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The 5rd International Conference on Advanced Materials and Nanotechnology Hanoi, 2022
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Nguyen Duc Hoa1*, Nguyen Duc Cuong1,2, Nguyen Van Hieu1

1
International Institute for Materials Science, Hanoi University of Science and Technology, Hanoi, Vietnam
2
Faculty of Hospitality and Tourism, Hue University, 22 Lam Hoang, Vy Da Ward, Hue City, Vietnam
*Corresponding author: [email protected]
Abstract— Summarize your work in about 150 to 200 words. Summarize your work in about 150 to 200 words.
Summarize your work in about 150 to 200 words. Summarize your work in about 150 to 200 words. Summarize your
work in about 150 to 200 words. Summarize your work in about 150 to 200 words. Summarize your work in about 150
to 200 words Summarize your work in about 150 to 200 words. Summarize your work in about 150 to 200 words
Summarize your work in about 150 to 200 words Summarize your work in about 150 to 200 words. Summarize your
work in about 150 to 200 words. Summarize your work in about 150 to 200 words. Summarize your work in about 150
to 200 words Summarize your work in about 150 to 200 words Summarize your work in about 150 to 200 words
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work in about 150 to 200 words.
Keywords: Keyword 1, Keyword 2, Keyword 3, Upto 5 keywords
I. INTRODUCTION were dissolved in 100 ml HCl (pH=2). The

Manuscript must be prepared in formal English chemical precipitation was achieved by slowly
with average length of 4-6 pages including of adding a 0.1 M solution of NaOH with vigorous
Figures, but not limited. Main text must be in the stirring for 30 min at 80 °C. The precipitated Fe3O4
form of Times New Roman with font size of 12. products were recovered by filtering, washing, and
drying at 60 °C. The obtained Fe3O4 NPs were
Air pollution caused by toxic and flammable loaded in an alumina boat and inserted into a tube
gases, such as CO, NH3, NO2, and H2, is one of the furnace for calcinations at 600 °C for about 5 h.
critical problems contributory to global warming,
climate change, and damage to human health [1]. B. Subtitle 1 Co-precipitation synthesis of Fe2O3
Therefore, the development of gas sensors for the nanoparticles; font size of 12
detection of such gases has received considerable The microstructures and morphologies of the
interest in recent years [2]. Essentially, resistive
as-synthesized Fe3O4 and -Fe2O3 nanostructures
gas sensors based on different forms of metal
were characterized by X-ray diffraction (XRD, D8
oxides, organic compounds, and polymers have
Advance, Brucker, Germany), scanning electron
been developed for monitoring air quality; the
microscopy (SEM), and transmission electron
studies focused mainly on the enhancement of gas
microscopy (TEM).
sensor performance, as well as the realization of
fast response and recovery time, low cost, low
power consumption, and high sensitivity [3]. III. RESULTS AND DISCUSSION
The developed sensors could detect low A. Subtitle 1 Material characteristics; font size of
concentrations of analytic gases at the ppm level. 12
The phase formation, and crystal structure of
II. EXPERIMENTAL the as-synthesized and calcinated NPs fabricated
by the co-precipitation synthesis pathway and
A. Subtitle 1 Co-precipitation synthesis of Fe2O3
investigated by XRD are shown in Fig. 1(A, B).
nanoparticles; font size of 12
The XRD pattern of the as-synthesized NPs
The Fe2O3 NPs were synthesized by a co- exhibit a face-centered cubic profile typical of the
precipitation method and subsequent calcinations Fe3O4 crystal structure (JCPDS No. 65-3107). The
at high temperature. First, the Fe3O4 NPs were main peaks can be indexed to the (220), (311),
fabricated by a co-precipitation method using ferric
(400), (422), (422), (511), and (440) reflections
chlorides (Fe3+) and ferrous chlorides (Fe2+) as
(Fig. (A)). However, after calcination at 600 °C
precursors. In brief, ferric chlorides (2×10-3 mol)
and ferrous chlorides (10-3 mol) (molar ratio, 2:1) for 5 h (Fig. 1(B)), the cubic Fe3O4 was converted
into -Fe2O3 phase. The main peaks of -Fe2O3 are
The 5rd International Conference on Advanced Materials and Nanotechnology Hanoi, 2022
indexed to a rhombohedral profile characteristics from the XRD data. This result indicates that the
of the -Fe2O3 crystal structure (JCPDS No. 81– NPs are not single crystals but are polycrystalline
2810). No detectable peak of impurities and other in nature.
phases was observed, indicating the formation of
single-phase -Fe2O3. The average crystalline CONCLUSION
IV.
sizes of the Fe3O4 and -Fe2O3 NPs calculated For the practical application of gas sensors in
from the XRD data using the Scherrer equation (d the detection of toxic and/or flammable gases, the
= 0.9λ/(β cos θ)) are about 15 and 20 nm, development of suitable sensing devices with low
respectively. cost, fast response, and high sensitivity is very
important. In this work, we introduced two
different synthesis pathways for the scalable
synthesis of α-Fe2O3 NPs for effective gas sensor
applications. The effects of synthesis pathways on
the morphologies and gas sensing properties of
NPs were investigated and discussed. Our
experiments demonstrated that the nanoporousα-
Fe2O3 NPs fabricated by the one-step direct
hydrothermal method are highly promising
materials for the detection of toxic and flammable
gases, despite the selectivity of sensors needed to
be improved.
ACKNOWLEDGMENT
Figure 1. XRD patterns of the as-synthesized Fe3O4 The current work was financially supported by
(A) and -Fe2O3 (B) NPs fabricated by two-step post- the Application-oriented Basic Research Program
synthesis. (2009–2012, Code: 05/09/HÐ-DTÐL).
B. Subtitle ; font size of 12 REFERENCES

The morphologies of the -Fe2O3 NPs fabricated
by co-precipitation post-synthesis were [1] N. D. Hoa, N. V. Quy, Y. Cho, D. Kim, Porous single-
wall carbon nanotube films formed by in-situ arc-
characterized by SEM and TEM (Fig. 2). The - discharge deposition for gas sensors application, Sens.
Fe2O3 NPs are irregularly shaped and they are Actuators B, 135 (2009) 656–663
aggregated because of the grain growth that [2] D. Yang, I. Kamienchick, D. Y. Youn, A. Rothschild,
occurred at a high calcination temperature. The and I. D. Kim, Ultrasensitive and Highly Selective Gas
TEM image also confirms that the -Fe2O3 NPs Sensors Based on Electrospun SnO2 Nanofibers
Modified by Pd Loading, Adv. Funct. Mater. 20 (2010)
have a condensed structure without any
4258–4264.
observation of nanopores inside the NPs. The
[3] J. H. Lee, Gas sensors using hierarchical and hollow
particle size estimated by TEM image was about oxide nanostructures: Overview, Sens. Actuators B, 140
150 nm, which is larger than the value calculated (2009) 319–336.

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The 5rd International Conference on Advanced Materials and Nanotechnology Hanoi, 2022

Title of Paper in Times New Roman With Font Size of 16

Nguyen Duc Hoa1*, Nguyen Duc Cuong1,2, Nguyen Van Hieu1

Keywords: Keyword 1, Keyword 2, Keyword 3, Upto 5 keywords

I. INTRODUCTION were dissolved in 100 ml HCl (pH=2). The

B. Subtitle ; font size of 12 REFERENCES

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