may result in injury to personnel or
cause damage to the equipment.

• All conduit runs must have a fitting, which


contains explosion-proof sealing (potting)
located within 18 inches from the conduit
entrance to the explosion-proof housing.
• The conduit installation must be vapor
tight, with threaded hub fittings, sealed
conduit joints and gaskets on covers, or
other approved vapor-tight conduit fittings.

3.1.7 Sample System Requirements

Observe the following guidelines for installing


GC sample systems:

Precautions and Warnings SEP 2005


INSTALLATION AND SETUP 3-15
MODEL 700

Line Length:

If possible, avoid long sample lines. In case of a


long sample line, flow velocity can be increased
Stream switching requires a
by decreasing downstream pressure and using
sample pressure of 20 psig.
by-pass flow via a speed loop.

Sample Line Tubing Material:

• Use stainless steel tubing for noncorrosive


streams.
The calibration gas stream • Ensure tubing is clean and free of grease
inlet is the last stream inlet (see Figure 3-6 for details).
following the sample gas.
Model 700 Upper Enclosure

Stream 1 - 8
Gas Connections

Figure 3-6 Stream Inlets (Right side of unit)

SEP 2005 Precautions and Warnings


3-16 INSTALLATION AND SETUP
MODEL 700

Dryers and Filters:

Use small sizes to minimize time lag and


prevent back diffusion.
Install the probe/regulator
first, immediately followed
- Install a minimum of one filter to remove by the coalescing filter and
solid particles. Most applications require then the membrane filter.
fine-element filters upstream of the GC.
See Appendix C for a
The Model 700 hardware includes a 2 recommended natural gas
micron filter. installation.
- Do use ceramic or porous metallic type
filters. Do not use cork or felt filters.
Pressure Regulators and Flow Controllers:

- Do not use types containing cork or felt


filters, or absorbent diaphragms.
Pipe Threads, Dressing:

- Do use Teflon tape. Do not use pipe


thread compounds (dope).
Valving:

- Install a block valve downstream of


sample takeoff point for maintenance
and shutdown.
- Block valve should be needle valve or
cock valve type, of proper material and
packing, and rated for process line
pressure.

3.2 PREPARATION

Your Model 700 GC was started and checked


out before it left the factory. Program
parameters were installed and documented in
the PC Config Report furnished with your
Model 700.

Preparation SEP 2005


INSTALLATION AND SETUP 3-17
MODEL 700

3.2.1 Site Selection

Install the GC as close as possible to the


sample system but allow for adequate access
space for maintenance tasks and adjustments.
Allow a minimum of 14 inches (36 cm) in front
for enclosure opening and access.

• Allow a minimum of 14 inches (36 cm) above


the top of the dome enclosure for dome
removal and access.
• Ensure that exposure to radio frequency
(RF) interference is minimal.

3.2.2 Unpacking the Unit

See the following checklist for unpacking the


unit and inspecting for damage:

1. Unpack the equipment:


• Model 700 system
• software and manuals
• documentation package
2. Ensure that all documentation and software
are included:
• this manual Model 700 Gas
Chromatograph System Reference
Manual (P/N 3-9000-521)
• the software manual, MON2000
Software for Gas Chromatographs User
Manual (P/N 3-9000-522)
• diskette(s) or CD-ROMs with the
MON2000 Software for Gas
Chromatographs Windows software
program, Modbus Test software
program, and GC applications
(P/N 2-3-2350-400)

SEP 2005 Preparation


3-18 INSTALLATION AND SETUP
MODEL 700

3. Remove any packing materials from


internal areas of the unit (particularly in
the dome enclosure).

Installation and startup should proceed only if


all required materials are on hand and free
from obvious defects.

If any parts or assemblies appear to have


been damaged in shipment, first file a claim
with the carrier. Next, complete a full report
describing the nature and extent of the damage
and forward this report immediately to Daniel
Measurement Services for further instructions
(see the Customer Repair Report at the back of
this manual). Include complete model number
information. Disposition instructions will be
returned immediately.

3.2.3 Model 700 Installation Arrangements

The Model 700 GC can be ordered for


installation in the following mounting The wall should be strong
arrangements (see drawing P/N DE-20993): enough to support the 200
lb. load.
- wall mount
- pole mount
- floor mount

Wall Mount

The simplest arrangement is wall mount (see


drawing P/N DE-20993). The unit has two
mounting ears on each side. The ear-holes are
used to attach the unit to a wall.

The uppermost of the holes should be about 30


inches from the floor for the most efficient use
of the unit.

The space between the enclosures and the wall


(1.3 inches) allows adequate access above and
around the unit.

Preparation SEP 2005


INSTALLATION AND SETUP 3-19
MODEL 700

Pole Mount

The pole mount arrangement uses mounting


ears as attachment points for the plates
clamped to a pole (see drawing P/N DE-20993).
The plates accept the recommended u-bolt
systems for the 2 inch, 3 inch or 4 inch nominal
pipe sizes. The base attachment of the pole
being used must be able to accommodate the
weight of the unit.

Floor Mount

The floor mount arrangement includes


additional external framing that creates a
free-standing unit (see drawing P/N DE-
20993). The mounting ears, located on the base
of the frame, are used to anchor the unit to a
floor or instrument pad. The frame, also
provides a means for attaching sample-
conditioning plates or for anchoring
tubing-runs.

3.2.4 Required Tools and Components

You will need these tools and components to


install the Model 700:

• zero grade carrier gas (99.995% pure, with


less than 5 ppm water, and less than 0.5
ppm hydrocarbons)
• high pressure dual-stage regulator for the
carrier gas cylinder, high side up to 3000
pounds per square inch, gauge (psig), low
side capable of controlling pressure up to
150 psig
• calibration standard gas with correct
number of components and concentrations
(see Appendix Table C-1)

SEP 2005 Preparation


3-20 INSTALLATION AND SETUP
MODEL 700

• dual-stage regulator for the calibration gas


cylinder, low pressure side capable of
controlling pressure up to 30 psig
• sample probe regulator (fixture for
procuring the stream, or sample gas for
chromatographic analysis)
• coalescing filter
• membrane filter
• 1/8-inch stainless steel (SS) tubing for
connecting calibration standard to GC, 1/8
inch SS tubing for connecting carrier gas to
the GC, 1/8-inch SS tubing for connecting
stream gas to the GC
• heat tracing (as required) for sample
transport and calibration lines
• miscellaneous Swagelok tube fittings,
tubing benders and tubing cutter
• 14 AWG (American Wire Gauge) (18 Metric
Wire Gauge) or larger electrical wiring and
conduit to provide 115 or 230 volts AC,
single phase, 50 to 60 Hertz, from an
appropriate circuit breaker and power
disconnect switch (see guidelines in Section
3.1.2)
• liquid leak detector (Snoop or equivalent)
• digital volt-ohm meter with probe-type
leads
• flow measuring device such as Set-A-Flow
(P/N 4-4000-229)
• open-end wrenches sized 1/4, 5/16, 7/16, 1/2,
1/16 and 5/8-inch

Preparation SEP 2005


INSTALLATION AND SETUP 3-21
MODEL 700

3.2.5 Supporting Tools and Components

DANGER TO PERSONNEL AND EQUIPMENT


Do not use a PC or a printer in a hazardous area.
Serial port and Modbus communications links are
provided to connect the unit to the PC and to
connect to other computers and printers in a safe
area.
Failure to follow this warning may result in injury
to personnel or cause damage to the equipment.

Supporting tools and components include:

• Use an IBM-compatible PC and either a


direct or remote communications connection
to interface with the Model 700 system. See
Section 2.1 of the MON2000 Software for
Gas Chromatographs User Manual
(P/N 3-9000-522) for more information on
specific PC requirements.
• The Model 700 comes with serial Port 2 on
the Field Termination Board (FTB) factory-
wired with a DB 9-pin connection. Use the
You can use the serial cable
installed for the Model 700. provided serial cable (P/N 3-2350-068) to
hookup to a PC. See Table A-4 for more
For straight-through serial
information regarding these connections.
cable installation and
fabrication instructions, see
Appendix A.

SEP 2005 Preparation


3-22 INSTALLATION AND SETUP
MODEL 700

If a different serial cable is used to connect


from the PC to the pre-wired DB 9-pin,
follow these specifications:

Terminal Connection

DB 9-pin male Serial Port 2

DB 9-pin male PC serial port


DB 25-pin female

• Use items necessary for connecting the GC


to a network or other type of remote data
transfer system (an example item might be
an RS-232/RS-485 conversion box for long
distance serial transmission), as applicable.
• Use a printer, connected either at the PC or
the GC unit, to record analysis and other
data. See Section 3.4.6 for wiring
information.

Preparation SEP 2005


INSTALLATION AND SETUP 3-23
MODEL 700

3.3 MODEL 700 INSTALLATION

3.3.1 DC Power Supply

DANGER TO PERSONNEL AND EQUIPMENT


Ensure that the 24 VDC input power source is switched OFF
before connecting the wires. Also, ensure that the 24 VDC
input power is S.E.L.V. compliant by suitable electrical
separation from other circuits.
Failure to follow these warnings may result in injury or death
to personnel or cause damage to the equipment.

D
AMAGE TO EQUIPMENT
Check the unit prior to wiring to determine if it is equipped for
DC power.
Failure to observe this precaution may damage equipment.

SEP 2005 Model 700 Installation


3-24 INSTALLATION AND SETUP
MODEL 700

To connect 24 VDC power to the GC:

1. Locate the plug-together termination block


inside the lower enclosure.
Model 700 Lower Enclosure

DC Power Wiring

Figure 3-7 DC Power Wiring

2. Bring the two leads in through the left entry


on the bottom of the lower enclosure.
Connect to the termination plug provided
with the unit.
Use the following table for the DC power
wiring details:

Table 3-1 DC Power Wiring

Attribute Wire Color

+ (positive) red

– (negative) black

Model 700 Installation SEP 2005


INSTALLATION AND SETUP 3-25
MODEL 700

3. Each board that connects to the 24 VDC is


protected from lead reversal by the use of
blocking diodes. The following boards are
connected to the 24 VDC:
A new version of the
Solenoid/Heater Driver • Field Termination Board
Board that includes the
Diode protection will soon
• Isolated Analog Output Option Board
be released. • Solenoid/Heater Driver board
• Micro-FID/TCD Preamplifier Board
If the Red (+) and Black (-) leads are
inadvertently reversed, no damage will
occur, however, the system will not power
on.
4. Connect the DC power leads to the power
disconnect switch that is properly fused.
The recommended fuse size is 10 Amps.

3.3.2 Optional AC – DC Power Converter

To connect 115 or 230 VAC power to the GC:

DANGER TO PERSONNEL AND EQUIPMENT


Check the unit prior to wiring to determine if it is
equipped for optional AC power.
Failure to follow this warning may result in injury
to personnel or cause damage to the equipment.

SEP 2005 Model 700 Installation


3-26 INSTALLATION AND SETUP
MODEL 700

1. Locate the plug-together termination block


inside the lower enclosure (located on the
lower left side behind the power supply).
Model 700 Lower Enclosure

AC / DC Power
Converter

Figure 3-8 AC/DC Power Converter

DANGER TO PERSONNEL AND EQUIPMENT


Do not connect AC power leads without first
ensuring that AC power source is switched OFF.
Failure to follow this warning may result in injury
to personnel or cause damage to the equipment.

Model 700 Installation SEP 2005


INSTALLATION AND SETUP 3-27
MODEL 700

DAMAGE TO EQUIPMENT
Do not apply electrical power to the GC until all
interconnections and external signal connections
have been verified, and proper grounds have
been made.
Failure to observe this precaution may cause
damage to equipment.

AC wiring is usually colored as:

Table 3-2 AC Wiring

Attribute Wire Color

hot brown or black

neutral blue or white

ground green or green

2. Bring the power leads in through the left


entry on the bottom of the enclosure.
3. If necessary, connect the GC chassis ground
to an external copper ground rod (at remote
locations). See Section 3.1.5 regarding
electrical and signal grounding.

SEP 2005 Model 700 Installation


3-28 INSTALLATION AND SETUP
MODEL 700

3.3.3 Sample and Gas Lines

To install GC sample and gas lines:


Use SS tubing. Keep tubing
1. Remove the plug from the Sample Vent (SV) clean and dry internally to
line (1/16-inch tubing marked “SV” located avoid contamination. Before
on the Flow Panel Assembly). connecting the sample and
gas lines, flow clean air or
• If desired, connect the SV line to an gas through them. Blow out
external (ambient pressure) vent. If the internal moisture, dust, or
other contaminants.
vent line is terminated in an area
exposed to wind, protect the exposed
vent with a metal shield.
• Use 1/4-inch or 3/8-inch tubing for vent
lines longer than 10 feet.
Note that, at this stage in the installation,
the GC Measure Vent (MV) line (marked
“MV”) remains plugged until leak checks
are completed. For regular operation,
however, the MV line must be unplugged, or
open.
Do not discard the vent line plugs. They are
useful at any time when leak-checking the
GC and its sample or gas line connections.

Model 700 Installation SEP 2005


INSTALLATION AND SETUP 3-29
MODEL 700

2. Connect carrier gas to the GC. (The carrier


gas inlet is a 1/8-inch tee fitting located on
the left side of the upper enclosure.)

MAY CAUSE INJURY TO PERSONNEL OR


EQUIPMENT DAMAGE
Do not turn on gas until you have completed
leak checking the carrier and sample lines (see
Step 5).
Failure to follow this precaution may cause
injury to personnel or damage equipment.

Model 700 Lower Enclosure

Carrier Gas
Inlet

• Use 1/8-inch or 1/4-inch stainless steel


tubing to conduct carrier gas.
• Use a dual-stage regulator with high-
side capacity of 3000 psig and low-side
capacity of 150 psig.

SEP 2005 Model 700 Installation


3-30 INSTALLATION AND SETUP
MODEL 700

• See Appendix C for a description of a


dual-cylinder carrier gas manifold
(P/N 3-5000-050) with these features:.
- Carrier gas is fed from two bottles. The first stream is the
- When one bottle is nearly empty (100 calibration gas stream.
psig), the other bottle becomes the
primary supply.
- Each bottle can be disconnected for
refilling without interrupting GC
operation.
3. Connect calibration standard gas to the GC
• Use 1/8-inch stainless steel tubing to
conduct calibration standard gas.
When installing the
• Use a dual-stage regulator with low-side calibration standard gas line,
capacity of up to 30 psig. ensure that the correct
tubing connection is made.

Model 700 Installation SEP 2005


INSTALLATION AND SETUP 3-31
MODEL 700

• The Calibration gas inlet is the last inlet


following the sample gas
(see Figure 3-9).
Model 700 Upper Enclosure

Calibration
Gas Inlet

Figure 3-9 Calibration Gas Stream Inlet (Right side of unit)

4. Connect sample gas stream(s) to the GC.


• Use 1/8-inch or 1/4-inch stainless steel
tubing to conduct calibration standard
gas.
• Ensure that pressure of sample line is
regulated to maintain 15 to 30 psig
(±10%).

SEP 2005 Model 700 Installation


3-32 INSTALLATION AND SETUP
MODEL 700

• Gas stream inlet(s) are identified (see


Figure 3-10) for details.

Model 700 Upper Enclosure

Streams 1 - 7 Calibration
Gas Inlets Gas Inlet

Figure 3-10 Sample Stream Inlets (Right side of unit)

5. After all lines have been installed, proceed


with leak checking the carrier and sample
lines. See Section 3.5.1; note that it
requires the AC power to be turned on at
the GC.

Model 700 Installation SEP 2005


INSTALLATION AND SETUP 3-33
MODEL 700

3.4 SETTING THE COM ID

The Model 700 Com ID is determined by dual


Follow the steps in this
inline package (DIP) switch settings.
section only if you wish to
do the following:
• Change the Com ID
setting.
• Visually inspect and verify
the DIP switch settings.
Figure 3-11 Dip Switch

In most cases, the Com ID configuration made


at the factory will not need to be changed. The
factory DIP switch settings produce a Com ID
of 1.

3.4.1 Inspect or Change the Com ID

To visually inspect and verify the DIP switch


settings or to change the Com ID settings on
Note that the MON2000
the multifunction board,
software Com I.D.s will
override the hardware 1. Remove the dome from the upper enclosure.
settings. To use the
hardware Com I.D.
configuration, enter a zero
‘0’ in the MON2000 Com
I.D, settings. For details, MAY CAUSE INJURY TO PERSONNEL OR
refer to MON2000 Software EQUIPMENTDAMAGE
for Gas Chromatographs Use caution when accessing an enclosure. A
User Manual (P/N 3-9000- voltage of 115 to 230 VAC, along with various
522). DC voltages, are present.
Failure to follow this precaution may cause
injury to personnel or damage equipment.

2. Loosen the thumb screws on the Oven


System mounting plate.

SEP 2005 Setting the Com ID


3-34 INSTALLATION AND SETUP
MODEL 700

3. Carefully lift up the assembly and rotate so


that the enclosure opening is accessible.
Model 700 Upper Enclosure

Mounting Bracket
Thumb Screw

Figure 3-12 Oven Mounting Bracket

Setting the Com ID SEP 2005


INSTALLATION AND SETUP 3-35
MODEL 700

4. Locate the multifunction board. It is


mounted on a bracket towards the center of
the upper enclosure.

Model 700 Upper Enclosure

Multifunction
Board

Figure 3-13 Multifunction Board Location

5. On the multifunction board, locate the


Modbus slave address (Com ID) DIP switch.
It is labeled “S1” and mounted on the lower
right corner of the board.

Figure 3-14 Dip Switch

SEP 2005 Setting the Com ID


3-36 INSTALLATION AND SETUP
MODEL 700

6. Inspect or change the DIP switch as


necessary, using the wiring diagram as a
guide (see Table 3-3).
• Make settings on switch S1 located on
the multifunction board.
• Switches “1” through “5” form a 5-bit
binary number for setting the Modbus
slave address (also known as Com ID or
Device ID).
• Switch number “1” is the least
significant bit, and switch number “5” is
the most significant bit. Set these
switches either ON or OFF.
• Switch “6” and “7” are spares and switch
“8” is used to cold start the processor (see
Table 3-4).
Use the GC maintenance records to document
any changes made to the switch settings.
Table 3-3 Modbus Slave Address (Com ID) DIP Switch Settings

Com ID 1 2 3 4 5

1 ON OFF OFF OFF OFF

2 OFF ON OFF OFF OFF

3 ON ON OFF OFF OFF

4 OFF OFF ON OFF OFF

5 ON OFF ON OFF OFF

6 SPARE

7 SPARE

8 COLD START

Setting the Com ID SEP 2005


INSTALLATION AND SETUP 3-37
MODEL 700

Table 3-4 Switch Positions for Cold Start

Normal (Run) OFF

Cold Start ON

3.4.2 Preparing for Serial Connections

The method for operating a Model 700 system


is from a connected personal computer (PC).
The PC must be:

• Running MON2000 software (version 2.2 or


later). See the MON2000 User Manual
(P/N 3-9000-522) for more information.
• Connected to the Model 700 via a serial
link.

This section addresses the basic ways to wire a


serial connection between a PC and the GC
system.

SEP 2005 Setting the Com ID


3-38 INSTALLATION AND SETUP
MODEL 700

Before connecting a PC to the Model 700,


determine the following:

1. What serial ports are available at the PC?


When you select one, consider these points:
• Standard PC serial ports are type
RS-232.
• Usually there are two external serial
port jacks on a PC, located on the rear
panel. Most often, they are either DB-9
or DB-25 male (see below). Model 700 software
upgrades may be installed
via any available Com Port.

• PC serial ports can be used by other


peripheral equipment attached to the
PC, such as a printer, mouse, or modem,
etc.
To determine which PC serial ports are
already being used by other equipment
and which port can be used for
connecting to the GC, note existing serial
connections, refer to your PC user
manual, and use diagnostic software
(such as Norton Utilities).
2. What serial ports are available at the GC?
The Model 700 without the Micro-FID
comes equipped with three serial ports
(standard), unless the customer needs a LOI
Interface connection, then only two com
ports are standard. The installation of the
optional Com4A board (with or without a
LOI) brings the total number of available
serial ports to six.

Setting the Com ID SEP 2005


INSTALLATION AND SETUP 3-39
MODEL 700

When you select a serial port, consider these


points:

• Com1 and Com2 from the WinSystems


CPU board (J1) to Field Termination
board (J5 and J7) (standard
configuration)
• Com3 from WinSystems CPU board (J6)
to the multifunction board
• Com4 is reserved for the LOI (Local
Operator Interface), if installed.

The Model 700 with the Micro-FID comes


equipped with two serial ports (standard). The
installation of the optional Com4A board bring
the total number of available serial ports to six.

When you select a serial port, consider these


points:

• Com1 and Com2 from the WinSystems


CPU board (J1) to Field Termination
board (J5 and J7) standard configuration
• Com3 from WinSystems CPU board (J6)
to the multifunction board (J4)
• Com4 from the WinSystems board (J6) is
connected to the Micro-FID/TCD
Preamplifier board (J4)

For additional serial ports, the:

• Optional Com4A board may be installed


at the factory. Com5 through Com8 are
fully available to the user and are
factory-configured to RS-232 protocol.
See Appendix A for additional options
(RS-422/485).
• With the optional Com4A board
installed, six Com ports are available to
the user.

SEP 2005 Setting the Com ID


3-40 INSTALLATION AND SETUP
MODEL 700

3. Is the connection to be made in a …


• Short distance between the PC and GC?
• With temporary or permanent cable
connection?
See Section 3.4.3, FTB Connection (RS-232).
4. Is the connection to be made with a …
• Short distance between the PC and GC?
• Permanent cable connection (see
Section 3.4.4).
5. Is the connection to be made with a …
• Long distance between the PC and GC?
• Permanent cable connection (see
Section 3.4.5).

3.4.3 FTB Connection (RS-232)

The easiest way to connect a PC to the GC is


with an off-the-shelf, straight-through serial
cable connected to the GC serial port DB 9-pin
connector pre-wired on the FTB. You can buy this cable from
most computer supply
1. Obtain a straight-through serial cable with retailers.
these specifications: If, however, it is necessary
to custom-wire a cable
• 50 feet long (or less) because of circumstances,
• DB 9-pin or DB 25-pin female plug at see guidelines provided in
Appendix B.
one end (for PC connection)
• DB 9-pin male plug at the other end (for
GC connection)
2. Connect the serial cable plugs to the
appropriate serial port jacks at the PC and
GC. Use the MON2000 software to monitor
and operate the GC as needed.

Setting the Com ID SEP 2005


INSTALLATION AND SETUP 3-41
MODEL 700

3.4.4 PC to GC Cable Short Distance


Connection (RS-232)

For detailed information The PC-GC connection is made with straight-


concerning serial through serial cable connected to one of the GC
communications, refer to internal serial ports on the FTB.
Appendix A.
If the length of cable can be 50 feet or less,
connect the serial cable to one of the GC serial
ports configured for RS-232. (Recall that output
from a standard PC serial port follows RS-232
serial definition.) Cable that is longer than 50
feet, when used for RS-232 serial transmission,
can result in spurious loss or corruption of
data.

To connect your PC to one of the


Model 700 serial port jacks:

1. Access the GC FTB (see Figure 3-15).


located on the right wall of the lower
enclosure.
Model 700 Lower Enclosure

FTB

Figure 3-15 Field Termination Board

SEP 2005 Setting the Com ID


3-42 INSTALLATION AND SETUP
MODEL 700

2. Choose an available serial port on the FTB


(see P/N CE-21157 in Appendix D) that is
configured for RS-232 protocol.
Unless specified by the customer, serial Model 700, standard
configuration, has two
ports are configured for RS-232. communications ports
For further details, see Figure 3-16 and available on the FTB;
Com1 and Com2.
Figure 3-17.
Multifunction FID/TCD
Board Preamplifier Board
Com3 Com4

CPU Field Termination


Board Com 4 is dedicated to the
Com1 Com1 Micro-FID/TCD Preamplifier.
Com2 Com2 When the LOI becomes
Com3 available, it will use a video
Com4 board instead of a serial port
Com5
Com6 connection.
Com7
Com8

Figure 3-16 Configuration without Com4A Board

Setting the Com ID SEP 2005


INSTALLATION AND SETUP 3-43
MODEL 700

Multifunction FID/TCD
Board Preamplifier Board
Com3 Com4

Model 700, with the Com


4A board installed, has six
CPU Field Termination
communications ports
Board
available on the FTB; Com1
and Com2, and Com5, Com1 Com1
Com6, Com7, and Com8. Com2 Com2
Com3
Com4

Com4A

Com5 Com5
Com 4 is dedicated to the Com6 Com6
Micro-FID/TCD Preamplifier. Com7 Com7
When the LOI becomes Com8 Com8
available, it will use a video
board instead of a serial port
connection. Figure 3-17 Configuration with Com4A Board

SEP 2005 Setting the Com ID


3-44 INSTALLATION AND SETUP
MODEL 700

3. Connect the appropriate serial cable.


If using a direct 6 conductor serial cable,
connect the exposed cable leads to the FTB
serial port. A pinout of a female DB 9-pin See Appendix A for
instructions on fabricating
socket is shown in Figure 3-18. a direct serial cable.

Com1
P2

5
RI 1 9
DSR 1 4
RTS 1 8
RXD 1 3
CTS 1 7
TXD 1 2
DTR 1 6
DCD 1 1

GND Com2
P3

5
RI 2 9
DSR 2 4
RTS 2 8
RXD 2 3
CTS 2 7
TXD 2 2
DTR 2 6
DCD 2 1

Figure 3-18 FTB Com1 and Com2 DB 9-pin Connector

Setting the Com ID SEP 2005


INSTALLATION AND SETUP 3-45
MODEL 700

4. Field Termination Board serial


communications settings are shown in
Figure 3-19 through Figure 3-23.
Com1

RS-232 RS-485 RS-422 J5


DCD 1
1
RXD 1 TX/RX+ TX+
2
TXD 1 TX/RX- TX- 3
DTR 1
4
5
DSR 1 RX+
6
RTS 1 RX-
7
CTS 1 8
RI 1 9

Figure 3-19 FTB Com 1 DB 9-pin Phoenix Connector

Com2

RS-232 RS-485 RS-422 J7


DCD 2
1
RXD 2 TX/RX+ TX+
2
TXD 2 TX/RX- TX- 3
DTR 2
4
5
DSR 2 RX+
6
RTS 2 RX-
7
CTS 2 8
RI 2 9

Figure 3-20 FTB Com2 DB 9-pin Phoenix Connector

SEP 2005 Setting the Com ID


3-46 INSTALLATION AND SETUP
MODEL 700

Com5

RS-232 RS-485 RS-422 J9


RLSD 5
1
RXD 5 TX/RX+ TX+
2
TXD 5 TX/RX- TX- 3
DTR 5
4
5
DSR 5 RX+
6
RTS 5 RX-
7
CTS 5 8
RI 5 9

Figure 3-21 FTB Com5 DB 9-pin Phoenix Connector

Com6

RS-232 RS-485 RS-422


J13
RLSD 6
1
RXD 6 TX/RX+ TX+
2
TXD 6 TX/RX- TX- 3
DTR 6
4
5
DSR 6 RX+
6
RTS 6 RX-
7
CTS 6 8
RI 6 9

Figure 3-22 FTB Com6 DB 9-pin Phoenix Connector

Setting the Com ID SEP 2005


INSTALLATION AND SETUP 3-47
MODEL 700

Com7

RS-232 RS-485 RS-422 J17


RLSD 7
1
RXD 7 TX/RX+ TX+
2
TXD 7 TX/RX- TX- 3
DTR 7 4
5
DSR 7 RX+
6
RTS 7 RX-
7
CTS 7 8
RI 7 9

Figure 3-23 FTB Com7 DB 9-pin Phoenix Connector

Com8

RS-232 RS-485 RS-422 J18


RLSD 8
1
RXD 8 TX/RX+ TX+
2
TXD 8 TX/RX- TX- 3
DTR 8
4
5
DSR 8 RX+
6
RTS 8 RX-
7
CTS 8 8
RI 8 9

Figure 3-24 Com8 DB 9-pin Phoenix Connector


GC Phoenix Plug Port

SEP 2005 Setting the Com ID


3-48 INSTALLATION AND SETUP
MODEL 700

To make an RS-232 serial connection between


one of the Phoenix Plug serial ports of the GC,
and an external modem with DB 25-pin serial
port, you will need to manufacture the cable
and its DB 25-pin, male plug cable end as
illustrated below (see Figure 3-25).

Figure 3-25 GC Phoenix Plug Port to External Modem


DB 25-pin Port

3.4.5 Long Distance Connection (RS-422, RS-485)

RS-422 and RS-485 serial protocols are


recommended for longer distance serial
connections between the PC and GC System
(i.e., distances greater than the 50 feet).

Setting the Com ID SEP 2005


INSTALLATION AND SETUP 3-49
MODEL 700

To connect your PC to one of the internal


Model 700 RS-422/RS-485 serial port jacks:

5. Obtain the following equipment:


• An asynchronous line driver (or interface
device) with RS-232 input and RS-422/
RS-485 output. See Appendix A for
example brand and model.
• Shielded, computer-grade, twisted pair
cable (to connect the asynchronous line
driver device to the GC).
• A straight-through serial cable (to
connect the PC to the line driver).
6. Connect the straight-through serial cable
from the PC serial port to the RS-232 serial
port of the line driver device. Then connect
the twisted pair cable to the RS-422/RS-485
serial port of the line driver.
7. Configure the line driver for data
communications equipment (DCE)
operation. See Appendix A for an example
configuration.
8. Access the GC FTB (see Figure 3-15 in
Section 3.4.2).
9. Choose an available serial port on FTB that
is configured for RS-422 or RS-485 serial
protocol, and connect the twisted pair cable
Serial ports Com1 through from the line driver. See Appendix A for
Com3 are configured by
example connection. Also see Figure 3-19
default for RS-232.
through see Figure 3-23 for a list of ports
For further details or and terminals assigned for serial communi-
instructions on how to
cations.
configure these ports to RS-
422/485, see Appendix A.

SEP 2005 Setting the Com ID


3-50 INSTALLATION AND SETUP
MODEL 700

3.4.6 GC-Printer Wiring

A printer can be connected directly to the GC


the Field Termination Board (FTB) at one of The GC uses only a generic
the serial ports. The type and scheduling of printer driver. The PC printer
reports produced at the GC printer are allows more control and
determined by settings made in MON2000 better quality output.
(from the Reports menu, select GC Report
Request and/or GC Printer Control; see the
MON2000 Software for Gas Chromatographs
User Manual (P/N 3-9000-522) for more
information).

To connect a printer to the GC serial port:

1. Access the GC FTB (see Figure 3-15 in


Section 3.4.2).
2. Choose an available serial port on the FTB
that is configured for RS-232 serial protocol.
3. After the wiring connections have been See Appendix A for a
completed, use MON2000 to configure the complete listing of the serial
GC serial port. ports and corresponding
pinouts to fabricate a serial
(a) From the Application menu, select Serial printer cable.
Ports. The Serial Ports window appears.
(b) Select the appropriate Port row and set
Usage to “Report”, Protocol to “ASCII”
and RW to “W”.
(c) Ensure that the Com ID setting is
correct.
(d) Leave all other settings at the default
values (see the MON2000 User Manual
for more information).

Setting the Com ID SEP 2005


INSTALLATION AND SETUP 3-51
MODEL 700

3.4.7 Discrete Digital I/O Wiring

The Field Termination Board (P/N 3-0700-010)


has five discrete outputs and four discrete
inputs.

Discrete Digital Inputs

To connect digital signal input/output lines to


the GC (P/N 3-0700-010):

1. Access the FTB (see Figure 3-26)


(P/N 3-0700-010).
Model 700 Lower Enclosure

J14

J10

Figure 3-26 Field Termination Board

The FTB has five discrete outputs and four


discrete inputs. The discrete input,
DIG_IN4, is dedicated to a pressure switch.
The discrete inputs are located on J10 (10
pin Phoenix connector).

SEP 2005 Setting the Com ID


3-52 INSTALLATION AND SETUP
MODEL 700

2. Route digital I/O lines appropriately,


especially in the case of the explosion-proof
enclosure.
There are connections for four digital inputs
and five digital output lines (Phoenix 10-pin
connector), as follows:

Table 3-5 FTB Discrete Digital Inputs

J10 Function Description

Pin 1 DIG_IN1

Pin 2 GND

Pin 3 DIG_IN2

Pin 4 GND

Pin 5 DIG_IN3 to customer

Pin 6 GND
Pin 7 DIG_IN4 dedicated to a pressure switch

Pin 8 GND dedicated to a pressure switch

Pin 9 DIG_IN5
Pin 10 GND

Discrete Digital Outputs

The discrete outputs are located on J14


(P/N 3-0700-010) (Phoenix 10-pin connector)
have two “Form A” relays on the FTB. Outputs
3-5 are Solid State switches with a rating of
.375A @30 VDC. The relays, with sealed
enclosures, have a contact current rating of 1.0
Amperes each (see Figure 3-26).

Setting the Com ID SEP 2005


INSTALLATION AND SETUP 3-53
MODEL 700

For discrete digital outputs, see Table 3-6.

Table 3-6 FTB Discrete Digital Outputs

J14 Function

Pin 1 DIG_OUT

Pin 2 DIG_OUT

Pin 3 DIG_OUT

Pin 4 DIG_OUT

Pin 5 DIG_OUT_ 3+

Pin 6 DIG_OUT_ 3-

Pin 7 DIG_OUT_ 4+
Pin 8 DIG_OUT_ 4-

Pin 9 DIG_OUT_ 5+

Pin 10 DIG_OUT_ 5-

SEP 2005 Setting the Com ID


3-54 INSTALLATION AND SETUP
MODEL 700

3.4.8 Analog Input Wiring

There are four analog inputs on the Field


Termination Board (P/N 3-0700-010 and
drawing CE-21157) located at J4 (12-pin
Phoenix connector).

Table 3-7 FTB Analog Inputs

J4 Function

Pin 1 VIN+_1

Pin 2 VIN-_1

Pin 3 Shield

Pin 4 VIN+_2

Pin 5 VIN-_1

Pin 6 Shield

Pin 7 VIN+_3

Pin 8 VIN-_1

Pin 9 Shield

Pin 10 VIN+_4

Pin 11 VIN-_1

Pin 12 Shield

Setting the Com ID SEP 2005


INSTALLATION AND SETUP 3-55
MODEL 700

3.4.9 Analog Output Wiring

There are four standard analog outputs on the


standard FTB (P/N 3-0700-010 and drawing
CE-21157); located at J8 (12-pin Phoenix
connector). Additionally, if installed, the
optional analog board has eight analog outputs

Table 3-8 FTB Analog Outputs

J8 Function

Pin 1 IOUT+_1

Pin 2 IOUT-_1

Pin 3 Shield

Pin 4 IOUT+_2

Pin 5 IOUT-_2

Pin 6 Shield

Pin 7 IOUT+_3

Pin 8 IOUT-_3

Pin 9 Shield

Pin 10 IOUT+_4

Pin 11 IOUT-_4

Pin 12 Shield

There are eight analog outputs on the optional


analog output board (P/N 2-3-0580-037 and
drawing CE-21157); located at J3 (24-pin
Phoenix connector):

SEP 2005 Setting the Com ID


3-56 INSTALLATION AND SETUP
MODEL 700

Table 3-9 Optional Analog Outputs

J3 Function

Pin 1 IOUT+_5

Pin 13 IOUT-_5

Pin 2 Shield

Pin 14 IOUT+_6

Pin 3 IOUT-_6

Pin 15 Shield

Pin 4 IOUT+_7

Pin 16 IOUT-_7

Pin 5 Shield

Pin 17 IOUT+_8

Pin 6 IOUT-_8

Pin 18 Shield

Pin 7 IOUT+_9

Pin 19 IOUT-_9

Pin 8 Shield

Pin 20 IOUT+_10

Pin 9 IOUT-_10

Pin 21 Shield

Pin 10 IOUT+_11

Pin 22 IOUT-_11

Pin 11 Shield

Pin 23 IOUT+_12

Pin 12 IOUT+_12

Pin 24 Shield

Setting the Com ID SEP 2005


INSTALLATION AND SETUP 3-57
MODEL 700

3.4.10 Optional Boards

Optional modem boards are available for the


Model 700 GC.

The jumper settings and pinouts for each board


is shown below.

Optional WinSystems Modem

Table 3-10 J8 Modem Board Jumper Settings

Pin(s) Position

1 and 2 In

3 and 4 In

5 and 6 In

7 and 8 In

Table 3-11 J9 Modem Board Jumper Settings

Pin(s) Position

1 and 2 In

5 and 6 In

Table 3-12 J10 Modem Board Jumper Settings

Pin(s) Position

1 and 2 In

3 and 4 In

5 and 6 In

9 and 10 In

15 and 16 In

SEP 2005 Setting the Com ID


3-58 INSTALLATION AND SETUP
MODEL 700

Optional Radicom Modem Settings


Table 3-13 J26 Radicom Modem Jumper Settings

Pin(s) Position

1 and 2 In

Table 3-14 J27Radicom Modem Jumper Settings

Pin(s) Position

1 and 2 In

Table 3-15 J30 Radicom Modem Jumper Settings

Pin(s) Position

1 and 2 In

Table 3-16 J31 Radicom Modem Jumper Settings

Pin(s) Position

2 and 3 In

Setting the Com ID SEP 2005


INSTALLATION AND SETUP 3-59
MODEL 700

Ethernet Settings
Table 3-17 J1 PCM-NE2000 Ethernet Board Jumper Settings

Pin(s) Position

15 and 16 In

17 and 18 In

21 and 22 In

Table 3-18 J2 PCM-NE2000 Ethernet Board Jumper Settings

Pin(s) Position

1 and 2 In

Table 3-19 J3 PCM-NE2000 Ethernet Board Jumper Settings

Pin(s) Position

1 and 2 In

7 and 8 In

SEP 2005 Setting the Com ID


3-60 INSTALLATION AND SETUP
MODEL 700

3.5 LEAK CHECKS AND PURGING FOR


FIRST CALIBRATION

Apply AC power to the unit after verifying all


electrical connections are correct and safe.
Ensure that all interconnections and external
signal connections have been verified and
proper grounds have been made before turning
on the power.

3.5.1 Initial Leak Check

The focus of this section is for field connections


to the analyzer, during the installation process.
See Section 4.6 for an in depth discussion of
analyzer leak checks.

Carrier Gas Line Leak Checks

1. Plug the Measure Vent (labeled “MV”) to


block the free flow of Carrier Gas through
the GC.
The GC does not have an
2. Slowly pressurize the “GC side” of the inline Block Valve to shut
Carrier Gas to 110 psig (±2 percent) with off the Carrier Gas flow.
the dual-stage regulator at the Carrier Gas
cylinder.
3. After two minutes, shut off the Carrier Gas
bottle valve by turning it clockwise. Then,
observe the high-side regulator gauge on the
Carrier Gas bottle.
• The gauge should not bleed down more
than 200 psig in 10 minutes.
• If Carrier Gas is lost at a faster rate,
then all tube fittings between the
Carrier Gas bottle and the GC (including
the dual-stage regulator) must be
checked for leaks and tightened if
necessary.

Leak Checks and Purging FOR First Calibration SEP 2005


INSTALLATION AND SETUP 3-61
MODEL 700

Most leaks at this stage (Installation and


Setup) are usually found between the
Carrier Gas bottle and the GC.

The dual-stage regulator fitting


connecting to the Carrier bottle, may not
seat properly with some Carrier Gas
bottles and allow a leak. If this occurs,
carefully wrap a small length of Teflon
tape around the tip of the inlet tube on
the dual-stage regulator (which sits
against the Carrier Gas bottle valve
seat).
4. Once the GC passes the “Initial leak check”,
reopen the Carrier Gas bottle valve and
remove the Measurement Vent (MV) plug.
Calibration Line Leak Check

1. Slowly pressurize the Calibration line (up to


20 psig).
2. Block-in the line by turning the “Cal
Stream” blocking valve clockwise until
seated.
3. Shut off the Calibration gas at the gas bottle
by turning the valve clockwise.
4. Observe the high-side of the Calibration gas
dual-stage regulator making sure the
pressure holds. The pressure should not
decrease for a period of two to three
minutes.
5. When the GC passes the “Initial Calibration
Gas leak check”, re-open the Calibration gas
bottle valve and the in-line “Cal Stream”
block valve.

SEP 2005 Leak Checks and Purging FOR First Calibration


3-62 INSTALLATION AND SETUP
MODEL 700

Sample Lines (Streams) Leak Check

1. Slowly pressurize the Sample line (up to 20


psig).
2. Block-in the line.
3. Observe the regulator, making sure the
pressure holds. The pressure should not
decrease for a period of two to three
minutes.
4. When the GC passes the “Initial Sample
Gas leak check”, re-open the Sample Gas
lines.

3.5.2 Purging Carrier Gas Lines

Purging carrier and calibration gas lines


requires AC power.

To purge the Carrier Gas lines, Tubing should be clean and


dry internally. During
installation, the tubing
1. Ensure that the MV vent line plug has been
should have been blown
removed, and the vent line is open. free of internal moisture,
2. Ensure that the Carrier Gas bottle valve is dust, or other contaminants.
open.
3. Set the Carrier Gas line pressure at 110
psig. Use the dual stage regulator at the
Carrier Gas bottle to adjust pressure.
Do not use the “Carrier
4. Turn ON the AC power to the GC. Pressure Adjust” regulator
5. Establish communications with the GC via adjustment (on the Flow
Panel Assembly) to adjust
the MON2000 software. (Use the File >
Carrier Gas line pressure.
Quick Connect menu path; see Section 2.7.2 This pressure is factory-set
in the MON2000 Software for Gas and should not be adjusted.
Chromatographs User Manual
(P/N 3-9000-522) for more information.)

Leak Checks and Purging FOR First Calibration SEP 2005


INSTALLATION AND SETUP 3-63
MODEL 700

6. Use the Applications>Temperature Control


menu path to access this function. The
readouts of the block, column and SSS
A period of 4 to 8 hours (or heater controllers should indicate that the
overnight) is recommended, unit is warming up. Also, the yellow and red
during which all of the status indicators on the FTB4 should be on.
settings described in Steps
1 through 7 are maintained. 7. Allow the GC system temperature to
No other settings should be stabilize and the Carrier Gas lines to
made. become fully purged with Carrier Gas.
8. Select the Auto Sequence Function. Use the
Control > Auto Sequence menu path
described in Section 4 of the MON2000
Software for Gas Chromatographs User
Manual (P/N 3-9000-522).

SEP 2005 Leak Checks and Purging FOR First Calibration


3-64 INSTALLATION AND SETUP
MODEL 700

3.5.3 Purging Calibration Gas Lines

To purge the calibration gas lines, as


preparation for first calibration:

1. Ensure that the Carrier Gas lines have been


fully purged, as described in the previous
section, and that the SV plug has been
removed.
2. Close the calibration gas bottle valve.
3. Fully open the block valve associated with
calibration gas feed (the block valve should
be located on lower right-hand corner of the
front panel).
See Section 5.8 in the MON2000 Software
for Gas Chromatographs User Manual
(P/N 3-9000-522) for instructions on
selecting streams.
4. Open the calibration gas bottle valve.
5. At the calibration gas bottle regulator,
increase outlet pressure to 20 psig, ±5%.
6. Close the calibration gas bottle valve.
7. Let both gauges on the calibration gas bottle
valve bleed down to 0 (zero) psig.
8. Repeat Steps 4 through 7, five times.
9. Open the calibration gas bottle valve.

Leak Checks and Purging FOR First Calibration SEP 2005


INSTALLATION AND SETUP 3-65
MODEL 700

3.6 SYSTEM STARTUP

To perform system start-up,

1. For system startup, run an analysis of the


calibration gas.
(a) If equipped with an optional stream
switching board, ensure that the stream
switch for the calibration stream is set to
AUTO.
Otherwise, ensure that the calibration
gas supply is turned on and set to the
correct pressure (25 to 30 PSIG).
(b) Using the MON2000 software, run a
single stream analysis on the calibration
stream. Once proper operation of the GC
is verified, halt the analysis.
Use the Control > Calibration and
Control > Halt menu paths; see Sections
4.3 and 4.4 in the MON2000 Software for
Gas Chromatographs User Manual (P/N
3-9000-522) for more information.
2. Start Auto Sequence of the line gas
stream(s).
Use the Control > Auto Sequence menu
path; see Section 4.1 in the MON2000
Software for Gas Chromatographs User
Manual (P/N 3-9000-522) for more
information. The GC will begin the Auto
Sequence analysis mode.

SEP 2005 System Startup


3-66 INSTALLATION AND SETUP
MODEL 700

This page is intentionally left blank.

System Startup SEP 2005


MAINTENANCE AND TROUBLESHOOTINGTABLE OF CONTENTS 4-1
Model 700

MAINTENANCE AND TROUBLESHOOTING


4--

4.1 TROUBLESHOOTING AND REPAIR CONCEPT

The most efficient method for maintaining and


repairing the Model 700 GC system is a
component-replacement concept that allows
you to return the system to operation as
quickly as possible. Sources of trouble, such as
printed-circuit assemblies, valves, etc., are
identified during troubleshooting test
procedures and are replaced at the lowest level
practical with units in known working order.
The defective components are then either
repaired in the field or returned to Daniel
Measurement Services (DMS) for repair or
replacement.

4.2 ROUTINE MAINTENANCE

The Model 700 GC system will perform


accurately for long periods with very little
attention (except for maintaining the Carrier
Gas cylinders). A bimonthly record of certain
parameters will assist greatly in assuring that
your Model 700 is operating to specifications.
The maintenance checklist should be filled out
bimonthly, dated, and kept on file for access by
maintenance technicians as necessary (see
Table 4-1).This gives you a historical record of
the operation of your Model 700, enables a
maintenance technician to schedule
replacement of gas cylinders at a convenient
time, and allows quick troubleshooting and
repair when it becomes necessary.

SEP 2005 Troubleshooting and Repair Concept


4-2 MAINTENANCE AND TROUBLESHOOTINGTABLE OF CONTENTS
Model 700

A chromatogram, a Configuration Report, and


a Raw Data Report should also be made and
filed with the checklist, furnishing a positive
dated record of the Model 700. The
chromatogram and reports can also be
compared to the chromatograms and reports
run during the troubleshooting process.

4.2.1 Bimonthly Maintenance Checklist

Copy the sample maintenance checklist as


necessary for your files (see Table 4-1). If you
have a problem, please complete the checklist
and reports, and have the results available
when calling DMS with a problem. Also have
the Sales Order number. The Sales Order
number can be found on the nameplate located
on the left side wall of the upper housing of the
Model 700. The chromatograms and reports
archived when your Model 700 left the factory
are filed by this number.

Routine Maintenance SEP 2005


MAINTENANCE AND TROUBLESHOOTINGTABLE OF CONTENTS 4-3
Model 700

Table 4-1 Maintenance Checklist

Date Performed: Sales Order Number:

System Parameters As Found As Left Nominal

Carrier Gas Cylinder

Cylinder Pressure Reading (High) ____ psig ____ psig ____ psig
Cylinder Pressure Outlet Reading
____ psig ____ psig 110 psig

Carrier Pressure Panel Regulator ____ psig N/A 85 psig

Sample System

Sample Line Pressure(s) (1)____ psig ____ psig 20 psig

(2)____ psig ____ psig 20 psig

(3)____ psig ____ psig 20 psig

(4)____ psig ____ psig 20 psig

(5)____ psig ____ psig 20 psig

Sample Flows (1)___ cc/min ____cc/min 40-60 cc

Sample Vent 1 (SV1) (2)___ cc/min ____cc/min 40-60 cc

Sample Vent 2 (SV2) (3)___ cc/min ____cc/min 40-60 cc

(4)___ cc/min ____cc/min 40-60 cc

(5)___ cc/min ____cc/min 40-60 cc

Calibration Gas

High Pressure Reading ____ psig ____ psig

Outlet Pressure Reading ____ psig ____ psig 20 psig

Flow ____ cc/min ___ cc/min 40-60 cc

SEP 2005 Routine Maintenance


4-4 MAINTENANCE AND TROUBLESHOOTINGTABLE OF CONTENTS
Model 700

4.2.2 Routine Maintenance Procedures

• Complete the maintenance checklist


bi-monthly. Place the sales order number,
date, and time on the form and file it. This
gives you a basis for comparison in the
future if you need it.
• Save a Chromatogram of the operating
Model 700 on the PC with the
MON2000 software. Print Configuration,
Calibration, and Raw Data reports and file
them with the MON2000.
• Check the printer paper (if used) to ensure
that a sufficient supply of paper remains.
Check carrier and calibration gas supplies.

4.2.3 Contact Service

Daniel Measurement Services (DMS) offers


maintenance service programs that are tailored
to fit specific requirements. Contracts for
service and repair can be arranged by
contacting the DMS at the address or telephone
number on the Customer Repair Report at the
back of this manual.

Routine Maintenance SEP 2005


MAINTENANCE AND TROUBLESHOOTINGTABLE OF CONTENTS 4-5
Model 700

4.3 ACCESS TO GC EQUIPMENT ELEMENTS

4.3.1 Electrical/Electronic Components

DANGER TO PERSONNEL AND EQUIPMENT


The explosion-proof housing should not be opened
when the unit is exposed to an explosive environment.
If access to the explosion-proof housing is required,
precautions must be taken to ensure that an explosive
environment is not present.
Failure to do so may result in injury to personnel or
cause damage to the equipment.

The Model 700 electrical/electronic components


are located in the upper and lower explosion-
proof housings. All of the electrical/electronic
components are fully accessible from the front
and top of the Model 700.
Model 700 Micro-FID Assembly

Figure 4-1 Model 700 with TCD/Micro-FID Front View

SEP 2005 Access to GC Equipment Elements


4-6 MAINTENANCE AND TROUBLESHOOTINGTABLE OF CONTENTS
Model 700

Model 700 with TCD Upper Enclosure•


• Multifunction Board
• Dual Methods Adapter Board
• Dual Methods Preamplifier Board
• Solenoid Heater/Driver Board

Model 700 with TCD Lower Enclosure


• WinSystems CPU Board
• Analog Board
• Analog Board (optional)
• Com4A Board (optional)
• Ethernet Board (optional)
• Radicom Modem board (optional)
• DC/DC Field Termination Board

Model 700 with Micro-FID/TCD Upper


Enclosure

• Multifunction Board
• Solenoid/Heater Driver Board
• Micro-FID/TCD Preamplifier Board
• Micro-FID/TCD Preamplifier Power Supply
Board
• Micro-FID Connector Board

Model 700 with Micro-FID/TCD Lower


Enclosure

• Field Termination Board


• Backplane Board
• Interconnect Board
• WinSystems CPU (with PC104 interface)
• Com4A PC/104 Board (optional)

Access to GC Equipment Elements SEP 2005


MAINTENANCE AND TROUBLESHOOTINGTABLE OF CONTENTS 4-7
Model 700

• Ethernet Board (optional)


• Radicom Modem Board (optional)

The optional Radicom • Eight Channel Analog (non-isolated


Modem is always mounted 4-20mA) Output Board (optional)
on top of the PC//104 card
stack. • Four Channel Analog (isolated 4-20mA)
Output Board (optional)
• Front Panel Analytical and Stream Switch
Panel
• Dual Methods Adapter Board

Model 700 Lower Enclosure Electronics

Figure 4-2 CPU, Com4A, and Modem Boards

4.3.2 Detector Elements, Heater Elements, Valves


and Columns

The detector elements, heater elements, valves


and columns are located in the upper explosion-
proof housing of the Model 700 GC.

SEP 2005 Access to GC Equipment Elements


4-8 MAINTENANCE AND TROUBLESHOOTINGTABLE OF CONTENTS
Model 700

Remove the thermal cover and insulating


shield to gain access to these components.
Model 700 Upper Enclosure
The optional Ethernet board
is not shown, but plugs into
the CPU board or the
Com4A board.
Thermal
Cover

Figure 4-3 Upper Explosion-proof Housing

Access to GC Equipment Elements SEP 2005


MAINTENANCE AND TROUBLESHOOTINGTABLE OF CONTENTS 4-9
Model 700

The detector elements, including the Micro-


FID, are located in the block (TCD) and on the
Micro-FID Base attached to the valve block.
Model 700 TCD Upper Enclosure

Thermal
Conductivity
Detectors

Figure 4-4 Thermal Conductivity Detector

Model 700 Micro-FID Upper Enclosure

FID

FID Block

Figure 4-5 Flame Ionization Detector

SEP 2005 Access to GC Equipment Elements


4-10 MAINTENANCE AND TROUBLESHOOTINGTABLE OF CONTENTS
Model 700

There are five heater elements: three valve


block heaters, the column heater, and the
stream switching system heater
(see Figure 4-4).

The stream switching heater is a cartridge


heater inserted into the stream switch block
(manifold).

The column heater is a cartridge heater located


in the middle of the column mandrel.

The block heaters are cartridge heaters located


in the corners of the block. Column and block
heaters are identical and are installed from the
underside of the manifold (plastic base) of the
oven.

Access to GC Equipment Elements SEP 2005


MAINTENANCE AND TROUBLESHOOTINGTABLE OF CONTENTS 4-11
Model 700

4.4 PRECAUTIONS FOR HANDLING PC


ASSEMBLIES

Printed circuit assemblies contain CMOS


integrated circuits, which can be damaged if
the assemblies are not properly handled. The
following precautions must be observed when
working with the assemblies:

• Do not install or remove the Model 700


printed circuit assemblies while power is
applied to the units.
• Keep electrical components and assemblies
in their protective (conductive) carriers or
wrapping until ready for use.
• Use the protective carrier as a glove when
installing or removing printed circuit
assemblies.
• Maintain contact with a grounded surface to
prevent static discharge when installing or
removing printed circuit assemblies.

SEP 2005 Precautions for Handling PC Assemblies


4-12 MAINTENANCE AND TROUBLESHOOTINGTABLE OF CONTENTS
Model 700

4.5 GENERAL TROUBLESHOOTING

This section contains general troubleshooting


information for the Model 700. The information
Correct ALL alarms before
is arranged as appropriate either by major re-calibration.
subsystems or by major functions of the
instrument. See Table 4-2 for frequent possible
causes of the hardware alarms.

4.5.1 Hardware Alarms

Use the following table to identify the alarm


and possible cause to remedy the problem.

Table 4-2 Basic Hardware Troubleshooting via Alarms

Alarm Possible Cause

Application Checksum Failure DiskOnChip

ROM Checksum Failure DiskOnChip

RAM Diagnostics Failure bad RAM

Micro-FID/TCD Preamplifier
Alarms extinguished flame
Micro-FID Temperature High
Micro-FID Comm. Failure

Analog Output 1 High Measured value program for Analog Output


1 is greater than user-defined full scale
range.

Analog Output 2 High same as Analog Output 1 High


Analog Output 3 High same as Analog Output 1 High
Analog Output 4 High same as Analog Output 1 High
Analog Output 5 High same as Analog Output 1 High
Analog Output 6 High same as Analog Output 1 High
Analog Output 7 High same as Analog Output 1 High
Analog Output 8 High same as Analog Output 1 High
Analog Output 9 High same as Analog Output 1 High
Analog Output 10 High same as Analog Output 1 High
Analog Output 11 High same as Analog Output 1 High
Analog Output 12 High same as Analog Output 1 High

General Troubleshooting SEP 2005


MAINTENANCE AND TROUBLESHOOTINGTABLE OF CONTENTS 4-13
Model 700

Table 4-2 Basic Hardware Troubleshooting via Alarms (Continued)

Alarm Possible Cause

Analog Output 1 Low Measured value program for Analog Output


1 is lower than user-defined zero range.

Analog Output 2 Low same as Analog Output 1 Low


Analog Output 3 Low same as Analog Output 1 Low
Analog Output 4 Low same as Analog Output 1 Low
Analog Output 5 Low same as Analog Output 1 Low
Analog Output 6 Low same as Analog Output 1 Low
Analog Output 7 Low same as Analog Output 1 Low
Analog Output 8 Low same as Analog Output 1 Low
Analog Output 9 Low same as Analog Output 1 Low
Analog Output 10 Low same as Analog Output 1 Low
Analog Output 11 Low same as Analog Output 1 Low
Analog Output 12 Low same as Analog Output 1 Low

Analog Input High 1 Measured value program for Analog Input 1


is greater than the user-defined full scale
range.

Analog Input High 2 Same as Analog Input 1 High


Analog Input High 3 Same as Analog Input 1 High
Analog Input High 4 Same as Analog Input 1 High

Analog Input Low 1 Measured value program for Analog Input 1


is lower than the user-defined full scale
range.

Analog Input Low 2 Same as Analog Input 1 Low


Analog Input Low 3 Same as Analog Input 2 Low
Analog Input Low 4 Same as Analog Input 3 Low

Preamp Input 1 Out of Range Indicates either Carrier Gas gone; air not
purged from carrier lines; power failure; bad
thermistors; preamp out of balance or failed;
analyzer temperature low; interconnection
wiring.

Preamp Input 2 Out of Range same as Preamp Input 1 Out of Range

Preamp Input 3 Out of Range same as Preamp Input 1 Out of Range

Preamp Input 4 Out of Range same as Preamp Input 1 Out of Range

Preamp Failure same as Preamp Input 1 Out of Range

Analyzer Failure Indicates either the Carrier Gas is low


(below 90 psig at Carrier Gas bottle) or gone;
a bad solenoid; a Carrier Gas leak in system.

SEP 2005 General Troubleshooting


4-14 MAINTENANCE AND TROUBLESHOOTINGTABLE OF CONTENTS
Model 700

Table 4-2 Basic Hardware Troubleshooting via Alarms (Continued)

Alarm Possible Cause

Power Failure GC Controller has experienced a re-start


since alarms were last cleared, caused by
power failure. Automatically starts in RUN
mode and runs calibration gas until it iden-
tifies all retention times or for a maximum of
two hours before switching to line gas.

TCD
Fused Peak Overflow - Noisy Air not purged from carrier lines; bad ther-
Baseline mistors; shields.

RF% Deviation Calibration gas low or out; valve timing


error; faulty auto-calibration solenoid.

Warm Start Calibration same as RF% deviation


Failure

Valve Timing Failure same as RF% deviation

4.5.2 Troubleshooting Checklist

An online gas chromatograph can operate


properly only if flows are balanced and
constant, the temperature is constant, no leaks
are present, and the GC Controller is correctly
timed. Before going through the troubleshoot-
ing procedures, perform the routines of the
Basic Hardware Troubleshooting via Alarms
(see Table 4-2). Checklist records performed
regularly may indicate problems and prevent
any sudden breakdown.

Do not adjust any values if they are within the


nominal tolerance values on the Checklist.
Compare the values with those obtained in
preceding weeks. This may pinpoint your
problem immediately.

General Troubleshooting SEP 2005


MAINTENANCE AND TROUBLESHOOTINGTABLE OF CONTENTS 4-15
Model 700

The following is a guide for troubleshooting if a


problem with sample analysis occurs. See Table
4-2 for diagnostic data. This data will be useful
if it becomes necessary to call DMS for
assistance.

SEP 2005 General Troubleshooting


4-16 MAINTENANCE AND TROUBLESHOOTINGTABLE OF CONTENTS
Model 700

Table 4-3 Troubleshooting Checklist

Description As Found As Left Notes

Analyzer

Leak check with "Snoop" from


Carrier Gas bottle to Analyzer
regulator.

Leak check with "Snoop" from


calibration standard to auto-
calibration solenoid.

Pre-amp balance voltage ___________mV _________mV 0 (±0.5 mV)

Sample System

Leak check with "Snoop" from


sample probe to sample
solenoid

Controller Inputs

GRI (CH.1) 0.0 - 0.0


GRI (CH.2) 0.8 - 1.2
GRI (CH.3) 0.8 - 1.2
GRI (CH.4) 0.8 - 1.2
____________ ___________ 4800 to 6400
Value (12-bit AD) ____________ ___________ 4800 to 6400
PAZ1 ____________ ___________ 4800 to 6400
PAZ2 ____________ ___________ 9200 to 12000
PAZ3
PAZ4
____________ ____________ -32767 to 32767
Value (16-bit AD) ____________ ____________ -32767 to 32767
GC 1 ____________ ____________ -32767 to 32767
GC2 ____________ ____________ -32767 to 32767
GC3
GC4

General Troubleshooting SEP 2005


MAINTENANCE AND TROUBLESHOOTINGTABLE OF CONTENTS 4-17
Model 700

Table 4-3 Troubleshooting Checklist (Continued)

Description As Found As Left Notes

Power Supply (DC – DC) NOTE: See Figure 4-6


Input Voltage Ranges: through Figure 4-9 for test
(23V - 28VDC) point locations.

FTB:
+ 12V @ 0.25A (± 0.6)
+ 5V @ 3A (± 0.25V)
- 3.8V @ 0.1A (± 0.2V)
- 12 V @ 0.25A (C 0.6V)

Dual Methods Adapter


+ 20V @ 0.35A (± 1V)
- 20V @ 0.35A (± 1V)
+ 5VDC (± 0.25V)

The Dual Methods Board is


used on Model 700 GCs
with 2350A Controllers.
Power Supply (AC – DC)
SOL/HTR Driver
Input Voltage Range:
N/A
(90–130/180-264 VAC)
(Auto-ranging)
Output Voltage/Current:
24.0VDC
Output Power:
Continuous load demand
power, measured at the
Output Terminals of the
Power Supply, shall not
exceed 140 Watts.

SEP 2005 General Troubleshooting


4-18 MAINTENANCE AND TROUBLESHOOTINGTABLE OF CONTENTS
Model 700

Table 4-3 Troubleshooting Checklist (Continued)

Description As Found As Left Notes

Chromatogram

Check baseline

Check component values on


report

Number of peaks

Retention times

Date and file

Temperature

Column Module Temperature ____ °C ____°C 79.80 - 80.20 °C


____ °F ____°F 175.64 - 176.36 °F

Valve Block Temperature ____°C ____ °C 79.80 - 80.20 °C


____°F ____ °F 175.64 - 176.36 °F

Stream Switching System ____ °C ____ °C 64.0 - 66.0 °C


____ °F ____ °F 147.2 - 150.8 °F

Sample System Temperature ____ °C ____ °C **

Measure Vent Flow

Valve 3 ON ___ cc/min ____ cc/min 12-18 cc/min


Valve 3 OFF ___ cc/min ____ cc/min ± 2 cc between Valve 3
states of ON / OFF

**Refer to System Operational Parameters

General Troubleshooting SEP 2005


MAINTENANCE AND TROUBLESHOOTINGTABLE OF CONTENTS 4-19
Model 700

4.5.3 Test Points Dual Methods Board and FTB

This section applies to Model 700 GCs with the


TCD and 2350A Controllers. If your Model 700
GC is equipped with an Micro-FID or LSIV this
section does not apply.

Use the test points in Figure 4-6 through


Figure 4-9 to ensure that the voltage meets
specifications on the Dual Methods Adapter
Board and the Field Termination Board (see
Table 4-3 for voltage specifications).
Model 700 Upper Enclosure

Test Points

Figure 4-6 Test Points Dual Methods Board (Cut View)

SEP 2005 General Troubleshooting


4-20 MAINTENANCE AND TROUBLESHOOTINGTABLE OF CONTENTS
Model 700

Model 700 Upper Enclosure

Dual Methods Bd. Test Points

Figure 4-7 Test Points Dual Methods Board

Model 700 Lower Enclosure

FTB Test Points

Figure 4-8 Test Points Field Termination Board (Cut View)

General Troubleshooting SEP 2005


MAINTENANCE AND TROUBLESHOOTINGTABLE OF CONTENTS 4-21
Model 700

Model 700 Lower Enclosure

Test Points

Figure 4-9 Test Points Field Termination Board

SEP 2005 General Troubleshooting


4-22 MAINTENANCE AND TROUBLESHOOTINGTABLE OF CONTENTS
Model 700

4.5.4 Preamplifier

The preamplifier (P/N 3-0580-002) has no parts


that may be serviced in the field. If the unit
fails, return it to DMS for repair or
replacement.

4.5.5 Flow Balance Check

Ensure that the flow panel gauge is properly


set. Refer to the Model 700 Troubleshooting
Checklist (see Table 4-3) for values. Do not
adjust; check with DMS if your reading is
abnormal.

Check the flow at the measure vent and sample


vent (see Table 4-3).

4.5.6 Temperature

Use the Temperature Control function for


monitoring the Temperature of the Oven
(Detector/s and Columns) and the Stream
Switching block to determine when the Model
700 is thermally stable. The bottom row labeled
Temperature (C) displays the current
temperatures.

The settings and values shown in Figure 4-10


and described in Table 4-4 are preset at the
factory and are based on the specific customer
application. These values should not be
changed unless recommended by Daniel
Customer Service Personnel, or it is a factory
application requirement.

General Troubleshooting SEP 2005


MAINTENANCE AND TROUBLESHOOTINGTABLE OF CONTENTS 4-23
Model 700

When connected via MON2000, use the Appli-


cation>Temperature Control menu path to
access this function.

The Temperature Control dialog displays.

Figure 4-10 Temperature Control Dialog

Use the pull down menu to select the


appropriate mode setting (e.g. AUTOMATIC,
MANUAL, or OUT OF SERVICE). Ensure that the
temperature is constant for the Oven (i.e.
Multivalve System block and column module
kit) and the SSS.

SEP 2005 General Troubleshooting


4-24 MAINTENANCE AND TROUBLESHOOTINGTABLE OF CONTENTS
Model 700

Columns 1 through 3 (Zones 1-3) have a


temperature range of 20 oC to 100 oC (68 oF to
212 oF). Column 4 (Zone 4) has a temperature
range of 20 oC to 450 oC (68 oF to 842 oF).
Table 4-4 Temperature Control Dialog

Column Function Typical Setting

Column 1 Detector/s or Block Temperature 80 oC (176.0 oF)

Column 2 Column Temperature 80 oC (176.0 oF)

Column 3 Sample Stream Block or ValcoTM 40 oC (104 oF)


Valve 60 oC (140 oF)

Column 4 Spare N/A


Or, Methanator 300 oC (572 oF)
Or, LSIV
150 oC (302 oF)

The Model 700 with a Micro-FID or LSIV has the


Multifunction board (P/N 2-3-0700-004 Revision B with an
extended temperature range for Column 4 (Zone 4) from
20 oC to 450 oC (68 oF to 842 oF). The board is labeled:

2-3-0700-004

A B B

General Troubleshooting SEP 2005


MAINTENANCE AND TROUBLESHOOTINGTABLE OF CONTENTS 4-25
Model 700

4.5.7 FID Configuration

When connected to the GC via MON2000, use


the Application>FID Configuration menu to
access the FID Configuration dialog. Refer to
the MON2000 Software for Gas
Chromatographs User Manual (P/N 3-9000-
522) for additional configuration details.

Configure the following fields from the FID


Configuration dialog:

• FID Ignition - Manual or Automatic


• Number of Ignition attempts
• Wait time between attempts
• Igniter ON duration
• Flame ON sense temperature Degrees C
• Flame OUT sense temperature Degrees C
• Electrometer (TCD) gain

SEP 2005 General Troubleshooting


4-26 MAINTENANCE AND TROUBLESHOOTINGTABLE OF CONTENTS
Model 700

Baseline Drift

To ensure that the baseline is not drifting,


compare the baseline upsets caused by valve
actuations with those of the spectrum
chromatogram provided with the Operational
Parameters Sheet.

Ensure that no evidence of component elutions


is present when sample is not being injected.

If differences exist between the two spectrum


chromatograms, the problem may be due to one
or more of the following:

• programming of events
• contamination of the multivalve sealing
diaphragms by foreign matter
• improperly adjusted flows
• leaks in the carrier system
• column deterioration due to liquid
contamination from a sample
• mis-identifying peaks

A noisy baseline can be caused by carrier leaks,


an electronic failure in the preamplifier, a
faulty power supply, or defective thermistors in
the detector. If the baseline is still noisy after
correcting for leaks, perform the Detector
Bridge Balance procedure (see Section 4.8)
before replacing the detector thermistors or the
preamplifier board.

General Troubleshooting SEP 2005


MAINTENANCE AND TROUBLESHOOTINGTABLE OF CONTENTS 4-27
Model 700

4.6 Leak Checks

4.6.1 Field Service

To perform a field-service leak check of the


Model 700,

1. Plug all Model 700 vents.


2. Make sure the setting of the carrier cylinder
regulator is 115 psig (pounds per square
inch, gauge).
3. Check all fittings at the pressure regulator
flow panel and at the carrier cylinder
regulator with a leak detector. Correct any
leaks detected by a bubble indication.
4. Turn the Carrier Gas shut-off valve
clockwise to close. Observe the carrier
pressure for ten minutes to check for a drop
in carrier pressure.
The drop should be less than 200 psig on the
high side of the regulator/gauge. If the
When the valves are carrier pressure remains constant, no leaks
switched, some pressure are present.
change is normal because of
carrier loss. 5. Using MON2000, manually actuate the
valves ON and OFF and observe the
Momentarily open the
cylinder valve to restore pressure with the valves in different
pressure if necessary (see positions (see Step 4).
Step 5).
6. If the pressure does not hold constant, check
all valve fittings for tightness.
7. Repeat Step 5. If leaks persist, check the
valve ports with a commercial gas leak
detector.

Do not use a liquid leak


detector on the valve or
components within the MVS
insulated cover.

SEP 2005 Leak Checks


4-28 MAINTENANCE AND TROUBLESHOOTINGTABLE OF CONTENTS
Model 700

4.6.2 Factory Level Leak Check

This section describes how to perform a factory-


level leak check. Before performing the leak
check, plug the Measure Vent (labeled “MV”)
vent line if it is open. The Sample Vent (labeled
“SV”) line should be left open, or unplugged.

The following steps are performed to leak-check


the Model 700 at the factory when the unit is
quality-checked prior to release. This procedure
is more thorough and is designed to isolate
specific zones where a leak may occur.

Leak Checks SEP 2005


MAINTENANCE AND TROUBLESHOOTINGTABLE OF CONTENTS 4-29
Model 700

Leak check the Carrier Gas line first, according


to the steps that follow.

Do not use the “Carrier 1. Purge the valves with Carrier Gas:
Pressure Adjust” valve (on (a) Open the Carrier Gas bottle valve and
the Flow Panel of the Model
700 GC) to adjust Carrier
slowly increase the Carrier Gas feed line
Gas line pressure. The valve pressure to 110 psig, ±2%, with a dual-
is factory-set and should not stage regulator at the Carrier Gas bottle.
be adjusted. (b) Using MON2000, manually actuate the
valves ON and OFF about four to five
times.
2. Pressurize and check the Carrier Gas feed
line:
(a) Set all Model 700 valves to ON.
(b) Open the Carrier Gas bottle valve, and
ensure that the Carrier Gas feed line
pressure is 110 psig, ±2%.
(c) Shut the Carrier Gas bottle valve.
(d) Observe the pressure on the high-side
regulator gauge of the Carrier Gas
bottle. Because the MV vent line is
plugged, the pressure should not
decrease in 2 to 3 minutes.
(e) Set all valves to OFF position.
(f) Repeat Steps (b) through (d).
(g) Via MON2000, set all valves to AUTO
for regular operation.

Next, leak check the calibration gas feed line,


per the following steps:

Calibration gas line pressure 1. Plug the SV vent line.


of 50 psig is for leak check
and test purposes only. For 2. Pressurize the calibration gas line to
normal operation, the 50 psig.
calibration gas line pressure
is maintained at 20-30 psig.

SEP 2005 Leak Checks


4-30 MAINTENANCE AND TROUBLESHOOTINGTABLE OF CONTENTS
Model 700

(a) Shut the calibration gas bottle valve.


(b) Observe the pressure on the high-side
regulator gauge of the calibration gas
bottle. Because the SV vent line is
plugged, the pressure should not
decrease in a period of 2 to 3 minutes.

Next, leak check the sample gas lines, per the


following steps:

1. Ensure that the Sample valve (SV) vent line


is plugged.
(a) Pressurize the sample gas line to 50 psig
or a known pressure.
(b) Shut off the sample gas.
Calibration gas line pressure
(c) Observe the pressure on any gauge that of 50 psig is for leak check
indicates pressure between the closed and test purposes only. For
sample gas block valve and the plugged normal operation, the
SV vent line. Because the line is plugged, calibration gas line pressure
is maintained at 20-30 psig.
the pressure should not decrease during
a period of 2 to 3 minutes.
2. Leak test all other sample stream lines by
connecting gas to each of the sample
streams and repeating Step 1(a) through
1(b).

Finish the test and set up the Model 700 for


normal operation, as follows:

1. Using MON2000, ensure that all valves are


set to AUTO.
2. Unplug, or open, the MV and SV vent lines.
3. If the calibration gas bottle was used to leak
check the sample stream lines, reconnect
the calibration gas bottle to the calibration
gas line on the flow panel assembly.
Reconnect the sample stream lines.

Leak Checks SEP 2005


MAINTENANCE AND TROUBLESHOOTINGTABLE OF CONTENTS 4-31
Model 700

4.6.3 Plugged Lines, Columns, or Valves

To ensure that lines, columns, and valves are


not plugged, check the gas flow at valve ports.
For a reference, use the flow diagram in the
drawing package, and remember these points
about flow diagrams:

• Port-to-port flow paths are indicated by


solid or dashed lines.
• A dashed line indicates flow direction when
the valve is ON, that is, energized.
• A solid line indicates flow direction when
the valve is OFF, i.e., not energized.
• A combination of solid and dashed lines
indicates a constant flow path regardless of
the ON/OFF state of the valve.

4.7 CHROMATOGRAPH VALVES

Only minimal repair and maintenance is


required by the customer (e.g., replacing the
diaphragms). DMS recommends returning the
Oven Assembly for major repairs to maintain
the validity of the warranty.

4.7.1 Required Tools

The tools required for performing repair and


general maintenance on the valve assemblies
are:

• torque wrench, scaled in foot-pounds


• 1/2” socket
• 1/4” open-end wrench
• #1 flat screwdriver

SEP 2005 Chromatograph Valves


4-32 MAINTENANCE AND TROUBLESHOOTINGTABLE OF CONTENTS
Model 700

4.7.2 Chromatograph Valve Replacement Parts

Replacement parts required for each of the


chromatograph valves on the Oven Assembly If an existing unit has a
consists of the following parts: teflon gasket between the
lower actuation diaphragms
• Diaphragm Kit 6-port Valve and the kiosk block, install
(P/N 2-4-0700-187) gasket
P/N 2-4-0700-064 (for 6-
• Diaphragm Kit 10-port Valve port valves) and P/N 2-4-
(P/N 2-4-0700-171) 0700-160 (for 10-port
valves). Otherwise, the
teflon gasket is not required.

Model 700 TCD Upper Enclosure

6-port Valve 10-port Valve

Figure 4-11 Chromatograph Valve Assemblies

4.7.3 Valve Cleaning

For cleaning the valve, isopropyl alcohol


(P/N 9-9960-111) should be used.

Do not use an oil base


cleaner on the valve.

Chromatograph Valves SEP 2005


MAINTENANCE AND TROUBLESHOOTINGTABLE OF CONTENTS 4-33
Model 700

4.7.4 TCD Oven System Removal

Use the following procedure for removing the


The Oven System may be Oven System from the Model 700 unit:
removed and repaired at a
bench. However, it is not
necessary to remove the
oven.
DANGER TO PERSONNEL AND EQUIPMENT
Disconnect all electrical power to the unit and
ensure the area is free of explosive gases.
Failure to follow this warning may result in injury
or death to personnel or cause damage to the
equipment.

1. Disconnect all power to the unit.


2. Remove the explosion proof dome and the
thermal cover.
Model 700 Upper Enclosure

Thermal
Cover

Figure 4-12 Micro-FID Oven System Thermal Cover

SEP 2005 Chromatograph Valves


4-34 MAINTENANCE AND TROUBLESHOOTINGTABLE OF CONTENTS
Model 700

3. Loosen the screw on the mounting bracket


that secures the Oven Plate to the support
post (see Figure 4-13).
4. Lift up slightly and rotate the oven forward
one quarter turn so that the components are
accessible.

Model 700 TCD Upper Enclosure

Oven System

Wiring Plug

Connector
Blocks

Figure 4-13 TCD Upper Assembly Components

5. Unplug the solenoid wiring from the driver


board end.

Chromatograph Valves SEP 2005


MAINTENANCE AND TROUBLESHOOTINGTABLE OF CONTENTS 4-35
Model 700

6. Unplug the heat control wiring from the


driver board side.
7. Unplug the heater wiring from the driver
board end.
8. Loosen the screws on the connector blocks.
Model 700 TCD Upper Enclosure

Figure 4-14 TCD Oven System Disassembly

9. Disconnect the three Preamplifier wires and


the solenoid wire plug (see Figure 4-14).
10. Lift the oven assembly from the unit for
bench maintenance and repairs.
11. Reinstall in reverse order of Steps 1-9.

SEP 2005 Chromatograph Valves


4-36 MAINTENANCE AND TROUBLESHOOTINGTABLE OF CONTENTS
Model 700

4.7.5 Micro-FID Removal

Use the following procedure for removing the


Micro-FID from the Model 700 unit.

DANGER TO PERSONNEL AND EQUIPMENT


Disconnect all electrical power to the unit and
ensure the area is free of explosive gases.
Failure to follow this warning may result in injury or
death to personnel or cause damage to the
equipment.

1. Disconnect all power to the unit.


2. After powering down the Model 700, allow
at least 10 minutes for the components to
cool-down.
3. Remove the explosion proof dome and the
thermal cover.

MAY CAUSE INJURY TO PERSONNEL


This unit operates at high temperature. Allow a
cool-down period of at least 10 minutes after
shut-down and handle the unit carefully.
Failure to follow this precaution may result in
injury to personnel

Chromatograph Valves SEP 2005


MAINTENANCE AND TROUBLESHOOTINGTABLE OF CONTENTS 4-37
Model 700

Model 700 Micro-FID Upper Enclosure

FID

Oven System

Connector Blocks

Figure 4-15 Micro-FID Upper Assembly Components

4. Grasp the edges of the Connector Board on


top of the unit and pull and wiggle to
remove the six socket tubes that extend onto
the pins in the cap (see Figure 4-16).

SEP 2005 Chromatograph Valves


4-38 MAINTENANCE AND TROUBLESHOOTINGTABLE OF CONTENTS
Model 700

5. Remove the exhaust tube from the side by


pulling the 'U' shaped retainer from the top
of the exhaust body and moving the exhaust
tube away from the Micro-FID. Take care
not to lose the clip.

Model 700 Micro-FID Upper Enclosure

Connector Board 'U' shaped retainer

FID Shield FID Exhaust Tube

Figure 4-16 Model 700 with Micro-FID Upper Assembly

6. Loosen the two screws in the top of the


Micro-FID.
7. Grasp the shielded section and lift it over
the burner. Pull the cap out of the shield.
Remove the body from the shield, if
necessary.

Chromatograph Valves SEP 2005


MAINTENANCE AND TROUBLESHOOTINGTABLE OF CONTENTS 4-39
Model 700

4.7.6 Micro-FID Maintenance

The Micro-FID cap has no replaceable parts.


Damage like a broken RTD or broken igniter
coil requires a replacement cap.

The burner tip can be removed for cleaning.

1. Loosen the isolating nut one turn.


2. Gently lift out the burner tip tube. Use
short needle nose pliers if it is stubborn,
taking care not to bend the tube. The
alternative is to unscrew the assembly and
clean as an assembly.

4.7.7 Micro-FID Re-assembly

1. Insert burner tip tube into the isolating nut.


Be certain it is fully seated. There should
be about .350" of tube visible.
2. Tighten the isolating nut in small
increments until the tube ceases to pull free.
Slight additional tightening will ensure
proper sealing.
3. Place the cap onto the end of the body with
the deep cavity. Once the alignment pin is
in its mating hole, gently press the two
parts together and ensure the o-ring is
seated properly.
4. Slide the Micro-FID shield onto the body
from the bottom. Align the notch with the
exhaust fitting and insert the two screws.
5. Lower the Micro-FID body assembly onto
the base, placing the alignment pin in its
hole. Press the body into place, seating the
o-ring. Tighten the screws slightly more
than 'finger tight.'
6. Re-connect the ground lead.

SEP 2005 Chromatograph Valves


4-40 MAINTENANCE AND TROUBLESHOOTINGTABLE OF CONTENTS
Model 700

7. Press the Micro-FID exhaust tube onto the


fitting and anchor with the ‘U’ shaped clip.
(1/16" tubing makes an adequate clip.)
8. Plug the connector board onto the cap.
9. Replace the thermal cover on the upper
enclosure.
Model 700 FID/TCD Upper Enclosure

Thermal
Cover

10. Replace the explosion-proof cover on the


assembly, then apply power to the unit.

Chromatograph Valves SEP 2005


MAINTENANCE AND TROUBLESHOOTINGTABLE OF CONTENTS 4-41
Model 700

4.7.8 LSIV Maintenance

The LSIV can be maintained while attached to


the enclosure. However, the user may find it
easier to perform maintenance with the LSIV
removed from the Model 700 upper enclosure.

MAY CAUSE INJURY TO PERSONNEL


This unit operates at high temperature. Allow a
cool-down period of at least 10 minutes after
shut-down and handle the unit carefully.
Failure to follow this precaution may result in
injury or death to personnel

4.7.9 LSIV Removal

Inside the Model 700 upper enclosure there are


two insulation covers (which open like clam
shells that slide off of the end of the LSIV) to be
removed.

1. Disconnect the carrier and sample tubing


from the LSIV.
2. Remove the heater and RTD from the
heater block.
3. Disconnect sample and air tubing from the
outer portions of the LSIV.
4. Unscrew the retaining ring, using a pin
spanner wrench or other tool. With the
retaining ring loose, the LSIV assembly is
free to be pulled out of the upper enclosure.

SEP 2005 Chromatograph Valves


4-42 MAINTENANCE AND TROUBLESHOOTINGTABLE OF CONTENTS
Model 700

Replacing LSIV Seals

DAMAGE TO EQUIPMENT
Use of wrenches other than a strap wrench to
disassemble the LSIV can damage the valve
beyond repair.
Failure to follow this precaution may damage
equipment.

Tools Required for Disassembly:

• 2 each - 1 inch strap wrenches


• 1 each - assembly tool for seal nuts

1. Using two strap wrenches, if needed,


unscrew the seal assist housing from the
LSIV body. Once the threads are free, pull
the pieces apart taking care to avoid
bending the stem.
2. There are two seals with a central packing
gland between them to be removed, either
from the stem or the bore in the body. Use
care to avoid scratching the stem or bore
surfaces.
3. Replace the two seals with the central
packing gland between them onto the stem.
Carefully align the two assemblies and
insert the seals into the bore.
4. Screw the assemblies together hand-tight.

Chromatograph Valves SEP 2005


MAINTENANCE AND TROUBLESHOOTINGTABLE OF CONTENTS 4-43
Model 700

LSIV Disassembly

Use the following procedure to disassemble the


LSIV and refer to Figure 4-17.

Figure 4-17 Model 700 with LSIV

1. Use the one (1) inch strap wrenches and


unscrew the piston housing (counter-
clockwise) from the seal assist housing (use
one strap wrench on the piston housing and
one strap wrench on the seal assist
housing).

DAMAGE TO EQUIPMENT
Use care when disassembling the LSIV to prevent
bending the valve stem.
Failure to follow this precaution may cause
damage to the equipment.

SEP 2005 Chromatograph Valves


4-44 MAINTENANCE AND TROUBLESHOOTINGTABLE OF CONTENTS
Model 700

2. When the threads disengage, slowly


continue to pull apart the LSIV assembly.
Be careful not to bend the valve stem and
pull until the valve stem is free of the seal
assist housing or the piston is free of the
piston housing.
3. Separate the piston and valve stem
assembly from the piston housing or seal
assist housing by carefully pulling it
straight out.
4. Unscrew (counter-clockwise) the seal assist
housing from the lower body.
5. Unscrew (counter-clockwise) the retaining
ring from the body.
6. Pull the piston/packing gland out of the
lower body.
7. Push out the football seals and the central
packing gland from the body.
8. Unscrew (counter-clockwise) the stem lock
nut from the piston.
9. Remove the valve stem from the piston.
10. Unscrew the seal nut from the upper piston
packing gland.
11. Remove the o-rings and the collar.

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MAINTENANCE AND TROUBLESHOOTINGTABLE OF CONTENTS 4-45
Model 700

4.7.10 Methanator Maintenance

The optional Methanator, a catalytic converter,


converts otherwise undetectable CO2 and/or
CO into methane by adding hydrogen and heat
to the sample. The Methanator requires little
maintenance.
Model 700 Methanator Upper Enclosure

Figure 4-18 Model 700 Optional Methanator Assembly


The assembly consists of:
• A: Case
• B: Insulation
• C: Tube
• D: Catalytic Column
• E: Heater
• F: RTD (temperature detector)
• G: Two #6-20 x 1/2 stainless steel screws

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The RTD can be replaced , if necessary. If it is


replaced, care must be taken to anchor the RTD
cable to the tubing to prevent loosening over
time.

A catalytic column needing replacement should


be replaced with a full heater/column assembly
that includes the tube, column, heater and
RTD.

To replace the catalytic column


(see Figure 4-18),

1. Disconnect the tubing and wiring, then lift


the Methanator from the enclosure.
2. Remove the two screws and open the box
(enclosure). The catalytic column assembly
is housed inside this insulation-filled box.
3. Exchange the catalytic assembly and re-fill
the enclosure with insulation.
4. Reverse this procedure to reassemble the
Methanator.

4.7.11 Valve Overhaul

The chromatograph valves are designed to


withstand millions of actuation cycles without
leakage or failure. If service is required, the
valve can be overhauled using replacement Replacement factory-built
parts available from Daniel Measurement valves are available.
Services (DMS). DMS recommends returning
and replacing the 6-port
Valve for extensive repairs
or complete replacement.

Chromatograph Valves SEP 2005


MAINTENANCE AND TROUBLESHOOTINGTABLE OF CONTENTS 4-47
Model 700

Use the following procedure for overhauling a


6-Port Valve:

1. Shut off carrier and sample gas streams


entering the unit.
2. Remove the insulating cover from the Oven
The Oven System may be
removed and repaired at a
System.
bench. However, it is not 3. If the faulty valve is not easily accessible,
necessary to remove the
loosen the thumb screw and rotate the oven
oven.
forward (see Figure 4-13 and Figure 4-14).
4. Disconnect tubing and fittings that attach
to the valve from other locations.

Model 700 TCD Upper Enclosure

Valve
Attaching
Bolt

Fitting
Tubing

Figure 4-19 TCD Valve Tubing and Fittings

5. Loosen the attaching bolt on the valve to be


replaced or serviced (see Figure 4-19).

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6. Holding the lower piston plate, pull the


valve straight off the block. The alignment
pins may stick slightly.
7. Remove and discard the old valve Ensure that the primary seal
diaphragm is correctly
diaphragms and gaskets. Replace, in the
installed on the primary
same order, with the new ones supplied. plate.
8. Reinstall the valve using the following
steps:
(a) Clean the sealing surface as required
using Chemwipes with alcohol.
Blow the sealing surface with clean, dry
instrument air or Carrier Gas. Dirt Do not scratch the primary
including dust and lint can cause plate surface.
troublesome leakage.
(b) Align the pins with holes in the block
and push the valve assembly into place.
(c) Tighten the valve “attaching bolt” to 30
lbs./ft. (40 N-m) Do not use an oil base
cleaner on the valve.
(d) Reconnect all fittings and tubing
(see Figure 4-19).

4.7.12 Oven System and Stream Switching System


Solenoid Valve Replacement

Both the Oven System and the Stream


Switching System use the same solenoid
valves. The solenoids are replaced in both
systems using the same procedure
(see Section 4.7.13).

DANGER TO PERSONNEL AND EQUIPMENT


Disconnect all electrical power to the unit and
ensure the area is free of explosive gases.
Failure to follow this warning may result in
injury or death to personnel or cause damage
to the equipment.

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MAINTENANCE AND TROUBLESHOOTINGTABLE OF CONTENTS 4-49
Model 700

4.7.13 Solenoid Valve Replacement

Replace the Oven System and Stream


Switching System (SSS) solenoids using the
following steps.

1. Remove the dome from the upper enclosure.


2. Loosen the mounting bracket thumb screw
Carrier Gas leaks may be that secures the oven to the chassis, see
caused by the SSS Figure 4-20.
solenoids See Section 4.6
Model 700 TCD Upper Enclosure
for leak check procedures.

Thumb Screw

Figure 4-20 Side View TCD Oven System Mounting Bracket

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3. Holding the left side of the oven mounting


plate, gently lift up the assembly and rotate
it so that the enclosure opening is
accessible.
Model 700 TCD Upper Enclosure

Figure 4-21 Rotated TCD Upper Assembly

Chromatograph Valves SEP 2005


MAINTENANCE AND TROUBLESHOOTINGTABLE OF CONTENTS 4-51
Model 700

4. Loosen the thumb screws holding the valve


in place.
Model 700 TCD Upper Enclosure

Figure 4-22 Stream Switching Assembly

5. Lift the solenoid off of the alignment pins


(approximately 1/8”).
6. Slide out the solenoid block.
7. Disconnect the wire leads and remove the
gasket from the bottom of the solenoid
block.
The solenoids are not
8. Replace the old leads at the connector plug
polarity sensitive.
or splice the wires from the new solenoid to
the old leads.

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Model 700

9. Reassemble the SSS and Oven System in


reverse order of Steps 1 through 7.
Model 700 TCD Upper Enclosure

Figure 4-23 Stream Switching System Final Assembly

4.8 TCD DETECTOR BRIDGE BALANCE

The following procedure should be performed if


the Model 700 does not produce a
chromatogram.

If necessary to balance the detector bridge,

TCD Detector Bridge Balance SEP 2005


MAINTENANCE AND TROUBLESHOOTINGTABLE OF CONTENTS 4-53
Model 700

1. Remove the cover of the upper explosion-


proof housing and the thermal cover on the
Model 700 for access the preamplifier.
Model 700 FID/TCD Upper Enclosure

Figure 4-24 Model 700 Micro-FID/TCD Preamplifier

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2. Attach the negative lead of a digital


voltmeter to the black test point (-BRIDGE
BALANCE). Attach the positive lead of the
digital voltmeter to the red test point
(+BRIDGE BALANCE).
Model 700 TCD Upper Enclosure

Detector 1 Detector 2

Figure 4-25 Model 700 TCD Bridge Balance

Model 700 Micro-FID Upper Enclosure

Detector 1

Figure 4-26 Model 700 Micro-FID Bridge Balance

3. Check the detector bridge voltage. The


voltage should read 0 millivolts (mV), ±0.5
mV. Adjust the coarse and fine
potentiometers which are located
immediately to the left of each of the (red)
test points to obtain the specified reading.

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MAINTENANCE AND TROUBLESHOOTINGTABLE OF CONTENTS 4-55
Model 700

4.9 MEASURE VENT FLOW

You will need an accurate flow meter for this


measurement.

To measure the MV vent flow, proceed as


follows:

1. Attach a flow meter to the vent output on


the right side of the Model 700
“MV1”(marked on the tag).
The flow should measure 12-18 cc/min.
2. Attach a flow meter to the vent “MV2”
marked on the tag.
The flow should measure 12-18 cc/min.

Model 700 Upper Enclosure

MV1

(Marked on tags)

MV2

Figure 4-27 Measure Flow Vents

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Model 700

4.10 MODEL 700 ELECTRICAL COMPONENTS

The Model 700 GC is designed to operate for


long periods of time without need for
preventive or regularly scheduled
maintenance. The Model 700 is designed using
explosion-proof enclosures. The enclosure is
dust-proof, water-proof, and flame-proof.

DANGER TO PERSONNEL AND EQUIPMENT


Disconnect all electrical power to the unit and
ensure the area is free of explosive gases.
Failure to follow this warning may result in death
or injury to personnel or cause damage to the
equipment.

Should there be a need to open the explosion-


proof enclosure, first disconnect all electrical
power to the unit, and ensure the area is free of
explosive gases. Prior to opening the
Model 700, check the operating parameters of
the application with a PC using MON2000
software and attempt to isolate or fix any
incorrect parameters.

To access the GC electrical components,

1. Ensure electrical power is disconnected


from the unit and the environment is safe.

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MAINTENANCE AND TROUBLESHOOTINGTABLE OF CONTENTS 4-57
Model 700

2. Remove the lower enclosure cover and


access the card cage assembly holding the
circuit boards.
Model 700 Lower Enclosure

Explosion-proof Cover

Figure 4-28 Model 700 Lower Enclosure

Figure 4-29 Model 700 Card Stack Assembly

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4-58 MAINTENANCE AND TROUBLESHOOTINGTABLE OF CONTENTS
Model 700

3. Note the location and direction of any board


removed. Remove only one end of any cable
necessary to obtain access to the desired
board. Remember or make note of the cable After removing the cable(s),
installation so that the cables can be any board may be replaced
replaced in the same order. Release the without removing the card
catch(es) and remove/replace the circuit cage assembly.
board(s) as necessary.
Model 700 Lower Enclosure

Card Cage Assembly

Figure 4-30 Model 700 Lower Assembly

Model 700 Electrical Components SEP 2005


MAINTENANCE AND TROUBLESHOOTINGTABLE OF CONTENTS 4-59
Model 700

4.10.1 DC Power Supply Replacement Procedures

The DC/DC Power Supply is mounted on the


left wall of the lower enclosure (see Figure 4-
31) and is accessible by removing the threaded
cover plate from the housing.

DANGER TO PERSONNEL AND EQUIPMENT


Disconnect all electrical power to the unit and
ensure the area is free of explosive gases.
Failure to follow this warning may result in death or
injury to personnel or cause damage to the
equipment.

Model 700 Lower Enclosure

DC Power
Supply

Figure 4-31 DC Power Supply Lower Enclosure

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Model 700

Tools required to remove and replace the DC


Power Supply:

- Cross point #2 Phillips screw driver (long


Needle nose pliers may be
shank is helpful). used to turn rear
- Head lamp (flashlight) thumbscrews.

To remove and replace a faulty DC Power


supply:

1. Disconnect the cables from the CPU, the


Com4A board (if installed), the modem
board and the Ethernet board (if installed).
2. Unscrew the card cage thumb screws and
remove the card cage assembly.
3. Unscrew the two thumb screws on the
power supply bracket.
4. Remove the assembly from the unit.
5. Disconnect, label and bundle all leads.
6. Attach all leads to the new DC Power
Supply.
7. Align the power supply bracket and tighten
the two thumb screws.
8. Reinstall the card cage assembly, tighten
the thumb screws and reconnect all cables.
9. Replace the threaded cover plate on the
lower enclosure housing.

Model 700 Electrical Components SEP 2005


MAINTENANCE AND TROUBLESHOOTINGTABLE OF CONTENTS 4-61
Model 700

4.11 COMMUNICATIONS

Model 700 GC with the TCD


See Appendix A for a list of
the ports and terminals The Model 700 GC with the TCD has seven
(pins) assigned to serial communications channels available; without
communications. the LOI installed, three communications ports
from the WinSystems CPU board
(P/N CE-20765) and four communications ports
from the Com4A board. Six communication
channels are available; with the LOI installed,
two from the WinSystems CPU board and four
ports from the Com4A board.

Model 700 GC with the Micro-FID/TCD

The Model 700 GC with the TCD has two


communications channels available; without
the Com4A board installed. Model 700, with
the Com 4A board installed, has six
communications ports available on the FTB;
Com1 and Com2, and Com5, Com6, Com7, and
Com8.

Com 4 is dedicated to the Micro-FID/TCD


Preamplifier. When the LOI becomes available,
it will use a video board instead of a serial port
connection (see Figure 3-16 and Figure 3-17).

The communication protocols are selected


inside the Model 700 GC with jumpers. The
protocols are normally specified by the
customer and then set at the factory.

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4-62 MAINTENANCE AND TROUBLESHOOTINGTABLE OF CONTENTS
Model 700

If it becomes necessary to change the


communications settings at the site, access to
the boards inside the enclosure is required to
make changes. See Section 3.4.2 if a
communications change becomes necessary.

DANGER TO PERSONNEL AND EQUIPMENT


The enclosure should not be opened when
hazardous gases are present.
Failure to do so may result in death or injury to
personnel or cause damage to the equipment.

The jumpers to be changed are located on the


WinSystems CPU board and the WinSystems
Com4A board.

When the desired Model 700 GC address (Com


ID) is known, it will be set before the unit
leaves the factory. If the address (Com ID)
needs to be changed in the field, it will be
necessary to change the arrangement of an 8-
position DIP switch on the multifunction board.
Model 700 Upper Enclosure

Figure 4-32 Dip Switch

Communications SEP 2005


MAINTENANCE AND TROUBLESHOOTINGTABLE OF CONTENTS 4-63
Model 700

This board is mounted on a bracket towards the


center of the upper enclosure.
Model 700 TCD Upper Enclosure

Multifunction Board

Figure 4-33 Multifunction Board

Ensure the cables are replaced in the exact


order and positions.

(a) For example Model 700 GCs with a TCD,


- Switches "1" through "5" form a 5-bit
binary number for setting the
See Section 3.4.1 this Modbus slave address (also known as
manual, for an explanation
Com ID or Device ID.)
of DIP switch settings and
their determination of the - Switch number “1” is the least
GC Controller Modbus slave significant bit, and switch number “5”
address (Com ID). is the most significant bit. Set these
switches either ON or OFF.

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4-64 MAINTENANCE AND TROUBLESHOOTINGTABLE OF CONTENTS
Model 700

-Switch "6" is a spare for future use.


Switches "7" and "8" are set as
needed for the presence of an optional
LOI (Local Operator Interface)
connected via COM8 (when the
COM4A board is installed).
If the COM4A board is not installed,
the LOI is connected via COM4. This
address should display via the
MON2000 software.
(b) For example Model 700 GCs with a
Micro-FID ,
- Switch number “1” is the least
significant bit, and switch number “5”
is the most significant bit. Set these
switches either ON or OFF.
- Switch “6” and “7” are spares and
switch “8” is used to cold start the
processor (see Table 3-4).

Communications SEP 2005


MAINTENANCE AND TROUBLESHOOTINGTABLE OF CONTENTS 4-65
Model 700

4.12 ANALOG INPUTS/OUTPUTS

The analog outputs can be calibrated and or


adjusted via the MON2000 software. However,
these outputs should be measured with a good
digital meter upon initial installation at zero
scale and full scale. Then the span can be set
with MON2000 software so that it represents
values from zero to 100 percent of the user-
defined units in use.

Nominally, calibration is made within a range


of 4-20 milliamperes (mA) output from each
analog channel. However, zero scale
calibrations can be set with 0 mA output, and
full scale calibration can be set with up to 22.5
mA output. If there is reason to suspect that
the span on any particular channel might be off
after a period of time and heavy use, then the
analog output for that channel should be
recalibrated.

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4.12.1 Model 700 Analog Inputs

There are four analog inputs available on the


Field Termination Board (J4 - 12-pin Phoenix
connector).
Model 700 Upper Enclosure Analog
Inputs

J4

J8

Figure 4-34 Analog Board - Inputs

Analog Inputs/Outputs SEP 2005


MAINTENANCE AND TROUBLESHOOTINGTABLE OF CONTENTS 4-67
Model 700

The Model 700 analog inputs are configured as


follows:
J4
VIN +_1
1
AGND 2
Shield
3
VIN + _2
4
AGND 5
Shield
6
VIN + _3
7
AGND 8
Shield 9
VIN + _4
10
AGND 11
Shield
12

Figure 4-35 Analog Inputs

4.12.2 Analog Output Adjustment

The initial analog output adjustment will be set


at the factory, before shipment, at standard
values (4-20 mA). It may be necessary to check
and/or adjust these values depending on output
cabling/impedance. The adjustment may
require two persons if the units are some
distance apart. It will require a good digital
meter to check the zero and full scale values at
the receiving end. The scale or span value can
be adjusted by a PC with the Model 700 when
the values are known at the receiving end.

It is possible to calibrate the analog outputs


using different engineering units, volts and
percentages. For examples and detailed
instructions, refer to the MON2000 Software
for Gas Chromatographs Users Manual
(P/N 3-9000-522).

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4.12.3 Model 700 Analog Outputs

Standard Analog Outputs

The Model 700 has four standard analog


outputs (J8 - 12-pin Phoenix connector) on the
Field Termination board (P/N 3-0700-010).

Model 700 Upper Enclosure


Analog
Inputs

J4

J8

Analog
Outputs

Figure 4-36 FTB Board Analog Outputs

Analog Inputs/Outputs SEP 2005


MAINTENANCE AND TROUBLESHOOTINGTABLE OF CONTENTS 4-69
Model 700

The Model 700 analog outputs are configured


as follows:
J8
IOut +_1
1
IOut - _1
2
Shield
3
IOut +_2
4
IOut -_2
5
Shield
6
IOut +_3
7
IOut -_3
8
Shield 9
IOut +_4 10
IOut -_4
11
Shield
12

Figure 4-37 Analog Outputs


The analog outputs for the optional analog
board (P/N 2-3-0580-037) are configured as
follows
J3
IOut +_5
1
IOut - _5
13
Shield
2
IOut +_6
14
IOut - _6
3
Shield
15
IOut +_7
4
IOut - _7
16
Shield
5
IOut +_8 17
IOut - _8
6
Shield
18
IOut +_9 7
IOut - _9 19
Shield 8
IOut +_10
20
IOut - _10 9
Shield
21
IOut +_11
10
IOut - _11
22
Shield
11
IOut +_12 23
IOut - _12 12
Shield 24

Figure 4-38 Optional Analog Board Outputs

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4.13 DISCRETE DIGITAL INPUTS/OUTPUTS

For instructions on connecting digital inputs


and outputs to the GC Field Termination
Boards, see Section 3.4.7 for more details.

An external loopback test circuit can be built


for troubleshooting the Model 700 digital input/
output operation.

4.14 RECOMMENDED SPARE PARTS

See Appendix D for the lists of recommended


spare parts for approximately one year of
maintenance. The quantities represent the
number of spares to cover most contingencies
at facilities where GC systems are in operation.

Daniel Measurement Services offers service


and repair service contracts that make
maintaining most spares for the GC system
unnecessary. Details regarding service
contracts may be obtained by contacting DMS
at the address or telephone number on the
Customer Repair Report in the back of this
manual.

Discrete Digital Inputs/Outputs SEP 2005


MAINTENANCE AND TROUBLESHOOTINGTABLE OF CONTENTS 4-71
Model 700

4.15 UPGRADE PROCEDURES

4.15.1 Base Operating System


Refer to the MON2000
Software for Gas The Base Operating System performs functions
Chromatographs User similar to operating systems such as DOS or
Manual, Appendix F Windows® or Linux®.
(P/N 3-9000-522) for BOS
upgrade procedures.
BOS provides the basic resources and
interfaces to run the user's tasks. Unlike DOS
or Windows or Linux, since BOS is an
embedded real-time multi-tasking preemptive
operating system, there is no direct user level
interface to it. If a BOS upgrade is required to
your system, refer to the MON2000 Software
for Gas Chromatographs User Manual (P/N 3-
9000-522) for additional BOS information.

4.15.2 Applications

The GC application, which runs under BOS,


utilizes the tools provided by BOS to perform
the desired gas chromatograph functions for
the user. There are different applications to
provide for different gas chromatographic
needs. To load a new application or to upgrade
an existing application refer to the MON2000
Software for Gas Chromatographs User
Manual (P/N 3-9000-522) for details.

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Model 700

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Upgrade Procedures SEP 2005


COMMUNICATIONS SPECIFICATIONS A-1
Model 700

APPENDIX A, COMMUNICATIONS SPECIFICATIONS


A

Com4 is reserved for an A.1 TCD SERIAL COMMUNICATIONS


optional LOI. With the
Com4A board installed, The Model 700 with a TCD has three standard
Com8 is used for the LOI.
CPU serial communications ports: Com1,
Com3 is reserved for the Com2, Com4, and four optional Com4A board
multifunction board. serial ports: Com5 Com6, Com7, Com8 and
Com9 for the optional internal modem. Per the
matrix below, jumper settings can be
configured for either RS-232, RS-422, or
RS-485 serial signal definitions.
Table A-1 Matrix of Possible TCD Configurations Field Termination Board

Logical Address Operation Comments

Com1 and Com2 (WinSys RS-232, RS-422 or RS-485 PC, Flow Computer, Modem
CPU Board) J1 to FTB (external)

Com3 (WinSys CPU Board) RS-232 Reserved for Multifunction


J6 to Multifunction Board Board

Com4 (WinSys CPU Board) RS-232, RS-422 or RS-485 Unless LOI is installed, then
J6 to FTB (RS-422 and RS-484 needs Com 4 is reserved for the LOI
Chip Kit #CK 75176-2)

Com5 (WinSys Com4A Board) RS-232, RS-422 or RS-485 Modem (External)


J9 (9-pin Phoenix) (RS-422 and RS-484 needs
Chip Kit #CK 75176-2)

Com6 (WinSys Com4A Board) RS-232, RS-422 or RS-485


J13 (9-pin Phoenix) (RS-422 and RS-484 needs
Chip Kit #CK 75176-2)

Com7 (WinSys Com4A Board) RS-232, RS-422 or RS-485


J17 (9-pin Phoenix) (RS-422 and RS-484 needs
Chip Kit #CK 75176-2)

Com8 (WinSys Com4A Board) RS-232, RS-422 or RS-485 Reserved for LOI, when
J18 (9-pin Phoenix) (RS-422 and RS-484 needs installed
Chip Kit #CK 75176-2)

Com9 Reserved for internal modem

SEP 2005 TCD Serial Communications


A-2 COMMUNICATIONS SPECIFICATIONS
Model 700

A.1.1 Model 700 with a TCD Comm Ports

The WinSystems CPU Board has three


A telephone modem can be communications ports that can be used for the
connected to any of the GC PC or the Flow Computer, as the customer
serial ports configured for desires.
RS-232. When a keyboard and a display is required,
If an internal modem Com4 is used for the optional Local Operator
(WinSystems Interface (LOI).
P/N 3-0580-042) or (P/N 3- The four channel WinSystems Com4A board
0700-029 Radicom) is (optional) is installed for applications requiring
installed, it is assigned to
serial port Com9.
more than three communications ports. Each
channel is individually configured for RS-232,
If the Com4A board is RS-422, or RS-485 (for ports Com5, Com6,
installed, the modem is
assigned to Com9.
Com7, and Com8).
Configuration of each channel requires
With or without the Com4A installing and/or removing the appropriate line
board, the internal modem is
assigned to Com9.
driver ICs and installing jumpers. A Chip Kit
(P/N CK-75176-2) is used when configuring a
single channel for RS-422 mode or when
configuring a two channel (maximum) mode for
RS-485.
If a modem and a serial controller are both
required, an external modem will be assigned
to either Com1 or to Com5.
Serial ports configured for RS-232 are most
commonly used for direct serial communication
between the GC and a PC or modem.
Serial ports configured for RS-422 or RS-485
In any Modbus host-slave are most commonly used for long distance
DCS or network, there must serial communications systems, such as a DCS
only be one host to which or a network. For these systems, the GC can
any one of the GC serial communicate as a Modbus slave device.
ports can respond as a
Modbus slave.
To use the MON 2000
software to configure the
GC for Modbus
communication, see the
MON 2000 Software for
Gas Chromatographs User
Manual (P/N 3-9000-522).

TCD Serial Communications SEP 2005


COMMUNICATIONS SPECIFICATIONS A-3
Model 700

For further details, see Figure A-1 through


Figure A-4.

Multifunction
Model 700, Standard Board
configuration, has three
ports available on the FTB; Com3
Com 1, Com 2, and Com 5. CPU
Field Termination
Com1
Board
Com2
Com1
Com3 Com2
Com4
Com5
Com6
Com7
Com8

Figure A-1 Standard Configuration


without LOI and Com4A Board

Multifunction
Board

Model 700, with the LOI Com3


installed, has two CPU
communications ports Field Termination
Com1
available on the FTB; Com1 Board
Com2
and Com2. Com1
Com3 Com2
Com4
Com5
Com6
Com7
Com8
LOI

Com4

Figure A-2 Configuration with LOI

SEP 2005 TCD Serial Communications


A-4 COMMUNICATIONS SPECIFICATIONS
Model 700

Multifunction
Board
Model 700, with the
Com3
Com4A board installed, has
CPU
six communications ports
Com1 available on the FTB; Com1
Field Termination and Com2, and Com5,
Com2 Board Com6, Com7, and Com8.
Com3
Com1
Com4 Not
Connected Com2

Com5
Com 4A Com6
Com7
Com5
Com8
Com6
Com7
Com8

Figure A-3 Configuration with Com4A Board

TCD Serial Communications SEP 2005


COMMUNICATIONS SPECIFICATIONS A-5
Model 700

Multifunction
Board
Model 700, with the LOI
Com3
and Com4A board installed,
CPU
have six communications
ports available on the FTB; Com1
Com1 and Com2, and Com2
Com5, Com6, Com7, and Field Termination
Com3 Board
Com8.
Com4 Com1
LOI
Com2

Com5
Com4
Com6
Com7
Com8
Com4A

Com5
Com6
Com7
Com8

Figure A-4 Configuration with Com4A Board and LOI

SEP 2005 TCD Serial Communications


A-6 COMMUNICATIONS SPECIFICATIONS
Model 700

If using a direct 6-conductor serial cable,


connect the exposed cable leads to the FTB
serial port. A pinout of a female DB 9-pin
socket is shown in Figure A-5.

Com1
P2

5
RI 1 9
DSR 1 4
RTS 1 8
RXD 1 3
CTS 1 7
TXD 1 2
DTR 1 6
DCD 1 1

GND Com2
P3

5
RI 2 9
DSR 2 4
RTS 2 8
RXD 2 3
CTS 2 7
TXD 2 2
DTR 2 6
DCD 2 1

Figure A-5 FTB Com1 and Com2 DB9 Connector

TCD Serial Communications SEP 2005


COMMUNICATIONS SPECIFICATIONS A-7
Model 700

A.2 FID SERIAL COMMUNICATIONS

The Model 700 with a FID/TCD has two


Com3 is reserved for standard WinSystems CPU Board serial
Multifunction board. communications ports: Com1 and Com2 that
Com4 is reserved for the can be used for the PC or the Flow Computer,
FID/TCD board. as the customer desires.

The four channel WinSystems Com4A board


(optional) is installed for applications requiring
more than two communications ports. Each
channel is individually configured for RS_232,
RS-422 or RS-485 (for ports Com5 Com6,
Com7, Com8).
Table A-2 Matrix of Possible FID Configurations Field Termination Board

Logical Address Operation Comments

Com1 and Com2 (WinSys RS-232, RS-422 or RS-485 PC, Flow Computer, Modem
CPU Board) J1 to FTB (external)

Com3 (WinSys CPU Board) RS-232 Reserved for Multifunction PCB


J6 to Multifunction Board

Com4 (WinSys CPU Board) RS-232 Reserved for FID/TCD


J6 to FID/TCD Preamplifier Preamplifier PCB

Com5 (WinSys Com4A Board) RS-232, RS-422 or RS-485 Modem (External)


J9 on FTB (9-pin Phoenix) (RS-422 and RS-484 needs
Chip Kit #CK 75176-2)

Com5 (WinSys Com4A Board) RS-232, RS-422 or RS-485


J9 on FTB (9-pin Phoenix) (RS-422 and RS-484 needs
Chip Kit #CK 75176-2)

Com6 (WinSys CPU Board) RS-232, RS-422 or RS-485


J13 on FTB (9-pin Phoenix) (RS-422 and RS-484 needs
Chip Kit #CK 75176-2)

Com7 (WinSys Com4A Board) RS-232, RS-422 or RS-485


J17 on FTB (9-pin Phoenix) (RS-422 and RS-484 needs
Chip Kit #CK 75176-2)

Com8 (WinSys Com4A Board) RS-232, RS-422 or RS-485 Reserved for LOI, when
J18 on FTB (9-pin Phoenix) (RS-422 and RS-484 needs installed
Chip Kit #CK 75176-2)

Com9 Reserved for internal modem

SEP 2005 FID Serial Communications


A-8 COMMUNICATIONS SPECIFICATIONS
Model 700

Configuration of each channel requires


installing and/or removing the appropriate line
driver ICs and installing jumpers. A Chip Kit
In any Modbus host-slave (P/N CK-75176-2) is used when configuring a
DCS or network, there must single channel for RS-422 mode or when
only be one host to which configuring a two channel (maximum) mode for
any one of the GC serial RS-485.
ports can respond as a If a modem and a serial controller are both
Modbus slave.
required, an external modem will be assigned
To use the MON 2000 to either Com1 or to Com5.
software to configure the Serial ports configured for RS-232 are most
GC for Modbus
communication, see the
commonly used for direct serial communication
MON 2000 Software for between the GC and a PC or modem.
Gas Chromatographs User Serial ports configured for RS-422 or RS-485
Manual (P/N 3-9000-522). are most commonly used for long distance
serial communications systems, such as a DCS
or a network. For these systems, the GC can
communicate as a Modbus slave device.
For further details, see Figure A-6 and Figure
A-7.
Multifunction FID/TCD
Board Preamplifier Board
Com3 Com4

Model 700, standard


configuration, has two
CPU Field Termination
communications ports Board
available on the FTB;
Com1 and Com2. Com1 Com1
Com2 Com2
Com3
Com4
Com5
Com6
Com7
Com8

Figure A-6 Configuration without Com4A Board

Com 4 is dedicated to the


Micro-FID/TCD Preamplifier.
When the LOI becomes
available, it will use a video
board instead of a serial port
connection.

FID Serial Communications SEP 2005


COMMUNICATIONS SPECIFICATIONS A-9
Model 700

Multifunction FID/TCD
Board Preamplifier Board
Com3 Com4
Model 700, with the Com
4A board installed, has six
communications ports CPU Field Termination
available on the FTB; Com1 Board
and Com2, and Com5,
Com1 Com1
Com6, Com7, and Com8. Com2 Com2
Com3
Com4

Com4A

Com5 Com5
Com 4 is dedicated to the Com6 Com6
Micro-FID/TCD Preamplifier. Com7 Com7
When the LOI becomes Com8 Com8
available, it will use a video
board instead of a serial port
Figure A-7 Configuration with Com4A Board
connection.

SEP 2005 FID Serial Communications


A-10 COMMUNICATIONS SPECIFICATIONS
Model 700

A.2.1 Connecting Serial Communications to the GC

To connect serial communications lines to the


Serial communications for GC,
FTB (Com1- Com4) is
standard. Com3 reserved 1. Access the FTB in the lower enclosure.
for the Multifunction board.
2. Route serial communications lines
Serial communications with
optional Com4A board are appropriately.
available on ports Com5 - 3. Make serial communications line
Com8.
connections to the FTB. See Section A.1.1
for port numbers and pinouts.
Each of the various combinations available
for GC serial communications ports (i.e.,
RS-232, RS-422, or RS-485) require:
• specific jumper settings on the
WinSystems CPU board or the optional
Com4A board
In most instances, installation of these
jumper settings requires no modification.
Configurations have been performed at the
If you are changing or factory prior to shipment of the Model 700,
adding serial
communications to the GC,
according to customer specifications for
ensure that the correct serial communications.
jumpers are set.

FID Serial Communications SEP 2005


COMMUNICATIONS SPECIFICATIONS A-11
Model 700

RS-232 Ports
See Appendix A.2.2 for RS-232 port
connections
Voltage: ±5 volts or ±12 volts,
depending on jumper settings
Recommended Maximum Cable
Length: 50 feet (15 meters)
Pinouts: See Appendix A.2.2

RS-422 Ports
See Appendix A.2.2 for RS-422 port
connections.
Voltage: line drivers meet Electronics
Industries Association (EIA)
specifications for RS-422.
Recommended Maximum Cable
Length: 4000 feet (1219 meters)
Pinouts: See Appendix A.2.2

RS-485 Serial Specifications


See Appendix A.2.2 for RS-485 port
connections.
Voltage: line drivers meet Electronics
Industries Association (EIA)
specifications for RS-485
Recommended Maximum Cable
Length: 4000 feet (1219 meters)
Pinouts: See Appendix A.2.2

SEP 2005 FID Serial Communications


A-12 COMMUNICATIONS SPECIFICATIONS
Model 700

A.2.2 FTB Serial Communications

The settings are shown in Figure A-8 through


Figure A-13.
Com1

RS-232 RS-485 RS-422 J5


DCD 1
1
RXD 1 TX/RX+ TX+
2
TXD 1 TX/RX- TX- 3
DTR 1
4
5
DSR 1 RX+
6
RTS 1 RX-
7
CTS 1 8
RI 1 9

Figure A-8 FTB Com1 DB 9-pin Phoenix Connector

Com2

RS-232 RS-485 RS-422 J7


DCD 2
1
RXD 2 TX/RX+ TX+
2
TXD 2 TX/RX- TX- 3
DTR 2
4
5
DSR 2 RX+
6
RTS 2 RX-
7
CTS 2 8
RI 2 9

Figure A-9 FTB Com2 DB 9-pin Phoenix Connector

FID Serial Communications SEP 2005


COMMUNICATIONS SPECIFICATIONS A-13
Model 700

Com5

RS-232 RS-485 RS-422 J9


RLSD 5
1
RXD 5 TX/RX+ TX+
2
TXD 5 TX/RX- TX- 3
DTR 5
4
5
DSR 5 RX+
6
RTS 5 RX-
7
CTS 5 8
RI 5 9

Figure A-10 FTB Com5 DB 9-pin Phoenix Connector

Com6

RS-232 RS-485 RS-422


J13
RLSD 6
1
RXD 6 TX/RX+ TX+
2
TXD 6 TX/RX- TX- 3
DTR 6
4
5
DSR 6 RX+
6
RTS 6 RX-
7
CTS 6 8
RI 6 9

Figure A-11 FTB Com6 DB 9-pin Phoenix Connector

SEP 2005 FID Serial Communications


A-14 COMMUNICATIONS SPECIFICATIONS
Model 700

Com7

RS-232 RS-485 RS-422 J17


RLSD 7
1
RXD 7 TX/RX+ TX+
2
TXD 7 TX/RX- TX- 3
DTR 7
4
5
DSR 7 RX+
6
RTS 7 RX-
7
CTS 7 8
RI 7 9

Figure A-12 FTB Com7 DB 9-pin Phoenix Connector

Com8

RS-232 RS-485 RS-422 J18


RLSD 8
1
RXD 8 TX/RX+ TX+
2
TXD 8 TX/RX- TX- 3
DTR 8
4
5
DSR 8 RX+
6
RTS 8 RX-
7
CTS 8 8
RI 8 9

Figure A-13 FTB Com8 DB 9-pin Phoenix Connector

FID Serial Communications SEP 2005


COMMUNICATIONS SPECIFICATIONS A-15
Model 700

WinSystems CPU
Jumper settings and pinouts for the four
WinSystems CPU board serial communications
ports; Com1, Com2, Com3, and Com4 are
defined in the following tables.
Table A-3 Communication with WinSystems CPU

Com1

RS-232 Mode

J8 – Jumpers Pins 1 and 2

J13 – No jumpers

U2 – Installed (Standard)

U5 – Removed

U6 – Removed

RS-422 Mode (Need WinSys Chip Kit CK # 75176-2)

J8 – Jumper Pins 1 and 2

J13 – No jumpers

U2 – Removed

U5 – Installed

U6 – Installed

RS-485 Mode (Need WinSys Chip Kit CK # 75176-2)

J8 – Jumper Pins 1 and 2

J13 – Jumper Pins 2 and 3

U2 – Removed

U5 – Removed

U6 – Installed

SEP 2005 FID Serial Communications


A-16 COMMUNICATIONS SPECIFICATIONS
Model 700

Table A-4 Communication with WinSystems CPU

Com2

RS-232 Mode

J9 – Jumpers Pins 1 and 2

J16 – No jumpers

U9 – Installed (Standard)

U11 – Removed

U12 – Removed

RS-422 Mode (Need WinSys Chip Kit CK # 75176-2)

J9 – Jumper Pins 1 and 2

J16 – No jumpers

U9 – Removed

U11 – Installed

U12 – Installed

RS-485 Mode (Need WinSys Chip Kit CK # 75176-2)

J9 – Jumper Pins 1 and 2

J16 – Jumper pin 2 and 3

U9 – Removed

U11 – Removed

U12 – Installed

FID Serial Communications SEP 2005


COMMUNICATIONS SPECIFICATIONS A-17
Model 700

Table A-5 Communication with WinSystems CPU

Com3 Reserved for Multifunction Board

RS-232 Mode

J12 – Jumpers Pins 1 and 2

J14 – No jumpers

U4 – Installed (Standard)

U7 – Removed

U8 – Removed

SEP 2005 FID Serial Communications


A-18 COMMUNICATIONS SPECIFICATIONS
Model 700

Table A-6 Communication with WinSystems CPU

Com4 (Reserved for FID/TCD Preamplifier Board)

RS-232 Mode

J15 – Jumpers Pins 1 and 2

J17 – No jumpers

U10 – Installed (Standard)

U13 – Removed

U14 – Removed

RS-422 Mode (Need WinSys Chip Kit CK # 75176-2)

J15 – Jumpers Pins 1 and 2

J17 – No jumpers

U10 – Removed

U13 – Installed

U14 – Installed

RS-485 Mode (Need WinSys Chip Kit CK # 75176-2)

J15 – Jumpers Pins 1 and 2

J17 – Jumpers Pins 2 and 3

U10 – Removed

U13 – Removed

U14 – Installed

FID Serial Communications SEP 2005


COMMUNICATIONS SPECIFICATIONS A-19
Model 700

WinSystems MCM/LPM – Com4A Board


Jumper settings and pinouts for the four
WinSystems Com4A board (optional) serial
communications ports; Com5, Com6, Com7,
and Com8 are defined in the following tables.
Table A-7 Communication with WinSystems
MCM/LPM – Com4A Board (Optional)

Com5

RS-232 Mode

J2 – No jumpers

U6 – Installed (Standard)

U3 – Removed

U4 – Removed

RS-422 Mode (Need WinSys Chip Kit CK # 75176-2)

J2 – No jumpers

U6 – Removed

U3 – Installed

U4 – Installed

RS-485 Mode (Need WinSys Chip Kit CK # 75176-2)

J2 – Jumper Pins 2 and 3

U6 – Removed

U3 – Removed

U4 – Installed

SEP 2005 FID Serial Communications


A-20 COMMUNICATIONS SPECIFICATIONS
Model 700

Com6

RS-232 Mode

J5 – No jumpers

U13 – Installed (Standard)

U10 – Removed

U14 – Removed

RS-422 Mode (Need WinSys Chip Kit CK # 75176-2)

J5 – No jumpers

U13 – Removed

U10 – Installed

U14 – Installed

RS-485 Mode (Need WinSys Chip Kit CK # 75176-2)

J5 – Jumper pins 2 and 3

U13 – Removed

U10 – Removed

U14 – Installed

FID Serial Communications SEP 2005


COMMUNICATIONS SPECIFICATIONS A-21
Model 700

Com7

RS-232 Mode

J4 – No jumper

U11 – Installed (Standard)

U9 – Removed

U12 – Removed

RS-422 Mode (Need WinSys Chip Kit CK # 75176-2)

J4 – No jumpers

U11 – Removed

U9 – Installed

U12 – Installed

RS-485 Mode (Need WinSys Chip Kit CK # 75176-2)

J4 – Jumper pins 2 and 3

U11 – Removed

U9– Removed

U12 – Installed

SEP 2005 FID Serial Communications


A-22 COMMUNICATIONS SPECIFICATIONS
Model 700

Com8

RS-232 Mode

J1 – No jumpers

U5 – Installed (Standard)

U1 – Removed

U2 – Removed

RS-422 Mode (Need WinSys Chip Kit CK # 75176-2)

J1 – No jumpers

U5 – Removed

U1 – Installed

U2 – Installed

RS-485 Mode (Need WinSys Chip Kit CK # 75176-2)

J1 – Jumper pins 2 and 3

U5 – Removed

U1 – Removed

U2 – Installed

FID Serial Communications SEP 2005


COMMUNICATIONS SPECIFICATIONS A-23
Model 700

Com4A Board Compatibility Settings

Table A-8 J10 Jumper Settings

Pin(s) Position

1 and 2 In

3 and 4 In

7 and 8 In

9 and 10 In

Table A-9 J7 Jumper Settings

Pin(s) Position

1 and 2 Open

3 and 4 Open

5 and 6 Open

Table A-10 J8 Jumper Settings

Pin(s) Position

1 and 2 In

3 and 4 In

5 and 6 In

7 and 8 In

Table A-11 J9 Jumper Settings

Pin(s) Position

1 and 2 In

5 and 6 In

SEP 2005 FID Serial Communications


A-24 COMMUNICATIONS SPECIFICATIONS
Model 700

WinSystems Ethernet Board

The PCM-NE2000-16 PC-104 can be configured


by using the on-board jumper block
Jumper settings and pinouts used on the
Model 700 for the PCM-NE-2000-16 PC-104
Ethernet board (optional) are defined in the
following table:
Table A-12 Ethernet Board Pin Settings

Jumper Pin Position “In”

J1 13 and 14
15 and 16
17 and 18
23 and 24
27 and 28

J2 1 and 2

J3 1 and 2

FID Serial Communications SEP 2005


COMMUNICATIONS SPECIFICATIONS A-25
Model 700

Radicom 56K Baud Modem Board

The jumper settings and pinouts for the


Radicom Modem (P/N 3-0700-029) are shown
below: (see Section 3.4.10).
Table A-13 J26 Radicom Modem Jumper Settings

Pin(s) Position

1 and 2 In

Table A-14 J27 Radicom Modem Jumper Settings

Pin(s) Position

1 and 2 In

Table A-15 J30 Radicom Modem Jumper Settings

Pin(s) Position

1 and 2 In

Table A-16 J31 Radicom Modem Jumper Settings

Pin(s) Position

2 and 3 In

A.3 WIRING LOCAL RS-232 COMMUNICATIONS

A.3.1 GC Serial Port and Cable Configurations

This section provides more detailed


information about local serial port connections
for the Model 700. It identifies serial port pin
assignments and diagrams for designing
RS-232 serial cables.

SEP 2005 Wiring Local RS-232 Communications


A-26 COMMUNICATIONS SPECIFICATIONS
Model 700

GC serial ports are found on the Field


Termination Board and the connection points
for external devices are as follows:
Model 700 Lower Enclosure

Figure A-14 FTB Serial Connections

Model 700 Lower Enclosure

Figure A-15 FTB Serial Connections

Wiring Local RS-232 Communications SEP 2005


COMMUNICATIONS SPECIFICATIONS A-27
Model 700

Table A-17 Serial Ports on Field Termination Board

Phoenix Plug
Port Comments (bare-wire)
connection

Serial Port 1 (Com1) P2 DB 9-pin Connection J5

Serial Port 2 (Com2) P3 DB 9-pin Connection J7

Serial Port 3 (Com3) Reserved for Multifunction Board N/A

Serial Port 4 (Com4) Reserved for LOI N/A


with Com4A board (TCD units)

Reserved for FID/TCD Preamplifier


Board (FID/TCD units)

Serial Port 5 (Com5) J9

Serial Port 6 (Com6) J13

Serial Port 7 (Com7) J17

Serial Port 8 (Com8) J18

Phoenix plug (bare-wire) connections are


available to all four serial ports. Pin-outs are
identical for all four serial port Phoenix plugs
and jacks. Each Phoenix plug/jack (male)
combination allows a bare-wire connection and
uses 9-Pins as illustrated:

Figure A-16 Phoenix Connector (J5, J6, J10, and J11) Pinout

SEP 2005 Wiring Local RS-232 Communications


A-28 COMMUNICATIONS SPECIFICATIONS
Model 700

Null modem connections (DB 9-pin) are


available for Serial Ports 1 and 2 only, as noted
in Table A-17.

PC-to-GC connections, direct serial:


The GC serial ports were wired to appear as DCE, so a
straight-through serial cable is used for a direct serial
connection between the GC and the PC. (The PC is
Data Terminal Equipment, or DTE.) See Section A.3.2.
External modem-to-GC connections, serial: a null
modem cable and gender changes may be purchased
from any computer products store, for the GC to
external modem connection. However, a custom serial
cable may be built to emulate a null-modem cable for a
connection between the GC Controller and an external
modem. (The modem is Data Communications
Equipment, or DCE.) See Section A.4.

Both of the GC DB 9-pin jacks are female and


have identical pin assignments. Note that a
DB 9-pin male numbering scheme is also
illustrated, but for reference purposes only as
follows (see Figure A-17).

Figure A-17 DB 9-pin Connector (P2 and P3) and Pinout for Jacks

Wiring Local RS-232 Communications SEP 2005


COMMUNICATIONS SPECIFICATIONS A-29
Model 700

A.3.2 GC DB 9-pin Serial Port to PC DB 9-pin Port

To make an RS-232 serial connection between


one of the DB 9-pin serial ports of the GC, and
a PC with DB 9-pin serial port, use a straight-
through serial cable, terminated as DB 9-pin
male / DB 9-pin female. This will work if the
PC has a male DB 9-pin serial port, and its pin
assignments are identical to those found on a
typical DB 9-pin serial port of an IBM PC.

The straight-through serial cable can be


obtained from most computer products
suppliers, so custom-building a cable normally
is not necessary. Wiring and signal paths are
illustrated as follows (see Figure A-18).

Female DB-9 Male DB-9 Female DB-9


connector on GC cable end to GC cable end to PC
5 1 1 5 5 1

9 6 6 9 6
9

9 RI 9 RI 9 RI
8 RTS 8 CTS 8 CTS
7 CTS 7 RTS 7 RTS
6 DTR 6 DSR 6 DSR
5 GND 5 GND 5 GND
4 DSR 4 DTR 4 DTR
3 RxD 3 TxD 3 TxD
2 TxD 2 RxD 2 RxD
1 RLSD 1RLSD 1RLSD
(DCD) (DCD) Straight-through serial cable(DCD)

Figure A-18 GC DB 9-pin Port to PC DB 9-pin Port

SEP 2005 Wiring Local RS-232 Communications


A-30 COMMUNICATIONS SPECIFICATIONS
Model 700

A.3.3 GC DB 9-pin Serial Port to PC DB 25-pin Port

To make an RS-232 serial connection between


one of the DB 9-pin serial ports of the GC, and
a PC with DB 25-pin serial port, you may be
able to use a straight-through serial cable,
terminated as DB 9-pin male / DB 25-pin
female. This will work if the PC has a male
DB 25-pin serial port, and its pin assignments
are identical to those found on an IBM PC.
The necessary straight-through serial cable can
be obtained from most computer products
suppliers, so custom-building a cable normally
is not necessary. Wiring and signal path are
illustrated as follows (see Figure A-19).

Figure A-19 GC DB 9-pin Port to PC DB 25-pin Port

Wiring Local RS-232 Communications SEP 2005


COMMUNICATIONS SPECIFICATIONS A-31
Model 700

A.3.4 GC PHOENIX Plug Port to PC DB 9-pin Port

To make an RS-232 serial connection between


one of the Phoenix Plug serial ports of the GC,
The cable for this
application is also available
and a PC with DB 9-pin serial port, you will
(P/N 3-2350-068) in a need to manufacture the cable and its
customer-specified length DB 9-pin, female plug cable end as illustrated
with six exposed leads and below (see Figure A-20).
a female DB 9-pin
connector.

Figure A-20 GC DB 9-pin Port to PC DB 25-pin Port

SEP 2005 Wiring Local RS-232 Communications


A-32 COMMUNICATIONS SPECIFICATIONS
Model 700

A.3.5 GC PHOENIX Plug Port to PC DB 25-pin Port

To make an RS-232 serial connection between


one of the Phoenix Plug serial ports of the GC,
and a PC with DB 25-pin serial port, you will
need to manufacture the cable and its
DB 25-pin, female plug cable end as illustrated
below (see Figure A-21).

Figure A-21 GC Phoenix Plug Port to PC DB 25-pin Port

Wiring Local RS-232 Communications SEP 2005


COMMUNICATIONS SPECIFICATIONS A-33
Model 700

A.4 WIRING REMOTE RS-232 COMMUNICATIONS

A.4.1 GC DB 9-pin Serial Port to Modem


DB 25-pin Port

To make an RS-232 serial connection between


one of the DB 9-pin serial ports of the GC, and
an external modem with a DB 25-pin serial
port, you may use gender changes and a null
modem cable purchased from any computer
products supplier, or you may manufacture a
cable. The manufactured null modem cable will
need a male DB 9-pin connector and a male DB
25-pin connector. Wire the cable ends as
illustrated below (see Figure A-22).

The DB-9 connector on the GC serial port is wired to appear as


Data Communications Equipment (DCE). Use a custom null-
modem type cable to make the connection between the GC and
an external modem. (GC serial ports were wired to appear as
DCE so that a straight-through serial cable could be used for a
direct serial connection between the GC Controller and the PC,
which is Data Terminal Equipment [DTE].)

Female DB-9 Serial Male DB-9 cable end Male DB-25 cable end
connector on GC to GC Serial Port to External Modem DCE

5 1 1 5 1 13

9 6 6 9 14 25

9 RI 9 RI 22 RI
8 RTS 8 CTS 4 RTS
7 CTS 7 RTS 5 CTS
6 DTR 6 DSR 20 DTR
5 GND 5 GND 7 GND
4 DSR 4 DTR 6 DSR
3 RxD 3 TxD 3 RxD
2 TxD 2 RxD 2 TxD
1 RLSD 1 DCD 8 DCD
(DCD) Null Modem cable

Figure A-22 GC DB 9-pin Port to External Modem DB 25-pin Port

SEP 2005 Wiring Remote RS-232 Communications


A-34 COMMUNICATIONS SPECIFICATIONS
Model 700

A.4.2 GC PHOENIX Plug to Modem DB 25-pin Port

To make an RS-232 serial connection between


one of the Phoenix Plug serial ports of the GC,
and an external modem with DB 25-pin serial
port, you will need to manufacture the cable
and its DB 25-pin, male plug cable end as
illustrated below (see Figure A-23).

Figure A-23 GC Phoenix Plug Port to External Modem DB 25-pin Port

Wiring Remote RS-232 Communications SEP 2005


COMMUNICATIONS SPECIFICATIONS A-35
Model 700

A.5 EXAMPLE RS-422 PC-GC CONNECTION

This section demonstrates an example RS-422


See Section 3.4 for
connection from a PC to GC that is
additional details about accomplished through use of an asynchronous
serial communication line driver/interface device. The line driver
setups. device serves as an interface between the
RS-232 output of the PC and the RS-422
protocol needed for long distance serial input to
the GC. Specifics of the line driver are as
follows:
• Black Box brand
• Model LD485A-MP RS-232/RS-485
Multipoint Line Driver
• RS-232 input (to connect to the PC)
• RS-422 or RS-485 output (to connect to the
GC)
RS-422 line terminations are illustrated in
For this example, a straight- Figure A-24, below, and jumper and switch
through RS-232 serial cable settings to configure the line driver device are
is used to connect between listed in Table A-18 and Table A-19.
the PC and the line driver.

Figure A-24 Example RS-422 Serial Cable Terminations

SEP 2005 Example RS-422 PC-GC Connection


A-36 COMMUNICATIONS SPECIFICATIONS
Model 700

Table A-18 Switch Settings for LD485A-MP, RS-422 to GC

Switch Type Label Position Purpose

Front Panel Switch NORMAL / DLB NORMAL Uses normal operation,


instead of loopback testing.

DIP Switch Bank XW1A DCE / XW1A DCE Sets line driver to operate
XW1B DTE as data communications
equipment (DCE).

DIP Switch Bank S2 UNTERM Eliminates need for resistor


network termination to
connect one PC directly to
one GC.

Table A-19 Jumper Settings for LD485A-MP, RS-422 to GC

Jumper Position Purpose

W8 HALF half duplex operation

W9 ON no delay, clear to send (CTS) always true

W15 A-B RS-485 driver enabled by request to send (RTS)

W16 A-B half duplex turnaround delay at 5 ms

W17 B 100 ms disable timeout delay by 100 ms

W18 B-C RS-485 driver enabled by RTS

Example RS-422 PC-GC Connection SEP 2005


COMMUNICATIONS SPECIFICATIONS A-37
Model 700

A.6 EXAMPLE RS-485 PC-GC CONNECTION

This section demonstrates an example RS-485


See Section 3.4 for connection from a PC to GC that is
additional details about accomplished through use of an asynchronous
serial communication line driver/interface device. The line driver
setups. device serves as an interface between the
RS-232 output of the PC and the RS-485
protocol needed for long distance serial input to
the GC. Specifics of the line driver are as
follows:
• Black Box brand
• Model LD485A-MP RS-232/RS-485
Multipoint Line Driver
• RS-232 input (to connect to the PC)
• RS-422 or RS-485 output (to connect to the
GC)
Refer to Figure A-25 and Figure A-26 for
RS-485 line terminations, jumpers and switch
settings to configure the line driver device (also
For this example, a straight- listed in Table A-19).
through RS-232 serial cable
is used to connect between
the PC and the line driver.

Figure A-25 Example RS-485 Serial Cable Terminations, Line


Driver to GC Controller Com3

SEP 2005 Example RS-485 PC-GC Connection


A-38 COMMUNICATIONS SPECIFICATIONS
Model 700

Figure A-26 Example RS-485 Serial Cable Terminations, Line


Driver to GC Controller Com4

Example RS-485 PC-GC Connection SEP 2005


COMMUNICATIONS SPECIFICATIONS A-39
Model 700

Table A-20 Switch Settings for LD485A-MP, RS-485 to GC

Switch Type Label Position Purpose

Front Panel NORMAL / DLB NORMAL Normal operation used, instead of


Switch loopback testing.

DIP Switch XW1A DCE / XW1A DCE Sets line driver to operate as data
Banks XW1B DTE communications equipment (DCE).

DIP Switch S2 UNTERM Eliminates need for resistor


Banks network termination to connect one
PC directly to one GC.

Table A-21 Jumper Settings for LD485A-MP, RS-485 to GC

Jumper Position Purpose

W8 HALF half duplex operation

W9 0 ms 0 milliseconds delay from time request to send


(RTS) received as true until clear to send (CTS)
asserted as true

W15 A-B RS-485 driver enabled by RTS

W16 A-B half duplex turnaround delay at 5 ms

W17 B 100 ms disable timeout delay by 100 ms

W18 B-C RS-485 driver enabled by RTS

SEP 2005 Example RS-485 PC-GC Connection


A-40 COMMUNICATIONS SPECIFICATIONS
Model 700

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Example RS-485 PC-GC Connection SEP 2005


MODEM INSTALLATION B-1
Model 700

APPENDIX B, MODEM INSTALLATION


B

Revision C of the Internal This appendix provides information for


Modem requires MON2000 installing the optional Internal Modem for the
software, version 2.2 or Model 700 (P/N 3-0700-029). The modem
later.
communications is established via COM4 and
the MON2000 version 2.2 software, which then
redirects modem communications through to
Com9.

B.1 OPTIONAL INTERNAL MODEM

DANGER TO PERSONNEL AND EQUIPMENT


Before removing the cover from the GC, ensure
that the power supply switch is OFF and the AC
power cord is disconnected.
Failure to follow this warning may result in death or
injury to personnel or cause damage to the
equipment.

To install the internal modem,

1. Halt any ongoing analysis runs.


2. Disconnect the power from the unit.
3. Remove the explosion-proof dome and the
Oven System protective cover.

SEP 2004 Optional Internal Modem


B-2 MODEM INSTALLATION
Model 700

4. Disconnect the Analog cable from J6 of the


System Interface board, then disconnect all
CPU cables from the System Interface
board.
5. Remove the CPU assembly and install the
modem, with associated hardware into J19
and J20 PC/104 Bus connector on the CPU
assembly. The modem must be the top
board in the assembly. See Figure below.

Model 700 Lower Enclosure

Figure B-1 Radicom 56K Baud Modem Installation

6. Set communication port jumper settings on


the modem board (P/N 3-0700-029) as
follows:

Jumper Pin

J26 1-2

J27 1-2

J30 1-2

J31 2-3

Optional Internal Modem SEP 2004


MODEM INSTALLATION B-3
Model 700

7. Plug one end of the modem extension cable


(P/N 3-2350-075) into RJ11 of the modem
assembly. The in-line jack on the remaining
end of the modem extension cable attaches
to the lower left inside wall of the card cage
shield (after the CPU assembly is
reinstalled and all cables reconnected to the
System Interface board). No software setup
is required for this board.
8. Insert the phone line into the modem
extension assembly.

B.1.1 Optional Ethernet Board

To add an Ethernet Assembly:

1. Disconnect the Analog cable from J6 of the


FTB, then disconnect all CPU and optional
board cables and lines.
2. Remove the CPU assembly and install the
Ethernet assembly with associated
hardware into J19 and J20 PC/104 Bus
connector on the CPU assembly. If an option
board is already plugged into the PC/104
Bus on the CPU, install the Ethernet
assembly and mounting hardware into the
PC/104 Bus connector on the option board.
3. Plug one end of the Ethernet extension
cable (P/N 3-2350-088) into J5 of the
Ethernet assembly. The in-line jack on the
remaining end of the Ethernet extension
cable attaches to the lower left inside wall of
the card cage shield, after the CPU
assembly is reinstalled and all cables and
lines reconnected. No software setup is
required for this board.
4. Run the Ethernet line through the conduit
into the lower enclosure and connect it to
the Ethernet extension cable.

SEP 2004 Optional Internal Modem


B-4 MODEM INSTALLATION
Model 700

This page is intentionally left blank.

Optional Internal Modem SEP 2004


MANIFOLD CARRIER FOR GAS BOTTLES C-1
Model 700

APPENDIX C, MANIFOLD CARRIER FOR GAS BOTTLES


C

C.1 CARRIER GAS

This appendix provides a description of the


carrier manifold (P/N 3-5000-050) that permits
connection of two carrier gas bottles, or
The illustration and cylinders, to a gas chromatograph (GC) system.
information in this appendix The benefits of this manifold are as follows:
are adapted from drawing
AE-10098.
• When one bottle is nearly empty (i.e., 100
psig remaining), the other bottle becomes
the primary supply.
• Each bottle can be disconnected for refilling
without interrupting GC operation.

Figure C-1 Manifold for Two Carrier Gas Bottles to GC System

SEP 2004 Carrier Gas


C-2 MANIFOLD CARRIER FOR GAS BOTTLES
Model 700

C.2 INSTALLATION AND LINE PURGING

To install and purge the dual-bottle carrier gas


manifold, proceed as follows:

1. Install manifold as shown in Figure C-1.


Close all valves and tighten all fittings. Run
tubing to the Analyzer, but do not connect.
2. Back off pressure regulator (counter
clockwise) fully.
3. Open cylinder valve for Carrier Cylinder 1.
The pressure indicator will read the
cylinder pressure.
4. Open the shut-off valve attached to the
carrier regulator.
5. Regulate pressure out of the cylinder to 20
psig, then close the cylinder valve.
6. Open V-1 (bleed valve) and let the carrier
gas bleed to atmosphere until both gauges
read 0 psig, then close V-1.
7. Repeat Steps 4 and 5 two more times to
purge the line to V-2.
8. Purge the line to V-3 by repeating Steps 2
through 6; but this time, use bleed valve V-4
and Carrier Cylinder 2.
9. With valves 1-4 closed, open both cylinder
valves and regulate both carriers to
approximately 10 psig.
10. Open V-2 and V-3 simultaneously, then
turn both cylinder valves off and let the
carrier gasses bleed through the line to the
Analyzer until all gauges read 0 psig.
11. Repeat steps (8) and (9) two more times to
purge line to Analyzer.
12. Close V-3, leave V-2 open.

Installation and Line Purging SEP 2004


MANIFOLD CARRIER FOR GAS BOTTLES C-3
Model 700

13. Open cylinder valve of Carrier Cylinder 1


and, with carrier gas flowing at 10 psig or
below, connect carrier line to Analyzer.
14. Slowly regulate Carrier Cylinder 1 to 110
psig.
15. Open V-3 and slowly regulate Carrier
Cylinder 2 to 100 psig. (By doing this, all
but 100 pounds of Carrier Cylinder 1 will be
used before any of Carrier Cylinder 2 is
used. When Carrier Cylinder 1 gets to 100
pounds, replace the cylinder). Leak-check
all of the fittings carefully.
16. Let the Analyzer run overnight before
calibrating.

C.3 REPLACING CARRIER CYLINDER

To replace one carrier cylinder without


interrupting GC operation, proceed as follows:

1. Turn cylinder valve off.


2. Back off on cylinder pressure regulator until
handle turns freely. Remove cylinder.
3. Attach new cylinder to regulator and repeat
Steps 3 through 7 of Installation
Instructions, Section C.2, using appropriate
bleed valve to purge line. Leak-check the
fitting.
4. Open the appropriate block valve to the
Analyzer (V-2 or V-3) and regulate outlet
pressure to appropriate level. (See Steps 14
and 15 of Installation Instructions, Section
C.2.)

SEP 2004 Replacing Carrier Cylinder


C-4 MANIFOLD CARRIER FOR GAS BOTTLES
Model 700

C.4 CALIBRATION GAS

The calibration gas used for BTU analysis


should be blended of gases specified as Primary
Standards. Primary Standard gases are
blended using weights that are traceable to the
National Institute of Standards and
Technology (N.I.S.T). For other applications,
the calibration gas should be blended to the
specifications detailed in the analyzer’s
Application Data Sheets.

The calibration gas should not have any


component that could drop out at the coldest
temperature to which the gas will be subjected.
A typical blend for a temperature of zero
degrees Fahrenheit is listed in the following
table (Table C-1). No dropout will occur in this
calibration gas if it is blended at a pressure
below 250 psig.

Table C-1 Contents of Example Calibration Gas

Mole
Gas
Percent

Nitrogen 2.5

Carbon 0.5
Dioxide

Methane Balance

Propane 1.0

Isobutane 0.3

N-butane 0.3
Neopentane 0.1

Isopentane 0.1

N-pentane 0.1
N-hexane 0.03

The sampling system should be carefully


planned for the best chromatographic analyses.

Calibration Gas SEP 2004


ENGINEERING DRAWINGS D-1
Model 700

APPENDIX D, ENGINEERING DRAWINGS


D

D.1 LIST OF ENGINEERING DRAWINGS

This addendum contains the following


engineering drawings for the Model 700 Gas
Chromatograph.

BE-21154 Assembly Modem Board


Model 700 GC

CE-20765 Assembly CPU 2350A/700


(Sheets 1 and 2)

CE-20931 Assembly Radial 6-port Valve,


Kiosk Oven Model 700 GC

CE-20958 Assembly 10-port Valve


Model 700 GC

CE-21276 Assembly Micro-FID


Model 700 GC

CE-21345 Methanator Assembly

CE-25002 C9+ Flow Config. Det. 1 B/F to


Meas.D/C Det. 2 to Meas.
Model 700

CE-25003 C6+ Flow Config. Det. 1 B/F to


Meas.D/C Det. 2 to Meas.
Model 700

CE-25004 C6+ Flow Config. Det. 1 B/F to


Meas.to Meas. Model 700

CE-25006 C6+ and O2 Flow Config. Det. 1


B/F to Meas.D/C, DC Model 700

SEP 2005 List of Engineering Drawings


D-2 ENGINEERING DRAWINGS
Model 700

CE-25007 Flow Configuration


Det. 1 B/F to Meas. (Helium)
Det. 2 B/F to Meas. (Argon)
Model 700

DE-20991 Internal Cable Wiring Model 700


Analyzer (Sheets 1 & 2)

DE-20992 Field Wiring Field Termination


Board Model 700 GC

DE-20993 Outline and Dimensional Pole,


Wall & Floor Mounting Units
Model 700 GC

DE-21405 Internal Wiring Micro-FID

SP-00700 Spare Parts List Model 700 GC

SP-00701 Spare Parts List Model 700 GC

List of Engineering Drawings SEP 2005


WARRANTY CLAIM PROCEDURES

To make a warranty claim, you, the Purchaser, must:

1. Provide Daniel with proof of the Date of Purchase and proof of the
Date of Shipment of the product in question.
2. Return the product to Daniel within twelve (12) months of the date of
original shipment of the product, or within eighteen (18) months of the
date of original shipment of the product to destinations outside of the
United States. The Purchaser must prepay any shipping charges. In
addition, the Purchaser is responsible for insuring any product
shipped for return, and assumes the risk of loss of the product during
shipment.
3. To obtain Warranty service or to locate the nearest DMS office, sales,
or service center call (713) 827-6314, Fax (713) 827-6312, or write to:
Daniel Measurement Services
11100 Brittmore Park Drive
Houston, Texas 77041

Or contact DMS via the following site


www.emersonprocess.com/daniel

4. When contacting DMS for product service, the Purchaser is asked to


provide information as indicated on the following page entitled
"Customer Repair Report".
5. For product returns from locations outside the United States, it will be
necessary for you to obtain the import consignment address so that
DMS's customs broker can handle the importation with the U.S.
Customs Service.
6. DMS offers both on call and contract maintenance service designed to
afford single source responsibility for all its products.
7. DMS reserves the right to make changes at any time to any product to
improve its design and to insure the best available product.
This page is intentionally left blank.
CUSTOMER REPAIR REPORT

FOR SERVICE, COMPLETE THIS FORM, AND RETURN IT ALONG WITH THE AFFECTED EQUIPMENT
TO CUSTOMER SERVICE AT THE ADDRESS INDICATED BELOW.

COMPANY NAME: ___________________________________________________________________________

TECHNICAL CONTACT:_____________________________________ PHONE: _________________________

REPAIR P. O. #:________________________ IF WARRANTY, UNIT S/N: _____________________________

INVOICE ADDRESS: __________________________________________________________________________

_____________________________________________________________________________________________

_____________________________________________________________________________________________

SHIPPING ADDRESS: _________________________________________________________________________

_____________________________________________________________________________________________

RETURN SHIPPING METHOD: _________________________________________________________________

EQUIPMENT MODEL #:____________________ S/N:__________________FAILURE DATE: _____________

DESCRIPTION OF PROBLEM: __________________________________________________________________

_____________________________________________________________________________________________

_____________________________________________________________________________________________

WHAT WAS HAPPENING AT TIME OF FAILURE? _______________________________________________

_____________________________________________________________________________________________

ADDITIONAL COMMENTS: ____________________________________________________________________

_____________________________________________________________________________________________

_____________________________________________________________________________________________

REPORT PREPARED BY:__________________________________ TITLE: _____________________________

IF YOU REQUIRE TECHNICAL ASSISTANCE, PLEASE FAX OR WRITE THE CUSTOMER SERVICE
DEPARTMENT AT:

DANIEL MEASUREMENT SERVICES


DIVISION OF EMERSON PROCESS MANAGEMENT PHONE: (713) 827-6314
ATTN: CUSTOMER SERVICE FAX: (713) 827-6312
11100 BRITTMOORE PARK DRIVE
HOUSTON, TEXAS 77041

FOR FASTEST SERVICE CONTACT DANIEL VIA OUR WEBSITE:


www.emersonprocess.com/daniel
This page is intentionally left blank.
Daniel Measurement and Control, Inc., Daniel Measurement Services, Inc., and Rosemount
Analytical Inc., Divisions of Emerson Process Management, reserves the right to make
changes to any of its products or services at any time without prior notification in order to
improve that product or service and to supply the best product or service possible.

www.emersonprocess.com

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